CN106281797A - Radix Apioris Fortunei (Radix Lespedezae Buergeri) soap and preparation method thereof - Google Patents
Radix Apioris Fortunei (Radix Lespedezae Buergeri) soap and preparation method thereof Download PDFInfo
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- CN106281797A CN106281797A CN201610652302.6A CN201610652302A CN106281797A CN 106281797 A CN106281797 A CN 106281797A CN 201610652302 A CN201610652302 A CN 201610652302A CN 106281797 A CN106281797 A CN 106281797A
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- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D9/00—Compositions of detergents based essentially on soap
- C11D9/02—Compositions of detergents based essentially on soap on alkali or ammonium soaps
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- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D9/00—Compositions of detergents based essentially on soap
- C11D9/04—Compositions of detergents based essentially on soap containing compounding ingredients other than soaps
- C11D9/22—Organic compounds, e.g. vitamins
- C11D9/26—Organic compounds, e.g. vitamins containing oxygen
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- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D9/00—Compositions of detergents based essentially on soap
- C11D9/04—Compositions of detergents based essentially on soap containing compounding ingredients other than soaps
- C11D9/22—Organic compounds, e.g. vitamins
- C11D9/26—Organic compounds, e.g. vitamins containing oxygen
- C11D9/262—Organic compounds, e.g. vitamins containing oxygen containing carbohydrates
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- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D9/00—Compositions of detergents based essentially on soap
- C11D9/04—Compositions of detergents based essentially on soap containing compounding ingredients other than soaps
- C11D9/22—Organic compounds, e.g. vitamins
- C11D9/26—Organic compounds, e.g. vitamins containing oxygen
- C11D9/265—Organic compounds, e.g. vitamins containing oxygen containing glycerol
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- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D9/00—Compositions of detergents based essentially on soap
- C11D9/04—Compositions of detergents based essentially on soap containing compounding ingredients other than soaps
- C11D9/22—Organic compounds, e.g. vitamins
- C11D9/30—Organic compounds, e.g. vitamins containing nitrogen
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- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D9/00—Compositions of detergents based essentially on soap
- C11D9/04—Compositions of detergents based essentially on soap containing compounding ingredients other than soaps
- C11D9/22—Organic compounds, e.g. vitamins
- C11D9/38—Products in which the composition is not well defined
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- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D9/00—Compositions of detergents based essentially on soap
- C11D9/04—Compositions of detergents based essentially on soap containing compounding ingredients other than soaps
- C11D9/44—Perfumes; Colouring materials; Brightening agents ; Bleaching agents
- C11D9/442—Perfumes
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- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D9/00—Compositions of detergents based essentially on soap
- C11D9/04—Compositions of detergents based essentially on soap containing compounding ingredients other than soaps
- C11D9/48—Superfatting agents
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Abstract
The present invention relates to a kind of Radix Apioris Fortunei (Radix Lespedezae Buergeri) soap and preparation method thereof, the present invention with the addition of Radix Apioris Fortunei (Radix Lespedezae Buergeri) mixing breaking cellular wall stock solution in soap formula, this Radix Apioris Fortunei (Radix Lespedezae Buergeri) mixing breaking cellular wall stock solution uses spectrum sterilization, the ultralow fine preparation method of constant temperature vibration Wet-type wall-breaking to obtain, prepare at temperature is 2 ± 0.1 DEG C, 2～0 DEG C of cryopreservation, cell-wall breaking ratio reaches more than 98.5%, has been sufficiently reserved its bioactive ingredients, improves the utilization rate of medical material, adds its added value；The present invention also adds the composition such as natural oil in the formula of soap, moistens, the effect such as anti-inflammation, antioxidation reaches best；Soap lye, when preparing interpolation Radix Apioris Fortunei (Radix Lespedezae Buergeri) mixing breaking cellular wall stock solution during soap, is sufficiently mixed when 60 DEG C～70 DEG C after saponification by the present invention with mixing breaking cellular wall stock solution, and drug effect is lossless；It addition, added with the form of stock solution by Radix Apioris Fortunei (Radix Lespedezae Buergeri), Radix Apioris Fortunei (Radix Lespedezae Buergeri) release efficiency can be made to increase substantially while medical material consume is minimum, what it was full and uniform incorporates in soap, preferably plays drug effect.
Description
Technical field
The present invention relates to the preparation method technical field of soaps and soaps, refer specifically to a kind of Radix Apioris Fortunei (Radix Lespedezae Buergeri) soap and preparation side thereof
Method.
Background technology
The Ji Yuan of Radix Apioris Fortunei (Radix Lespedezae Buergeri) is Vitaceae Tetrastigma plant tetratigma hemsleyanum Tetrastigma hemsleyanum
Diels et.Gilg, different name is Radix Tetrastigmatis Hemsleyani " Zhiwu Mingshi Tukao ", Shi Baozi " Jiangxi medical herbs ", gold thread hoist, SANYE pair
" Zhejiang conventional medical herbs among the people ", little Caulis et Radix Tetrastigmatis Planicaulis, SANYE Caulis et Radix Tetrastigmatis Planicaulis, block mountain tiger " Guangxi practicality Chinese herbal medicine newly selects ", thunder courage " Hunan medium-height grass
Medicine new therapy that combines both Chinese and Western medical practices data is selected and compile ".Radix Apioris Fortunei (Radix Lespedezae Buergeri) is flat, mildly bitter flavor, has the effects such as heat-clearing and toxic substances removing, dispelling pathogenic wind and eliminating phlegm, promoting blood circulation and stopping pain.Three
Ye Qing is eaten for a long time safety non-toxic and can improve the function of immunity, and Radix Apioris Fortunei (Radix Lespedezae Buergeri) enhancing human immunity is mainly reflected in and not only can improve
Cellular immunization, moreover it is possible to improve humoral immunization, i.e. promote the generation of interferon, interleukin, the conjunction of induced tumor necrosin
Become.It addition, Radix Apioris Fortunei (Radix Lespedezae Buergeri) can be used for treating venom, tonsillitis, tuberculous lymphadenitis, traumatic injury, little with hemostasia and detumescence
The diseases such as youngster's hyperpyrexia convulsion, are Western medicine " bouvardins " that cannot replace.
