CN106307476A - Functional sucrose composition and preparation method thereof - Google Patents

Functional sucrose composition and preparation method thereof Download PDF

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Publication number
CN106307476A
CN106307476A CN201610687416.4A CN201610687416A CN106307476A CN 106307476 A CN106307476 A CN 106307476A CN 201610687416 A CN201610687416 A CN 201610687416A CN 106307476 A CN106307476 A CN 106307476A
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CN
China
Prior art keywords
function
sucrose
preparation
sucrose composition
composition
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Pending
Application number
CN201610687416.4A
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Chinese (zh)
Inventor
黄向阳
张平军
许广球
陈骏佳
高俊永
胡彪
孙潇
莫柳珍
谢武装
陆金
杨欢
梁波
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Guangdong Institute of Bioengineering Guangzhou Cane Sugar Industry Research Institute
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Guangdong Institute of Bioengineering Guangzhou Cane Sugar Industry Research Institute
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Application filed by Guangdong Institute of Bioengineering Guangzhou Cane Sugar Industry Research Institute filed Critical Guangdong Institute of Bioengineering Guangzhou Cane Sugar Industry Research Institute
Priority to CN201610687416.4A priority Critical patent/CN106307476A/en
Publication of CN106307476A publication Critical patent/CN106307476A/en
Pending legal-status Critical Current

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    • AHUMAN NECESSITIES
    • A23FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23VINDEXING SCHEME RELATING TO FOODS, FOODSTUFFS OR NON-ALCOHOLIC BEVERAGES AND LACTIC OR PROPIONIC ACID BACTERIA USED IN FOODSTUFFS OR FOOD PREPARATION
    • A23V2002/00Food compositions, function of food ingredients or processes for food or foodstuffs

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  • Coloring Foods And Improving Nutritive Qualities (AREA)
  • Pharmaceuticals Containing Other Organic And Inorganic Compounds (AREA)

Abstract

The invention belongs to the technical field of sugar industry and discloses a functional sucrose composition and a preparation method thereof. The functional sucrose composition is prepared by performing spray drying or evaporation, concentration and crystallization on the following solutions in percentage by mass: 59.5-69.6% of sucrose, 0.0001-0.001% of mineral substance, 0.01-0.05% of vitamins, 0.01-0.2% of polysaccharides, 0.01-0.2% of oligosaccharide, 0.01-0.1% of polyphenol, 0.001-0.01% of carotenoid and 30-40% of water. According to the invention, the sucrose serves as a raw material, a healthy special sugar product with high additional value is developed by accurately adding health factors and adopting the crystallization technology, and the functional sucrose composition has significances for extending the traditional sugaring industrial chain, reducing the production cost, improving the corporate profits and realizing the sustainable development.

