CN106389300B - Red autumnal leaves crape myrtle skin care compositions and methods and preparation method thereof - Google Patents
Red autumnal leaves crape myrtle skin care compositions and methods and preparation method thereof Download PDFInfo
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/98—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution of animal origin
- A61K8/987—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution of animal origin of species other than mammals or birds
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/02—Preparations for care of the skin for chemically bleaching or whitening the skin
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/08—Anti-ageing preparations
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Abstract
The present invention discloses a kind of red autumnal leaves crape myrtle skin care compositions and methods and preparation method thereof, red autumnal leaves crape myrtle skin care compositions and methods, in parts by weight, by 10-15 parts of plant extracts, 5-9 parts of animal extracts, 12-15 parts of rice washing waters, 0.5-1 parts of thickeners, 0.5-2.5 parts of moisturizer, 0.01-0.02 portions of preservatives, 0.01-0.05 parts of essence and 17-25 parts of deionized water compositions, plant extracts is made of 20-30 parts of red autumnal leaves banaba extracts and 6-10 parts of citrus extracts, animal extracts are made of 5-6 parts of oyster extracts and 3-7 parts of slug extracts, using the beneficial effects of the invention are as follows skin care compositions and methods provided by the invention plant extracts rich in and animal extracts, the two makes up while displaying one's respective advantages The deficiency of other side is suitble to the people of each age group difference skin quality to use, and is especially suitable for 30 years old or more crowd and uses, can significantly improve humidity, the fairness of skin, wrinkle is delayed to grow, promote the sophistication and smoothness of skin.
Description
Technical field
The present invention relates to cosmetic fields, and in particular to a kind of red autumnal leaves crape myrtle skin care compositions and methods and preparation method thereof.
Background technique
The complete entitled Japanese red autumnal leaves arbor crape myrtle of red autumnal leaves crape myrtle, it is long with its Ye Hong, florescence, is 160 days or more, the flowers are in blossom
It is gorgeous, Ji Guan flower, reward leaf is integrated and world-famous, red autumnal leaves crape myrtle very drought resisting, cold-resistant, and to sulfur dioxide, hydrogen fluoride and
The content of pernicious gas in air, dust can be effectively reduced in the resistance of nitrogen, be the first choice of cities and towns coloured silk, greening, at present I
Cutting propagation that state mainly concentrates the research of red autumnal leaves crape myrtle, blooming period prolonging etc., it is otherwise for red autumnal leaves crape myrtle to grind
Study carefully, the research such as edible value, medical value is considerably less, and to the research of its cosmetic values almost without.
Summary of the invention
In order to solve the above technical problems, the present invention provides a kind of red autumnal leaves crape myrtle skin care compositions and methods and preparation method thereof,
The composition has filled up the blank of red autumnal leaves crape myrtle market application.
Technical solution is as follows: a kind of red autumnal leaves crape myrtle skin care compositions and methods, key are: in parts by weight, by
10-15 parts of plant extracts, 5-9 parts of animal extracts, 12-15 parts of rice washing waters, 0.5-1 parts of thickeners, 0.5-2.5 parts of moisturizings
Agent, 0.01-0.02 portions of preservatives, 0.01-0.05 parts of essence and 17-25 parts of deionized water compositions；
In parts by weight, the plant extracts is extracted by 20-30 parts of red autumnal leaves banaba extracts and 6-10 portions of citruses
Object composition, the animal extracts are made of 5-6 parts of oyster extracts and 3-7 parts of slug extracts.
In parts by weight, the red autumnal leaves banaba extract is red by 20-38 parts of red autumnal leaves crape myrtle floral extracts and 7-11 parts
Leaf crape myrtle berry extract composition.
Natural plant extracts was not only contained using the technical program skin care compositions and methods provided by the present invention, but also had contained
There is natural animal extract, the two supplements the deficiency of other side while displaying one's respective advantages, meaning dimension abundant in rice washing water
Raw element compensates for simple plant, animal extracts the deficiency of nursing object.
Above-mentioned red autumnal leaves crape myrtle floral extract is made by following steps:
Step a: sealing is super after 75% ethyl alcohol is added in the ratio that solid-liquid ratio is 1:1-3 after taking fresh red autumnal leaves common crapemyrtle flower to smash to pieces
Then sonication 20-30min filters separating filtrate and filter residue；
Step b: ultrasonic treatment is sealed after dehydrated alcohol is added in the ratio that solid-liquid ratio is 1:3-5 in filter residue obtained by step a
Then 20-30min filters separating filtrate and filter residue；
Step c: gained filtrate in step a and step b is merged, glacial acetic acid is added and is adjusted to the pH of filtrate after merging
6.2 ± 0.3 and with the speed of 30-50r/min stir 15-25min, centrifuging and taking supernatant；
Step d: by supernatant vacuum freeze drying described in step c up to the red autumnal leaves crape myrtle floral extract.
Above-mentioned red autumnal leaves crape myrtle berry extract is made by following steps:
Step is 1.: it is the anhydrous of 30-50% that concentration, which is added, in the ratio for being 1:4-5 in solid-liquid ratio after taking red autumnal leaves crape myrtle fruit powder broken
Sealing and standing 10-12h after ethyl alcohol, collected by suction filtrate；
Step is 2.: it is added the NaCl solution of 2-3% in the filtrate, the volume ratio of the filtrate and NaCl solution is 1:
2-3, then heating and refluxing extraction 1.5-2h, collects crude extract；
Step is 3.: water-oil separating after crude extract centrifugation seals gained oil liquid at a temperature of -10 DEG C to -20 DEG C
It takes supernatant liquor to obtain after standing 15-24h and slightly mentions extract；
Step is 4.: it is described slightly mention in extract petroleum ether is added after stand 6-10h and take lower layer's heavy-fluid, it is described thick to extract
The volume ratio of object and petroleum ether is 1:1-2；
Step is 5.: lower layer's heavy-fluid being carried out heating and refluxing extraction 1.5-2h again, collects refining liquid；
Step is 6.: water-oil separating after refining liquid centrifugation seals gained oil liquid at a temperature of -10 DEG C to -20 DEG C
Take supernatant up to the red autumnal leaves crape myrtle berry extract after standing 15-24h.
