CN106309212A - Skin-care cosmetic capable of resisting ultraviolet radiation and preparation method thereof - Google Patents
Skin-care cosmetic capable of resisting ultraviolet radiation and preparation method thereof Download PDFInfo
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
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- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
- A61K8/34—Alcohols
- A61K8/345—Alcohols containing more than one hydroxy group
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
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- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/84—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds obtained by reactions otherwise than those involving only carbon-carbon unsaturated bonds
- A61K8/86—Polyethers
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/92—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof
- A61K8/922—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof of vegetable origin
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q17/00—Barrier preparations; Preparations brought into direct contact with the skin for affording protection against external influences, e.g. sunlight, X-rays or other harmful rays, corrosive materials, bacteria or insect stings
- A61Q17/04—Topical preparations for affording protection against sunlight or other radiation; Topical sun tanning preparations
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Abstract
A skin-care cosmetic capable of resisting ultraviolet radiation and a preparation method thereof belong to the field of cosmetics. The skin-care cosmetic capable of resisting ultraviolet radiation at least comprises lignin, water, a bitter chrysanthemum extract, xylitol, propanediol and polyethylene glycol (PEG), and also comprises disodium EDTA (ethylene diamine tetraacetic acid), citric acid, sodium hyaluronate, glycerinum, allantoin, iodopropynyl butylcarbamate and essence. The cosmetic has a function of resisting ultraviolet radiation; meanwhile, the lignin adopted by the cosmetic is an ultraviolet strong absorbent, the bitter chrysanthemum extract adopted by the cosmetic has the characteristic of oxidation resistance, and the two raw materials are safe and highly available.
Description
Technical field
The invention provides skin protection cosmetics of a kind of ultra-violet radiation resisting and preparation method thereof, belong to cosmetic field.
Background technology
Outdoor activities, because can be liked by a lot of people with Our Nature, and during outdoor activities, the strong sun
Light becomes the problem of everybody headache, particularly summer and goes to the beach, and sinister solar energy is by the skin sunburn on health.This wound
Evil skin is exactly ultraviolet.Wavelength according to ultraviolet can be divided into long wave UVA, medium wave UVB and shortwave UVC tri-kinds.Ripple
The longest, penetration capacity is the strongest.
Long wave UVA, wavelength, between 320～400 nanometers, has a strongest penetration power, and throughout the year, no matter rain or shine, court
Sunset all exists.The long wave ultraviolet contained in daylight has more than 98% can penetrate ozone layer and cloud layer arrival earth surface, UVA energy
Go deep into the deep layer of skin, injure skin skin corium, make the ossein in skin and elastin laminin be inflicted heavy losses on；In the course of time, skin
Skin produces the problems such as loose, wrinkle, blood capillary emerge.Meanwhile, it can activate again tryrosinase, causes instant melanin deposition
Formed with new melanin, make skin darkening, lack gloss.UVA can cause long-term, chronic and lasting damage, makes skin mistake
Presenility.
Medium wave UVB, wavelength, between 290～320 nanometers, can make the lipid layer oxidation of epidermis tool protective effect, make skin become
Dry；The most then making the nucleic acid in epidermis cell and protein denaturation, produce the symptoms such as acute dermatitis (i.e. sunburn), skin can become
Red, sore.Time serious, tan by the sun the most for a long time, be also easy to cause skin canceration.Additionally, the long-term injury of UVB also can cause
The variation of melanocyte, causes the sun speckle being difficult to eliminate.
Shortwave UVC, wavelength, between 200～290 nanometers, is the most just absorbed by ozone layer, scatters, it is impossible to reach ground
Face.
The document of science and clinical trial shows, the skin lesion that UVB causes is instant and serious, and UVA is to skin
Damage is then long-term chronic.
Liginon Resource is the abundantest, is the total amount of the photosynthesis of plant manufacture organic compound that is only second to cellulose.
Lignin is that a kind of complicated phenols formed by four kinds of alcohol monomers (to tonquinol, 4-hydroxy-3-methoxycinnamic alcohol, 5-hydroxyl 4-hydroxy-3-methoxycinnamic alcohol, sinapinic alcohol) gathers
Compound, annual production at about 50,000,000,000 tons, but, Liginon Resource is not effectively utilized, substantial amounts of lignin conduct
The by-product " black liquor " of paper industry is burnt after being directly discharged in rivers or concentrating, and is not only the one of resource and wastes greatly, and
Serious environment pollution.
