CN102579296B - Sun block composition containing momordica charantia extract and application thereof - Google Patents
Sun block composition containing momordica charantia extract and application thereof Download PDFInfo
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- CN102579296B CN102579296B CN 201210066035 CN201210066035A CN102579296B CN 102579296 B CN102579296 B CN 102579296B CN 201210066035 CN201210066035 CN 201210066035 CN 201210066035 A CN201210066035 A CN 201210066035A CN 102579296 B CN102579296 B CN 102579296B
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- momordicae charantiae
- fructus momordicae
- charantiae extract
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Abstract
The invention discloses a sun block composition containing a momordica charantia extract. The sun block composition includes, by weight, 60% to 70% of momordica charantia extract, 10% to 20% of bamboo leaf extract, 9.7% to 19.7% of polyol moisturizer, 0.2% of methyl hydroxybenzoate, and 0.1% of ethyl hydroxybenzoate. The preparing method includes heating the polyol moisturizer to 50 DEG C to 60 DEG C, adding the methyl hydroxybenzoate and the ethyl hydroxybenzoate into the polyol moisturizer, lowering the temperature of the mixture to 25 DEG C after even stirring and complete dissolution, sequentially adding the momordica charantia extract, the bamboo leaf extract, and obtaining the sun block composition containing the momordica charantia extract after even stirring. The sun block composition has the advantages of low stimulation, good sun block effect, low cost, light color, no effect on product color, and skin whitening effect simultaneously. The preparation process of the sun blockcomposition is simple and practicable.
Description
Technical field
The present invention relates to a kind of antitan agent compositions, relate in particular a kind of sunscreen composition and application thereof that contains Fructus Momordicae charantiae extract, have safety, efficient characteristics.
Technical background
Long-term scientific research proves that ultraviolet can change structure or the function of individual cells component, and a large amount of ultraviolet can make the ditch concerted effort of this cell forfeiture and peripheral cell to the radiation of cell, or common apoptosis.Ultraviolet in the sunlight is the aging one of the main reasons of human body skin, it to the direct irradiation of skin can cause skin erythema, burn, a series of skin problems such as melanism, dermatitis even skin carcinoma.
Nowadays a sun-proof main trend that has become the development of current cosmetics, in the process of exploitation sunscreen product, some have sun-proof and natural plant composition anti-ultraviolet function has performance gentleness, the advantage such as efficient, obtain people's concern.Has beyond the medicinal herb components decapacitation absorbing ultraviolet of anti-sunlight function the effect that also has treatment solar dermatitis, skin protection jade-like stone face and freckle removing and whitening concurrently that has.Compare with traditional organic synthesis UV absorbent, it is low that natural plant sunscreen component has zest, few side effects, and more safe and reliable advantage can avoid traditional Orangic sunscreen to stimulation and the allergic phenomena of human body skin.Correlational study shows, extract in the Fructus Momordicae charantiae contains the various bioactivators such as Saponin, protein, polypeptide, triterpene, steroid class, alkaloid, albumen, organic acid, bitter melon polysaccharide, effect with antioxidation, antiinflammatory and uv absorption, also contain the GONA-Y whitening factor in the Fructus Momordicae charantiae simultaneously, in sun-proof, also have repair after certain solarization, can be used for preparing safely and effectively sunscreen composition.The said composition ultraviolet absorption effect is good, and cost is low, and the extract color is colourless or light yellow, is easy to add in the sun care preparations, does not affect product colour.
List of references:
[1] Cheng Yan, Dong Yiyang, Dong Yinmao, Betula platyphylla Suk., He Congfen, Wang Changtao, Wang Junbing, Li Ming, Zou Yundong, Yang Xiaoran, Ren Dongmei, Zheng Hongyan. In silico technology is to the human body exposure assessment of component of sun. daily chemical industry, 2009,39 (3): 176-178.
Summary of the invention
The object of the present invention is to provide a kind of the have sunscreen composition that contains Fructus Momordicae charantiae extract of good ultraviolet absorption effect and the application process in cosmetics thereof.