Above-mentioned slug extract is made by following steps:
Step (1): taking fresh slug, and the salting liquid that the concentration that 8-10 times of slug weight is added is 3-5% stands 20-
After 30min, the salting liquid containing slug is poured into tissue mashing machine and smashs to obtain slug slurries to pieces；
Step (2): the pH value for adjusting slug slurries is 1.5-2.5, and in parts by weight, every portion slug slurries are added
0.1-0.3 parts of pepsins, then digest 1.5-2h at 35-37 DEG C；
Step (3): after the slug slurries after enzymatic hydrolysis are warming up to 80-100 DEG C of holding 2-5min, centrifuging and taking supernatant；
Step (4): being added the active carbon of 2-3% in the supernatant, filter after mixing evenly, collect filtrate, will be described
Filtrate is concentrated by evaporation the 1/4-1/3 to original volume with rotation after bag filter flowing water dialysis 20-30h up to the slug extract.
Above-mentioned oyster extract is made by following steps:
Step 1: oyster being cleaned up into gutting, the oyster meat after cleaning is added 1-2 times together with oyster shell
The pure water of weight simultaneously boils 20-30 minutes, then pulls oyster meat and oyster shell out natural cooling and stores respectively stand-by；
Step 2: oyster meat is taken, homogenate after the pure water of 2-3 times of its weight is added, subtilopeptidase A is then added,
The mass ratio of the subtilopeptidase A and oyster meat slurries is 3-5:50, and holding oyster slurries are 38-42 DEG C of enzymatic hydrolysis 3-4h,
Then filtering removal impurity, gained filtrate is oyster meat hydrolyzate；
Step 3: the oyster shell in step 1 be crushed into 400-500 mesh, 2-3 times of oyster shell powder weight is then added
Acid, and adjusting pH value is 4-4.5 acidolysis 2-3h, during which every the pH value of the hydrolyzate of test in 10-20 minutes, when hydrolyzate
Supplemental acid or alkali make the pH value of hydrolyzate remain at 4-4.5 when pH value is less than 4 or greater than 4.5, adjust water after acidolysis
The pH to 6.5-7.7 of liquid is solved, bromelain is added and is digested, the quality of the bromelain is the 1/ of hydrolyzate quality
, keeping hydrolyzate temperature is 50-55 DEG C, continues to filter after digesting 1-2h, and gained filtrate is oyster shell hydrolyzate；
Step 4: in parts by weight, the 3-5 parts of oyster meat hydrolyzates and 1 part of oyster shell hydrolyzate being mixed
Uniformly up to the oyster extract.
The rice washing water is made by following steps:
Step A: taking rice, is added after the sterile water of 2-3 times of its weight after being ultrasonically treated 3-5min and filters, gained filtrate is
First washing lotion；
Step B: taking the rice in step A after previous cleaning, is ultrasonically treated 5- after the sterile water of 1-2 times of its weight is added again
10min, then again with the speed stirring 3-5min filtering of 700-900r/min, gained filtrate is again washing lotion；
Step C: by the uniformly mixed rice washing water to obtain the final product of the just washing lotion and again washing lotion.
In parts by weight, the thickener is by 2-3 parts of algins, 1-3 parts of gloiopeltis glue, 1-2 parts of seaweed glues and 4-7
Part carbomer composition.
In parts by weight, the moisturizer is by 5-7 parts of hyaluronic acids, 4-6 parts of chondroitin sulfates and 1-3 parts of lactic acid
Composition.
A kind of red autumnal leaves crape myrtle skin care compositions and methods preparation method, key are: including above-mentioned red autumnal leaves crape myrtle skin
Care composition is made according to the following steps: is added after thickener in deionized water at 60-70 DEG C cold after stirring 10-15min
But it to room temperature, is stirred after then sequentially adding the plant extracts, animal extracts, rice washing water, moisturizer, preservative and essence
It mixes and is filtered after standing 12-15h at a temperature of being uniformly placed in 3-5 DEG C, gained filtrate is the red autumnal leaves crape myrtle skin nursing combination
Object.
The utility model has the advantages that using the beneficial effects of the invention are as follows skin care compositions and methods provided by the invention plants rich in
Object extract and animal extracts, the two make up the deficiency of other side while displaying one's respective advantages, and are suitble to each age group different
The people of skin quality uses, and is especially suitable for 30 years old or more crowd and uses, can significantly improve humidity, the fairness of skin, delay wrinkle
Growth, promotes the sophistication and smoothness of skin.
Specific embodiment
Below with reference to embodiment, the invention will be further described.
Embodiment 1, a kind of red autumnal leaves crape myrtle skin care compositions and methods, in parts by weight, and by 10 parts of plant extracts, 5
Part animal extracts, 12 parts of rice washing waters, 0.5 part of thickener, 0.5 part of moisturizer, 0.01 portion of preservative, 0.01 part of essence and 17 parts
Deionized water composition, the plant extracts are made of 20 parts of red autumnal leaves banaba extracts and 6 parts of citrus extracts, and the animal mentions
Object is taken to be made of 5 parts of oyster extracts and 3 parts of slug extracts, the red autumnal leaves banaba extract is extracted by 20 parts of red autumnal leaves common crapemyrtle flowers
Object and 7 parts of red autumnal leaves crape myrtle berry extract compositions, the thickener is by 2 parts of algins, 1 part of gloiopeltis glue, 1 part of seaweed glue and 4 parts
Carbomer composition, the moisturizer are made of 5 parts of hyaluronic acids, 4 parts of chondroitin sulfates and 1 part of lactic acid, and the preservative is by 2
Part propylben and 1 part of nisin composition, the citrus extracts are commercially available citrus extracts, and the essence is to change
Cosmetic often uses essence.
