CN106309196A - Natural skin activating essence and preparation method thereof - Google Patents

Natural skin activating essence and preparation method thereof Download PDF

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Publication number
CN106309196A
CN106309196A CN201510389920.1A CN201510389920A CN106309196A CN 106309196 A CN106309196 A CN 106309196A CN 201510389920 A CN201510389920 A CN 201510389920A CN 106309196 A CN106309196 A CN 106309196A
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Prior art keywords
parts
extracting solution
component
skin
water
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CN201510389920.1A
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Chinese (zh)
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李红伟
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Qingdao Lannonggu Agricultural Products Research and Development Co Ltd
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Qingdao Lannonggu Agricultural Products Research and Development Co Ltd
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Priority to CN201510389920.1A priority Critical patent/CN106309196A/en
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  • Medicines Containing Plant Substances (AREA)

Abstract

The invention discloses natural skin activating essence and a preparation method thereof. The natural skin activating essence is characterized by being prepared from the following raw materials in parts by weight: a component A: 10 to 15 parts of a seaweed extracting solution, 2 to 3 parts of allantoin, 6 to 8 parts of glycerinum, 1.2 to 1.5 parts of xanthan gum and 50 parts of deionized water; a component B: 8 to 10 parts of a Nuphar pumilum (Hoffm.) DC. extracting solution, 2 to 3 parts of glyceryl stearate, 1.2 to 1.4 parts of methylparaben, 0.6 to 0.8 part of carbomer 941, 2 to 4 parts of polydimethylsiloxane, 0.5 to 0.7 part of panthenol, 0.08 to 0.1 part of essential oil and 0.06 to 0.08 part of ethylene diamine tetraacetic acid; and a component C: 8 to 10 parts of a water nymph extracting solution, 3 to 5 parts of hyaluronic acid, 1 to 2 parts of squalane, 0.5 to 0.7 part of nicotinamide and 0.1 to 0.3 part of a preservative. Active components in a water-based plant have the effects of delaying senescence and maintaining moisture; the seaweed extracting solution can suppress peroxidation of skin lipid and delay skin senescence; the Nuphar pumilum (Hoffm.) DC. extracting solution has a good effect of suppressing tyrosinase and can inhibit formation of melanin; and the water nymph extracting solution and the nicotinamide work cooperatively and have a deep water locking effect and a good moisture maintaining effect.