Technical scheme of the present invention
A kind of sunscreen composition that contains Fructus Momordicae charantiae extract, percent calculates by weight, and its composition and content are as follows:
Fructus Momordicae charantiae extract 60-70%
Folium Bambosae extract 10-20%
Polyhydric alcohol wetting agent 9.7-19.7%
Methyl hydroxybenzoate 0.2%
Ethyl hydroxybenzoate 0.1%;
Described Fructus Momordicae charantiae extract prepares by the following method:
After the dried Frutus Momordicae Charantiae pulverizing, accurately take by weighing 5g, place the 100mL volumetric flask, add the 50mL distilled water, at 50 ℃ of lower lixiviate 30min, then ultrasonic 20min, use again 0.45 μ m filtering with microporous membrane, the extracting solution rotary evaporation that obtains to 5mL, is obtained the Fructus Momordicae charantiae extract sample.
Described Folium Bambosae extract prepares by the following method:
After the pulverizing of Folium Bambusae dry product, accurately take by weighing 5g, place the 100mL volumetric flask, add 50 mL distilled water, at 50 ℃ of lower lixiviate 30min, then ultrasonic 20min, use again 0.45 μ m filtering with microporous membrane, the extracting solution rotary evaporation that obtains to 5mL, is obtained the Folium Bambosae extract sample.
Using Fructus Momordicae charantiae extract in the above-mentioned sunscreen composition, is because Fructus Momordicae charantiae extract has obvious uv absorption in the scope of wavelength 290-380nm, can effectively resist ultraviolet (UV) A and UVB to the injury of skin.In addition, the bioactive substances such as the Saponin in the Fructus Momordicae charantiae extract, bitter melon polysaccharide also have the effect of antioxidation, antiinflammatory, in sun-proof, also have repair after certain solarization, can be used for preparing safely and effectively sunscreen composition;
Using bamboo leaf extract in the above-mentioned sunscreen composition, because Folium Bambosae extract, the Folium Bambusae total flavones that contains, has good free radical resisting, antioxidation, defying age, antibiotic, antiinflammation, can effectively remove active oxidation free radical in the human body, prevent that the biomembrane lipid is by superoxide radical and hydroxyl radical free radical oxidation, promote skin cell proliferation, prevent the oxidative damage of skin, it is synthetic to reduce melanocyte, can play and shine rear repair, and do not contain any harmful components and antinutritional factor, and non-stimulated to human body skin and mucosa, anaphylactic reaction, safety, gentle, Stability Analysis of Structures is difficult for being degraded;
In sum, Fructus Momordicae charantiae has sun-proof, whitening effect, Folium Bambusae have that the melanin of minimizing is synthetic, antiinflammatory shine after repairing effect.
Described polyhydric alcohol wetting agent is propylene glycol or 1,3 butylene glycol, is preferably 1,3 butylene glycol;
Above-mentioned a kind of preparation method that contains the sunscreen composition of Fructus Momordicae charantiae extract comprises the steps:
After the polyhydric alcohol wetting agent is heated to 50-60 ℃, methyl hydroxybenzoate and ethyl hydroxybenzoate are added in the polyhydric alcohol wetting agent, stir and fully dissolving, when then being reduced to 25 ℃, add successively Fructus Momordicae charantiae extract, Folium Bambosae extract, stir and namely obtain a kind of sunscreen composition that contains Fructus Momordicae charantiae extract.
The above-mentioned a kind of application process of sunscreen composition in sun care preparations that contains Fructus Momordicae charantiae extract, calculate in mass ratio, namely in a kind of sunscreen composition that contains Fructus Momordicae charantiae extract: sun care preparations is the ratio of 10～30:100, and described a kind of sunscreen composition that contains Fructus Momordicae charantiae extract is added in the sun care preparations.
Beneficial effect of the present invention
A kind of sunscreen composition that contains the natural plants Fructus Momordicae charantiae extract of the present invention, owing to adopted the Fructus Momordicae charantiae extract with sun-proof, whitening effect as the sun-prevention component in the sunscreen composition, thereby this sunscreen composition has, and zest is low, sun-proof result good, cost is low, lighter color, do not affect product colour, and have simultaneously characteristics of white-skinned face function, preparation technology's simple possible of this sunscreen composition.