Description

A kind of function sucrose composition and preparation method thereof
Technical field
The invention belongs to sugar industry technical field, be specifically related to a kind of function sucrose composition and preparation method thereof.
Background technology
In U.S., European and Japanese, the market share of health type special type sugar products gradually expands, and sales volume is much larger than common Sugar products, added value is the highest.The U.S. produces extraordinary sugar about 1,100,000 tons, Taiwan special type candy output nearly 2/3, and demand per year at present Increasing year by year, the U.S. in 2015 also need to be from country's nearly 250,000 tons of extraordinary sugar products of import such as India, and import volume the most significantly goes up Rise.
China is third place in the world great Chan Tang state and second largest sugar country of consumption, year consumption sugar more than 1,600 ten thousand tons.But for a long time with Coming, China's sugar industry product variety is dull, and extraordinary Sucrose products ingredient is complicated and uncertain, there is sugar products and asks safely Topic.Such as, brown sugar is lived because remaining the multiple nutrients materials such as trace element, aminoacid, vitamin and abundant flavone sugar glycoside Property material, product special flavour is unique, and health-care effect is obvious.But the concrete composition of brown sugar and the distribution of every batch various health ingredients amount All there is uncertain and uncontrollability.Along with improving constantly of living standard, the demand of healthy extraordinary sugar products can be got over by China Coming the biggest, by 20% calculating of U.S.'s consumption figure, 5 Nian Nei China are up to 1,000,000 tons to the year demand of function special type sugar, relate to The output value more than 8,000,000,000 yuan, has good application prospect at civilian sugar and high-end product market.
Therefore, develop the healthy extraordinary sugar products of high added value, to extend tradition sugaring industrial chain, to reduce production cost, Improve enterprise profit, to realize the sustainable development of self, be those skilled in the art and enterprise's problem demanding prompt solution.
Summary of the invention
In place of solving the shortcoming and defect of above prior art, the primary and foremost purpose of the present invention is to provide a kind of function The preparation method of sucrose composition.
Another object of the present invention is to provide a kind of function sucrose composition prepared by said method.
The object of the invention is achieved through the following technical solutions:
A kind of preparation method of function sucrose composition, including following preparation process:
(1) by the component configuration solution of following weight/mass percentage composition:
(2) solution step (1) prepared is by being spray-dried or evaporating, concentrating and crystallizing, obtains the combination of described function sucrose Thing.
One or both mixing in the preferred potassium chloride of described mineral and calcium chloride.
One or more mixing in the preferred vitamin B1 of described vitamin, B2, B6 and B12.
The preferred lycium barbarum polysaccharide of described polysaccharide or ganoderan.
The preferred manna oligosaccharide of described oligosaccharide or acetylglucosamine.
The preferred tea polyphenols of described polyphenol, Caulis Sacchari sinensis polyphenol or grape seed polyphenols.
The preferred lycopene of described carotenoid or phylloxanthin.
The condition being spray-dried described in step (2) is: hot wind inlet temperature 160 DEG C~250 DEG C, air outlet temperature 45 C ~90 DEG C.
The process of described evaporating, concentrating and crystallizing is: the solution that step (1) is prepared absolute pressure be 0.012~ 0.025MPa, condensing crystallizing under the conditions of temperature 55 DEG C~70 DEG C, obtaining concentration is 95 ° of Bx~the massecuite of 99 ° of Bx, the most directly coagulates Break up Gu be dried, obtain described function sucrose composition.
A kind of function sucrose composition, is prepared by said method.
Preferably, the moisture content mass fraction of described function sucrose composition is less than 0.001%.
Preparation method and the obtained product of the present invention have the advantage that and beneficial effect:
(1) ground that the preparation method of the present invention can be qualitative with quantitative becomes subpackage above-mentioned various natural healthy efficiency factors Being hidden among Sucrose products, food safety hidden danger and the assurance function that can thoroughly eliminate current extraordinary saccharide existence the most on the market are lived Property material stability, meanwhile, edible after, these active skull cap components cooperate, synergism, beneficially health, Improve the living standard of people;
(2) the healthy efficiency factor composition that the present invention adds is evenly distributed in the Sucrose products of preparation;
(3) present invention is with sucrose as raw material, by precisely adding health factor, using crystallization technique, develops high additional The healthy extraordinary sugar products of value, for extending tradition sugaring industrial chain, reducing production cost, improves enterprise profit, to realize self Sustainable development significant.
