CN106309247A - Production technique for nymphaea hybrid extractive and application - Google Patents
Production technique for nymphaea hybrid extractive and application Download PDFInfo
- Publication number
- CN106309247A CN106309247A CN201610887116.0A CN201610887116A CN106309247A CN 106309247 A CN106309247 A CN 106309247A CN 201610887116 A CN201610887116 A CN 201610887116A CN 106309247 A CN106309247 A CN 106309247A
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- CN
- China
- Prior art keywords
- flos nelumbinis
- perfume flos
- protease
- nelumbinis extract
- perfume
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- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
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Classifications
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/02—Preparations for care of the skin for chemically bleaching or whitening the skin
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/08—Anti-ageing preparations
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/80—Process related aspects concerning the preparation of the cosmetic composition or the storage or application thereof
- A61K2800/805—Corresponding aspects not provided for by any of codes A61K2800/81 - A61K2800/95
Abstract
The invention discloses a production technique for nymphaea hybrid extractive and an application. The production technique comprises the following steps: (1) performing enzymolysis; (2) extracting; (3) purifying; and (4) concentrating and drying. The production technique disclosed by the invention is efficient, quick and energy-saving; no harmful solvent is added; the temperature of the whole extraction process is not above 70 DEG C; and the functional components of the nymphaea hybrid are effectively maintained. The nymphaea hybrid extractive can be widely applied to a cosmetic formula so as to achieve the functions of obviously resisting oxidation, resisting wrinkles, moisturizing and whitening skin, relieving color spots, brightening skin, and the like.
Description
Technical field
The present invention relates to production technology and the application of a kind of perfume Flos Nelumbinis extract, belong to biological technical field.
Background technology
Perfume Flos Nelumbinis original producton location is Taiwan, belongs to composition warm in nature, lemon acid decaffeinated, single, nonirritant, without pesticide and
Any additive, the thing of natural sky one-tenth, world's difficulty is sought.Rich in anthocyanin, natural pigment, flavone, many in perfume Flos Nelumbinis extract
The active skull cap components such as sugar, SOD, active polypeptide, vitamin, mineral element, in cosmetic formulations, play significant antioxygen
Change, crease-resistant, moisturizing, whitening, desalination mottle, the effect such as skin lightening.Natural constituent in perfume Flos Nelumbinis extract can penetrate
Deep skin, improves skin state through blood transport oxygen, moisture, nutrition to cell, strong activation cell, entirety, makes skin
Obtain Regeneration and Repair, from source, block and solve that female face is low and deep, coarse, wrinkle, mottle, lax, acne etc. many
Problem.
In technique, much plant carry product use be spray-dried, high-temperature vacuum is dried, lyophilization carries out plant extract
Produce.But, perfume Flos Nelumbinis extract is rich in anthocyanin, natural pigment, flavone, polysaccharide, SOD, active polypeptide, vitamin E etc.
Active skull cap components, be spray-dried, high-temperature vacuum be dried all can make a lot of active component at high temperature can deactivation, and vacuum
The shortcomings such as dry then existence is consumed energy greatly, time length, part macromole biological structure are damaged.The present invention uses vitrescence seasoning to do
Dry perfume Flos Nelumbinis extract, vitrescence dry technology full name is vitrescence bio-reversible dry technology, is according to cytobiology principle,
With reference to superconductor technology and low-temperature biological electron microscopy, modern biology investigative technique is injected in traditional handicraft and is developed
A kind of new dry technology, the more current vacuum freeze drying technology of its design principle is very different, is current latest generation
Dry technology, be also the upgrade technique of future generation of vacuum freeze-drying technology, current vacuum lyophilization can be solved
High energy consumption problem in the presence of technology, it is possible to improve the raw material such as food, biological product and medicine after dry,
The degree reverting to fresh state during rehydration, so being referred to as bioreversible dry technology, and current all of dry skill
Art, in addition to vacuum freeze drying technology, other dry technologies are all irreversible, and its dry products nearly all can not after rehydration
Return to its fresh state, and the degree of reversibility that vitrescence is dried is higher than lyophilization.It addition, the present invention uses hyperfiltration technique to carry out
Purification, Ultra filtration membrane technology is separating-purifying and the concentration technique of an emerging multi-crossed disciplines, have equipment simple, can
Normal-temperature operation, without phase transformation and chemical change, selectivity high and low power consumption and other advantages, be suitable to process heat-sensitive substance and biological activity
Material.