Effect of Radix Apioris Fortunei (Radix Lespedezae Buergeri) soap mainly show as following some:
1, skin is nourished: Radix Apioris Fortunei (Radix Lespedezae Buergeri) originally has and just contains oils and fats, adds again natural oil in soap, to the moisturizing effect of skin more
Good；
2, antioxidation: Radix Apioris Fortunei (Radix Lespedezae Buergeri), rich in the composition such as flavonoid, anthocyan, is natural antioxidant, can effectively remove
Internal oxygen-derived free radicals, as anthocyanidin can overflow with the full stage of oil-control peroxide, this ability stoping oxidation
Being more than ten times of vitamin E, this antioxidation can stop the degeneration of cell, aging, it is possible to stops the generation of cancer；
3, improve skin immunization power: Radix Apioris Fortunei (Radix Lespedezae Buergeri) can promote that interferon, interleukin generate after absorbing, thus improve thin
Born of the same parents' immunity, strengthen skin resist various pathogenic bacterias invasion and attack from anti-ability；
4, anti-inflammation: oozing out of suppression inflammatory enzyme, can promote wound healing and pain relieving, kill in time in skin
Harmful pathogenic bacteria, remove inflammation (all kinds of recessiveness and can see), preventing and treating scytitis development in time.Including mosquito
Sting, insect bite, all kinds of recessive and visible inflammation such as pox, bleb occur in skin.
Radix Apioris Fortunei (Radix Lespedezae Buergeri) is added in soap, can improve the immunologic function of skin, and play effect of anti-inflammation, but, how
The application of effect and Radix Apioris Fortunei (Radix Lespedezae Buergeri) deep processing of playing Radix Apioris Fortunei (Radix Lespedezae Buergeri) to greatest extent all becomes people and is devoted to research in recent years
A difficult problem.At present, relatively conventional Radix Apioris Fortunei (Radix Lespedezae Buergeri) addition manner is to be made into Radix Apioris Fortunei (Radix Lespedezae Buergeri) powder, or carries out by the way of steaming and decocting
Extracting, being directly prepared into the mode cell of Radix Apioris Fortunei (Radix Lespedezae Buergeri) powder, to break ratio low, carries out extracting by steaming and decocting mode, can destroy SANYE
The biological activity of blue or green fresh goods, causes the overall utilization rate of medical material and added value relatively low, is difficult to mix homogeneously with adding main body, enters one
Step affects the performance of drug effect.
Summary of the invention
The technical problem to be solved is the present situation for prior art, it is provided that a kind of medical material utilization rate is high, medicine
Imitate significant Radix Apioris Fortunei (Radix Lespedezae Buergeri) soap.
To be solved by this invention another technical problem is that the present situation for prior art, it is provided that a kind of above-mentioned Radix Apioris Fortunei (Radix Lespedezae Buergeri)
The preparation method of soap, the method can be effectively improved the utilization rate of Radix Apioris Fortunei (Radix Lespedezae Buergeri), completely retain biological activity, make Radix Apioris Fortunei (Radix Lespedezae Buergeri) full and uniform
Incorporate in soap, play more preferable drug effect.
The present invention solves the technical scheme that above-mentioned technical problem used: a kind of Radix Apioris Fortunei (Radix Lespedezae Buergeri) soap, it is characterised in that by weight
Gauge includes following components:
Radix Apioris Fortunei (Radix Lespedezae Buergeri) mixing breaking cellular wall stock solution 3.4～17.8 parts, Oleum Cocois 5～15 parts, Petiolus Trachycarpi oil 10～25 parts, olive oil 5～
15 parts, Semen pruni armeniacae oil 6～18 parts, water 5.5～15.5 parts, sucrose 5～15 parts, sodium hydroxide 3～17 parts, glycerol 4～12 parts, food
With essence 0.1～3 parts, EDETATE SODIUM 0.005～0.3 part and butylated hydroxytoluene 0.005～0.3 part.
As preferably, described Radix Apioris Fortunei (Radix Lespedezae Buergeri) soap includes following components by weight:
Radix Apioris Fortunei (Radix Lespedezae Buergeri) mixing breaking cellular wall stock solution 7～16 parts, Oleum Cocois 8～12 parts, Petiolus Trachycarpi oil 15～20 parts, olive oil 8～11 parts,
Semen pruni armeniacae oil 9～12 parts, water 7～13 parts, sucrose 9～12 parts, sodium hydroxide 6～12 parts, glycerol 5～10 parts, edible essence 0.8
～2 parts, EDETATE SODIUM 0.01～0.1 part and butylated hydroxytoluene 0.005～0.1 part.
Further preferably, described Radix Apioris Fortunei (Radix Lespedezae Buergeri) soap includes following components by weight:
Radix Apioris Fortunei (Radix Lespedezae Buergeri) mixing breaking cellular wall stock solution 11.5 parts, Oleum Cocois 10 parts, Petiolus Trachycarpi oil 20 parts, 10 parts of olive oil, Semen pruni armeniacae oil 12
Part, 10.46 parts of water, sucrose 10 parts, sodium hydroxide 7 parts, glycerol 8 parts, edible essence 1 part, EDETATE SODIUM 0.03 part and fourth hydroxyl
Toluene 0.01 part.
As improvement, according to weight meter, described Radix Apioris Fortunei (Radix Lespedezae Buergeri) mixing breaking cellular wall stock solution includes Radix Apioris Fortunei (Radix Lespedezae Buergeri) 3～15 parts, green tea 0.3
～2 parts, Radix Notoginseng 0.1～0.8 part and ultra-pure water, described Radix Apioris Fortunei (Radix Lespedezae Buergeri), green tea, the gross weight of Radix Notoginseng and the weight ratio of ultra-pure water
≤1:1.3.More preferably, Radix Notoginseng has anti-inflammation, analgesic acts on for Radix Apioris Fortunei (Radix Lespedezae Buergeri), Radix Notoginseng, green tea mixed stock solution drug effect, and tea
Catechin, theaflavin and phenol in leaf has notable antibacterial action to enteritis pathogenic bacteria, many to staphylococcus aureus, Bacillus typhi etc.
Plant malignant bacteria and also have obvious inhibitory action, this and the hemostasia and detumescence of Radix Apioris Fortunei (Radix Lespedezae Buergeri), anti-inflammation, enhancing cellular immunity effect
Blending, three plays synergism, thus effectively strengthens the anti-inflammation function of soap, and meanwhile, Radix Apioris Fortunei (Radix Lespedezae Buergeri) becomes rich in flavonoid
Point, the composition such as anthocyan have preferable whitening and protective action for the skin of human body, anthocyanidin can be with oil-control
Full stage of oxide overflows, and this ability stoping oxidation is more than ten times of vitamin E, and safety, gentleness, can be the most clear
Deoxygenation free radical, the natural oil such as three kinds of stock solutions mixed and the Oleum Cocois of interpolation, Petiolus Trachycarpi oil, give soap with moist benefit
Water, whitening, antioxidation, effect of defying age, play more preferable skin care effect.
