CN110237003A - A kind of perfume Flos Nelumbinis extract and its application in skin care item - Google Patents
A kind of perfume Flos Nelumbinis extract and its application in skin care item Download PDFInfo
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- CN110237003A CN110237003A CN201910619139.7A CN201910619139A CN110237003A CN 110237003 A CN110237003 A CN 110237003A CN 201910619139 A CN201910619139 A CN 201910619139A CN 110237003 A CN110237003 A CN 110237003A
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- Prior art keywords
- flos nelumbinis
- nelumbinis extract
- filtrate
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
- A61K8/9783—Angiosperms [Magnoliophyta]
- A61K8/9789—Magnoliopsida [dicotyledons]
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/02—Preparations for care of the skin for chemically bleaching or whitening the skin
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/08—Anti-ageing preparations
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/80—Process related aspects concerning the preparation of the cosmetic composition or the storage or application thereof
- A61K2800/805—Corresponding aspects not provided for by any of codes A61K2800/81 - A61K2800/95
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- Health & Medical Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Veterinary Medicine (AREA)
- Public Health (AREA)
- General Health & Medical Sciences (AREA)
- Animal Behavior & Ethology (AREA)
- Dermatology (AREA)
- Microbiology (AREA)
- Epidemiology (AREA)
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- Mycology (AREA)
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- Biotechnology (AREA)
- Engineering & Computer Science (AREA)
- Gerontology & Geriatric Medicine (AREA)
- Cosmetics (AREA)
Abstract
The invention belongs to field of biotechnology, disclose a kind of preparation method of perfume Flos Nelumbinis extract, include the following steps: that (1) crushes perfume lotus flower, the aqueous solution for blending 6-10 times of object weight is added, alkali protease and pectase is added, 2.5-4h is digested at 45 DEG C -55 DEG C, is then filtered, and filtrate and filtrate A are obtained；(2) dehydrated alcohol is added into filtrate, microwave treatment to mixeding liquid temperature reaches 60-80 DEG C, and then ultrasonic extraction 20-40min, filters to obtain filter residue, deionized water ultrasonic extraction 15-30min will be added in filter residue, obtains liquor B；(3) filtrate A and liquor B are merged, after filtering, desalination, decoloration and sterilization treatment, obtains extracting solution；(4) extracting solution is dried by vacuum refrigeration, obtains perfume Flos Nelumbinis extract.The perfume Flos Nelumbinis extract of the method for the present invention preparation can be widely used in cosmetic formulations, play significant anti-oxidant, crease-resistant, moisturizing, whitening, lighten the stain, skin lightening the effects of.
Description
Technical field
The invention belongs to field of biotechnology, in particular to a kind of perfume Flos Nelumbinis extract and the application in skin care item.
Background technique
The needed protein of human body, carbohydrate, vitamin, active peptides, mineral are rich in perfume Flos Nelumbinis extract
The nutritions such as matter, cellulose, while the plant placeula element contained in perfume lotus flower plays balanced human's endocrine system
Very crucial effect can propose that it is obscure that long-time service can improve skin for skin nutrition element and minerals, lubricate skin
It is careful glossy, play significant anti-oxidant, crease-resistant, moisturizing, whitening, lighten the stain, skin lightening the effects of.
Currently, traditional plant extraction process mostly uses greatly vacuum drying, spray drying, it is rich in perfume Flos Nelumbinis extract
The active skull cap components such as anthocyanin, natural pigment, flavones, polysaccharide, SOD, active peptides, vitamin E can be denaturalized at high temperature
Inactivation, the effect of leading to active reduction, influence skin care item.
Summary of the invention
The technical problem to be solved by the present invention is to overcome drawbacks described above, a kind of perfume Flos Nelumbinis extract is provided and in skin care item
In application.
In order to solve the above-mentioned technical problem, the technical solution of the present invention is as follows:
A kind of preparation method of perfume Flos Nelumbinis extract, which comprises the following steps:
(1) perfume lotus flower is crushed, the aqueous solution for blending 6-10 times of object weight is added, alkali protease and pectin is added
Enzyme digests 2.5-4h at 45 DEG C -55 DEG C, is then filtered, and obtains filtrate and filtrate A；
(2) dehydrated alcohol is added into filtrate, microwave treatment to mixeding liquid temperature reaches 60-80 DEG C, then ultrasonic extraction
20-40min filters to obtain filter residue, deionized water ultrasonic extraction 15-30min will be added in filter residue, obtains liquor B；
(3) filtrate A and liquor B are merged, after filtering, desalination, decoloration and sterilization treatment, obtains extracting solution；
(4) extracting solution is dried by vacuum refrigeration, obtains perfume Flos Nelumbinis extract.