Summary of the invention
It is an object of the invention to provide the skin protection cosmetics of a kind of ultra-violet radiation resisting, these cosmetics have opposing ultraviolet
The function of radiation, meanwhile, the lignin that these cosmetics use is the strong absorbent of ultraviolet, has raw material and is easy to get, safety and environmental protection
Feature.
The technical solution adopted for the present invention to solve the technical problems is:
The skin protection cosmetics of a kind of ultra-violet radiation resisting, this skin protection cosmetics at least includes lignin, Herba Lactucae versicoloris extract, xylose
Alcohol, water, propylene glycol and Polyethylene Glycol (PEG), also comprise EDETATE SODIUM, citric acid, hyaluronate sodium, glycerol, allantoin, iodine third
Alkynol butyl mephenesin Carbamate and essence；Each component is by weight:
50 ~ 70 parts of water,
Herba Lactucae versicoloris extract 0.5 ~ 1 part,
Xylitol 2 ~ 3 parts,
Lignin 1 ~ 2 part,
Propylene glycol 0.5 ~ 1 part,
Polyethylene Glycol (PEG) 10 ~ 15 parts,
EDETATE SODIUM 2 ~ 5 parts,
Citric acid 0.3 ~ 0.5 part,
Hyaluronate sodium 2.5 ~ 5 parts,
Glycerol 3 ~ 5 parts,
Allantoin 1 ~ 3 part,
Iodine propilolic alcohol butyl mephenesin Carbamate 0.1 ~ 0.3 part,
0.05 ~ 0.1 part of essence.
As preferably, described essence is the one in Folium Menthae extract, rose extract or jasmine extract.
As preferably, described Polyethylene Glycol (PEG) is in PEG-60 castor oil hydrogenated or Cremophor RH40
A kind of.
The preparation method of the skin protection cosmetics of a kind of described ultra-violet radiation resisting, comprises the following steps:
The first step: lignin is added in 0.1 ~ 0.3mol/L NaOH solution, carries out supersound process, ultrasonic power is 100 ~
200W, ultrasonic time is 20 ~ 30min, and time ultrasonic, temperature ensures below 50 DEG C；Lignin after supersound process, with 0.1 ~
The HCl regulation pH value of 0.3mol/L is 4 ~ 5, precipitation, microporous filter, pulverizes after drying.
Second step: water, EDETATE SODIUM, Herba Lactucae versicoloris extract and xylitol are sufficiently mixed dissolving, by propylene glycol, Polyethylene Glycol
(PEG), citric acid, hyaluronate sodium, glycerol, allantoin, iodine propilolic alcohol butyl mephenesin Carbamate, perfume ingredient add in container,
Stir, add the lignin after supersound process, 50 ~ 60 DEG C of process 1 ~ 2h that homogenize, prepare ultra-violet radiation resisting
Skin protection cosmetics.
In described step one, the amount of the NaOH of addition is can fully dissolved lignin be as the criterion.
The ultraviolet light that chromophore absorption wavelength is 300 ~ 400nm main in lignin, the ultraviolet light of absorption makes wooden
Some ether chain interruptions of element produce free radical so that lignin has the function of opposing ultraviolet radiation.
Exposure to Sunlight and environmental pollution can allow free radical produce, thus the situations such as skin dimness, hydropenia, microgroove occur, bitter
Chrysanthemum extract has antioxidant content, the cosmetics prepared with it, has removing free radical, antioxidative effect, its mechanism of action
It is by ultraviolet screener outside skin, there is sun-proof result.