Preferably, the usage amount of described Radix Apioris Fortunei (Radix Lespedezae Buergeri), green tea and Radix Notoginseng be respectively Radix Apioris Fortunei (Radix Lespedezae Buergeri) 10 parts, green tea 0.9 part, three
7 0.6 parts.
Described Radix Apioris Fortunei (Radix Lespedezae Buergeri) mixing breaking cellular wall stock solution is obtained by following steps:
Step 1:
A, the Radix Apioris Fortunei (Radix Lespedezae Buergeri) sorting of fresh harvesting are cleaned；
B, by clean Radix Apioris Fortunei (Radix Lespedezae Buergeri) spectrum sterilizing 5～10 minutes；
C, the Radix Apioris Fortunei (Radix Lespedezae Buergeri) after spectrum sterilizing is shredded, obtain cutting off thing, and be placed under spectrum sterilized environment stand-by；
Step 2:
A, the green tea sorting of fresh harvesting are cleaned；
B, by clean green tea spectrum sterilizing 5～10 minutes；
C, the green tea after spectrum sterilizing is shredded, obtain cutting off thing, and be placed under spectrum sterilized environment stand-by；
Step 3:
It is broken that a, sterilization step 1 and step 2 obtained cut-out thing and Radix Notoginseng carry out wall-broken micro powder in gnotobasis；
B, interpolation ultra-pure water, make the weight ratio≤1:1.3 of medicine total amount and water；
C, to carry out wall-broken micro powder broken, produces mixing breaking cellular wall stock solution at temperature is for-1.9～-2.1 DEG C, and cell-wall breaking ratio is
More than 98.5%；
D, the mixing breaking cellular wall stock solution produced first is sterilized with spectrum, then preserve at gnotobasis ,-2 DEG C～0 DEG C.
The preparation method of a kind of above-mentioned Radix Apioris Fortunei (Radix Lespedezae Buergeri) soap, it is characterised in that comprise the following steps:
Step one:
The sodium hydroxide taking formula ratio is slowly added in water, and limit bevelling stirs 3～5 minutes, obtains sodium hydroxide solution, and
Control temperature at 40～50 DEG C；
Step 2:
Oleum Cocois, Petiolus Trachycarpi oil, olive oil and Semen pruni armeniacae oil are pressed formula proportion mix and blend, keep pressure-
0.5MPa～-0.1Mpa, stirs and maintains the temperature at 65 DEG C～75 DEG C；Sodium hydroxide solution and sucrose are slowly added
Entering in above-mentioned fluid, limit bevelling stirs until soap lye becomes the pasty state of thickness；Continuously add the glycerol of corresponding proportion, EDTA bis-
Sodium, butylated hydroxytoluene, stir, and temperature is still maintained at 60 DEG C～70 DEG C and carries out saponification；
Step 3:
The Radix Apioris Fortunei (Radix Lespedezae Buergeri) mixing breaking cellular wall stock solution of corresponding proportion, edible essence is added, quickly in saponification completely mixed solution
Uniform stirring, injects evacuation in mould, cooling by soap lye after stirring, chilling temperature is 0～5 DEG C, after being cooled to solidification
I.e. obtain described Radix Apioris Fortunei (Radix Lespedezae Buergeri) soap.
In the preparation method of above-mentioned Radix Apioris Fortunei (Radix Lespedezae Buergeri) soap, according to weight meter, described Radix Apioris Fortunei (Radix Lespedezae Buergeri) mixing breaking cellular wall stock solution includes SANYE
Blue or green 3～15 parts, green tea 0.3～2 parts, Radix Notoginseng 0.1～0.8 part and ultra-pure water, described Radix Apioris Fortunei (Radix Lespedezae Buergeri), green tea, the gross weight of Radix Notoginseng
Amount and the weight ratio≤1:1.3 of ultra-pure water.
In the preparation method of above-mentioned Radix Apioris Fortunei (Radix Lespedezae Buergeri) soap, described Radix Apioris Fortunei (Radix Lespedezae Buergeri) mixing breaking cellular wall stock solution is obtained by following steps:
Step 1:
A, the Radix Apioris Fortunei (Radix Lespedezae Buergeri) sorting of fresh harvesting are cleaned；
B, by clean Radix Apioris Fortunei (Radix Lespedezae Buergeri) spectrum sterilizing 5～10 minutes；
C, the Radix Apioris Fortunei (Radix Lespedezae Buergeri) after spectrum sterilizing is shredded, obtain cutting off thing, and be placed under spectrum sterilized environment stand-by；
Step 2:
A, the green tea sorting of fresh harvesting are cleaned；
B, by clean green tea spectrum sterilizing 5～10 minutes；
C, the green tea after spectrum sterilizing is shredded, obtain cutting off thing, and be placed under spectrum sterilized environment stand-by；
Step 3:
It is broken that a, sterilization step 1 and step 2 obtained cut-out thing and Radix Notoginseng carry out wall-broken micro powder in gnotobasis；
B, interpolation ultra-pure water, make the weight ratio≤1:1.3 of medicine total amount and water；
C, to carry out wall-broken micro powder broken, produces mixing breaking cellular wall stock solution at temperature is for-1.9～-2.1 DEG C, and cell-wall breaking ratio is
More than 98.5%；
D, the mixing breaking cellular wall stock solution produced first is sterilized with spectrum, then preserve at gnotobasis ,-2 DEG C～0 DEG C.
The consumption of described sodium hydroxide is that the consumption of Oleum Cocois, Petiolus Trachycarpi oil, olive oil and Semen pruni armeniacae oil is multiplied by respective soap
Change value sum, it may be assumed that m (NaOH)=m (Oleum Cocois) * Cortex cocois radicis oil saponification value+m (Petiolus Trachycarpi oil) * palmitic saponification number+m (Fructus Canarii albi
Oil) * Fructus Canarii albi oil saponification value+m (Semen pruni armeniacae oil) * Semen pruni armeniacae oil saponification value.