Preferably, the mass ratio of step (1) alkali protease and pectase is 1:2-5.
Preferably, the additional amount of step (2) described dehydrated alcohol is 8-12 times of filtrate weight.
Preferably, step (2) microwave power is 400-600W, and the supersonic frequency is 20-30KHz, ultrasonic power
For 200-300W.
Preferably, step (4) vacuum freeze drying is in -30 DEG C of freezing 2-5h, and then 2-3h is warming up to 25-30
DEG C, dry 4-6h obtains perfume Flos Nelumbinis extract.
It is a further object of the present invention to provide a kind of perfume Flos Nelumbinis extract the answering in skin care item of above method preparation
With, including energy water, lotion, essential oil, facial mask.
Compared with prior art the beneficial effects of the present invention are:
(1) when the fragrant lotus extract of the present invention extracts, the filter residue in perfume lotus flower is extracted, perfume lotus flower is improved
Recovery rate, effectively shortens extraction time under the premise of guaranteeing recovery rate, and when being dried, separating during will not be by perfume
Lotus flower component damage.
(2) it can be widely used in cosmetic formulations, play significant anti-using the fragrant lotus extract of the method for the present invention preparation
Oxidation, crease-resistant, moisturizing, whitening, lighten the stain, skin lightening the effects of.
Specific embodiment
Specific embodiments of the present invention will be further explained below.It should be noted that for these implementations
The explanation of mode is used to help understand the present invention, but and does not constitute a limitation of the invention.In addition, invention described below
Technical characteristic involved in each embodiment can be combined with each other as long as they do not conflict with each other.
Embodiment 1
A kind of preparation method of perfume Flos Nelumbinis extract, which comprises the following steps:
(1) perfume lotus flower is crushed, addition blends 6 times of object weight of aqueous solution, and the basic protein that mass ratio is 1:2 is added
Enzyme and pectase digest 4h at 45 DEG C, are then filtered, and obtain filtrate and filtrate A；
(2) 8 times of dehydrated alcohol of filtrate weight is added into filtrate, microwave treatment is to mixed liquor temperature at 400W
Degree is up to 60 DEG C, and in 20KHz, ultrasonic power is ultrasonic extraction 40min under 200W, filters to obtain filter residue, deionization will be added in filter residue
Water ultrasonic extraction 15min, obtains liquor B；
(3) filtrate A and liquor B are merged, after filtering, desalination, decoloration and sterilization treatment, obtains extracting solution；
(4) by extracting solution in -30 DEG C of freezing 2h, then 3h is warming up to 25 DEG C, and dry 4h obtains perfume Flos Nelumbinis extract.
Using: 3% perfume Flos Nelumbinis extract is added in energy water formula, energy water formula includes the original of following parts by weight
Material: perfume Flos Nelumbinis extract 3%, triethanolamine 0.2%, hyaluronic acid 0.05%, panthenol 2%, rilanit special 1%, poly- second
Glycol -90M0.2%, triethanolamine 0.5%, Phenoxyethanol 0.3%, carbomer 0.2%, essence 0.1%, glycerol 5%, water
88.65%.The simple and elegant delicate fragrance that lotus flower is distributed using energy water prepared by perfume Flos Nelumbinis extract of the present invention, can purify skin lightening,
Skin nutrition and moisture are supplemented, skin water humidity and glossiness are improved.