SPF (Sun Protection Factor), adds that numerical value thereafter is referred to as SPF (sun protection factor) or sun-proof multiple, uses
The effect of UVB is resisted in assessment sunscreen product.The height of spf value objectively reflects sunscreen product to UVB protective capacities
Size.The present invention measures the method for spf value, smears the skin protection cosmetics of the embodiment of the present invention on one piece of selected skin,
Another block skin is not the most coated with any product.Then irradiate respectively with UVB until erythema all occur in two pieces of skins, and record two kinds of bars
Irradiation times different under part, its ratio is exactly the spf value of this sunscreen products.Wherein, spf value computing formula is:
SPF=smears the MED/ of sunscreen products skin and does not smears the MED of sunscreen products skin
Wherein, MED(Minimal Erythema Dose) it is minimal erythema dose, guide the slightest visible erythema (general red) institute
The lowest dose level (J/m2) needed or the shortest irradiation time.
It is an advantage of the current invention that: Cremophor RH40, eye pouch, slow down aging under eliminating are played well work
With.Xylitol has moisturizing, the effect of conditioning skin.These cosmetics have the function of opposing ultraviolet radiation, are somebody's turn to do meanwhile
The lignin that cosmetics use is the strong absorbent of ultraviolet, has raw material and is easy to get, the feature of safety and environmental protection, and these cosmetics use
Herba Lactucae versicoloris extract there is antioxidative effect, and ultraviolet screener can be played sun-proof result.Through test SPF, it is prevented
Shine effect and can reach the commercially available sun-proof result containing chemical sun.
Detailed description of the invention
Below in conjunction with specific embodiment case, the present invention it is described and is further appreciated by the present invention, not representing structure of the present invention
Whole technical scheme under Siing, it is impossible to be interpreted as the restriction to technical scheme.
In the present invention, if not refering in particular to, all of part, percentage ratio are unit of weight, the equipment used and raw material etc.
All it is commercially available or commonly used in the art.Method in following embodiment, if no special instructions, is the normal of this area
Rule method.
The preparation method of the Herba Lactucae versicoloris extract that following example use is:
Commercial natural green Herba Lactucae versicoloris is placed under ventilation sunlight and is dried；
Dried Herba Lactucae versicoloris is put in apparatus,Soxhlet's, and addition dehydrated alcohol, at 100 ~ 120 DEG C, after extracting 1 ~ 2h, changes solvent
Extracting more than 3 times, wherein, the dehydrated alcohol of addition and the mass ratio of Herba Lactucae versicoloris are 1:100 ~ 1:150；
Filter gained filtrate after extraction, carry out vacuum decompression distillation, when alcohol solvent is 50 ~ 60%, stop distillation；To distillation
After material in add petroleum ether, again extracting more than 3 times, wherein, the petroleum ether of addition and the mass ratio of Herba Lactucae versicoloris be 1:200 ~
1:250；
The ethanol extracted being removed through decompression distillation, until there is no ethanol taste, after adding water, adding ethyl acetate extracting 3
More than secondary, the water of addition: ethyl acetate: the mass ratio of Herba Lactucae versicoloris is 1:200:300 ~ 1:200:350；
Through activity alumina adsorption water after extracting, decompression distillation, obtain Herba Lactucae versicoloris extract after concentration.
Embodiment 1
A kind of skin protection cosmetics of ultra-violet radiation resisting, its raw material is following components by weight:
60 parts of water,
Lignin 2 parts,
Herba Lactucae versicoloris extract 0.5 part,
Xylitol 3 parts,
Propylene glycol 1 part,
Cremophor RH40 10 parts,
EDETATE SODIUM 2 parts,
Citric acid 0.3 part,
Hyaluronate sodium 4 parts,
Glycerol 4 parts,
Allantoin 2 parts,
Iodine propilolic alcohol butyl mephenesin Carbamate 0.3 part,
Rose extract 0.1 part.
The preparation method of the skin protection cosmetics of the ultra-violet radiation resisting of the present embodiment, step specifically:
The first step: being added by lignin in 0.1mol/L NaOH solution, carry out supersound process, ultrasonic power is 200W, time ultrasonic
Between be 20min, time ultrasonic, temperature ensures below 50 DEG C；Lignin after supersound process, regulates pH with the HCl of 0.1mol/L
Value is 4, precipitation, microporous filter, pulverizes after drying.
Second step: water, EDETATE SODIUM, Herba Lactucae versicoloris extract and xylitol are sufficiently mixed dissolving, by propylene glycol, Polyethylene Glycol
(PEG), citric acid, hyaluronate sodium, glycerol, allantoin, iodine propilolic alcohol butyl mephenesin Carbamate, perfume ingredient add in container,
Stir, add the lignin after supersound process, 50 DEG C of process 2h that homogenize, prepare the skin protection of ultra-violet radiation resisting
Cosmetic.