Compared with prior art, it is an advantage of the current invention that: the present invention with the addition of Radix Apioris Fortunei (Radix Lespedezae Buergeri) mixing breaking cellular wall in soap formula
Stock solution, this Radix Apioris Fortunei (Radix Lespedezae Buergeri) mixing breaking cellular wall stock solution uses spectrum sterilization, the ultralow fine preparation method of constant temperature vibration Wet-type wall-breaking to obtain
, in temperature for producing mixing breaking cellular wall stock solution at-2 ± 0.1 DEG C ,-2 DEG C～0 DEG C of cryopreservation, cell-wall breaking ratio reach 98.5% with
On, it is sufficiently reserved its bioactive ingredients, has dashed forward simultaneously for being that one is technical for single Chinese herbal medicine grinding mode
Broken, improve the utilization rate of medical material, add its added value；The present invention also with the addition of natural oil in the formula of soap, reduces
While the addition of glycerol, moisturizing effect also can reach best；The present invention adds Radix Apioris Fortunei (Radix Lespedezae Buergeri) mixing breaking cellular wall during preparing soap
During stock solution, it is after saponification is complete, when 60 DEG C～70 DEG C, soap lye is stirred with mixing breaking cellular wall stock solution Quick uniform, in alkalescence
Quickly add time minimum and be sufficiently reserved its biological activity；It addition, added with the form of stock solution by Radix Apioris Fortunei (Radix Lespedezae Buergeri), Radix Apioris Fortunei (Radix Lespedezae Buergeri) can be made to discharge
Efficiency increases substantially, and the consume of medical material is also down to minimum, and for comparing traditional handicraft, the highest saving 70%, it is full and uniform
Incorporate in soap, preferably play drug effect.
Detailed description of the invention
Below in conjunction with embodiment, the present invention is described in further detail.
Embodiment 1:
The Radix Apioris Fortunei (Radix Lespedezae Buergeri) soap of the present embodiment includes following components by weight:
Radix Apioris Fortunei (Radix Lespedezae Buergeri) mixing breaking cellular wall stock solution 11.5 parts, Oleum Cocois 10 parts, Petiolus Trachycarpi oil 20 parts, 10 parts of olive oil, Semen pruni armeniacae oil 12
Part, 10.46 parts of water, sucrose 10 parts, sodium hydroxide 7 parts, glycerol 8 parts, edible essence 1 part, EDETATE SODIUM 0.03 part and fourth hydroxyl
Toluene 0.01 part.
Above-mentioned Radix Apioris Fortunei (Radix Lespedezae Buergeri) mixing breaking cellular wall stock solution includes Radix Apioris Fortunei (Radix Lespedezae Buergeri) 10 parts, green tea 0.9 part, Radix Notoginseng 0.6 part and ultra-pure water, its
In, Radix Apioris Fortunei (Radix Lespedezae Buergeri), green tea, the gross weight of Radix Notoginseng and the weight ratio of ultra-pure water are 1:1.3.
Above-mentioned Radix Apioris Fortunei (Radix Lespedezae Buergeri) mixing breaking cellular wall stock solution is obtained by following steps:
Step 1:
A, the Radix Apioris Fortunei (Radix Lespedezae Buergeri) sorting of fresh harvesting are cleaned；
B, by clean Radix Apioris Fortunei (Radix Lespedezae Buergeri) spectrum sterilizing 5 minutes；
C, the Radix Apioris Fortunei (Radix Lespedezae Buergeri) after spectrum sterilizing is shredded, obtain cutting off thing, and be placed under spectrum sterilized environment stand-by；
Step 2:
A, the green tea sorting of fresh harvesting are cleaned；
B, by clean green tea spectrum sterilizing 5 minutes；
C, the green tea after spectrum sterilizing is shredded, obtain cutting off thing, and be placed under spectrum sterilized environment stand-by；
Step 3:
It is wet that a, sterilization step 1 and step 2 obtained cut-out thing and Radix Notoginseng carry out ultralow constant temperature vibration in gnotobasis
Formula wall-broken micro powder is broken；
B, interpolation ultra-pure water, making medicine total amount is 1:1.3 with the weight ratio of water
C, to carry out wall-broken micro powder broken, produces mixing breaking cellular wall stock solution at temperature is for-1.9～-2.1 DEG C, and cell-wall breaking ratio is
More than 98.5%；
D, the mixing breaking cellular wall stock solution produced first is sterilized with spectrum, then preserve at gnotobasis ,-2 DEG C～0 DEG C.
The preparation method of the present embodiment Radix Apioris Fortunei (Radix Lespedezae Buergeri) comprises the following steps:
Step one:
Taking appropriate sodium hydroxide to be slowly added in water, limit bevelling stirs 3 minutes, obtains sodium hydroxide solution, and controls temperature
Degree is at 40 DEG C；
Step 2:
Oleum Cocois, Petiolus Trachycarpi oil, olive oil and Semen pruni armeniacae oil are pressed formula proportion mix and blend, keep pressure-
0.5MPa～-0.1Mpa, mixing speed is 3000 turns per minute, stirs and maintain the temperature at 60 DEG C；By hydroxide
Sodium solution and sucrose are slowly added in above-mentioned fluid, stir until soap lye becomes the pasty state of thickness；Continuously add corresponding proportion
Glycerol, EDETATE SODIUM, butylated hydroxytoluene, stir, temperature is still maintained at 60 DEG C and carries out saponification；
Step 3:
Adding edible essence, Radix Apioris Fortunei (Radix Lespedezae Buergeri) mixing breaking cellular wall stock solution in saponification completely mixed solution, Quick uniform stirs, stirs
The time of mixing be 1 point 45 seconds, after stirring, soap lye is injected evacuation in mould, cooling, chilling temperature is 0～5 DEG C, during cooling
Between be 10 minutes, i.e. obtain Radix Apioris Fortunei (Radix Lespedezae Buergeri) soap after being cooled to solidification, then stripping and slicing, mark, pack, inspect shipment by random samples.
Embodiment 2:
The Radix Apioris Fortunei (Radix Lespedezae Buergeri) soap of the present embodiment includes following components by weight:
Radix Apioris Fortunei (Radix Lespedezae Buergeri) mixing breaking cellular wall stock solution 4.4 parts, Oleum Cocois 5 parts, Petiolus Trachycarpi oil 10 parts, 5 parts of olive oil, Semen pruni armeniacae oil 6 parts, water
5.5 parts, sucrose 5 parts, sodium hydroxide 3 parts, glycerol 4 parts, edible essence 0.1 part, EDETATE SODIUM 0.005 part and butylated hydroxytoluene
0.005 part.