Description

A kind of natural skin-active elite and preparation method thereof
Technical field
The invention belongs to cosmetic technical field, be specifically related to a kind of natural skin-active elite and preparation method thereof.
Background technology
Skin is the barrier of human body, is the real picture of health.Impact due to the factor such as internal organs function, endocrine, heredity, medicine, ultraviolet irradiation, stress, traumatic, malnutrition, in poor quality cosmetic, reduce such as the antioxidant system activity of body self and immunity degradation, that human body skin is exposed to external environment condition is medium-term and long-term by reasons such as ultraviolet irradiation, atmospheric pollution, internal oxygen-derived free radicals increases, tryrosinase increases and activity increases, mottle will be produced, pigmentation, xerosis cutis is wrinkling, make face tarnish, be in the state of subhealth state.Photoaging is mainly the skin aging caused by ultraviolet damage accumulation, it is naturally-aged and the ultraviolet coefficient result of irradiation, it is limited to skin exposure portion, being mainly characterized by pachylosis matt, walk steady overstriking and deepen, pigmentation is deepened, skin microcirculation is deteriorated, elastosis, the phenomenons such as epidermis shows as removing power, collagen protein and elastin laminin synthesis capability and immunity degradation, dermis thickness generation thinning, easy allergy inflammation.
Water plant refers to growing plants in water, heavy water raw referring broadly to natural pond or floating plant.Water plant well developed root system, cane are tough, have the aerating tissue of prosperity, and leaf is soft and transparent, being formed as of having thread (such as hornwort).Filiform leaves can be greatly increased the contact area with water, makes leaf can obtain little getable illumination in water to greatest extent and absorb the carbon dioxide dissolving seldom in water, it is ensured that photosynthetic carries out.Currently marketed whitening, speckle removing, antisenescence product is a feast for the eyes, but the lead in most products, hydrargyrum, phenol content exceed standard, although in a short time can whitening and speckle dispelling, but life-time service can make, and keratodermatitis is thinning to come off, skin resistance is caused to decline, form new more mottle, be unfavorable for further skin protection.Therefore, the natural elite skin-protection product that exploitation safety is high, effective, it has also become one of main direction of studying of current medicine and cosmetic industry, has good market prospect.
Summary of the invention
For problems of the prior art, it is an object of the invention to provide a kind of natural skin-active elite and preparation method thereof.
The technical scheme that the present invention takes is:
A kind of natural skin-active elite, it is characterised in that feed components is as follows according to weight portion composition:
A component: seaweed extracted liquor 10-15 part, allantoin 2-3 part, glycerol 6-8 part, HANSHENGJIAO 1.2-1.5 part, deionized water 50 parts;
B component: spatterdock extracting solution 8-10 part, glyceryl stearate 2-3 part, methyl hydroxybenzoate 1.2-1.4 part, Carbopol 941 0.6-0.8 part, polydimethylsiloxane 2-4 part, pantothenylol 0.5-0.7 part, quintessence oil 0.08-0.1 part, disodiumedetate 0.06-0.08 part;
C component: Flos nymphaeae (Nymphaea teragona Georgi) extracting solution 8-10 part, hyaluronic acid 3-5 part, squalane 1-2 part, nicotiamide 0.5-0.7 part, preservative 0.1-0.3 part.
Further, described preservative is the mixture that sorbic acid, propiconazole, tribromphenol and Oleum sesami form according to weight ratio 2:2:3.
The preparation method of a kind of natural skin-active elite, it is characterised in that specifically include following steps:
(1) seaweed extracted liquor processed: take Sargassum and clean up, adds 70% ethanol of 15 times amount, is heated to 80 DEG C, reflux, extract, 1.5h, cross leaching filtrate, add 3% powdered active carbon, regulate pH=3.0 with hydrochloric acid, controlling temperature is 55 DEG C, control supersonic frequency is 200Hz, ultrasonic vibration decolouring 30min, filters gained filtrate, reclaim ethanol with Rotary Evaporators, be concentrated into 2g/mL;
(2) spatterdock extracting solution processed: take the spatterdock cleaned up, add the deionized water of 12 times amount, extracting 2 times in 50 DEG C of water-baths, each 20min, the 100mL that added water by residue after filtration extract 2 times at 75 DEG C, each 15 minutes, merging twice extracting solution, 3 times amount 60% ethanol stand 24h, filter, reclaim ethanol with Rotary Evaporators, be evaporated to 2g/mL;
(3) Flos nymphaeae (Nymphaea teragona Georgi) extracting solution processed: take the chopping of the Flos nymphaeae (Nymphaea teragona Georgi) blade after cleaning, put in iodine flask after grinding 0.5h, pH=4 is regulated with dilute hydrochloric acid, Flos nymphaeae (Nymphaea teragona Georgi) after homogenate is soaked 2h, decolouring, the filtrate after sucking filtration controls in temperature 128-130 DEG C, and regulation pressure is 3-5MPa, ripening sterilizing 20-22min, is evaporated to 1g/mL;
(4) elite finished product processed: take mixed raw material A component, B component and C component according to weight proportion respectively, at 85-90 DEG C, stirring and dissolving is abundant, does acid-base modifier with natural lemon acid, pH value of solution is adjusted to 6.0.
Described natural skin-active elite purposes in preparation moisturizing serial cosmetics.
The invention have the benefit that