Testing the cosmetics of the present embodiment, its spf value is 18.
Embodiment 2
A kind of skin protection cosmetics of ultra-violet radiation resisting, its raw material is following components by weight:
60 parts of water,
Lignin 2 parts,
Herba Lactucae versicoloris extract 1 part,
Xylitol 2 parts,
Propylene glycol 1 part,
Cremophor RH40 15 parts,
EDETATE SODIUM 3 parts,
Citric acid 0.4 part,
Hyaluronate sodium 3 parts,
Glycerol 5 parts,
Allantoin 3 parts,
Iodine propilolic alcohol butyl mephenesin Carbamate 0.2 part,
Jasmine extract 0.05 part.
The preparation method of the skin protection cosmetics of the ultra-violet radiation resisting of the present embodiment, step specifically:
The first step: being added by lignin in 0.3mol/L NaOH solution, carry out supersound process, ultrasonic power is 100W, time ultrasonic
Between be 30min, time ultrasonic, temperature ensures below 50 DEG C；Lignin after supersound process, regulates pH with the HCl of 0.3mol/L
Value is 5, precipitation, microporous filter, pulverizes after drying.
Second step: water, EDETATE SODIUM, Herba Lactucae versicoloris extract and xylitol are sufficiently mixed dissolving, by propylene glycol, Polyethylene Glycol
(PEG), citric acid, hyaluronate sodium, glycerol, allantoin, iodine propilolic alcohol butyl mephenesin Carbamate, perfume ingredient add in container,
Stir, add the lignin after supersound process, 60 DEG C of process 1h that homogenize, prepare the skin protection of ultra-violet radiation resisting
Cosmetic.
Testing the cosmetics of the present embodiment, its spf value is 25.
Embodiment 3
A kind of skin protection cosmetics of ultra-violet radiation resisting, its raw material is following components by weight:
70 parts of water,
Lignin 1 part,
Herba Lactucae versicoloris extract 0.5 part,
Xylitol 2.5 parts,
Propylene glycol 0.5 part,
Cremophor RH40 10 parts,
EDETATE SODIUM 5 parts,
Citric acid 0.3 part,
Hyaluronate sodium 2.5 parts,
Glycerol 5 parts,
Allantoin 1 part,
Iodine propilolic alcohol butyl mephenesin Carbamate 0.1 part,
Folium Menthae extract 0.1 part.
The preparation method of the skin protection cosmetics of the ultra-violet radiation resisting of the present embodiment, step specifically:
The first step: being added by lignin in 0.2mol/L NaOH solution, carry out supersound process, ultrasonic power is 200W, time ultrasonic
Between be 20min, time ultrasonic, temperature ensures below 50 DEG C；Lignin after supersound process, regulates pH with the HCl of 0.3mol/L
Value is 5, precipitation, microporous filter, pulverizes after drying.
Second step: water, EDETATE SODIUM, Herba Lactucae versicoloris extract and xylitol are sufficiently mixed dissolving, by propylene glycol, Polyethylene Glycol
(PEG), citric acid, hyaluronate sodium, glycerol, allantoin, iodine propilolic alcohol butyl mephenesin Carbamate, perfume ingredient add in container,
Stir, add the lignin after supersound process, 50 DEG C of process 1h that homogenize, prepare the skin protection of ultra-violet radiation resisting
Cosmetic.
Testing the cosmetics of the present embodiment, its spf value is 15.
Embodiment 4
A kind of skin protection cosmetics of ultra-violet radiation resisting, its raw material is following components by weight:
50 parts of water,
Lignin 2 parts,
Herba Lactucae versicoloris extract 1 part,
Xylitol 2 parts,
Propylene glycol 1 part,
PEG-60 castor oil hydrogenated 12 parts,
EDETATE SODIUM 2 parts,
Citric acid 0.5 part,
Hyaluronate sodium 5 parts,
Glycerol 3 parts,
Allantoin 2 parts,
Iodine propilolic alcohol butyl mephenesin Carbamate 0.1 part,
Rose extract 0.05 part.