Above-mentioned Radix Apioris Fortunei (Radix Lespedezae Buergeri) mixing breaking cellular wall stock solution includes Radix Apioris Fortunei (Radix Lespedezae Buergeri) 3 parts, green tea 0.3 part, Radix Notoginseng 0.1 part and ultra-pure water, its
In, Radix Apioris Fortunei (Radix Lespedezae Buergeri), green tea, the gross weight of Radix Notoginseng and the weight ratio of ultra-pure water are 1:1.3.
Above-mentioned Radix Apioris Fortunei (Radix Lespedezae Buergeri) mixing breaking cellular wall stock solution is obtained by following steps:
Step 1:
A, the Radix Apioris Fortunei (Radix Lespedezae Buergeri) sorting of fresh harvesting are cleaned；
B, by clean Radix Apioris Fortunei (Radix Lespedezae Buergeri) spectrum sterilizing 10 minutes；
C, the Radix Apioris Fortunei (Radix Lespedezae Buergeri) after spectrum sterilizing is shredded, obtain cutting off thing, and be placed under spectrum sterilized environment stand-by；
Step 2:
A, the green tea sorting of fresh harvesting are cleaned；
B, by clean green tea spectrum sterilizing 10 minutes；
C, the green tea after spectrum sterilizing is shredded, obtain cutting off thing, and be placed under spectrum sterilized environment stand-by；
Step 3:
It is wet that a, sterilization step 1 and step 2 obtained cut-out thing and Radix Notoginseng carry out ultralow constant temperature vibration in gnotobasis
Formula wall-broken micro powder is broken；
B, interpolation ultra-pure water, making medicine total amount is 1:1.3 with the weight ratio of water；
C, to carry out wall-broken micro powder broken, produces mixing breaking cellular wall stock solution at temperature is for-1.9～-2.1 DEG C, and cell-wall breaking ratio is
More than 98.5%；
D, the mixing breaking cellular wall stock solution produced first is sterilized with spectrum, then preserve at gnotobasis ,-2 DEG C～0 DEG C.
The preparation method of the present embodiment Radix Apioris Fortunei (Radix Lespedezae Buergeri) comprises the following steps:
Step one:
Taking appropriate sodium hydroxide to be slowly added in water, limit bevelling stirs 5 minutes, obtains sodium hydroxide solution, and controls temperature
Degree is at 50 DEG C；
Step 2:
Oleum Cocois, Petiolus Trachycarpi oil, olive oil and Semen pruni armeniacae oil are pressed formula proportion mix and blend, keep pressure-
0.5MPa～-0.1Mpa, mixing speed is 4000 turns per minute, stirs and maintain the temperature at 70 DEG C；By hydroxide
Sodium solution and sucrose are slowly added in above-mentioned fluid, stir until soap lye becomes the pasty state of thickness；Continuously add corresponding proportion
Glycerol, EDETATE SODIUM, butylated hydroxytoluene, stir, temperature is still maintained at 70 DEG C and carries out saponification；
Step 3:
Adding edible essence, Radix Apioris Fortunei (Radix Lespedezae Buergeri) mixing breaking cellular wall stock solution in saponification completely mixed solution, Quick uniform stirs, stirs
The time of mixing be 1 point 45 seconds, after stirring, soap lye is injected evacuation in mould, cooling, chilling temperature is 0～5 DEG C, during cooling
Between be 10 minutes, i.e. obtain Radix Apioris Fortunei (Radix Lespedezae Buergeri) soap after being cooled to solidification, then stripping and slicing, mark, pack, inspect shipment by random samples.
Embodiment 3:
The Radix Apioris Fortunei (Radix Lespedezae Buergeri) soap of the present embodiment includes following components by weight:
Radix Apioris Fortunei (Radix Lespedezae Buergeri) mixing breaking cellular wall stock solution 17.8 parts, Oleum Cocois 15 parts, Petiolus Trachycarpi oil 25 parts, 15 parts of olive oil, Semen pruni armeniacae oil 18
Part, 15.5 parts of water, sucrose 15 parts, sodium hydroxide 17 parts, glycerol 12 parts, edible essence 3 parts, EDETATE SODIUM 0.3 part and fourth hydroxyl
Toluene 0.3 part.
Above-mentioned Radix Apioris Fortunei (Radix Lespedezae Buergeri) mixing breaking cellular wall stock solution includes Radix Apioris Fortunei (Radix Lespedezae Buergeri) 15 parts, green tea 2 parts, Radix Notoginseng 0.8 part and ultra-pure water, its
In, Radix Apioris Fortunei (Radix Lespedezae Buergeri), green tea, the gross weight of Radix Notoginseng and the weight ratio of ultra-pure water are 1:1.4.
Above-mentioned Radix Apioris Fortunei (Radix Lespedezae Buergeri) mixing breaking cellular wall stock solution is obtained by following steps:
Step 1:
A, the Radix Apioris Fortunei (Radix Lespedezae Buergeri) sorting of fresh harvesting are cleaned；
B, by clean Radix Apioris Fortunei (Radix Lespedezae Buergeri) spectrum sterilizing 10 minutes；
C, the Radix Apioris Fortunei (Radix Lespedezae Buergeri) after spectrum sterilizing is shredded, obtain cutting off thing, and be placed under spectrum sterilized environment stand-by；
Step 2:
A, the green tea sorting of fresh harvesting are cleaned；
B, by clean green tea spectrum sterilizing 8 minutes；
C, the green tea after spectrum sterilizing is shredded, obtain cutting off thing, and be placed under spectrum sterilized environment stand-by；
Step 3:
It is wet that a, sterilization step 1 and step 2 obtained cut-out thing and Radix Notoginseng carry out ultralow constant temperature vibration in gnotobasis
Formula wall-broken micro powder is broken；
B, interpolation ultra-pure water, making medicine total amount is 1:1.4 with the weight ratio of water；
C, to carry out wall-broken micro powder broken, produces mixing breaking cellular wall stock solution at temperature is for-1.9～-2.1 DEG C, and cell-wall breaking ratio is
More than 98.5%；
D, the mixing breaking cellular wall stock solution produced first is sterilized with spectrum, then preserve at gnotobasis ,-2 DEG C～0 DEG C.
