CN106389194A - Double-layer spray essence with efficacies of preserving moisture, brightening skin and weakening wrinkles and preparation method of double-layer spray essence - Google Patents
Double-layer spray essence with efficacies of preserving moisture, brightening skin and weakening wrinkles and preparation method of double-layer spray essence Download PDFInfo
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/02—Cosmetics or similar toiletry preparations characterised by special physical form
- A61K8/04—Dispersions; Emulsions
- A61K8/046—Aerosols; Foams
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/92—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof
- A61K8/922—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof of vegetable origin
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/08—Anti-ageing preparations
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/40—Chemical, physico-chemical or functional or structural properties of particular ingredients
- A61K2800/52—Stabilizers
- A61K2800/524—Preservatives
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Abstract
The invention provides double-layer spray essence with the efficacies of preserving moisture, brightening skin and weakening wrinkles and a preparation method of the double-layer spray essence. The double-layer spray essence is prepared from the following components in percentage by weight: 1-25 % of fructus rosae oil, 1-15 % of sodium PCA, 1-10 % of natural moisturizing factors, 0-10 % of rose flower extract, 1-15 % of isododecane, 0-10 % of glycerinum, 0.1-3 % of mung bean seed extract, 0-5 % of calendula oil, 0-2 % of rose essential oil, 0-2 % of tocopheryl acetate, 0.1-2 % of sodium chloride, 0-1 % of rosemary leaf extract, 0.05-1 % of decyl glucoside, 0.1-2 % of a preservative, and the balance of water. The double-layer spray essence can comprehensively supplement and regulate the moisture and nutrition of the skin, effectively enhance the moist and lubrication properties of the skin, and also can effectively eliminate free radicals and resist glycosylation, so that the skin color is bright, the skin is compact, the wrinkles are faded, and then the skin is smooth and elastic, and has the natural luster.
Description
Technical field
The invention belongs to cosmetic technical field is and in particular to a kind of double-deck spraying essence with moisturizing skin lightening light stricture of vagina effect
China and preparation method thereof.
Background technology
Improve with living standard and scientific and technical development, the requirement more and more higher to cosmetics and skincare product for the people, thus
Promote cosmetic industry fast-developing, various both effectiveness, dosage form cosmetics persistently come out, and the cosmetics of water preparation type are more
It is to take the course of its own, occupy important position.In recent years, people gradually recognize that skin is coarse, drying is due to cuticlar water
Divide content not enough caused；Easily microgroove, the skin problem such as obscure in the skin being simultaneously dried.But water preparation in the market
Essence skincare product is typically uniform one, rare clear and legible double-deck spraying elite；Simultaneously to some skin problems of solution
Still suffer from certain limitation, so the water preparation elite that exploitation has skin lightening moisture-keeping efficacy has wide market prospect.
Content of the invention
For the defect of prior art, it is an object of the invention to provide a kind of double-deck spray with moisturizing skin lightening light stricture of vagina effect
Mist elite and preparation method thereof, what a kind of dosage form of exploitation was novel, easy to use extracts the double of elite rich in nature moisturizing factor and plant
Layer spraying elite, system adopts skin water oil golden ratio 75:25 are compounded, and can not only supplement comprehensively and adjust skin
Moisture and nutrient, are effectively increased moist degree and the lubricity of skin, and effectively can remove free radical, anti-glycosylation, from
And bright color, the skin that compacts, desalinate wrinkle, make skin smooth, high resilience, recover skin naturally brilliance.
The purpose of the present invention is achieved through the following technical solutions：
The invention provides a kind of double-deck spraying elite with moisturizing skin lightening light stricture of vagina effect, contain including following weight percent
Each component of amount：
1-25% Rosehips oil, 1-15%PCA sodium, 1-10% nature moisturizing factor, 0-10% Flos Rosae Rugosae extract, 1-
10% Fancol ID, 1-10% glycerol, 0.1-3% Semen phaseoli radiati seed extract, 0-2% Flos Inulae oil, 0-2% Flos Rosae Rugosae quintessence oil, 0-2%
Tocopherol acetass, 0-2% sodium chloride, 0-1% rosemary leaf extract, 0-0.5% decyl glucoside, appropriate preservative, remaining
Measure as water.