The preparation method of the Herba Lactucae versicoloris extract that the present embodiment uses is:
Commercial natural green Herba Lactucae versicoloris is placed under ventilation sunlight and to be dried by 1；Dried Herba Lactucae versicoloris is put in apparatus,Soxhlet's, adds
Dehydrated alcohol, at 100 ~ 120 DEG C, after extracting 1 ~ 2h, changes solvent extraction more than 3 times, wherein, the dehydrated alcohol of addition and Herba Lactucae versicoloris
Mass ratio be 1:120；
Filter gained filtrate after 2 extractions, carry out vacuum decompression distillation, when alcohol solvent is 60%, stop distillation；After distillation
Material in add petroleum ether, again extracting more than 3 times, wherein, the petroleum ether of addition and the mass ratio of Herba Lactucae versicoloris are 1:200；
The ethanol extracted is removed by 3 through decompression distillation, until not having ethanol taste, after adding water, adds ethyl acetate extracting 3
Secondary, the water of addition: ethyl acetate: the mass ratio of Herba Lactucae versicoloris is 1:200:300；Through activity alumina adsorption water, decompression after extracting
Distillation, obtains Herba Lactucae versicoloris extract after concentration.
The preparation method of the skin protection cosmetics of the ultra-violet radiation resisting of the present embodiment, step specifically:
The first step: being added by lignin in 0.1mol/L NaOH solution, carry out supersound process, ultrasonic power is 200W, time ultrasonic
Between be 20min, time ultrasonic, temperature ensures below 50 DEG C；Lignin after supersound process, regulates pH with the HCl of 0.1mol/L
Value is 4, precipitation, microporous filter, pulverizes after drying.
Second step: water, EDETATE SODIUM, Herba Lactucae versicoloris extract and xylitol are sufficiently mixed dissolving, by propylene glycol, Polyethylene Glycol
(PEG), citric acid, hyaluronate sodium, glycerol, allantoin, iodine propilolic alcohol butyl mephenesin Carbamate, perfume ingredient add in container,
Stir, add the lignin after supersound process, 50 DEG C of process 1h that homogenize, prepare the skin protection of ultra-violet radiation resisting
Cosmetic.
Testing the cosmetics of the present embodiment, its spf value is 20.
Test example
Skin protection cosmetics to the ultra-violet radiation resisting of embodiment 1 preparation carries out the detection of ultra-violet absorption
Use commercially available chromatographic grade solvent: the ultrasonic 15min of oxolane is de-gassed process；
Other solvents are commercially available chromatographic grade solvent, and water is deionized water.
Sample treatment: skin protection cosmetics is placed in centrifuge tube, add 0.5ml concentration be 1mol/L sulphuric acid and
The methanol of 20mL, supersound process 30min, in supersound process, it is ensured that temperature, below 35 DEG C, is centrifuged 15min with 800r/min, carries
Take supernatant；Residual liquid extracts the most again, again extracts supernatant, and constant volume is standby.
Test equipment use waters1525 type high performance liquid chromatograph, Waters 2487 dual pathways UV-detector and
Agilent 3397A integrator.
Test parameter is: solvent is oxolane, flow velocity 1mL/min, column temperature 30 DEG C, tests temperature 30 DEG C, sample introduction
Volume 10 μ L, detects wavelength 290 ~ 330nm, integrator chart speed 0.5cm/min.
Test analysis:
(1) by the sample after 10 μ L constant volumes, carry out efficient liquid phase chromatographic analysis, record its retention time, and combine Waters
Different detection wavelength is detected by 2487 dual pathways UV-detector, can obtain the assimilation effect of lignin 300 ~
The assimilation effect of 330nm is notable, has to anti-ultraviolet function.
(2) record peak area, makes a look up on standard curve and obtains the concentration of corresponding ultraviolet absorber lignin and be
0.8%, and the lignin concentration added is close.