Embodiment 2
A kind of preparation method of perfume Flos Nelumbinis extract, which comprises the following steps:
(1) perfume lotus flower is crushed, addition blends 8 times of object weight of aqueous solution, and the basic protein that mass ratio is 1:3 is added
Enzyme and pectase digest 3h at 48 DEG C, are then filtered, and obtain filtrate and filtrate A；
(2) 10 times of dehydrated alcohol of filtrate weight is added into filtrate, microwave treatment is to mixed liquor at 500W
Temperature is up to 70 DEG C, and in 25KHz, ultrasonic power is ultrasonic extraction 30min under 250W, filters to obtain filter residue, will be added in filter residue go from
Sub- water ultrasonic extraction 20min, obtains liquor B；
(3) filtrate A and liquor B are merged, after filtering, desalination, decoloration and sterilization treatment, obtains extracting solution；
(4) by extracting solution in -30 DEG C of freezing 4h, then 2.5h is warming up to 28 DEG C, and dry 5h obtains the extraction of perfume lotus flower
Object.
Using: 2% perfume Flos Nelumbinis extract is added in facial mask essence formula, facial mask essence includes following parts by weight
Raw material: perfume Flos Nelumbinis extract 2%, bulk kelp extract 0.2%, hyaluronic acid 0.05%, galactolipin araban 2%,
Rilanit special 1%, carbomer 0.2%, triethanolamine 0.5%, Phenoxyethanol 0.3%, essence 0.1%, glycerol 5%, water
88.65%.There is facial mask using perfume Flos Nelumbinis extract of the present invention preparation firming and moisturizing, deep layer to releive, and can effectively improve flesh
Skin is obscure, ageing state, and bright color moisturizes nourishing, gives skin concentrated type moisturizing maintenance, allows the lasting water profit of skin.
Embodiment 3
A kind of preparation method of perfume Flos Nelumbinis extract, which comprises the following steps:
(1) perfume lotus flower is crushed, addition blends 10 times of object weight of aqueous solution, and the alkaline egg that mass ratio is 1:5 is added
White enzyme and pectase digest 2.5h at 55 DEG C, are then filtered, and obtain filtrate and filtrate A；
(2) 12 times of dehydrated alcohol of filtrate weight is added into filtrate, microwave treatment is to mixed liquor at 600W
Temperature is up to 80 DEG C, and in 30KHz, ultrasonic power is ultrasonic extraction 20min under 300W, filters to obtain filter residue, will be added in filter residue go from
Sub- water ultrasonic extraction 30min, obtains liquor B；
(3) filtrate A and liquor B are merged, after filtering, desalination, decoloration and sterilization treatment, obtains extracting solution；
(4) by extracting solution in -30 DEG C of freezing 5h, then 2h is warming up to 25 DEG C, and dry 6h obtains perfume Flos Nelumbinis extract.
Using: 1% perfume Flos Nelumbinis extract is added in emulsion formulations, emulsion formulations include the raw material of following parts by weight:
Perfume Flos Nelumbinis extract 2%, allantoin 0.2%, hyaluronic acid 0.05%, ring five dimethyl silicone polymer 1%, Sodium Polyacrylate
0.2%, polyethylene glycol 0.5%, Phenoxyethanol 0.3%, essence 0.1%, glycerol 5%, water 90.65%.Using perfume of the present invention
The lotion of Flos Nelumbinis extract preparation, moisture can penetrate into skin, water lock moisturizing layer by layer, and purification is releived, uniform tender skin, alleviate skin
It is solidifying saturating to assign skin jade-like stone profit for obscure and drying regime.
The above are present pre-ferred embodiments, it is only applicable to the principle for helping to understand the embodiment of the present invention；Meanwhile for this
The those skilled in the art in field, according to the present embodiment, there will be changes in terms of specific embodiments and scope of application, comprehensive
Upper described, the contents of this specification are not to be construed as limiting the invention.
Claims (6)
1. a kind of preparation method of perfume Flos Nelumbinis extract, which comprises the following steps:
(1) perfume lotus flower is crushed, the aqueous solution for blending 6-10 times of object weight is added, alkali protease and pectase is added,
2.5-4h is digested at 45 DEG C -55 DEG C, is then filtered, and filtrate and filtrate A are obtained；
(2) dehydrated alcohol is added into filtrate, microwave treatment to mixeding liquid temperature reaches 60-80 DEG C, then ultrasonic extraction 20-
40min filters to obtain filter residue, deionized water ultrasonic extraction 15-30min will be added in filter residue, obtains liquor B；
(3) filtrate A and liquor B are merged, after filtering, desalination, decoloration and sterilization treatment, obtains extracting solution；
(4) extracting solution is dried by vacuum refrigeration, obtains perfume Flos Nelumbinis extract.