Summary of the invention
The present invention provides production technology and the application of a kind of perfume Flos Nelumbinis extract, creative science to extract perfume lotus
Effective ingredient, and be applied in all kinds of cosmetics.The invention have the advantages that 1, through biological enzymolysis, make in perfume Flos Nelumbinis
Effective ingredient is fully dissolved out, and makes extraction more abundant；2, use vitrescence dry technology to be dried, there is efficiency height, low, life of consuming energy
Thing reversibility high；3, whole production process is less than 70 DEG C, it is ensured that the activity in perfume Flos Nelumbinis extract and nutrient
Matter is not destroyed；4, use Ultra filtration membrane technology to be purified, do not introduce harmful chemical.
The production technology of a kind of perfume Flos Nelumbinis extract of the present invention and application, is characterized in that: 1, described perfume Flos Nelumbinis
The production technology of extract comprises the steps:
(1) enzymolysis: with perfume Flos Nelumbinis as raw material, mixes with 5～6 times of weight water, add 0.1～0.5% pectase and 0.2～
1.0% protease, stirs 4～5h at 40～60 DEG C；
(2) extracting: with edible ethanol, feed liquid being adjusted to ethanol content is 30%, boiling reflux extracts 1.5～2.5h, filters to obtain filter
Liquid；
(3) purification: enzymolysis solution is carried out ultrafiltration with the ultrafilter membrane that molecular weight is 20000 Da, when trapped fluid reaches total enzymolysis solution volume
1/8～1/10 time, stop ultrafiltration, obtain permeate；
(4) concentrate drying: use vacuum concentrate methool to remove ethanol, and be concentrated into the 1/10 of feed liquid, uses vitrescence seasoning to be dried
Obtain perfume Flos Nelumbinis extract dry powder.
2, according in the step (1) described in 1, protease is papain, trypsin, compound protease, neutral egg
One or several in white enzyme and pepsin.
3, according in the step (4) described in 1, vitrescence is dried method particularly includes: (1) concentrated solution puts into-40 DEG C of freeze dryers
Middle pre-freeze 3～4h；(2) to freeze dryer evacuation, make vacuum to 1～10Pa, maintain 3～4h；(3) it is warming up to-20 DEG C in 2h,
Maintain 2～3h；(4) 30min is warming up to 20 DEG C, maintains 8～10h；(5) it is passed through cleaned air, makes freeze dryer reply normal pressure, obtain fragrant
Water Flos Nelumbinis extract dry powder.
4, perfume Flos Nelumbinis extract can be widely used in cosmetic formulations, plays significant antioxidation, crease-resistant, moisturizing, U.S.
In vain, effect such as desalination mottle, skin lightening etc..
Detailed description of the invention
Embodiment 1: weigh perfume Flos Nelumbinis 100 kg, mixes with 550 kg water, adds 0.3% pectase and 0.7% wood
Melon protease, stirs 4.5h at 50 DEG C；With edible ethanol, feed liquid being adjusted to ethanol content is 30%, and boiling reflux extracts 2 h,
Filter to get filtrate；With the ultrafilter membrane that molecular weight is 20000 Da, enzymolysis solution is carried out ultrafiltration, when trapped fluid reaches total enzymolysis solution volume
1/9 time, stop ultrafiltration, obtain permeate；Using vacuum concentrate methool to remove ethanol, and be concentrated into the 1/10 of feed liquid, concentrated solution is put
Enter pre-freeze 3.5 h in-40 DEG C of freeze dryers, to freeze dryer evacuation, make vacuum to 3 Pa, maintain 3.5 h, be warming up in 2 h-
20 DEG C and maintain 2.5 h, 30min to be warming up to 20 DEG C, maintain 9 h, be passed through cleaned air, make freeze dryer reply normal pressure, obtain perfume
Flos Nelumbinis extract dry powder.In facial mask essence formula, add 0.2% perfume Flos Nelumbinis extract dry powder, facial film can be obviously enhanced
Moisturizing, whitening, skin lightening and effect of desalination mottle.
