CN106281344A - A kind of soil-repairing agent for eliminating noxious bacteria - Google Patents
A kind of soil-repairing agent for eliminating noxious bacteria Download PDFInfo
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- CN106281344A CN106281344A CN201610561697.9A CN201610561697A CN106281344A CN 106281344 A CN106281344 A CN 106281344A CN 201610561697 A CN201610561697 A CN 201610561697A CN 106281344 A CN106281344 A CN 106281344A
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09K—MATERIALS FOR MISCELLANEOUS APPLICATIONS, NOT PROVIDED FOR ELSEWHERE
- C09K17/00—Soil-conditioning materials or soil-stabilising materials
- C09K17/40—Soil-conditioning materials or soil-stabilising materials containing mixtures of inorganic and organic compounds
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- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N65/00—Biocides, pest repellants or attractants, or plant growth regulators containing material from algae, lichens, bryophyta, multi-cellular fungi or plants, or extracts thereof
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- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N65/00—Biocides, pest repellants or attractants, or plant growth regulators containing material from algae, lichens, bryophyta, multi-cellular fungi or plants, or extracts thereof
- A01N65/40—Liliopsida [monocotyledons]
- A01N65/42—Aloeaceae [Aloe family] or Liliaceae [Lily family], e.g. aloe, veratrum, onion, garlic or chives
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09K—MATERIALS FOR MISCELLANEOUS APPLICATIONS, NOT PROVIDED FOR ELSEWHERE
- C09K2101/00—Agricultural use
Abstract
The invention discloses a kind of soil-repairing agent for eliminating noxious bacteria, described renovation agent mainly includes following component: Radix Cissi Kerrii, Radix Seu Folium Ecdysantherae Roseae, Herba Chelidonii extract, Bulbus Allii extract, synergist, surfactant, organic solvent, emulsifying agent, surplus is water, the renovation agent of the present invention is with natural Chinese medicinal herb for Main Function composition, add the additive of multiple assosting effect, without any composition being difficult in soil and degrading, notable to the noxious bacteria repair effect in soil, after using, environment noresidue is polluted, vegetation in soil will not be produced untoward reaction, vegetation growth in soil also there is good antibacterial action simultaneously, there is fine application and popularization value.
Description
Technical field
The invention belongs to technical field of soil remediation, be specifically a kind of soil remediation for eliminating noxious bacteria
Agent.
Background technology
In recent years along with the deterioration of whole ecological environment, the biological pollution in soil is the most increasingly severe, but soil is
The primary growth source of human foods, the increase of its pollution level also can affect the quality of food significantly, and therefore soil is raw
It is one of emphasis of environment protection treating that thing pollutes, geobiont pollute refer to pathogen and in spite of illness etc. harmful organism population invade from the external world
Enter soil, destroy the balance of soil ecosystem, cause the phenomenon that soil quality declines.Harmful organism population source be with without
Sewage and the industrial wastewater that pathogen is contained in the human and animal excreta fertilising that processes, sanitary sewage, rubbish, hospital, and ill domestic animal corpse
Deal with improperly.By above-mentioned main path containing a large amount of infective bacterials, virus, worm's ovum band people's soil, cause plant
Various bacterial pathogen diseases, and then cause human body to suffer from various bacillary and viral disease, threaten human survival.
Infective bacterial and virus contaminated soil after even more serious to the harm of health.It is generally from feces and city
The malignant bacteria of sanitary sewage belongs to: Salmonella, Shigella, bacillus, Bacteroides, fusobacterium, false list
Born of the same parents' Bacillus, Bacterionema, Streptococcus, Mycobacterium etc..Additionally, with Excreta, secretions or its corpse of infected animal
Body enters soil and infects the pathogen also having the diseases such as anthrax, tetanus, malignant edema, erysipelas to human body.In soil
Have been found that kind more than 100 may cause the virus of human disease, such as poliovirus, people enterocyte pathological changes orphan sick
Poison, Coxsackie virus etc..The most it is a risk that infectious hepatitis virus.The plant virus of soil infection has tobacco mosaic disease
Poison, tobacco necrosis virus, wheat streak mosaic virus and Caulis et Folium Lactucae sativae large pluse virus etc..
Control currently for the physicochemical property repairing mainly change soil and the moisture condition of noxious bacteria in soil
The propagation of pathogenic microorganism, reinforcement ground mulching, to suppress airborne dust, cuts off the airborne spread approach of pathogenic bacterium, it is also possible to the most right
Soil pesticide sterilizing and virus killing, conventional sterilizing and virus killing, again can be multiple to bringing in soil while playing rehabilitating soil
Harmful chemical substance, destroys the growth of later stage vegetation, it is therefore desirable to a kind of soil-repairing agent taken as the leading factor with natural component,
The production of later stage vegetation can be promoted again while noxious bacteria in eliminating soil.