Description of drawings
The uv absorption spectra of Fig. 1, Fructus Momordicae charantiae extract;
The uv absorption spectra of Fig. 2, octyl methoxycinnamate.
Specific implementation method
Also by reference to the accompanying drawings the present invention is further set forth below by embodiment, but do not limit the present invention.
The preparation method of used Fructus Momordicae charantiae extract is as follows in the embodiments of the invention:
After the dried Frutus Momordicae Charantiae pulverizing, accurately take by weighing 5g, place the 100mL volumetric flask, add 50 mL distilled water, at 50 ℃ of lower lixiviate 30min, then ultrasonic 20min, use again 0.45 μ m filtering with microporous membrane, the extracting solution rotary evaporation that obtains to 5mL, is obtained Fructus Momordicae charantiae extract;
Get 0.1g after the Fructus Momordicae charantiae extract lyophilization with gained, behind the 100mL deionized water dissolving, analyze with ultraviolet spectrophotometer, the uv absorption spectra of gained as shown in Figure 1, as can be seen from Figure 1 the aqueous solution of Fructus Momordicae charantiae effective ingredient has obvious uv absorption in wavelength 290～380nm scope, illustrates that this constituents has the ultraviolet protection effect at UVA and UVB wave band.
The preparation method of used Folium Bambosae extract is as follows in the embodiments of the invention:
After the pulverizing of Folium Bambusae dry product, accurately take by weighing 5g, place the 100mL volumetric flask, add 50 mL distilled water, at 50 ℃ of lower lixiviate 30min, then ultrasonic 20min, use again 0.45 μ m filtering with microporous membrane, the extracting solution rotary evaporation that obtains to 5mL, is obtained Folium Bambosae extract.
Embodiment 1
A kind of sunscreen composition that contains Fructus Momordicae charantiae extract, percent calculates by weight, and its composition and content are as follows: Fructus Momordicae charantiae extract 13g (65%)
Folium Bambosae extract 3g (15%)
Polyhydric alcohol wetting agent 3.94g (19.7%)
Methyl hydroxybenzoate 0.04g (0.2%)
Ethyl hydroxybenzoate 0.02g (0.1%)
Described polyhydric alcohol wetting agent is 1,3 butylene glycol.
Above-mentioned a kind of preparation method that contains the sunscreen composition of Fructus Momordicae charantiae extract, step is as follows:
After 1,3 butylene glycol is heated to 50-60 ℃, methyl hydroxybenzoate and ethyl hydroxybenzoate are added in the butanediol, stir and fully dissolving, when then being reduced to 25 ℃, add successively Fructus Momordicae charantiae extract, Folium Bambosae extract stirs and namely gets a kind of sunscreen composition A that contains Fructus Momordicae charantiae extract.
Embodiment 2
A kind of sunscreen composition that contains Fructus Momordicae charantiae extract, percent calculates by weight, and its composition and content are as follows: Fructus Momordicae charantiae extract 14g (70%)
Folium Bambosae extract 4g (20%)
Polyhydric alcohol wetting agent 1.94g (9.7%)
Methyl hydroxybenzoate 0.04g (0.2%)
Ethyl hydroxybenzoate 0.02g (0.1%)
Described polyhydric alcohol wetting agent is 1,3 butylene glycol.
Above-mentioned a kind of preparation method that contains the sunscreen composition of Fructus Momordicae charantiae extract, step is as follows:
After 1,3 butylene glycol is heated to 50-60 ℃, methyl hydroxybenzoate and ethyl hydroxybenzoate are added in the butanediol, stir and fully dissolving, when then being reduced to 25 ℃, add successively Fructus Momordicae charantiae extract, Folium Bambosae extract stirs and namely gets a kind of sunscreen composition B that contains Fructus Momordicae charantiae extract.