2. the preparation method of perfume Flos Nelumbinis extract according to claim 1, it is characterised in that: step (1) described alkalinity
The mass ratio of protease and pectase is 1:2-5.
3. the preparation method of perfume Flos Nelumbinis extract according to claim 1, it is characterised in that: step (2) is described anhydrous
The additional amount of ethyl alcohol is 8-12 times of filtrate weight.
4. the preparation method of perfume Flos Nelumbinis extract according to claim 1, it is characterised in that: step (2) described microwave
Power is 400-600W, and the supersonic frequency is 20-30KHz, ultrasonic power 200-300W.
5. the preparation method of perfume Flos Nelumbinis extract according to claim 1, it is characterised in that: step (4) described vacuum
Freeze-drying is, in -30 DEG C of freezing 2-5h, then 2-3h is warming up to 25-30 DEG C, and dry 4-6h obtains perfume Flos Nelumbinis extract.
6. a kind of application of perfume Flos Nelumbinis extract of the described in any item method preparations of claim 1-5 in skin care item.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201910619139.7A CN110237003A (en) | 2019-07-10 | 2019-07-10 | A kind of perfume Flos Nelumbinis extract and its application in skin care item |
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| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201910619139.7A CN110237003A (en) | 2019-07-10 | 2019-07-10 | A kind of perfume Flos Nelumbinis extract and its application in skin care item |
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| CN110237003A true CN110237003A (en) | 2019-09-17 |
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| CN201910619139.7A Pending CN110237003A (en) | 2019-07-10 | 2019-07-10 | A kind of perfume Flos Nelumbinis extract and its application in skin care item |
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Cited By (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN110251433A (en) * | 2019-07-11 | 2019-09-20 | 广州栋方生物科技股份有限公司 | A kind of perfume Flos Nelumbinis extract and preparation method thereof, the perfume lotus flower water comprising it and lotus flower moisturizing Shu Minshui |
| CN112245350A (en) * | 2020-10-25 | 2021-01-22 | 刘鑫 | Process for extracting effective substances of fresh flowers for skin care products |
| CN114029503A (en) * | 2021-11-12 | 2022-02-11 | 中国科学院合肥物质科学研究院 | Method and application for green synthesis of nano platinum by using lotus flower aqueous extract |
| CN114052113A (en) * | 2021-11-01 | 2022-02-18 | 菏泽尧舜牡丹生物科技有限公司 | Preparation method of pollen tablet candy |
| CN114917160A (en) * | 2022-06-06 | 2022-08-19 | 青蛙王子（福建）婴童护理用品有限公司 | Nymphaea hybrid fermentation product with antioxidant, anti-inflammatory and repairing effects and preparation and application thereof |
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Cited By (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN110251433A (en) * | 2019-07-11 | 2019-09-20 | 广州栋方生物科技股份有限公司 | A kind of perfume Flos Nelumbinis extract and preparation method thereof, the perfume lotus flower water comprising it and lotus flower moisturizing Shu Minshui |
| CN110251433B (en) * | 2019-07-11 | 2023-02-03 | 广州栋方生物科技股份有限公司 | Nymphaea hybrid extract, preparation method thereof, nymphaea hybrid water containing same and lotus moisturizing Shu Minshui |
| CN112245350A (en) * | 2020-10-25 | 2021-01-22 | 刘鑫 | Process for extracting effective substances of fresh flowers for skin care products |
| CN114052113A (en) * | 2021-11-01 | 2022-02-18 | 菏泽尧舜牡丹生物科技有限公司 | Preparation method of pollen tablet candy |
| CN114029503A (en) * | 2021-11-12 | 2022-02-11 | 中国科学院合肥物质科学研究院 | Method and application for green synthesis of nano platinum by using lotus flower aqueous extract |
| CN114917160A (en) * | 2022-06-06 | 2022-08-19 | 青蛙王子（福建）婴童护理用品有限公司 | Nymphaea hybrid fermentation product with antioxidant, anti-inflammatory and repairing effects and preparation and application thereof |
| CN114917160B (en) * | 2022-06-06 | 2023-09-08 | 青蛙王子（福建）婴童护理用品有限公司 | A flos Nelumbinis ferment with antioxidant, antiinflammatory and repairing effects, and its preparation method and application |
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Application publication date: 20190917 |
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