The red autumnal leaves crape myrtle floral extract is made by following steps:
Step a: ultrasound is sealed after 75% ethyl alcohol is added in the ratio that solid-liquid ratio is 1:1 after taking fresh red autumnal leaves common crapemyrtle flower to smash to pieces
20min is handled, separating filtrate and filter residue are then filtered, the ultrasonic treatment condition is 25kHz, ultrasonic power 120w；
Step b: ultrasonic treatment is sealed after dehydrated alcohol is added in the ratio that solid-liquid ratio is 1:3 in filter residue obtained by step a
20min, then filters separating filtrate and filter residue, and the ultrasonic treatment condition is 25kHz, ultrasonic power 150w；
Step c: gained filtrate in step a and step b is merged, glacial acetic acid is added and is adjusted to the pH of filtrate after merging
5.9 and with the speed of 30r/min stir 15min, with 2500r/min centrifugation 5min take supernatant；
Step d: by supernatant described in step c, vacuum freeze drying 5h under -10 DEG C of temperature, vacuum degree 78KPa to obtain the final product
The red autumnal leaves crape myrtle floral extract.
The red autumnal leaves crape myrtle berry extract is made by following steps:
Step is 1.: the dehydrated alcohol that concentration is 30% is added in the ratio for being 1:4 in solid-liquid ratio after taking red autumnal leaves crape myrtle fruit powder broken
Collected by suction filtrate after sealing and standing 10h afterwards；
Step is 2.: it is added 2% NaCl solution in the filtrate, the volume ratio of the filtrate and NaCl solution is 1:2,
Then heating and refluxing extraction 1.5h collects crude extract；
Step is 3.: the crude extract 4000r/min is centrifuged after 7min and carries out water-oil separating with separatory funnel, gained is oily
Liquid takes supernatant liquor to obtain and slightly mentions extract at a temperature of -10 DEG C after sealing and standing 15h；
Step is 4.: it is described slightly mention in extract petroleum ether is added after stand 6h and take lower layer's heavy-fluid, it is described slightly to mention extract
Volume ratio with petroleum ether is 1:1；
Step is 5.: lower layer's heavy-fluid being carried out heating and refluxing extraction 1.5h again, collects refining liquid；
Step is 6.: will the refining liquid 4000r/min be centrifuged 5min after carry out water-oil separating with separatory funnel again, by institute
Obtain oil liquid takes supernatant up to the red autumnal leaves crape myrtle berry extract at a temperature of -10 DEG C after sealing and standing 15h.
The slug extract is made by following steps:
Step (1): taking fresh slug, after the salting liquid that the concentration for being added 8 times of slug weight is 3% stands 20min, will contain
The salting liquid of slug, which pours into tissue mashing machine, smashs to obtain slug slurries to pieces, and the salting liquid is NaCl solution；
Step (2): the pH value for adjusting slug slurries is 1.5, and in parts by weight, every portion slug slurries are added 0.1
Part pepsin, then digests 1.5h at 35 DEG C；
Step (3): after the slug slurries after enzymatic hydrolysis are warming up to 80 DEG C of holding 2min, centrifuging and taking supernatant；
Step (4): 2% active carbon is added in the supernatant, filters after mixing evenly, filtrate is collected, by the filter
Liquid is concentrated by evaporation to the 1/4 of original volume with rotation after bag filter flowing water dialysis 20h up to the slug extract.
The oyster extract is made by following steps:
Step 1: oyster being cleaned up into gutting, the oyster meat after cleaning is added its 1 times together with oyster shell
The pure water of weight simultaneously boils 20 minutes, then pulls oyster meat and oyster shell out natural cooling and stores respectively stand-by；
Step 2: oyster meat is taken, homogenate after the pure water of 2 times of its weight is added, subtilopeptidase A is then added, institute
The mass ratio for stating subtilopeptidase A and oyster meat slurries is 3:50, and holding oyster slurries are 38 DEG C of enzymatic hydrolysis 3h, is then filtered
Impurity is removed, gained filtrate is oyster meat hydrolyzate；
Step 3: the oyster shell in step 1 be crushed into 400 meshes, 2 times of oyster shell powder weight of hydrochloric acid is then added, and
Adjusting pH value is 4 acidolysis 2h, during which every the pH value of the hydrolyzate of test in 10 minutes, when the pH value of hydrolyzate is less than 4 or big
Supplemental acid (hydrochloric acid) or alkali (potassium hydroxide or sodium hydroxide) make the pH value of hydrolyzate remain at 4-4.5, acidolysis when 4.5
After adjust the pH to 6.5 of hydrolyzate, bromelain is added and is digested, the quality of the bromelain is hydrolyzate
The 1/15 of quality, keeping hydrolyzate temperature is 50 DEG C, continues to filter after digesting 1h, and gained filtrate is oyster shell hydrolyzate；
Step 4: in parts by weight, 3 parts of oyster meat hydrolyzates and 1 part of oyster shell hydrolyzate being mixed equal
The even oyster extract to obtain the final product.