Preferably, including each component of following weight percentage：
2-20% Rosehips oil, 1-10%PCA sodium, 1-5% nature moisturizing factor, 1-10% Flos Rosae Rugosae extract, 1-
10% Fancol ID, 1-5% glycerol, 0.1-1% Semen phaseoli radiati seed extract, 1-5% Flos Inulae oil, 0.1-1% Flos Rosae Rugosae quintessence oil, 0.1-
1% tocopherol acetass, 0.1-1.5% sodium chloride, 0.1-0.5% rosemary leaf extract, 0.05-0.5% decyl glucoside,
0.5-1.5% preservative, balance of water.
The present invention contains Rosehips oil, Flos Rosae Rugosae extract and Flos Rosae Rugosae quintessence oil simultaneously, and the synergism of three can reach non-
Often good moisturizing skin lightening result.
Preferably, described water, Anjidew NL50, nature moisturizing factor, glycerol, sodium chloride, Flos Rosae Rugosae extract, Semen phaseoli radiati seed extract
Thing, decyl glucoside and preservative composition aqueous phase, described Rosehips oil, Fancol ID, Flos Inulae oil, tocopherol acetass, fan
Repeatedly Herba Pelargonii Graveolentis extract and Flos Rosae Rugosae quintessence oil composition oil phase, the weight of aqueous phase and oil phase ratio is for 75:25.
Preferably, described preservative is the preservative that can be used for food.
It is highly preferred that described preservative includes sodium benzoate, at least one in potassium sorbate.
Present invention also offers a kind of double-deck spraying elite as claimed in claim 1 with moisturizing skin lightening light stricture of vagina effect
Preparation method, comprise the following steps：
S1, weigh each component according to percentage by weight, by water, Anjidew NL50, nature moisturizing factor, glycerol, sodium chloride are put into instead
After answering pot stirring, insulation；
By Flos Rosae Rugosae extract after S2, cooling, Semen phaseoli radiati seed extract, sodium benzoate, decyl glucoside and potassium sorbate add
Enter the mixture A that stirs in reaction pot to obtain；
S3, by Rosehips oil, Fancol ID, Flos Inulae oil, tocopherol acetass, rosemary leaf extract and Flos Rosae Rugosae quintessence oil
Mixture B is obtained after mixing and stirring；
S4, mixture A is mixed the double-deck spraying elite described in obtaining final product with moisturizing skin lightening light stricture of vagina effect with mixture B.
Preferably, in step S1, described holding temperature is 85 DEG C, and temperature retention time is 20 minutes.
Preferably, in step S2, described it is cooled to 50 DEG C.
Compared with prior art, the present invention has following beneficial effect：
The essence of the present invention, first, the present invention be that a kind of dosage form is novel, easy to use rich in nature moisturizing factor and
Plant the double-deck spraying elite of extraction elite；Secondth, the present invention is food without any essence, pigment, the preservative being used
Class preservative, makes integral formula safer；3rd, this formula system is faintly acid, and normal pH range matches with skin,
The skin moisture-keeping factor being rich in can not only be supplemented from flesh bottom comprehensively and be adjusted moisture and the nutrient of skin, be effectively increased the taste of skin
Humidity and lubricity, and the plant extraction elite containing effectively can remove free radical, and anti-glycosylation, thus bright color, compact flesh
Skin, desalinate wrinkle, make skin smooth, high resilience, recover skin naturally brilliance.