It is raw material that the present invention chooses Sargassum in water plant, spatterdock and Flos nymphaeae (Nymphaea teragona Georgi), extract in the active component in plant, active component has the effect of defying age and moisturizing, seaweed extracted liquor can suppress the peroxidating of skin lipid, effectively penetrates skin, promotes the propagation of Skin Cell, to delay skin aging, spatterdock extracting solution has the effect of good suppression tryrosinase, melanin can be suppressed to be formed, skin whitening;Flos nymphaeae (Nymphaea teragona Georgi) extracting solution and nicotiamide synergism, have deep layer lock water effect, and moistening effect is good.Elite in the present invention is by PROCESS FOR TREATMENT such as extraction, concentrations, it is possible to fully extracts active nutrient component, can avoid the waste of resource, be substantially reduced cost, has natural environmental-protective performance.
Detailed description of the invention
Embodiment 1
A kind of natural skin-active elite, it is characterised in that feed components is as follows according to weight portion composition:
A component: seaweed extracted liquor 10 parts, allantoin 2 parts, glycerol 6 parts, HANSHENGJIAO 1.2 parts, deionized water 50 parts;
B component: spatterdock extracting solution 8 parts, glyceryl stearate 2 parts, methyl hydroxybenzoate 1.2 parts, Carbopol 941 0.6 part, polydimethylsiloxane 2 parts, pantothenylol 0.5 part, quintessence oil 0.08 part, disodiumedetate 0.06 part;
C component: Flos nymphaeae (Nymphaea teragona Georgi) extracting solution 8 parts, hyaluronic acid 3 parts, squalane 1 part, nicotiamide 0.5 part, preservative 0.1 part.
Further, described preservative is the mixture that sorbic acid, propiconazole, tribromphenol and Oleum sesami form according to weight ratio 2:2:3.
Embodiment 2
A kind of natural skin-active elite, it is characterised in that feed components is as follows according to weight portion composition:
A component: seaweed extracted liquor 12 parts, allantoin 2.5 parts, glycerol 7 parts, HANSHENGJIAO 1.3 parts, deionized water 50 parts;
B component: spatterdock extracting solution 9 parts, glyceryl stearate 2.5 parts, methyl hydroxybenzoate 1.3 parts, Carbopol 941 0.7 part, polydimethylsiloxane 3 parts, pantothenylol 0.6 part, quintessence oil 0.09 part, disodiumedetate 0.07 part;
C component: Flos nymphaeae (Nymphaea teragona Georgi) extracting solution 9 parts, hyaluronic acid 4 parts, squalane 1.5 parts, nicotiamide 0.6 part, preservative 0.2 part.
Further, described preservative is the mixture that sorbic acid, propiconazole, tribromphenol and Oleum sesami form according to weight ratio 2:2:3.
Embodiment 3
A kind of natural skin-active elite, it is characterised in that feed components is as follows according to weight portion composition:
A component: seaweed extracted liquor 15 parts, allantoin 3 parts, glycerol 8 parts, HANSHENGJIAO 1.5 parts, deionized water 50 parts;
B component: spatterdock extracting solution 10 parts, glyceryl stearate 3 parts, methyl hydroxybenzoate 1.4 parts, Carbopol 941 0.8 part, polydimethylsiloxane 4 parts, pantothenylol 0.7 part, quintessence oil 0.1 part, disodiumedetate 0.08 part;
C component: Flos nymphaeae (Nymphaea teragona Georgi) extracting solution 10 parts, hyaluronic acid 5 parts, squalane 2 parts, nicotiamide 0.7 part, preservative 0.3 part.
Further, described preservative is the mixture that sorbic acid, propiconazole, tribromphenol and Oleum sesami form according to weight ratio 2:2:3.
Table 1: the physical and chemical index of the defying age essence of embodiment 1 to 3.
Embodiment sensory testing PH value Centrefuge experiment Resistance to Thermal test Cold-resistant test Hydroscopicity (%)
Embodiment 1 Uniform color, exquisite quality, tend to smear out 6.58 Without layering Without layering Without layering -0.46
Embodiment 2 Uniform color, exquisite quality, tend to smear out 6.59 Without layering Without layering Without layering -0.46
Embodiment 3 Uniform color, exquisite quality, tend to smear out 6.60 Without layering Without layering Without layering -0.45
(6) skin experiment on probation
Defying age is tested:
1, skin elasticity test: test object is 30 for women, and the age is 35 years old, healthy.Test instrunment is the Reviscometer RV600(elastic fibrous tissue test probe of Germany CK company skin elasticity tester MPA580), survey and average for five times.
Test condition: (1) indoor environment;(2) without sunburst or light direct projection;(3) ambient temperature 20 ± 2 DEG C, ambient humidity 40-60%.
Test zone: left cheekbone portion.
Testing procedure: first measure the blank value (R2, R5, R7) of 30min after tested region clean, then sooner or later adhere to regulation experimenter every day using the product of embodiment 1, test 1 week respectively, 2 weeks, 3 weeks and test zone skin elasticity index R2, R5, R7 value (in test process, negative pressure is constant for 450mbar) after 4 weeks.
Index illustrates: skin elasticity index R2, R5, R7 are closer to 1, and the elasticity of skin is the best.Wherein, R2=Ua/Uf;
R5=Ur/Ue ;R7=Ur/Uf.Uf is skin maximum tension amount, and Ue is after constant negative pressure is added on skin, the amount of tension of skin during 0.1s, positioning elastic part amount of tension.Ur is for cancelling after negative pressure, and skin can restore to the original state rapidly state, is divided into elastic score value Ur equally, after i.e. cancelling negative pressure 0.1s, and the recovery value of skin and visco-elastic portions value, or claim shaping part value.Ua is that acquired results is shown in Table 2 to the recovery value of skin when follow-on test skin surface adds negative pressure more next time from cancellation negative pressure.
Table 2: skin elasticity test result
By table 2 it can be seen that use the product of embodiment 1 after 4 weeks, the skin elasticity index of experimenter has had the biggest lifting, illustrates that the present invention has preferable anti-aging effects.
The above is not limitation of the present invention; it is noted that, for those skilled in the art; on the premise of without departing from essential scope of the present invention, it is also possible to making some changes, retrofit, add or replace, these improvements and modifications also should be regarded as protection scope of the present invention.