The rice washing water is made by following steps:
Step A: taking rice, is added after the sterile water of 2 times of its weight after being ultrasonically treated 3min and filters, and gained filtrate is previous cleaning
Liquid, the condition of the ultrasonic treatment are 22kHz, 150w；
Step B: taking the rice in step A after previous cleaning, is ultrasonically treated 5min after the sterile water of 1 times of its weight is added again,
Then again with the speed stirring 3min filtering of 700r/min, gained filtrate is again washing lotion；
Step C: by the uniformly mixed rice washing water to obtain the final product of the just washing lotion and again washing lotion.
The red autumnal leaves crape myrtle skin care compositions and methods are made by following steps: being added after thickener 60 in deionized water
It is cooled to room temperature after stirring 10min at DEG C, then sequentially adds the plant extracts, animal extracts, rice washing water, moisturizing
It is stirred evenly after agent, preservative and essence after standing 12h at a temperature of being placed in 3 DEG C with 200 mesh net filtrations, gained filtrate is
The red autumnal leaves crape myrtle skin care compositions and methods.
Embodiment 2, a kind of red autumnal leaves crape myrtle skin care compositions and methods, in parts by weight, and by 15 parts of plant extracts, 9
Part animal extracts, 15 parts of rice washing waters, 1 part of thickener, 2.5 parts of moisturizer, 0.02 portion of preservative, 0.05 part of essence and 25 parts are gone
Ionized water composition, the plant extracts are made of 30 parts of red autumnal leaves banaba extracts and 10 parts of citrus extracts, and the animal mentions
Object is taken to be made of 6 parts of oyster extracts and 7 parts of slug extracts, the red autumnal leaves banaba extract is extracted by 38 parts of red autumnal leaves common crapemyrtle flowers
Object and 11 parts of red autumnal leaves crape myrtle berry extract compositions, the thickener is by 3 parts of algins, 3 parts of gloiopeltis glue, 2 parts of seaweed glues and 7 parts
Carbomer composition, the moisturizer are made of 7 parts of hyaluronic acids, 6 parts of chondroitin sulfates and 3 parts of lactic acid, and the preservative is by 3
Part propylben and 2 parts of nisins compositions, the citrus extracts are commercially available citrus extracts, and the essence is to change
Cosmetic often uses essence.
The red autumnal leaves crape myrtle floral extract is made by following steps:
Step a: ultrasound is sealed after 75% ethyl alcohol is added in the ratio that solid-liquid ratio is 1:3 after taking fresh red autumnal leaves common crapemyrtle flower to smash to pieces
30min is handled, separating filtrate and filter residue, the ultrasonic treatment condition are as follows: 25kHz, ultrasonic power 130w are then filtered；
Step b: ultrasonic treatment is sealed after dehydrated alcohol is added in the ratio that solid-liquid ratio is 1:5 in filter residue obtained by step a
Then 30min filters separating filtrate and filter residue, the ultrasonic treatment condition are as follows: 25kHz, ultrasonic power 140w；
Step c: gained filtrate in step a and step b is merged, glacial acetic acid is added and is adjusted to the pH of filtrate after merging
6.5 and with the speed of 50r/min stir 25min, with 2500r/min centrifugation 5min take supernatant；
Step d: by supernatant described in step c, vacuum freeze drying 6h under -10 DEG C of temperature, vacuum degree 78KPa to obtain the final product
The red autumnal leaves crape myrtle floral extract.
The red autumnal leaves crape myrtle berry extract is made by following steps:
Step is 1.: the dehydrated alcohol that concentration is 50% is added in the ratio for being 1:5 in solid-liquid ratio after taking red autumnal leaves crape myrtle fruit powder broken
Collected by suction filtrate after sealing and standing 12h afterwards；
Step is 2.: it is added 3% NaCl solution in the filtrate, the volume ratio of the filtrate and NaCl solution is 1:3,
Then heating and refluxing extraction 2h collects crude extract；
Step is 3.: the crude extract 4000r/min is centrifuged after 7min and carries out water-oil separating with separatory funnel, gained is oily
Liquid sealing and standing at a temperature of -20 DEG C takes supernatant liquor to obtain afterwards for 24 hours and slightly mentions extract；
Step is 4.: it is described slightly mention in extract petroleum ether is added after stand 10h Hou Qu lower layer heavy-fluid, it is described thick to extract
The volume ratio of object and petroleum ether is 1:2；
Step is 5.: lower layer's heavy-fluid being carried out heating and refluxing extraction 2h again, collects refining liquid；
Step is 6.: will the refining liquid 4000r/min be centrifuged 5min after carry out water-oil separating with separatory funnel again, by institute
Obtain oil liquid sealing and standing at a temperature of -20 DEG C takes supernatant up to the red autumnal leaves crape myrtle berry extract afterwards for 24 hours.
The slug extract is made by following steps:
Step (1): taking fresh slug, will after the salting liquid that the concentration for being added 10 times of slug weight is 5% stands 30min
Salting liquid containing slug, which pours into tissue mashing machine, smashs to obtain slug slurries to pieces, and the salting liquid is KCl solution；
Step (2): the pH value for adjusting slug slurries is 2.5, and in parts by weight, every portion slug slurries are added 0.3
Part pepsin, then digests 2h at 37 DEG C；
Step (3): after the slug slurries after enzymatic hydrolysis are warming up to 100 DEG C of holding 5min, centrifuging and taking supernatant；
Step (4): 3% active carbon is added in the supernatant, filters after mixing evenly, filtrate is collected, by the filter
Liquid is concentrated by evaporation to the 1/3 of original volume with rotation after bag filter flowing water dialysis 30h up to the slug extract.