Specific embodiment
With reference to specific embodiment, the present invention is described in detail.Following examples will be helpful to the technology of this area
Personnel further understand the present invention, but the invention is not limited in any way.It should be pointed out that the ordinary skill to this area
For personnel, without departing from the inventive concept of the premise, some deformation can also be made and improve.These broadly fall into the present invention
Protection domain.
Each component raw material involved by following examples and comparative example is the commercially available universal product, involved experimental technique
It is method commonly used in the art.
Embodiment 1
Present embodiments provide a kind of double-deck spraying elite with moisturizing skin lightening light stricture of vagina effect, including following weight percent
Each component of content：
47.2% water, 15% Rosehips oil, 10% Flos Rosae Rugosae extract, 8% Fancol ID, 5%PCA sodium, 5% natural guarantor
The wet factor, 5% glycerol, 0.6% Flos Inulae oil, 1% sodium chloride, 0.5% tocopherol acetass, 0.5% rosemary leaf extract,
0.5% Semen phaseoli radiati seed extract, 0.4% Flos Rosae Rugosae quintessence oil, 0.4% sodium benzoate, 0.5% decyl glucoside, 0.4% potassium sorbate.
The preparation method of the double-deck spraying elite with moisturizing skin lightening light stricture of vagina effect described in the present embodiment is as follows：
According to percentage by weight, aqueous phase first includes water, Anjidew NL50, nature moisturizing factor, glycerol, and sodium chloride puts into reaction
Pot, to 85 DEG C, insulation at a temperature of being somebody's turn to do is cooled to 50 DEG C of addition Flos Rosae Rugosae extracts after 20 minutes, Semen phaseoli radiati seed extracts for the stirring that heats up
Thing, sodium benzoate, decyl glucoside and potassium sorbate, after stirring, discharging is standby；Secondly oil phase is included Rosehips oil, different
After dodecane, Flos Inulae oil, tocopherol acetass, rosemary leaf extract and Flos Rosae Rugosae quintessence oil mixing and stirring, discharging is standby；
Finally aqueous phase and oil phase are mixed, you can obtain double-deck spraying elite.
Embodiment 2
Present embodiments provide a kind of double-deck spraying elite with moisturizing skin lightening light stricture of vagina effect, including following weight percent
Each component of content：
55.7% water, 10% Rosehips oil, 5% Flos Rosae Rugosae extract, 10% Fancol ID, 1%PCA sodium, 5% natural guarantor
The wet factor, 5% glycerol, 3% Flos Inulae oil, 1% sodium chloride, 1% tocopherol acetass, 0.1% rosemary leaf extract, 1%
Semen phaseoli radiati seed extract, 0.9% Flos Rosae Rugosae quintessence oil, 0.5% sodium benzoate, 0.2% decyl glucoside, 0.6% potassium sorbate.
The preparation method of double-deck spraying elite and embodiment 1 phase with moisturizing skin lightening light stricture of vagina effect described in the present embodiment
With.
Embodiment 3
Present embodiments provide a kind of double-deck spraying elite with moisturizing skin lightening light stricture of vagina effect, including following weight percent
Each component of content：59.8% water, 20% Rosehips oil, 1% Flos Rosae Rugosae extract, 1% Fancol ID, 10%PCA sodium, 1%
Nature moisturizing factor, 1% glycerol, 3% Flos Inulae oil, 1.5% sodium chloride, 0.1% tocopherol acetass, 0.5% leaf of Herba Rosmarini Officinalis
Extract, 0.1% Semen phaseoli radiati seed extract, 0.4% Flos Rosae Rugosae quintessence oil, 0.15% sodium benzoate, 0.05% decyl glucoside, 0.4%
Potassium sorbate.
The preparation method of double-deck spraying elite and embodiment 1 phase with moisturizing skin lightening light stricture of vagina effect described in the present embodiment
With.
Comparative example 1-5
Comparative example 1-5 provides a kind of double-deck spraying elite, weight percentage such as table 1 institute of its component and each component
Show.