Detailed description of the invention
Below in conjunction with embodiment, the present invention is described in further detail, but embodiments of the present invention are not limited to this.
Embodiment 1
(1) solution is first prepared: solution is many by sucrose, potassium chloride, vitamin B1, the mixture of B2, B6, B12, Fructus Lycii Sugar, manna oligosaccharide, tea polyphenols, lycopene, water are mixed to prepare, wherein the mass percent of sucrose be 59.5%, potassium chloride Mass percent be 0.0001%, vitamin B1, the mass percent of mixture of B2, B6, B12 be 0.01%, Fructus Lycii many The mass percent of sugar is 0.2%, the mass percent of manna oligosaccharide is 0.2%, the mass percent of tea polyphenols is 0.0889%, the mass percent of lycopene be 0.001%, the mass percent of water be 40%.
(2) solution prepared is passed through spray drying device at hot wind inlet temperature 160 DEG C, air outlet temperature 45 C bar The health type special type Sucrose products that moisture content mass fraction is 0.0008% is prepared under part.Under similarity condition, the spy of production Kind of Sucrose products preserve respectively 0 day, 30 days, 180 days, after 360 days, use DPPH method to detect the radical scavenging activity of product respectively Power is respectively 35.8%, 35.7%, 35.6%, 35.6%.Embodiment 2
(1) solution is first prepared: solution is many by sucrose, calcium chloride, vitamin B1, the mixture of B2, B6, B12, Ganoderma Sugar, acetylglucosamine, Caulis Sacchari sinensis polyphenol, phylloxanthin, water are mixed to prepare, wherein the mass percent of sucrose be 69.6%, chlorine The mass percent changing calcium is 0.001%, vitamin B1, the mass percent of mixture of B2, B6, B12 are 0.05%, Ganoderma The mass percent of polysaccharide is 0.039%, the mass percent of acetylglucosamine is 0.2%, the quality hundred of Caulis Sacchari sinensis polyphenol Mark is 0.1%, the mass percent of phylloxanthin is 0.01%, the mass percent of water is 30%.
(2) solution prepared is passed through spray drying device at hot wind inlet temperature 250 DEG C, 90 DEG C of bars of air outlet temperature The health type special type Sucrose products that moisture content mass fraction is 0.0005% is prepared under part.Under the same conditions, 3 are taken at random The extraordinary Sucrose products of part, uses the radical scavenging activity of DPPH method detection product to be respectively 36.2%, 36.2%, 36.2%.
Embodiment 3
(1) solution is first prepared: solution is many by sucrose, potassium chloride, vitamin B1, the mixture of B2, B6, B12, Fructus Lycii Sugar, manna oligosaccharide, grape seed polyphenols, lycopene, water are mixed to prepare, wherein the mass percent of sucrose be 64%, chlorination The mass percent of potassium is 0.001%, vitamin B1, the mass percent of mixture of B2, B6, B12 are 0.05%, Fructus Lycii is many The mass percent of sugar is 0.01%, the mass percent of manna oligosaccharide is 0.129%, the mass percent of grape seed polyphenols Be 0.1%, the mass percent of lycopene be 0.01%, the mass percent of water be 35.7%.
(2) by the solution prepared absolute pressure be 0.012MPa, condensing crystallizing under the conditions of temperature 55 DEG C, obtain concentration Being the massecuite of 95 ° of Bx, then directly solidification is dry breaks up, and obtains the health type special type sugarcane that moisture content mass fraction is 0.0006% Sugar product.Under similarity condition, the extraordinary Sucrose products of production preserve respectively 0 day, 30 days, 180 days, after 360 days, use DPPH method The radical scavenging activity detecting product respectively is respectively 38.3%, 38.3%, 38.2%, 38.2%.
Embodiment 4
(1) solution is first prepared: solution is by sucrose, potassium chloride and the mixture of calcium chloride, vitamin B1, B2, B6, B12 Mixture, ganoderan, acetylglucosamine, tea polyphenols, phylloxanthin, water be mixed to prepare, the wherein percent mass of sucrose Number be the mass percent of the mixture of 66%, potassium chloride and calcium chloride be 0.0001%, vitamin B1, B2, B6, B12 mixed The mass percent of compound is 0.015%, the mass percent of ganoderan is 0.1639%, the quality of acetylglucosamine Percent is 0.01%, the mass percent of tea polyphenols is 0.01%, the mass percent of phylloxanthin is 0.001%, the matter of water Amount percent is 33.8%.
(2) the solution condensing crystallizing under the conditions of absolute pressure is 0.025MPa, temperature 70 C that will prepare, obtains concentration Being the massecuite of 99 ° of Bx, then directly dry the breaing up of solidification obtains the health type special type sugarcane that moisture content mass fraction is 0.0003% Sugar product.Under the same conditions, take 3 parts of extraordinary Sucrose products at random, use the radical scavenging activity of DPPH method detection product It is 30.8%, 30.8%, 30.8%.
Above-described embodiment is the present invention preferably embodiment, but embodiments of the present invention are not by above-described embodiment Limit, the change made under other any spirit without departing from the present invention and principle, modify, substitute, combine, simplify, All should be the substitute mode of equivalence, within being included in protection scope of the present invention.