Embodiment 3
A kind of sunscreen composition that contains Fructus Momordicae charantiae extract, percent calculates by weight, and its composition and content are as follows: Fructus Momordicae charantiae extract 12g (60%)
Folium Bambosae extract 4g (20%)
Polyhydric alcohol wetting agent 3.94g (19.7%)
Methyl hydroxybenzoate 0.04g (0.2%)
Ethyl hydroxybenzoate 0.02g (0.1%)
Described polyhydric alcohol wetting agent is 1,3 butylene glycol.
Above-mentioned a kind of preparation method that contains the sunscreen composition of Fructus Momordicae charantiae extract, step is as follows:
After 1,3 butylene glycol is heated to 50-60 ℃, methyl hydroxybenzoate and ethyl hydroxybenzoate are added in the butanediol, stir and fully dissolving, when then being reduced to 25 ℃, add successively Fructus Momordicae charantiae extract, Folium Bambosae extract stirs and namely gets a kind of sunscreen composition C that contains Fructus Momordicae charantiae extract.
The comparative example 1
Compare with one of Orangic sunscreen commonly used in prior art octyl methoxycinnamate:
After getting 0.05g octyl methoxycinnamate usefulness 50mL ethanol dilution, analyze with ultraviolet spectrophotometer, the uv absorption spectra of gained as shown in Figure 2, can find out from the contrast of Fig. 2 and Fig. 1: under the same concentrations, both absorption peak strength are close, and Fructus Momordicae charantiae extract has obvious ultraviolet absorption ability in ultraviolet wavelength 290-380nm scope; And the ultraviolet absorption peak wave-length coverage of octyl methoxycinnamate is between 290-355nm, the aqueous solution uv absorption that has shown the Fructus Momordicae charantiae effective ingredient is wider than the uv absorption wave-length coverage of octyl methoxycinnamate alcoholic solution, be a kind of natural plant sunscreen component of safe, efficient, wide spectrum, can be used for sun care preparations.
Add up according to the study
[1]The skin allergy that is caused by Orangic sunscreen octyl methoxycinnamate, PAROSOL 1789, p-methoxy cinnamic acid isopentyl ester, Unisol S-22 and 4-dimethylaminobenzoic acid 2-Octyl Nitrite in the sunscreen product accounts for the sunscreen product crowd's 18% that uses; and other some sunscreen as: homosalate, benzophenone 1, octocrilene, 4 monomethyl benzyl subunit Camphoras and ethylhexyl salicylate cause that skin irritant probability is larger, can reach more than 90%.Because the aqueous solution of Fructus Momordicae charantiae effective ingredient can reduce the use of Orangic sunscreen commonly used, has reduced the chemical constituent of Orangic sunscreen to the generation of zest and the skin allergy phenomenon of skin.Therefore, the sunscreen composition that contains Fructus Momordicae charantiae extract of the present invention is a kind of comparatively desirable sunscreen composition that contains natural plants.
Foregoing only is the basic explanation of the present invention under conceiving, and according to any equivalent transformation that technical scheme of the present invention is done, all should belong to protection scope of the present invention.
Claims (4)
1. a sunscreen composition that contains Fructus Momordicae charantiae extract is characterized in that the described by weight percent calculating of sunscreen composition that contains Fructus Momordicae charantiae extract, and its composition and content are as follows:
Fructus Momordicae charantiae extract 60-70%
Folium Bambosae extract 10-20%
Polyhydric alcohol wetting agent 9.7-19.7%
Methyl hydroxybenzoate 0.2%
Ethyl hydroxybenzoate 0.1%
Described Fructus Momordicae charantiae extract prepares by the following method:
After dried Frutus Momordicae Charantiae pulverized, accurately take by weighing 5g, place the 100mL volumetric flask, add the 50mL distilled water, at 50 ℃ of lower lixiviate 30min, then ultrasonic 20min uses 0.45 μ m filtering with microporous membrane again, and the extracting solution rotary evaporation that obtains to 5mL, is obtained Fructus Momordicae charantiae extract;
Described Folium Bambosae extract prepares by the following method:
After the pulverizing of Folium Bambusae dry product, accurately take by weighing 5g, place the 100mL volumetric flask, add the 50mL distilled water, at 50 ℃ of lower lixiviate 30min, then ultrasonic 20min, use again 0.45 μ m filtering with microporous membrane, the extracting solution rotary evaporation that obtains to 5mL, is obtained Folium Bambosae extract;
Described polyhydric alcohol wetting agent is propylene glycol or 1,3 butylene glycol;
Above-mentioned a kind of preparation method that contains the sunscreen composition of Fructus Momordicae charantiae extract, step is as follows:
After the polyhydric alcohol wetting agent is heated to 50-60 ℃, methyl hydroxybenzoate and ethyl hydroxybenzoate are joined in the polyhydric alcohol wetting agent, stir and fully dissolving, when then being reduced to 25 ℃, add successively Fructus Momordicae charantiae extract, Folium Bambosae extract, stir and namely obtain a kind of sunscreen composition that contains Fructus Momordicae charantiae extract.