Table 1
| Component | Comparative example 1 | Comparative example 2 | Comparative example 3 | Comparative example 4 | Comparative example 5 |
| Rosehips oil | 0 | 10 | 10.9 | 20 | 2 |
| Fancol ID | 10 | 10 | 10 | 10 | 8 |
| Flos Inulae oil | 3 | 3 | 3 | 3 | 3 |
| Tocopherol acetass | 1 | 1 | 1 | 1 | 1 |
| Rosemary leaf extract | 0.1 | 0.1 | 0.1 | 0.1 | 0.1 |
| Flos Rosae Rugosae quintessence oil | 10.9 | 0.9 | 0 | 0.9 | 0.9 |
| Flos Rosae Rugosae extract | 5 | 0 | 5 | 5 | 10 |
| Sodium chloride | 1 | 1 | 1 | 1 | 1 |
| Anjidew NL50 | 1 | 1 | 1 | 1 | 1 |
| Nature moisturizing factor | 5 | 5 | 5 | 5 | 5 |
| Semen phaseoli radiati seed extract | 1 | 1 | 1 | 1 | 1 |
| Glycerol | 5 | 5 | 5 | 5 | 5 |
| Sodium benzoate | 0.5 | 0.5 | 0.5 | 0.5 | 0.5 |
| Decyl glucoside | 0.2 | 0.2 | 0.2 | 0.2 | 0.2 |
| Potassium sorbate | 0.6 | 0.6 | 0.6 | 0.6 | 0.6 |
| Water | 55.7 | 60.7 | 55.7 | 45.7 | 60.7 |
Compliance test result：
1st, moisturizing test
Method：It is divided into short-acting moisturizing to measure the mensure with long-acting moisturizing.30 healthy dry skin volunteers participate in
This experiment, men and women do not limit, the age 18-65 year between, do not participated within nearest three months any medicine, cosmetics or health care
The clinical trial of product.
1.1 short-acting moisturizings
Identify 8 regions of Instrument measuring, left and right shank mark with shifting to an earlier date ready template in experimenter's left and right arm
Know 6 regions Instrument measuring, size is 4*2.5cm2；
Remove the blank district of left and right arm, use sample in all test sections, sample usage amount is 2mg/cm2；
Skin is first washed, skin is measured after doing again after 30min before basic value test；Sample uses afterwards
1h afterwards, 4h, 8h are measured；
This test instrunment is Corneometer (CK), for measuring the moisture of skin；First use before testing every time
Water clearing skin, after 30min, skin is measured after doing again；
Laboratory ambient temperature controls at 22 ± 2 DEG C, and relative humidity is 50 ± 5%.
1.2 long-acting moisturizings
Identify 8 regions of Instrument measuring with shifting to an earlier date ready template in experimenter's left and right arm, size is 4*
2.5cm2；
Remove the blank district of left and right arm, in all test sections skin marking pen labelling, sooner or later respectively use once,
Continuously use 30d sample, sample usage amount is 2mg/cm2；
Other any skin care item or medicine can not be used in 30d
This test instrunment is Corneometer (CK), for measuring the moisture of skin；Testing time point is sample
Using front, after sample use 1w, 2w, 3w, 4w；Skin is first washed, after skin is done after 30min again before testing every time
It is measured (laboratory ambient temperature controls at 22 ± 2 DEG C, and relative humidity is 50 ± 5%), during experiment, keep original life
Rule.
The double-deck spraying elite with moisturizing skin lightening light stricture of vagina effect of embodiment 1-3 and the preparation of comparative example 1-6 is protected
Wet compliance test result, its experimental result is as shown in table 2 and table 3.
The short-acting moisturizing test result of table 2.
The long-acting moisturizing test result of table 3.
The result of table 2 and table 3 shows, the double-deck spraying elite of present invention preparation has good moistening effect.