The oyster extract is made by following steps:
Step 1: oyster being cleaned up into gutting, the oyster meat after cleaning is added its 2 times together with oyster shell
The pure water of weight simultaneously boils 30 minutes, then by oyster meat and oyster shell pull out cooled to room temperature then store respectively to
With；
Step 2: oyster meat is taken, homogenate after the pure water of its 3 times of weight is added, subtilopeptidase A is then added, institute
The mass ratio for stating subtilopeptidase A and oyster meat slurries is 5:50, and holding oyster slurries are 42 DEG C of enzymatic hydrolysis 4h, is then filtered
Impurity is removed, gained filtrate is oyster meat hydrolyzate；
Step 3: the oyster shell in step 1 be crushed into 500 meshes, 3 times of oyster shell powder weight of hydrochloric acid is then added, and
Adjusting pH value be 4.5 acidolysis 3h, during which every 20 minutes test hydrolyzate pH value, when hydrolyzate pH value less than 4 or
Supplemental acid (hydrochloric acid) or alkali (potassium hydroxide or sodium hydroxide) make the pH value of hydrolyzate remain at 4-4.5 when greater than 4.5, acid
The pH to 7.7 that hydrolyzate is adjusted after solution is added bromelain and is digested, and the quality of the bromelain is hydrolysis
The 1/10 of liquid quality, keeping hydrolyzate temperature is 55 DEG C, continues to filter after digesting 2h, and gained filtrate is oyster shell hydrolyzate；
Step 4: in parts by weight, 5 parts of oyster meat hydrolyzates and 1 part of oyster shell hydrolyzate being mixed equal
The even oyster extract to obtain the final product.
The rice washing water is made by following steps:
Step A: taking rice, is added after the sterile water of 3 times of its weight after being ultrasonically treated 5min and filters, and gained filtrate is previous cleaning
Liquid, the condition of the ultrasonic treatment are 22kHz, 150w；
Step B: taking the rice in step A after previous cleaning, is ultrasonically treated again after the sterile water of 2 times of its weight is added again
10min, then again with the speed stirring 5min filtering of 900r/min, gained filtrate is again washing lotion；
Step C: by the uniformly mixed rice washing water to obtain the final product of the just washing lotion and again washing lotion.
The red autumnal leaves crape myrtle skin care compositions and methods are made by following steps: being added after thickener 70 in deionized water
It is cooled to room temperature after stirring 15min at DEG C, then sequentially adds the plant extracts, animal extracts, rice washing water, moisturizing
It is stirred evenly after agent, preservative and essence after standing 15h at a temperature of being placed in 5 DEG C with 300 mesh net filtrations, gained filtrate is
The red autumnal leaves crape myrtle skin care compositions and methods.
Embodiment 3, a kind of red autumnal leaves crape myrtle skin care compositions and methods, in parts by weight, and by 13 parts of plant extracts, 7
Part animal extracts, 2 parts of rice washing waters, 0.7 part of thickener, 1.5 parts of moisturizer, 0.01 portion of preservative, 0.03 part of essence and 21 parts
Deionized water composition, the plant extracts are made of 25 parts of red autumnal leaves banaba extracts and 8 parts of citrus extracts, and the animal mentions
Object is taken to be made of 5.5 parts of oyster extracts and 5 parts of slug extracts, the red autumnal leaves banaba extract is soaked by 27 parts of red autumnal leaves common crapemyrtle flowers
Extract and 9 parts of red autumnal leaves crape myrtle berry extracts composition, the thickener by 2.5 parts of algins, 2 parts of gloiopeltis glue, 1.5 parts of seaweed glues with
And 5 parts of carbomer compositions, the moisturizer are made of 6 parts of hyaluronic acids, 5 parts of chondroitin sulfates and 2 parts of lactic acid, the anti-corrosion
Agent is made of 2 parts of propylbens and 1.5 parts of nisins, and the citrus extracts are commercially available citrus extracts, described
Essence is that cosmetics often use essence.
The red autumnal leaves crape myrtle floral extract is made by following steps:
Step a: ultrasound is sealed after 75% ethyl alcohol is added in the ratio that solid-liquid ratio is 1:2 after taking fresh red autumnal leaves common crapemyrtle flower to smash to pieces
25min is handled, separating filtrate and filter residue, the ultrasonic treatment condition are as follows: 25kHz, ultrasonic power 130w are then filtered；
Step b: ultrasonic treatment is sealed after dehydrated alcohol is added in the ratio that solid-liquid ratio is 1:4 in filter residue obtained by step a
Then 25min filters separating filtrate and filter residue, the ultrasonic treatment condition are as follows: 25kHz, ultrasonic power 140w；
Step c: gained filtrate in step a and step b is merged, glacial acetic acid is added and is adjusted to the pH of filtrate after merging
6.2 and with the speed of 40r/min stir 20min, with 2500r/min centrifugation 5min take supernatant；
Step d: by supernatant described in step c, vacuum freeze drying 8h under -10 DEG C of temperature, vacuum degree 78KPa to obtain the final product
The red autumnal leaves crape myrtle floral extract.
The red autumnal leaves crape myrtle berry extract is made by following steps:
Step is 1.: the anhydrous second that concentration is 40% is added in the ratio for being 1:4.5 in solid-liquid ratio after taking red autumnal leaves crape myrtle fruit powder broken
Sealing and standing 11h after alcohol, collected by suction filtrate；
Step is 2.: it is added 2.5% NaCl solution in the filtrate, the volume ratio of the filtrate and NaCl solution is 1:
2.5, then heating and refluxing extraction 2h, collects crude extract；
Step is 3.: the crude extract 4000r/min is centrifuged after 7min and carries out water-oil separating with separatory funnel, gained is oily
Liquid takes supernatant liquor to obtain and slightly mentions extract at a temperature of -15 DEG C after sealing and standing 19h；
Step is 4.: it is described slightly mention in extract petroleum ether is added after stand 8h Hou Qu lower layer heavy-fluid, it is described thick to extract
The volume ratio of object and petroleum ether is 1:1.5；
Step is 5.: lower layer's heavy-fluid being carried out heating and refluxing extraction 1.8h again, collects refining liquid；
Step is 6.: will the refining liquid 4000r/min be centrifuged 5min after carry out water-oil separating with separatory funnel again, by institute
Obtain oil liquid takes supernatant up to the red autumnal leaves crape myrtle berry extract at a temperature of -15 DEG C after sealing and standing 18h.