2. a kind of sunscreen composition that contains Fructus Momordicae charantiae extract as claimed in claim 1 is characterized in that the described by weight percent calculating of sunscreen composition that contains Fructus Momordicae charantiae extract, and its composition and content are as follows:
Fructus Momordicae charantiae extract 65%
Folium Bambosae extract 15%
Polyhydric alcohol wetting agent 19.7%
Methyl hydroxybenzoate 0.2%
Ethyl hydroxybenzoate 0.1%.
3. a kind of sunscreen composition that contains Fructus Momordicae charantiae extract as claimed in claim 1 is characterized in that the described by weight percent calculating of sunscreen composition that contains Fructus Momordicae charantiae extract, and its composition and content are as follows:
Fructus Momordicae charantiae extract 70%
Folium Bambosae extract 20%
Polyhydric alcohol wetting agent 9.7%
Methyl hydroxybenzoate 0.2%
Ethyl hydroxybenzoate 0.1%.
4. a kind of sunscreen composition that contains Fructus Momordicae charantiae extract as claimed in claim 1 is characterized in that the described by weight percent calculating of sunscreen composition that contains Fructus Momordicae charantiae extract, and its composition and content are as follows:
Fructus Momordicae charantiae extract 60%
Folium Bambosae extract 20%
Polyhydric alcohol wetting agent 19.7%
Methyl hydroxybenzoate 0.2%
Ethyl hydroxybenzoate 0.1%.
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| CN104055724A (en) * | 2014-07-01 | 2014-09-24 | 吴雪琴 | Preparation method of bitter gourd chlorophyll mask paste and product thereof |
| CN105064018A (en) * | 2015-09-08 | 2015-11-18 | 湖州南浔宏亮纺织有限公司 | Novel plant-type pure cotton fabric uvioresistant anticrease finishing agent |
| CN106974865A (en) * | 2017-04-05 | 2017-07-25 | 广州市聚吉科绿色化学共性技术研究院有限公司 | A kind of water moistens sun-proof Essence |
| CN107898733A (en) * | 2017-12-30 | 2018-04-13 | 广州市中通生化制品有限公司 | A kind of after-sun composition and preparation method and application |
| CN111053723B (en) * | 2020-01-17 | 2022-09-06 | 深圳市大同创新科技有限公司 | Anti-aging emulsion |
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| CN1277839A (en) * | 2000-05-23 | 2000-12-27 | 李雪涛 | Bamboo nutrient facemask and its prepn. method |
| JP5053519B2 (en) * | 2005-03-30 | 2012-10-17 | 株式会社ナリス化粧品 | Plant trypsin inhibitor |
| CN101073544A (en) * | 2006-05-16 | 2007-11-21 | 刘学文 | Spot-relieving face mask |
| CN101336879A (en) * | 2008-08-07 | 2009-01-07 | 北京昂立达技术有限责任公司 | Art pumpkin extract and use as anti-corrosive bacteria inhibitor and anti acne agent in cosmetics |
| CN101606896A (en) * | 2009-07-02 | 2009-12-23 | 烟台新时代健康产业日化有限公司 | New purposes of Folium Bambosae extract and method for making, its skin-care bath composition and method for making |
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