The preparation method of the present embodiment Radix Apioris Fortunei (Radix Lespedezae Buergeri) comprises the following steps:
Step one:
Taking appropriate sodium hydroxide to be slowly added in water, limit bevelling stirs 4 minutes, obtains sodium hydroxide solution, and controls temperature
Degree is at 45 DEG C；
Step 2:
Oleum Cocois, Petiolus Trachycarpi oil, olive oil and Semen pruni armeniacae oil are pressed formula proportion mix and blend, keep pressure-
0.5MPa～-0.1Mpa, mixing speed is 3500 turns per minute, stirs and maintain the temperature at 65 DEG C；By hydroxide
Sodium solution and sucrose are slowly added in above-mentioned fluid, stir until soap lye becomes the pasty state of thickness；Continuously add corresponding proportion
Glycerol, EDETATE SODIUM, butylated hydroxytoluene, stir, temperature maintains 70 DEG C and carries out saponification；
Step 3:
Adding edible essence, Radix Apioris Fortunei (Radix Lespedezae Buergeri) mixing breaking cellular wall stock solution in saponification completely mixed solution, Quick uniform stirs, stirs
The time of mixing be 1 point 45 seconds, after stirring, soap lye is injected evacuation in mould, cooling, chilling temperature is 0～5 DEG C, during cooling
Between be 10 minutes, i.e. obtain Radix Apioris Fortunei (Radix Lespedezae Buergeri) soap after being cooled to solidification, then stripping and slicing, mark, pack, inspect shipment by random samples.
Embodiment 4:
The Radix Apioris Fortunei (Radix Lespedezae Buergeri) soap of the present embodiment includes following components by weight:
Radix Apioris Fortunei (Radix Lespedezae Buergeri) mixing breaking cellular wall stock solution 7 parts, Oleum Cocois 8 parts, Petiolus Trachycarpi oil 15 parts, 8 parts of olive oil, Semen pruni armeniacae oil 9 parts, water 7
Part, sucrose 9 parts, sodium hydroxide 6 parts, glycerol 5 parts, edible essence 0.8 part, EDETATE SODIUM 0.01 part and butylated hydroxytoluene 0.005
Part.
Above-mentioned Radix Apioris Fortunei (Radix Lespedezae Buergeri) mixing breaking cellular wall stock solution includes Radix Apioris Fortunei (Radix Lespedezae Buergeri) 5.5 parts, green tea 1 part, Radix Notoginseng 0.5 part and ultra-pure water, its
In, Radix Apioris Fortunei (Radix Lespedezae Buergeri), green tea, the gross weight of Radix Notoginseng and the weight ratio of ultra-pure water are 1:1.5.
Above-mentioned Radix Apioris Fortunei (Radix Lespedezae Buergeri) mixing breaking cellular wall stock solution is obtained by following steps:
Step 1:
A, the Radix Apioris Fortunei (Radix Lespedezae Buergeri) sorting of fresh harvesting are cleaned；
B, by clean Radix Apioris Fortunei (Radix Lespedezae Buergeri) spectrum sterilizing 9 minutes；
C, the Radix Apioris Fortunei (Radix Lespedezae Buergeri) after spectrum sterilizing is shredded, obtain cutting off thing, and be placed under spectrum sterilized environment stand-by；
Step 2:
A, the green tea sorting of fresh harvesting are cleaned；
B, by clean green tea spectrum sterilizing 10 minutes；
C, the green tea after spectrum sterilizing is shredded, obtain cutting off thing, and be placed under spectrum sterilized environment stand-by；
Step 3:
It is wet that a, sterilization step 1 and step 2 obtained cut-out thing and Radix Notoginseng carry out ultralow constant temperature vibration in gnotobasis
Formula wall-broken micro powder is broken；
B, interpolation ultra-pure water, making medicine total amount is 1:1.5 with the weight ratio of water；
C, to carry out wall-broken micro powder broken, produces mixing breaking cellular wall stock solution at temperature is for-1.9～-2.1 DEG C, and cell-wall breaking ratio is
More than 98.5%；
D, the mixing breaking cellular wall stock solution produced first is sterilized with spectrum, then preserve at gnotobasis ,-2 DEG C～0 DEG C.
The preparation method of the present embodiment Radix Apioris Fortunei (Radix Lespedezae Buergeri) comprises the following steps:
Step one:
Taking appropriate sodium hydroxide to be slowly added in water, limit bevelling stirs 5 minutes, obtains sodium hydroxide solution, and controls temperature
Degree is at 50 DEG C；
Step 2:
Oleum Cocois, Petiolus Trachycarpi oil, olive oil and Semen pruni armeniacae oil are pressed formula proportion mix and blend, keep pressure-
0.5MPa～-0.1Mpa, mixing speed is 3800 turns per minute, stirs and maintain the temperature at 70 DEG C；By hydroxide
Sodium solution and sucrose are slowly added in above-mentioned fluid, stir until soap lye becomes the pasty state of thickness；Continuously add corresponding proportion
Glycerol, EDETATE SODIUM, butylated hydroxytoluene, stir, temperature is still maintained at 70 DEG C and carries out saponification；
Step 3:
Adding edible essence, Radix Apioris Fortunei (Radix Lespedezae Buergeri) mixing breaking cellular wall stock solution in saponification completely mixed solution, Quick uniform stirs, stirs
The time of mixing be 1 point 45 seconds, after stirring, soap lye is injected evacuation in mould, cooling, chilling temperature is 0～5 DEG C, during cooling
Between be 10 minutes, i.e. obtain Radix Apioris Fortunei (Radix Lespedezae Buergeri) soap after being cooled to solidification, then stripping and slicing, mark, pack, inspect shipment by random samples.
The present embodiment Radix Apioris Fortunei (Radix Lespedezae Buergeri) mixing breaking cellular wall stock solution to using the inventive method the to prepare minimum inhibitory concentration to antibacterial
Being detected, detailed process is:
By fluid medium and centrifuge tube in 121 DEG C of sterilizing 20min, after cooling, each in test tube add 0.5mL liquid culture
Base, according to doubling dilution, Radix Apioris Fortunei (Radix Lespedezae Buergeri) mixing breaking cellular wall stock solution doubling dilution joins 1.5mg/mL, 1mg/mL, 0.75mg/mL,
0.5mg/mL, 0.25mg/mL and 0.125mg/mL.Often the corresponding test organisms 0.1mL of each addition in group test tube, shakes up.Test tube is put
In 37 DEG C of constant incubators, cultivate 24h, observe bacterial growth situation.
Result:
Table 1 Radix Apioris Fortunei (Radix Lespedezae Buergeri) mixing breaking cellular wall stock solution is to antibacterial minimum inhibitory concentration (mg/ml)
Note: (A) aerobic conditions.