The slug extract is made by following steps:
Step (1): taking fresh slug, after the salting liquid that the concentration for being added 9 times of slug weight is 4% stands 25min, will contain
The salting liquid of slug, which pours into tissue mashing machine, smashs to obtain slug slurries to pieces, and the salting liquid is NaCl solution or KCl solution；
Step (2): the pH value for adjusting slug slurries is 2, and in parts by weight, every portion slug slurries are added 0.2 part
Then pepsin digests 1.7h at 36 DEG C；
Step (3): after the slug slurries after enzymatic hydrolysis are warming up to 90 DEG C of holding 3min, centrifuging and taking supernatant；
Step (4): 3% active carbon is added in the supernatant, filters after mixing evenly, filtrate is collected, by the filter
Liquid is concentrated by evaporation to the 1/3 of original volume with rotation after bag filter flowing water dialysis 25h up to the slug extract.
The oyster extract is made by following steps:
Step 1: oyster is cleaned up into gutting, by the oyster meat after cleaning together with oyster shell be added its 1.5
The pure water of times weight simultaneously boils 25 minutes, then pulls oyster meat and oyster shell out cooled to room temperature and then stores respectively
For use；
Step 2: oyster meat is taken, homogenate after the pure water of its 2.5 times of weight is added, subtilopeptidase A is then added,
The mass ratio of the subtilopeptidase A and oyster meat slurries is 4:50, and holding oyster slurries are 40 DEG C of enzymatic hydrolysis 3.5h, then
Filtering removal impurity, gained filtrate is oyster meat hydrolyzate；
Step 3: the oyster shell in step 1 be crushed into 450 meshes, 2.5 times of oyster shell powder weight of hydrochloric acid is then added,
And adjusting pH value is 4.3 acidolysis 2.5h, during which every the pH value of the hydrolyzate of test in 15 minutes, when the pH value of hydrolyzate is less than
4 or be greater than 4.5 when supplemental acid (hydrochloric acid) or alkali (potassium hydroxide or sodium hydroxide) so that the pH value of hydrolyzate is remained at 4-
4.5, the pH to 7.0 of hydrolyzate is adjusted after acidolysis, and bromelain is added and is digested, the quality of the bromelain
It is the 1/12 of hydrolyzate quality, keeping hydrolyzate temperature is 53 DEG C, continues to filter after digesting 1.5h, and gained filtrate is oyster shell water
Solve liquid；
Step 4: in parts by weight, 4 parts of oyster meat hydrolyzates and 1 part of oyster shell hydrolyzate being mixed equal
The even oyster extract to obtain the final product.
The rice washing water is made by following steps:
Step A: taking rice, is added after the sterile water of 2.5 times of its weight after being ultrasonically treated 4min and filters, gained filtrate is first
Washing lotion, the condition of the ultrasonic treatment are 22kHz, 150w；
Step B: taking the rice in step A after previous cleaning, is ultrasonically treated again after the sterile water of 1.5 times of its weight is added again
8min, then again with the speed stirring 4min filtering of 800r/min, gained filtrate is again washing lotion；
Step C: by the uniformly mixed rice washing water to obtain the final product of the just washing lotion and again washing lotion.
The red autumnal leaves crape myrtle skin care compositions and methods are made by following steps: being added after thickener 65 in deionized water
It is cooled to room temperature after stirring 12min at DEG C, then sequentially adds the plant extracts, animal extracts, rice washing water, moisturizing
It is stirred evenly after agent, preservative and essence after standing 13h at a temperature of being placed in 4 DEG C with 250 mesh net filtrations, gained filtrate is
The red autumnal leaves crape myrtle skin care compositions and methods.
The present invention is further illustrated below with reference to test example.
One, test material
It randomly selects -30 years old 20 years old and (is named as 20+Section), (be named as 30 within 30-40 years old+Section) and section (name in 40-50 years old
It is 40+Section) volunteer each 60 of three age brackets, the volunteer of each age bracket is randomly divided into six groups and uses blank respectively
The face uniformly smeared after the composition morning and evening face cleaning that group, control group and test group provide simultaneously gently is patted to fully absorbing, one
A month, two months and the roughness, humidity, fairness of skin of face are measured after five months respectively, and it is comprehensive to evaluate cutaneous sense
Index.
Two, test method:
1, roughness test: using dermatoglyph scanner Visioscan VC98 detection face skin roughness SEr with
The comprehensive score of wrinkle SEw, the smaller skin roughness of score are lower i.e. more smooth.
2, facial humidity of skin is tested using III humidity of skin tester of Akon SM-, humidity of skin is greater than 35% or more person
Frequent moisturizing is needed when normally, lower than 35%, humidity of skin indicates that skin condition is better.
3, whitening skin degree is tested using II flesh age tester of Sk-, test score 50 divides following whiteness poor, 50-75 mono-
As it is white, 75 or more is whiter.
4, cutaneous sense integrated evaluating method:
It randomly selects 10 males and 10 women respectively feels the skin of test group, control group and blank group personnel
Official's evaluation, it is each that assessment item is respectively as follows: whiteness, wrinkle, color spot, sophistication, elasticity, greasy degree and pore size, each project
10 parts are accounted for, comprehensive score is higher, and person's skin condition is better, and specific methods of marking is as shown in table 2.