Embodiment 2: weigh perfume Flos Nelumbinis 100 kg, mixes with 500 kg water, adds 0.1% pectase and 0.2% pancreas
Protease, stirs 4 h at 40 DEG C；With edible ethanol, feed liquid being adjusted to ethanol content is 30%, and boiling reflux extracts 1.5 h,
Filter to get filtrate；With the ultrafilter membrane that molecular weight is 20000 Da, enzymolysis solution is carried out ultrafiltration, when trapped fluid reaches total enzymolysis solution volume
1/8 time, stop ultrafiltration, obtain permeate；Using vacuum concentrate methool to remove ethanol, and be concentrated into the 1/10 of feed liquid, concentrated solution is put
Enter pre-freeze 3 h in-40 DEG C of freeze dryers, to freeze dryer evacuation, make vacuum to 1 Pa, maintain 3 h, in 2 h, be warming up to-20 DEG C
And maintain 2 h, 30 min to be warming up to 20 DEG C, maintain 8 h, be passed through cleaned air, make freeze dryer reply normal pressure, obtain perfume Flos Nelumbinis and carry
Take thing dry powder.In eye cream formula, add 0.1% perfume Flos Nelumbinis extract dry powder, can be obviously enhanced eye cream moisturizing, crease-resistant with
And eye haustra-dsipelling effect.
Embodiment 3: weigh perfume Flos Nelumbinis 100 kg, mixes with 600 kg water, adds 0.5% pectase and 1% and is combined
Protease, stirs 5 h at 60 DEG C；With edible ethanol, feed liquid being adjusted to ethanol content is 30%, and boiling reflux extracts 2.5 h,
Filter to get filtrate；With the ultrafilter membrane that molecular weight is 20000 Da, enzymolysis solution is carried out ultrafiltration, when trapped fluid reaches total enzymolysis solution volume
1/10 time, stop ultrafiltration, obtain permeate；Using vacuum concentrate methool to remove ethanol, and be concentrated into the 1/10 of feed liquid, concentrated solution is put
Enter pre-freeze 4 h in-40 DEG C of freeze dryers, to freeze dryer evacuation, make vacuum to 10 Pa, maintain 4 h, in 2 h, be warming up to-20
DEG C and maintain 3 h, 30 min to be warming up to 20 DEG C, maintain 10 h, be passed through cleaned air, make freeze dryer reply normal pressure, obtain perfume lotus
Flower extract dry powder.In day cream or late frost formula, add 0.3% perfume Flos Nelumbinis extract dry powder, day cream or evening can be obviously enhanced
The moisturizing of frost, whitening effect.
Finally, in addition it is also necessary to be only several specific embodiments of the present invention it is noted that listed above.Obviously, this
Bright it is not limited to above example, it is also possible to have many deformation.Those of ordinary skill in the art can be from present disclosure
The all deformation directly derived or associate, are all considered as protection scope of the present invention.
Claims (4)
1. the production technology of a perfume Flos Nelumbinis extract, it is characterised in that comprise the steps:
(1) enzymolysis: with perfume Flos Nelumbinis as raw material, mixes with 5～6 times of weight water, add 0.1～0.5% pectase and 0.2～
1.0% protease, stirs 4～5h at 40～60 DEG C；
(2) extracting: with edible ethanol, feed liquid being adjusted to ethanol content is 30%, boiling reflux extracts 1.5～2.5h, filters to obtain filter
Liquid；
(3) purification: enzymolysis solution is carried out ultrafiltration with the ultrafilter membrane that molecular weight is 20000Da, when trapped fluid reaches total enzymolysis solution volume
1/8～1/10 time, stop ultrafiltration, obtain permeate；
(4) concentrate drying: use vacuum concentrate methool to remove ethanol, and be concentrated into the 1/10 of feed liquid, uses vitrescence seasoning to be dried
Obtain perfume Flos Nelumbinis extract dry powder.
In step the most according to claim 1 (1), protease be papain, trypsin, compound protease, in
One or several in property protease and pepsin.