Claims (5)
1. the skin protection cosmetics of a ultra-violet radiation resisting, it is characterised in that this skin protection cosmetics at least includes lignin, Herba Lactucae versicoloris
Extract, xylitol, water, propylene glycol and Polyethylene Glycol (PEG), also comprise EDETATE SODIUM, citric acid, hyaluronate sodium, glycerol,
Allantoin, iodine propilolic alcohol butyl mephenesin Carbamate and essence；Each component is by weight:
50 ~ 70 parts of water,
Lignin 1 ~ 2 part,
Herba Lactucae versicoloris extract 0.5 ~ 1 part,
Xylitol 2 ~ 3 parts,
Propylene glycol 0.5 ~ 1 part,
Polyethylene Glycol (PEG) 10 ~ 15 parts,
EDETATE SODIUM 2 ~ 5 parts,
Citric acid 0.3 ~ 0.5 part,
Hyaluronate sodium 2.5 ~ 5 parts,
Glycerol 3 ~ 5 parts,
Allantoin 1 ~ 3 part,
Iodine propilolic alcohol butyl mephenesin Carbamate 0.1 ~ 0.3 part,
0.05 ~ 0.1 part of essence.
The skin protection cosmetics of ultra-violet radiation resisting the most according to claim 1, it is characterised in that described essence is Herba Menthae
One in extract, rose extract or jasmine extract.
The skin protection cosmetics of ultra-violet radiation resisting the most according to claim 1, it is characterised in that described Polyethylene Glycol
(PEG) it is the one in PEG-60 castor oil hydrogenated or Cremophor RH40.
4. the preparation method of the skin protection cosmetics of the ultra-violet radiation resisting of a claim 1, it is characterised in that include following step
Rapid:
The first step: lignin is added in 0.1 ~ 0.3mol/L NaOH solution, carries out supersound process, ultrasonic power is 100 ~
200W, ultrasonic time is 20 ~ 30min, and time ultrasonic, temperature ensures below 50 DEG C；Lignin after supersound process, with 0.1 ~
The HCl regulation pH value of 0.3mol/L is 4 ~ 5, precipitation, microporous filter, pulverizes after drying；
Second step: water, EDETATE SODIUM, Herba Lactucae versicoloris extract and xylitol are sufficiently mixed dissolving, by propylene glycol, Polyethylene Glycol
(PEG), citric acid, hyaluronate sodium, glycerol, allantoin, iodine propilolic alcohol butyl mephenesin Carbamate, perfume ingredient add in container,
Stir, add the lignin after supersound process, 50 ~ 60 DEG C of process 1 ~ 2h that homogenize, prepare ultra-violet radiation resisting
Skin protection cosmetics.
The preparation method of the skin protection cosmetics of a kind of ultra-violet radiation resisting the most according to claim 4, it is characterised in that institute
Stating in step one, the amount of the NaOH of addition is can fully dissolved lignin be as the criterion.
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| CN201610692015.8A CN106309212A (en) | 2016-08-20 | 2016-08-20 | Skin-care cosmetic capable of resisting ultraviolet radiation and preparation method thereof |
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| CN201610692015.8A CN106309212A (en) | 2016-08-20 | 2016-08-20 | Skin-care cosmetic capable of resisting ultraviolet radiation and preparation method thereof |
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Cited By (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN108456314A (en) * | 2018-03-15 | 2018-08-28 | 华南理工大学 | A kind of broad spectrum type lignin macromolecule ultra-violet protecting agent and preparation method thereof |
| CN109481729A (en) * | 2018-11-23 | 2019-03-19 | 南京华开生物科技有限公司 | A kind of low molecular weight sodium hyaluronate isotonic liquid dressing and preparation method thereof |
| CN110882183A (en) * | 2019-12-30 | 2020-03-17 | 霖汐(北京)生物科技有限公司 | Anti-radiation skin care product and preparation method thereof |
| CN111803402A (en) * | 2020-08-21 | 2020-10-23 | 长春科技学院 | Preparation method of lignin-based sunscreen cream |
| WO2022133566A1 (en) | 2020-12-22 | 2022-06-30 | Botica Comercial Farmacêutica Ltda. | Method for obtaining a lignin composition associated with zno and tio2 for a cosmetic product with coloring for black skin, to boost blue light protection, and to protect the skin against external oxidizing agents, and respective obtained product |