2 cutaneous sense integrated evaluating method of table
Three, experimental result
From table 3 it can be seen that either to 20+Section or 30+Section or 40+For the user of section, the group of blank group is used
After closing object for a period of time, humidity, fairness, roughness and the sense organ comprehensive score of user face are before using compared to without showing
Variation is write, this is because in addition to basic moisturizer is free of any other skin caring ingredient in blank group, and wherein contain
Preservative, thickener, essence etc., after prolonged use possibly even have an adverse effect to skin；Use the group of control group
After closing object for a period of time, the skin condition of the user of three age brackets has all obtained a degree of improvement, this is because right
According to the reason provided by organizing in composition containing oyster extract provided by the present invention, slug extract and rice washing water, this
A little ingredients can prevent cutaneous pigmentation, delay skin aging, the speed of growth for reducing wrinkle to a certain extent, promote skin
Humidity etc., to improve skin on the whole, we are not difficult to find out from data, have just begun to use the composition of control group
When skin humidity, fairness, roughness etc. improvement it is smaller, this is mainly due to certain with meaning in the composition of control group
The skin caring ingredient of amount, but nutrition relatively delays the improvement of skin at not comprehensive, distribution ratio is incomplete, therefore at the initial stage of use
Slowly, but after long-time use the state of skin has still obtained more significant improvement compared to the blank group；It is provided using test group
Composition for a period of time after, humidity of skin, fairness, roughness and the sense organ comprehensive score of the volunteer of three age brackets
It is all significantly improved, improvement is significantly higher than blank group and control group in this, and improves with the rising at volunteer's age
Effect is more significant, needs to use the composition one of test group for the rougher crowd of moisturizing, skin especially for those
The humidity of skin can quickly recover to normal level after a month, and the smoothness of skin also significantly rises.
Finally, it should be noted that foregoing description is only the preferred embodiment of the present invention, the ordinary skill people of this field
Member under the inspiration of the present invention, without prejudice to the purpose of the present invention and the claims, can make multiple similar tables
Show, such transformation is fallen within the scope of protection of the present invention.
Claims (5)
1. a kind of red autumnal leaves crape myrtle skin care compositions and methods, it is characterised in that: in parts by weight, by 10-15 parts of plant extracts
Object, 5-9 parts of animal extracts, 12-15 parts of rice washing waters, 0.5-1 parts of thickeners, 0.5-2.5 parts of moisturizer, 0.01-0.02 parts anti-
Rotten agent, 0.01-0.05 parts of essence and 17-25 parts of deionized water compositions；
In parts by weight, the plant extracts is by 20-30 parts of red autumnal leaves banaba extracts and 6-10 parts of citrus extracts groups
At the animal extracts are made of 5-6 parts of oyster extracts and 3-7 parts of slug extracts；
In parts by weight, the red autumnal leaves banaba extract is purple by 20-38 parts of red autumnal leaves crape myrtle floral extracts and 7-11 parts of red autumnal leaves
Common vetch berry extract composition；
The red autumnal leaves crape myrtle floral extract is made by following steps:
Step a: it is sealed at ultrasound after 75% ethyl alcohol is added in the ratio that solid-liquid ratio is 1:1-3 after taking fresh red autumnal leaves common crapemyrtle flower to smash to pieces
20-30min is managed, separating filtrate and filter residue are then filtered；
Step b: sealing is ultrasonically treated 20- after dehydrated alcohol is added in the ratio that solid-liquid ratio is 1:3-5 in filter residue obtained by step a
Then 30min filters separating filtrate and filter residue；
Step c: gained filtrate in step a and step b is merged, be added glacial acetic acid the pH of filtrate after merging is adjusted to 6.2 ±
0.3 and with the speed of 30-50r/min stir 15-25min, centrifuging and taking supernatant；
Step d: by supernatant vacuum freeze drying described in step c up to the red autumnal leaves crape myrtle floral extract；
The red autumnal leaves crape myrtle berry extract is made by following steps:
Step is 1.: the dehydrated alcohol that concentration is 30-50% is added in the ratio for being 1:4-5 in solid-liquid ratio after taking red autumnal leaves crape myrtle fruit powder broken
Sealing and standing 10-12h afterwards, collected by suction filtrate；
Step is 2.: it is added the NaCl solution of 2-3% in the filtrate, the volume ratio of the filtrate and NaCl solution is 1:2-3,
Then heating and refluxing extraction 1.5-2h collects crude extract；
Step is 3.: by water-oil separating after crude extract centrifugation, by gained oil liquid at a temperature of -10 DEG C to -20 DEG C sealing and standing
It takes supernatant liquor to obtain after 15-24h and slightly mentions extract；
Step is 4.: it is described slightly mention in extract petroleum ether is added after stand 6-10h and take lower layer's heavy-fluid, it is described slightly mention extract and
The volume ratio of petroleum ether is 1:1-2；
Step is 5.: lower layer's heavy-fluid being carried out heating and refluxing extraction 1.5-2h again, collects refining liquid；
Step is 6.: by water-oil separating after refining liquid centrifugation, by gained oil liquid at a temperature of -10 DEG C to -20 DEG C sealing and standing
Take supernatant up to the red autumnal leaves crape myrtle berry extract after 15-24h；