2nd, antioxidation testDPPH free radical scavenging is tested
Principle：DPPH method was suggested in 1958, was widely used in the oxidation resistance of quantitative determination Biosample and food.
This method is that have single electron according to DPPH free radical, has the last one to absorb at 517nm, and its alcoholic solution is in the characteristic of purple.When have from
In the presence of base scavenger, so that it is absorbed and fade away due to matching with its single electron, the electricity that its fading extent is accepted with it
Quantum count becomes quantitative relationship, thus available spectrophotometer carries out quick quantitative analyses.
Experiment flow：
(1) configure DPPH solution：Accurately weigh 20mgDPPH, with dehydrated alcohol constant volume in 250ml volumetric flask, obtain dense
Spend the DPPH solution for 2.0 × 10-4mol/L, keep in Dark Place standby.
(2) take 2ml sample liquid respectively in tool plug test tube, add the DPPH solution that 2ml is configured, mix homogeneously, in 25
After airtight standing 30min in DEG C water-bath, pour the cuvette that optical path is 1cm into, go out to record its absorbance A i in 517nm, survey simultaneously
2ml sample adds absorbance A j of 2ml ethanol, and 2ml DPPH solution adds the absorbance A 0 of 2ml redistilled water.Often survey one
Used in amounts will survey three panel datas.Sample liquid adopts the extracting solution in embodiment and comparative example.
(3) clearance rate of DPPH=[1 one (Ai-Aj)/A0] * 100%
Experimental result is as shown in table 4：
Table 4
As shown in Table 4, the double-deck spraying elite of present invention preparation has good antioxidant effect.
3rd, desalination wrinkle test
Select 90 people as tester, all have obvious crows-feet, be equally divided into 10 groups, the face of 10 groups of subjects
Try out the double-deck spraying elite with moisturizing skin lightening light stricture of vagina effect of embodiment 1-3 respectively, the daily morning and evening respectively uses 1 time, shares
30 days, observe trial effect, acquired results are shown in Table 6.
Test index：Significantly crows-feet be ×；Shallower crows-feet is zero；Crows-feet is not had to be √；
Test condition：(1) indoor environment；(2) no sunburst or light direct projection；(3) 20 ± 2 DEG C of ambient temperature, environment
Humidity 40-60%.
The crows-feet test result of the economic benefits and social benefits maintenance elite stock solution of table 6 embodiment 1-3
As can be seen from Table 6, the present invention has preferably light stricture of vagina effect.
In sum, the formula system of the present invention is faintly acid, and normal pH range matches with skin, the skin being rich in
Skin Moisture factor can not only be supplemented from flesh bottom comprehensively and be adjusted moisture and the nutrient of skin, be effectively increased moist degree and the profit of skin
Slip, and the plant extraction elite containing effectively can remove free radical, anti-glycosylation, thus bright color, the skin that compacts, desalination wrinkle
Stricture of vagina, make skin smooth, high resilience, recover skin naturally brilliance.
Concrete application approach of the present invention is a lot, and the above is only the preferred embodiment of the present invention.It should be pointed out that more than
Embodiment is merely to illustrate the present invention, and is not limited to protection scope of the present invention.Common skill for the art
For art personnel, under the premise without departing from the principles of the invention, some improvement can also be made, these improvement also should be regarded as this
Bright protection domain.
Claims (7)
1. a kind of double-deck spraying elite with moisturizing skin lightening light stricture of vagina effect is it is characterised in that include following weight percentage
Each component：
1-25% Rosehips oil, 1-15%PCA sodium, 1-10% nature moisturizing factor, 0-10% Flos Rosae Rugosae extract, 1-15% is different
Dodecane, 0-10% glycerol, 0.1-3% Semen phaseoli radiati seed extract, 0-5% Flos Inulae oil, 0-2% Flos Rosae Rugosae quintessence oil, 0-2% tocopherol
Acetass, 0.1-2% sodium chloride, 0-1% rosemary leaf extract, 0.05-1% decyl glucoside, 0.1-2% preservative, remaining
Measure as water.