| WO2023062562A1 (en) * | 2021-10-12 | 2023-04-20 | Universidade Católica Portuguesa - Ucp | Lignin, methods of extraction and uses thereof |
| CN118236288A (en) * | 2023-12-29 | 2024-06-25 | 中国热带农业科学院农产品加工研究所 | Sun-proof skin care product and preparation method thereof |
Citations (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| WO2002013608A1 (en) * | 2000-08-11 | 2002-02-21 | Virginia Tech Intellectual Properties, Inc. | Water soluble uv-protective coatings for biological pesticides and process for making same |
| US20030152531A1 (en) * | 2001-02-05 | 2003-08-14 | Amcol International Corp. | Multifunctional particulate additive for personal care and cosmetic compositions, and the process of making the same |
| JP2004131672A (en) * | 2002-10-15 | 2004-04-30 | Yamagata Public Corp For The Development Of Industry | Ultraviolet absorber |
| CN101869299A (en) * | 2010-06-25 | 2010-10-27 | 王爱平 | Cichorium endivia L. extract and application thereof |
| CN102366038A (en) * | 2011-09-07 | 2012-03-07 | 张奎昌 | Cichorium endivia L. chewable tablet and production technology thereof |
| CN104434558A (en) * | 2013-09-25 | 2015-03-25 | 徐娟 | Lignin-containing cosmetic |
-
2016
- 2016-08-20 CN CN201610692015.8A patent/CN106309212A/en active Pending
Patent Citations (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| WO2002013608A1 (en) * | 2000-08-11 | 2002-02-21 | Virginia Tech Intellectual Properties, Inc. | Water soluble uv-protective coatings for biological pesticides and process for making same |
| US20030152531A1 (en) * | 2001-02-05 | 2003-08-14 | Amcol International Corp. | Multifunctional particulate additive for personal care and cosmetic compositions, and the process of making the same |
| JP2004131672A (en) * | 2002-10-15 | 2004-04-30 | Yamagata Public Corp For The Development Of Industry | Ultraviolet absorber |
| CN101869299A (en) * | 2010-06-25 | 2010-10-27 | 王爱平 | Cichorium endivia L. extract and application thereof |
| CN102366038A (en) * | 2011-09-07 | 2012-03-07 | 张奎昌 | Cichorium endivia L. chewable tablet and production technology thereof |
| CN104434558A (en) * | 2013-09-25 | 2015-03-25 | 徐娟 | Lignin-containing cosmetic |
Non-Patent Citations (3)
| Title |
|---|
| XU0ANJING: ""韩后绿茶细肤达人面膜"", 《获取网址：HTTP://WWW.COSDNA.COM/CHS/COSMETIC_63E8195677.HTML》 * |
| YONG QIAN等: ""Lignin: a nature-inspired sun blocker for broadspectrum sunscreens"", 《GREEN CHEMISTRY》 * |
| 李忠正: "《植物纤维资源化学》", 30 June 2012, 中国轻工业出版社 * |
Cited By (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN108456314A (en) * | 2018-03-15 | 2018-08-28 | 华南理工大学 | A kind of broad spectrum type lignin macromolecule ultra-violet protecting agent and preparation method thereof |
| CN109481729A (en) * | 2018-11-23 | 2019-03-19 | 南京华开生物科技有限公司 | A kind of low molecular weight sodium hyaluronate isotonic liquid dressing and preparation method thereof |
| CN110882183A (en) * | 2019-12-30 | 2020-03-17 | 霖汐(北京)生物科技有限公司 | Anti-radiation skin care product and preparation method thereof |
| CN111803402A (en) * | 2020-08-21 | 2020-10-23 | 长春科技学院 | Preparation method of lignin-based sunscreen cream |
| WO2022133566A1 (en) | 2020-12-22 | 2022-06-30 | Botica Comercial Farmacêutica Ltda. | Method for obtaining a lignin composition associated with zno and tio2 for a cosmetic product with coloring for black skin, to boost blue light protection, and to protect the skin against external oxidizing agents, and respective obtained product |
| WO2023062562A1 (en) * | 2021-10-12 | 2023-04-20 | Universidade Católica Portuguesa - Ucp | Lignin, methods of extraction and uses thereof |
| CN118236288A (en) * | 2023-12-29 | 2024-06-25 | 中国热带农业科学院农产品加工研究所 | Sun-proof skin care product and preparation method thereof |
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