As shown in Table 1, the Radix Apioris Fortunei (Radix Lespedezae Buergeri) mixing breaking cellular wall that in the present invention, the ultralow constant temperature vibration broken mode of formula wall-broken micro powder obtains is former
Liquid is strong for the inhibitory action of the harmful bacterias such as staphylococcus aureus, escherichia coli, salmonella.Illustrate by super in the present invention
Radix Apioris Fortunei (Radix Lespedezae Buergeri) that the low constant temperature vibration broken mode of formula wall-broken micro powder obtains, Radix Notoginseng, the green tea mixing effective dissolution rate of stock solution are high, drug effect
By force, the effect of bactericidal antiphlogistic is more preferably.
The Radix Apioris Fortunei (Radix Lespedezae Buergeri) mixing breaking cellular wall stock solution using the inventive method to prepare, Radix Apioris Fortunei (Radix Lespedezae Buergeri) soap xylol are also caused by the present embodiment
Mice auricle swelling impact is detected, and detailed process is:
Taking female rats 40, be randomly divided into 4 groups, often group 10, gives corresponding external dimethylbenzene in each treated animal auricle
Uniform application (consumption 0.1ml), to cause inflammatory reaction.It is blank group (water, 30ml/kg), SANYE after causing scorching latter 1 hour
Blue or green soap (1.38g/kg is equivalent to fresh medical material 0.135g/kg), Radix Apioris Fortunei (Radix Lespedezae Buergeri) vibration micropowder breaking cellular wall stock solution (0.12g/kg), SANYE
Auris dextra exterior feature smeared by blue or green micropowder breaking cellular wall stock solution (0.14g/kg) that rotates.Mice takes off after smearing 1 hour cervical vertebra put to death, by ear right, left
Exterior feature is cut, and makes round auricle (diameter 9mm), and analytical balance is weighed, every animal auricle weight difference right, left, i.e. reflection inflammation swells
Swollen degree.Between many groups, mean compares employing variance analysis, and all data process with by SPSS17.0 statistical software.
Result:
Table 2 Radix Apioris Fortunei (Radix Lespedezae Buergeri) mixing breaking cellular wall stock solution xylol causes the impact of mice auricle swelling
As shown in Table 2, in the Radix Apioris Fortunei (Radix Lespedezae Buergeri) soap of the present invention and the present invention, the ultralow constant temperature vibration broken mode of formula wall-broken micro powder obtains
Radix Apioris Fortunei (Radix Lespedezae Buergeri) mixing breaking cellular wall stock solution suppression ratio is higher, illustrates that breaking cellular wall stock solution fully incorporates in soap, and detumescence effect is more preferable.
Claims (10)
1. a Radix Apioris Fortunei (Radix Lespedezae Buergeri) soap, it is characterised in that include following components by weight:
Radix Apioris Fortunei (Radix Lespedezae Buergeri) mixing breaking cellular wall stock solution 3.4～17.8 parts, Oleum Cocois 5～15 parts, Petiolus Trachycarpi oil 10～25 parts, olive oil 5～15 parts,
Semen pruni armeniacae oil 6～18 parts, water 5.5～15.5 parts, sucrose 5～15 parts, sodium hydroxide 3～17 parts, glycerol 4～12 parts, edible perfume
Essence 0.1～3 part, EDETATE SODIUM 0.005～0.3 part and butylated hydroxytoluene 0.005～0.3 part.
Radix Apioris Fortunei (Radix Lespedezae Buergeri) soap the most according to claim 1, it is characterised in that include following components by weight:
Radix Apioris Fortunei (Radix Lespedezae Buergeri) mixing breaking cellular wall stock solution 7～16 parts, Oleum Cocois 8～12 parts, Petiolus Trachycarpi oil 15～20 parts, olive oil 8～11 parts, sweet Fructus Pruni
Core oil 9～12 parts, water 7～13 parts, sucrose 9～12 parts, sodium hydroxide 6～12 parts, glycerol 5～10 parts, edible essence 0.8～2
Part, EDETATE SODIUM 0.01～0.1 part and butylated hydroxytoluene 0.005～0.1 part.
Radix Apioris Fortunei (Radix Lespedezae Buergeri) soap the most according to claim 2, it is characterised in that include following components by weight:
Radix Apioris Fortunei (Radix Lespedezae Buergeri) mixing breaking cellular wall stock solution 11.5 parts, Oleum Cocois 10 parts, Petiolus Trachycarpi oil 20 parts, 10 parts of olive oil, Semen pruni armeniacae oil 12 parts, water
10.46 parts, sucrose 10 parts, sodium hydroxide 7 parts, glycerol 8 parts, edible essence 1 part, EDETATE SODIUM 0.03 part and butylated hydroxytoluene
0.01 part.
Radix Apioris Fortunei (Radix Lespedezae Buergeri) soap the most according to claim 1, it is characterised in that: according to weight meter, described Radix Apioris Fortunei (Radix Lespedezae Buergeri) mixing breaking cellular wall is former
Liquid includes Radix Apioris Fortunei (Radix Lespedezae Buergeri) 3～15 parts, green tea 0.3～2 parts, Radix Notoginseng 0.1～0.8 part and ultra-pure water, described Radix Apioris Fortunei (Radix Lespedezae Buergeri), green tea,
The gross weight of Radix Notoginseng and the weight ratio≤1:1.3 of ultra-pure water.
Radix Apioris Fortunei (Radix Lespedezae Buergeri) soap the most according to claim 4, it is characterised in that: the usage amount of described Radix Apioris Fortunei (Radix Lespedezae Buergeri), green tea and Radix Notoginseng
It is respectively Radix Apioris Fortunei (Radix Lespedezae Buergeri) 10 parts, green tea 0.9 part, Radix Notoginseng 0.6 part.
Radix Apioris Fortunei (Radix Lespedezae Buergeri) soap the most according to claim 4, it is characterised in that: described Radix Apioris Fortunei (Radix Lespedezae Buergeri) mixing breaking cellular wall stock solution is by following steps
Obtain:
Step 1:
A, the Radix Apioris Fortunei (Radix Lespedezae Buergeri) sorting of fresh harvesting are cleaned；
B, by clean Radix Apioris Fortunei (Radix Lespedezae Buergeri) spectrum sterilizing 5～10 minutes；
C, the Radix Apioris Fortunei (Radix Lespedezae Buergeri) after spectrum sterilizing is shredded, obtain cutting off thing, and be placed under spectrum sterilized environment stand-by；
Step 2:
A, the green tea sorting of fresh harvesting are cleaned；
B, by clean green tea spectrum sterilizing 5～10 minutes；
C, the green tea after spectrum sterilizing is shredded, obtain cutting off thing, and be placed under spectrum sterilized environment stand-by；
Step 3:
It is broken that a, sterilization step 1 and step 2 obtained cut-out thing and Radix Notoginseng carry out wall-broken micro powder in gnotobasis；
B, interpolation ultra-pure water, make the weight ratio≤1:1.3 of medicine total amount and water；
C, to carry out wall-broken micro powder broken, produces mixing breaking cellular wall stock solution at temperature is for-1.9～-2.1 DEG C, and cell-wall breaking ratio is
More than 98.5%；
D, the mixing breaking cellular wall stock solution produced first is sterilized with spectrum, then preserve at gnotobasis ,-2 DEG C～0 DEG C.