Claims (10)

1. the preparation method of a function sucrose composition, it is characterised in that include following preparation process:
(1) by the component configuration solution of following weight/mass percentage composition:
(2) solution step (1) prepared is by being spray-dried or evaporating, concentrating and crystallizing, obtains described function sucrose composition.
The preparation method of a kind of function sucrose composition the most according to claim 1, it is characterised in that: described mineral is One or both mixing in potassium chloride and calcium chloride.
The preparation method of a kind of function sucrose composition the most according to claim 1, it is characterised in that: described vitamin is One or more mixing in vitamin B1, B2, B6 and B12.
The preparation method of a kind of function sucrose composition the most according to claim 1, it is characterised in that: described polysaccharide is Chinese holly Qi polysaccharide or ganoderan.
The preparation method of a kind of function sucrose composition the most according to claim 1, it is characterised in that: described oligosaccharide is Manna oligosaccharide or acetylglucosamine.
The preparation method of a kind of function sucrose composition the most according to claim 1, it is characterised in that: described polyphenol is tea Polyphenol, Caulis Sacchari sinensis polyphenol or grape seed polyphenols.
The preparation method of a kind of function sucrose composition the most according to claim 1, it is characterised in that: described carotenoids Element is lycopene or phylloxanthin.
The preparation method of a kind of function sucrose composition the most according to claim 1, it is characterised in that described in step (2) The condition being spray-dried is: hot wind inlet temperature 160 DEG C~250 DEG C, air outlet temperature 45 C~90 DEG C;Described evaporation and concentration is tied Brilliant process is: solution step (1) prepared is 0.012~0.025MPa in absolute pressure, 55 DEG C~70 DEG C conditions of temperature Lower condensing crystallizing, obtaining concentration is 95 ° of Bx~the massecuite of 99 ° of Bx, and then directly solidification is dry breaks up, and obtains described function sucrose Compositions.
9. a function sucrose composition, it is characterised in that: prepared by the method described in any one of claim 1~8.
A kind of function sucrose composition the most according to claim 9, it is characterised in that: described function sucrose composition Moisture content mass fraction is less than 0.001%.
CN201610687416.4A 2016-08-18 2016-08-18 Functional sucrose composition and preparation method thereof Pending CN106307476A (en)

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Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN115886171A (en) * 2022-11-01 2023-04-04 黑龙江乌苏里江制药有限公司 Composite solid beverage and preparation method thereof

Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN101011087A (en) * 2007-02-14 2007-08-08 内蒙古蒙牛乳业(集团)股份有限公司 Gas-filled milk-containing beverage and its production method
CN101897420A (en) * 2009-10-29 2010-12-01 山东福田药业有限公司 Novel functional healthy sugar and preparation technology thereof
EP2692243A1 (en) * 2012-08-03 2014-02-05 Krüger GmbH & Co. KG Composition for delayed resorption

Patent Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN101011087A (en) * 2007-02-14 2007-08-08 内蒙古蒙牛乳业(集团)股份有限公司 Gas-filled milk-containing beverage and its production method
CN101897420A (en) * 2009-10-29 2010-12-01 山东福田药业有限公司 Novel functional healthy sugar and preparation technology thereof
EP2692243A1 (en) * 2012-08-03 2014-02-05 Krüger GmbH & Co. KG Composition for delayed resorption

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN115886171A (en) * 2022-11-01 2023-04-04 黑龙江乌苏里江制药有限公司 Composite solid beverage and preparation method thereof
CN115886171B (en) * 2022-11-01 2024-02-02 黑龙江乌苏里江制药有限公司 Composite solid beverage and preparation method thereof

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