In step the most according to claim 1 (4), vitrescence is dried method particularly includes: (1) concentrated solution is put into-40 DEG C and frozen
Pre-freeze 3～4h in dry machine；(2) to freeze dryer evacuation, make vacuum to 1～10Pa, maintain 3～4h；(3) be warming up in 2h-
20 DEG C, maintain 2～3h；(4) 30min is warming up to 20 DEG C, maintains 8～10h；(5) it is passed through cleaned air, makes freeze dryer often reply
Pressure, obtains perfume Flos Nelumbinis extract dry powder.
4. perfume Flos Nelumbinis extract can be widely used in cosmetic formulations, plays significant antioxidation, crease-resistant, moisturizing, whitening, light
Change the effect such as mottle, skin lightening.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201610887116.0A CN106309247A (en) | 2016-10-12 | 2016-10-12 | Production technique for nymphaea hybrid extractive and application |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201610887116.0A CN106309247A (en) | 2016-10-12 | 2016-10-12 | Production technique for nymphaea hybrid extractive and application |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN106309247A true CN106309247A (en) | 2017-01-11 |
Family
ID=57821394
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201610887116.0A Pending CN106309247A (en) | 2016-10-12 | 2016-10-12 | Production technique for nymphaea hybrid extractive and application |
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| CN (1) | CN106309247A (en) |
Cited By (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN106727065A (en) * | 2017-03-31 | 2017-05-31 | 佛山汇沐化学科技有限公司 | A kind of antibacterial lip gloss |
| CN109303734A (en) * | 2018-12-13 | 2019-02-05 | 北京天奇益人健康科技有限公司 | A kind of perfume Flos Nelumbinis extract and its preparing the application in cosmetics |
| CN110237003A (en) * | 2019-07-10 | 2019-09-17 | 西双版纳宝翠香莲生物科技有限公司 | A kind of perfume Flos Nelumbinis extract and its application in skin care item |
| CN113632897A (en) * | 2021-08-18 | 2021-11-12 | 合肥童学密码教育咨询有限公司 | Beverage based on water lily and preparation process thereof |
| CN115737495A (en) * | 2022-10-26 | 2023-03-07 | 现代百朗德生物科技(江苏)有限公司 | Siji flower essence extracting solution with anti-inflammatory, antioxidant, whitening and anti-wrinkle effects and preparation method thereof |
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- 2016-10-12 CN CN201610887116.0A patent/CN106309247A/en active Pending
Patent Citations (1)
| Publication number | Priority date | Publication date | Assignee | Title |
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| CN104664405A (en) * | 2014-09-04 | 2015-06-03 | 杭州隽艺生物技术有限公司 | Fat-reducing and weight-losing fruit enzyme powder and preparation method thereof |
Non-Patent Citations (3)
| Title |
|---|
| 宋丽雅等: "《化妆品植物功效添加剂的研究与开发》", 30 September 2011, 中国轻工业出版社 * |
| 车璐: "香水莲花抗氧化及抑制5α-还原酶的研究", 《中国优秀硕士学位论文数据库 医药卫生科技辑》 * |
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Cited By (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN106727065A (en) * | 2017-03-31 | 2017-05-31 | 佛山汇沐化学科技有限公司 | A kind of antibacterial lip gloss |
| CN109303734A (en) * | 2018-12-13 | 2019-02-05 | 北京天奇益人健康科技有限公司 | A kind of perfume Flos Nelumbinis extract and its preparing the application in cosmetics |
| CN110237003A (en) * | 2019-07-10 | 2019-09-17 | 西双版纳宝翠香莲生物科技有限公司 | A kind of perfume Flos Nelumbinis extract and its application in skin care item |
| CN113632897A (en) * | 2021-08-18 | 2021-11-12 | 合肥童学密码教育咨询有限公司 | Beverage based on water lily and preparation process thereof |
| CN115737495A (en) * | 2022-10-26 | 2023-03-07 | 现代百朗德生物科技(江苏)有限公司 | Siji flower essence extracting solution with anti-inflammatory, antioxidant, whitening and anti-wrinkle effects and preparation method thereof |
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| PB01 | Publication | ||
| SE01 | Entry into force of request for substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| WD01 | Invention patent application deemed withdrawn after publication | ||
| WD01 | Invention patent application deemed withdrawn after publication |
Application publication date: 20170111 |