2. there is the double-deck spraying elite of moisturizing skin lightening light stricture of vagina effect as claimed in claim 1 it is characterised in that including following
Each component of weight percentage：
2-20% Rosehips oil, 1-10%PCA sodium, 1-5% nature moisturizing factor, 1-10% Flos Rosae Rugosae extract, 1-10% is different
Dodecane, 1-5% glycerol, 0.1-1% Semen phaseoli radiati seed extract, 1-5% Flos Inulae oil, 0.1-1% Flos Rosae Rugosae quintessence oil, 0.1-1% gives birth to
Educate phenol acetass, 0.1-1.5% sodium chloride, 0.1-0.5% rosemary leaf extract, 0.05-0.5% decyl glucoside, 0.5-
1.5% preservative, balance of water.
3. there is the double-deck spraying elite of moisturizing skin lightening light stricture of vagina effect as claimed in claim 1 or 2 it is characterised in that described
Water, Anjidew NL50, nature moisturizing factor, glycerol, sodium chloride, Flos Rosae Rugosae extract, Semen phaseoli radiati seed extract, decyl glucoside and anti-corrosion
Agent forms aqueous phase, described Rosehips oil, Fancol ID, Flos Inulae oil, tocopherol acetass, rosemary leaf extract and rhodamine toner
Line of oils becomes the weight of oil phase, aqueous phase and oil phase than for 75:25.
4. there is the double-deck spraying elite of moisturizing skin lightening light stricture of vagina effect as claimed in claim 4 it is characterised in that described anti-corrosion
Agent is the preservative that can be used for food.
5. a kind of preparation method of the double-deck spraying elite as claimed in claim 1 with moisturizing skin lightening light stricture of vagina effect, it is special
Levy and be, comprise the following steps：
S1, weigh each component according to percentage by weight, by water, Anjidew NL50, nature moisturizing factor, glycerol, sodium chloride put into reaction pot
After stirring, insulation；
By Flos Rosae Rugosae extract after S2, cooling, Semen phaseoli radiati seed extract, in decyl glucoside and preservative addition reaction pot, stirring is equal
Even mixture A；
S3, by Rosehips oil, Fancol ID, Flos Inulae oil, tocopherol acetass, rosemary leaf extract and Flos Rosae Rugosae quintessence oil mix
Mixture B is obtained after stirring；
S4, mixture A is mixed the double-deck spraying elite described in obtaining final product with moisturizing skin lightening light stricture of vagina effect with mixture B.
6. there is the preparation method of the double-deck spraying elite of moisturizing skin lightening light stricture of vagina effect as claimed in claim 5, its feature exists
In in step S1, described holding temperature is 85 DEG C, and temperature retention time is 20 minutes.
7. there is the preparation method of the double-deck spraying elite of moisturizing skin lightening light stricture of vagina effect as claimed in claim 5, its feature exists
In, in step S2, described being cooled to 50 DEG C.
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| CN108078850A (en) * | 2018-01-05 | 2018-05-29 | 湖北瑞晟生物有限责任公司 | A kind of fragrant profit moisturizing elite and preparation method thereof |
| CN110585088A (en) * | 2019-10-15 | 2019-12-20 | 广州环亚化妆品科技有限公司 | Skin brightening composition and preparation method and application thereof |
| CN110891548A (en) * | 2017-05-16 | 2020-03-17 | Lvmh研究公司 | Cosmetic composition comprising rose extract |
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| CN105663020A (en) * | 2016-02-19 | 2016-06-15 | 天津天狮生物发展有限公司 | Spraying water with long-acting moisture-preserving capacity and preparation method thereof |
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| CN110585088B (en) * | 2019-10-15 | 2023-03-21 | 广州环亚化妆品科技股份有限公司 | Skin brightening composition and preparation method and application thereof |
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