7. the preparation method of a Radix Apioris Fortunei (Radix Lespedezae Buergeri) soap as claimed in claim 1, it is characterised in that comprise the following steps:
Step one:
Taking sodium hydroxide to be slowly added in water, limit bevelling stirs 3～5 minutes, obtains sodium hydroxide solution, and controls temperature 40
～50 DEG C；
Step 2:
Oleum Cocois, Petiolus Trachycarpi oil, olive oil and Semen pruni armeniacae oil are pressed formula proportion mix and blend, keep pressure-0.5MPa～-
0.1Mpa, stirs and maintains the temperature at 65 DEG C～75 DEG C；Sodium hydroxide solution and sucrose are slowly added to above-mentioned oil
In liquid, stir until soap lye becomes the pasty state of thickness；Continuously add the glycerol of corresponding proportion, EDETATE SODIUM, butylated hydroxytoluene, stir
Mixing uniformly, temperature is still maintained at 60 DEG C～70 DEG C and carries out saponification；
Step 3:
The Radix Apioris Fortunei (Radix Lespedezae Buergeri) mixing breaking cellular wall stock solution of corresponding proportion, edible essence, Quick uniform is added in saponification completely mixed solution
Stirring, after stirring, soap lye is injected evacuation in mould, cooling, chilling temperature is 0～5 DEG C, be cooled to solidification after and get final product
To described Radix Apioris Fortunei (Radix Lespedezae Buergeri) soap.
The preparation method of Radix Apioris Fortunei (Radix Lespedezae Buergeri) soap the most according to claim 7, it is characterised in that: according to weight meter, described Radix Apioris Fortunei (Radix Lespedezae Buergeri) mixes
Close breaking cellular wall stock solution and include Radix Apioris Fortunei (Radix Lespedezae Buergeri) 3～15 parts, green tea 0.3～2 parts, Radix Notoginseng 0.1～0.8 part and ultra-pure water, described Radix Apioris Fortunei (Radix Lespedezae Buergeri),
Green tea, the gross weight of Radix Notoginseng and the weight ratio≤1:1.3 of ultra-pure water.
The preparation method of Radix Apioris Fortunei (Radix Lespedezae Buergeri) soap the most according to claim 8, it is characterised in that described Radix Apioris Fortunei (Radix Lespedezae Buergeri) mixing breaking cellular wall stock solution by
Following steps obtain:
Step 1:
A, the Radix Apioris Fortunei (Radix Lespedezae Buergeri) sorting of fresh harvesting are cleaned；
B, by clean Radix Apioris Fortunei (Radix Lespedezae Buergeri) spectrum sterilizing 5～10 minutes；
C, the Radix Apioris Fortunei (Radix Lespedezae Buergeri) after spectrum sterilizing is shredded, obtain cutting off thing, and be placed under spectrum sterilized environment stand-by；
Step 2:
A, the green tea sorting of fresh harvesting are cleaned；
B, by clean green tea spectrum sterilizing 5～10 minutes；
C, the green tea after spectrum sterilizing is shredded, obtain cutting off thing, and be placed under spectrum sterilized environment stand-by；
Step 3:
It is broken that a, sterilization step 1 and step 2 obtained cut-out thing and Radix Notoginseng carry out wall-broken micro powder in gnotobasis；
B, interpolation ultra-pure water, make the weight ratio≤1:1.3 of medicine total amount and water；
C, to carry out wall-broken micro powder broken, produces mixing breaking cellular wall stock solution at temperature is for-1.9～-2.1 DEG C, and cell-wall breaking ratio is
More than 98.5%；
D, the mixing breaking cellular wall stock solution produced first is sterilized with spectrum, then preserve at gnotobasis ,-2 DEG C～0 DEG C.
The preparation method of Radix Apioris Fortunei (Radix Lespedezae Buergeri) soap the most according to claim 7, it is characterised in that: the consumption of described sodium hydroxide is coconut palm
The consumption of seed oil, Petiolus Trachycarpi oil, olive oil and Semen pruni armeniacae oil is multiplied by respective saponification number sum.
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Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN109044885A (en) * | 2018-08-10 | 2018-12-21 | 三明学院 | A kind of lipstick made from Chinese medicine and preparation method thereof improving effective component |
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| CN103948668A (en) * | 2014-03-20 | 2014-07-30 | 武义寿仙谷中药饮片有限公司 | Preparation method of radix tetrastigme powder |
| CN105002016A (en) * | 2015-06-29 | 2015-10-28 | 广西健宝石斛有限责任公司 | Production method of Dendrobium officinale polysaccharide handmade soap |
| CN105012551A (en) * | 2015-07-30 | 2015-11-04 | 浙江五养堂药业有限公司 | Ethanol extract of radix tetrastigmae leaves as well as preparation method and application of ethanol extract |
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| CN103948668A (en) * | 2014-03-20 | 2014-07-30 | 武义寿仙谷中药饮片有限公司 | Preparation method of radix tetrastigme powder |
| CN105002016A (en) * | 2015-06-29 | 2015-10-28 | 广西健宝石斛有限责任公司 | Production method of Dendrobium officinale polysaccharide handmade soap |
| CN105012551A (en) * | 2015-07-30 | 2015-11-04 | 浙江五养堂药业有限公司 | Ethanol extract of radix tetrastigmae leaves as well as preparation method and application of ethanol extract |
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| Publication number | Priority date | Publication date | Assignee | Title |
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| CN109044885A (en) * | 2018-08-10 | 2018-12-21 | 三明学院 | A kind of lipstick made from Chinese medicine and preparation method thereof improving effective component |
| CN109044885B (en) * | 2018-08-10 | 2021-07-23 | 三明学院 | Chinese herbal medicine lipstick capable of improving effective components and preparation method thereof |
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Application publication date: 20170104 |