Claims (4)

1. a natural skin-active elite, it is characterised in that feed components is as follows according to weight portion composition:
A component: seaweed extracted liquor 10-15 part, allantoin 2-3 part, glycerol 6-8 part, HANSHENGJIAO 1.2-1.5 part, deionized water 50 parts;
B component: spatterdock extracting solution 8-10 part, glyceryl stearate 2-3 part, methyl hydroxybenzoate 1.2-1.4 part, Carbopol 941 0.6-0.8 part, polydimethylsiloxane 2-4 part, pantothenylol 0.5-0.7 part, quintessence oil 0.08-0.1 part, disodiumedetate 0.06-0.08 part;
C component: Flos nymphaeae (Nymphaea teragona Georgi) extracting solution 8-10 part, hyaluronic acid 3-5 part, squalane 1-2 part, nicotiamide 0.5-0.7 part, preservative 0.1-0.3 part.
A kind of natural skin-active elite, it is characterised in that described preservative is the mixture that sorbic acid, propiconazole, tribromphenol and Oleum sesami form according to weight ratio 2:2:3.
3. the preparation method of a natural skin-active elite, it is characterised in that specifically include following steps:
(1) seaweed extracted liquor processed: take Sargassum and clean up, adds 70% ethanol of 15 times amount, is heated to 80 DEG C, reflux, extract, 1.5h, cross leaching filtrate, add 3% powdered active carbon, regulate pH=3.0 with hydrochloric acid, controlling temperature is 55 DEG C, control supersonic frequency is 200Hz, ultrasonic vibration decolouring 30min, filters gained filtrate, reclaim ethanol with Rotary Evaporators, be concentrated into 2g/mL;
(2) spatterdock extracting solution processed: take the spatterdock cleaned up, add the deionized water of 12 times amount, extracting 2 times in 50 DEG C of water-baths, each 20min, the 100mL that added water by residue after filtration extract 2 times at 75 DEG C, each 15 minutes, merging twice extracting solution, 3 times amount 60% ethanol stand 24h, filter, reclaim ethanol with Rotary Evaporators, be evaporated to 2g/mL;
(3) Flos nymphaeae (Nymphaea teragona Georgi) extracting solution processed: take the chopping of the Flos nymphaeae (Nymphaea teragona Georgi) blade after cleaning, put in iodine flask after grinding 0.5h, pH=4 is regulated with dilute hydrochloric acid, Flos nymphaeae (Nymphaea teragona Georgi) after homogenate is soaked 2h, decolouring, the filtrate after sucking filtration controls in temperature 128-130 DEG C, and regulation pressure is 3-5MPa, ripening sterilizing 20-22min, is evaporated to 1g/mL;
(4) elite finished product processed: take mixed raw material A component, B component and C component according to weight proportion respectively, at 85-90 DEG C, stirring and dissolving is abundant, does acid-base modifier with natural lemon acid, pH value of solution is adjusted to 6.0.
4. according to the natural skin-active elite described in any one of claim 1-3 preparation moisturizing serial cosmetics in purposes.
CN201510389920.1A 2015-07-06 2015-07-06 Natural skin activating essence and preparation method thereof Pending CN106309196A (en)

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Cited By (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN107320404A (en) * 2017-06-14 2017-11-07 佛山市汇汾化妆品科技有限公司 A kind of anti-acne repairs facial mask
CN107510628A (en) * 2017-08-16 2017-12-26 佛山市三水区嘉信农业技术研究院(普通合伙) It is a kind of with the plant residue composition of anti-inflammatory efficacy and its application
CN111150667A (en) * 2019-07-05 2020-05-15 山东省科学院生物研究所 Seaweed smoothing toner and preparation method thereof
US11786451B2 (en) 2019-06-28 2023-10-17 The Procter & Gamble Company Skin care composition
US12102707B2 (en) 2023-08-28 2024-10-01 The Procter & Gamble Company Skin care composition

Cited By (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN107320404A (en) * 2017-06-14 2017-11-07 佛山市汇汾化妆品科技有限公司 A kind of anti-acne repairs facial mask
CN107510628A (en) * 2017-08-16 2017-12-26 佛山市三水区嘉信农业技术研究院(普通合伙) It is a kind of with the plant residue composition of anti-inflammatory efficacy and its application
US11786451B2 (en) 2019-06-28 2023-10-17 The Procter & Gamble Company Skin care composition
CN111150667A (en) * 2019-07-05 2020-05-15 山东省科学院生物研究所 Seaweed smoothing toner and preparation method thereof
US12102707B2 (en) 2023-08-28 2024-10-01 The Procter & Gamble Company Skin care composition

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Application publication date: 20170111