The oyster extract is made by following steps:
Step 1: oyster being cleaned up into gutting, 1-2 times of weight is added together with oyster shell in the oyster meat after cleaning
Pure water and boil 20-30 minutes, then by oyster meat and oyster shell pull out natural cooling and respectively storage it is stand-by；
Step 2: oyster meat is taken, homogenate after the pure water of 2-3 times of its weight is added, subtilopeptidase A is then added, it is described
The mass ratio of subtilopeptidase A and oyster meat slurries is 3-5:50, and holding oyster slurries are 38-42 DEG C of enzymatic hydrolysis 3-4h, then
Filtering removal impurity, gained filtrate is oyster meat hydrolyzate；
Step 3: the oyster shell in step 1 be crushed into 400-500 mesh, the acid of 2-3 times of oyster shell powder weight is then added, and
Adjusting pH value is 4-4.5 acidolysis 2-3h, during which every the pH value of the hydrolyzate of test in 10-20 minutes, when the pH value of hydrolyzate
Supplemental acid or alkali make the pH value of hydrolyzate remain at 4-4.5 when less than 4 or greater than 4.5, adjust hydrolyzate after acidolysis
PH to 6.5-7.7, bromelain is added and is digested, the quality of the bromelain is the 1/15- of hydrolyzate quality
1/10, keeping hydrolyzate temperature is 50-55 DEG C, continues to filter after digesting 1-2h, and gained filtrate is oyster shell hydrolyzate；
Step 4: in parts by weight, the 3-5 parts of oyster meat hydrolyzates and 1 part of oyster shell hydrolyzate being uniformly mixed
Up to the oyster extract；
The slug extract is made by following steps:
Step (1): taking fresh slug, after the salting liquid that the concentration that 8-10 times of slug weight is added is 3-5% stands 20-30min,
Salting liquid containing slug is poured into tissue mashing machine and smashs to obtain slug slurries to pieces；
Step (2): the pH value for adjusting slug slurries is 1.5-2.5, and in parts by weight, 0.1- is added in every portion slug slurries
0.3 part of pepsin, then digests 1.5-2h at 35-37 DEG C；
Step (3): after the slug slurries after enzymatic hydrolysis are warming up to 80-100 DEG C of holding 2-5min, centrifuging and taking supernatant；
Step (4): the active carbon of 2-3% is added in the supernatant, filters after mixing evenly, collects filtrate, the filtrate is used
Rotation is concentrated by evaporation the 1/4-1/3 to original volume up to the slug extract after bag filter flowing water dialysis 20-30h.
2. red autumnal leaves crape myrtle skin care compositions and methods according to claim 1, it is characterised in that: the rice washing water is by following step
It is rapid to be made:
Step A: taking rice, is added after the sterile water of 2-3 times of its weight after being ultrasonically treated 3-5min and filters, and gained filtrate is previous cleaning
Liquid；
Step B: taking the rice in step A after previous cleaning, is ultrasonically treated 5-10min after the sterile water of 1-2 times of its weight is added again,
Then again with the speed stirring 3-5min filtering of 700-900r/min, gained filtrate is again washing lotion；
Step C: by the uniformly mixed rice washing water to obtain the final product of the just washing lotion and again washing lotion.
3. red autumnal leaves crape myrtle skin care compositions and methods according to claim 1, it is characterised in that: in parts by weight, institute
Thickener is stated to be made of 2-3 parts of algins, 1-3 parts of gloiopeltis glue, 1-2 parts of seaweed glues and 4-7 parts of carbomers.
4. red autumnal leaves crape myrtle skin care compositions and methods according to claim 1, it is characterised in that: in parts by weight, institute
Moisturizer is stated to be made of 5-7 parts of hyaluronic acids, 4-6 parts of chondroitin sulfates and 1-3 parts of lactic acid.
5. a kind of red autumnal leaves crape myrtle skin care compositions and methods preparation method, it is characterised in that: including described in claim any one of 1-4
Red autumnal leaves crape myrtle skin care compositions and methods, be made according to the following steps: in deionized water be added thickener after stirred at 60-70 DEG C
It is cooled to room temperature after mixing 10-15min, then sequentially adds the plant extracts, animal extracts, rice washing water, moisturizer, prevents
It stirs evenly after rotten agent and essence and is filtered after standing 12-15h at a temperature of being placed in 3-5 DEG C, gained filtrate is that the red autumnal leaves are purple
Common vetch skin care compositions and methods.
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| CN113456561A (en) * | 2021-07-09 | 2021-10-01 | 广西和桂集团有限公司 | Preparation method and application of essence containing polypeptide and plant extract |
Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101012285A (en) * | 2007-02-16 | 2007-08-08 | 大连水产学院 | Oyster polysaccharide, preparing method and its application in preparing cosmetics |
| CN104188883A (en) * | 2014-08-29 | 2014-12-10 | 广西大学 | Moisturizer and preparation method thereof |
| CN105395444A (en) * | 2015-11-19 | 2016-03-16 | 威海新异生物科技有限公司 | Method for preparing oyster facial mask |
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2016
- 2016-12-08 CN CN201611123448.8A patent/CN106389300B/en not_active Expired - Fee Related
Patent Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101012285A (en) * | 2007-02-16 | 2007-08-08 | 大连水产学院 | Oyster polysaccharide, preparing method and its application in preparing cosmetics |
| CN104188883A (en) * | 2014-08-29 | 2014-12-10 | 广西大学 | Moisturizer and preparation method thereof |
| CN105395444A (en) * | 2015-11-19 | 2016-03-16 | 威海新异生物科技有限公司 | Method for preparing oyster facial mask |
Non-Patent Citations (2)
| Title |
|---|
| 畅销整个亚洲的泡泡你见过吗;女人部落;《http://weidian.com/p5/diary/pages/diary.php?id=8776012》;20160503;女神泡泡成分及功效 |
| 紫薇提取物面部去皱作用的研究;张云青等;《中国美容医学》;20141231;第23卷(第10期);822页倒数第一段-823页第1段 |
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