Summary of the invention
Present invention solves the technical problem that to be to provide a kind of bactericidal effect good, environment friendly and pollution-free with natural Chinese medicinal herb composition
It it is main soil-repairing agent.
Technical scheme is as follows:
A kind of soil-repairing agent for eliminating noxious bacteria, described soil-repairing agent mainly includes following weight group
Part: Radix Cissi Kerrii 5-15%, Radix Seu Folium Ecdysantherae Roseae 4-8%, Herba Chelidonii 3-6%, Bulbus Allii extract 2-5%, synergist 3-5%, surface
Activating agent 1.5-3.5%, organic solvent 5-15%, emulsifying agent 5-10%, surplus are water.
Further, described Bulbus Allii extract is allicin, and its preparation method is: after unerupted tooth garlic peeling
Smash to pieces, be subsequently adding the ethanol solution that mass concentration is 55-65% of Bulbus Allii quality 4-6 times amount, use ultrasonic extraction 10-
15min, Extracting temperature 35-45 DEG C, after filtration, concentrating under reduced pressure reclaims ethanol, obtains garlic extract, is then loaded by extracting solution
Carrying out cold drying in distillator under vacuum, described distillator refers to continuous vacuum distilling apparatus, in reduced pressure
Under, can well reduce vapo(u)rizing temperature and improve separation efficiency, enable allicin degree of depth in extracting solution to purify, work as pressure
Being reduced to the vapour pressure of compound, compound begins to boiling, and distillation just can be carried out, and promotes to decompose, and baking temperature is 40
± 2 DEG C, drying time is 5-8h, and to moisture content≤3% measured, the yellow oily liquid obtained is allicin, and Bulbus Allii is peppery
Element has streptococcus and belongs to the antibacterial actions such as bacterium, Cryptococcus bacterium and Trichophyton mentagrophytes, can do the renovation agent of plant.
Further, described synergist specifically include that Octacide 264 5-10 part, calcium superphosphate 4-6 part, potassium nitrate 1-3 part,
Poly-propionic acid amide. 1-2 part, polypeptide liquid 20-40 part, its preparation method is: the polypeptide liquid of described composition by weight is added in reactor and adds
Heat to 50-55 DEG C, adds calcium superphosphate, stirs, fully dissolve, be warmed up to 80-85 DEG C, adds nitric acid under stirring
Potassium, poly-propionic acid amide., cool 35-45 DEG C, add Octacide 264, stir, and is cooled to room temperature, stirs 30 minutes, i.e.
Obtaining described synergist, described synergist purity is high, effective, and decomposable asymmetric choice net residual pesticide, nitrate, agricultural chemicals change
Kind soil environment, purifies and rehabilitating soil, strengthens the soil-repairing agent killing effect to noxious bacteria, improves soil ecology ring
Border, decomposes organic matter and improves soil organic matter content, abolish and harden, improve physico shape, culture fertility, makes thin field become fertile
Soil, improves the sustainable production capacity of soil.
Further, described surfactant is natural coconut oil fatty alcohol-ether sodium sulfate, fatty alcohol ether sulfosuccinic
Acid esters sodium, polyoxyethylene lauryl ether one or several mixture therein.
Further, described organic solvent is ethanol, methanol, acetone one or several mixture therein.
Further, described emulsifying agent is calcium dodecyl benzene sulfonate, styrylphenol polyoxyethylene ether, nonyl phenol
Polyoxyethylene ether, aliphatic acid polyethenoxy base ester one or several mixture therein.
A kind of soil-repairing agent for eliminating noxious bacteria, preparation method is:
(1) Chinese herbal medicine effective ingredients extracts: according to described part by weight by Radix Cissi Kerrii, Radix Seu Folium Ecdysantherae Roseae, Herba Chelidonii mixing
Rear pulverizing, adds the water of 8-12 times amount, is heated to 100 DEG C and decocts 2 hours, filters after extracting decoction liquor, and filtering residue is according still further to above-mentioned
Operation is extracted 2 times, is then combined with the extracting solution of 3 times, is d=1.05-by extracting solution concentrating under reduced pressure transpiring moisture to proportion
The extractum of 1.15, uses spray drying tower to carry out spray drying and makes extract powder, cross 100 mesh sieves, and the three kinds of Chinese herbal medicine obtained carry
Take the effective ingredient mixture of thing;
(2) by the polypeptide liquid addition reactor of described composition by weight is heated to 50-55 DEG C, calcium superphosphate, stirring are added
Uniformly, fully dissolving, be warmed up to 80-85 DEG C, add potassium nitrate, poly-propionic acid amide. under stirring, cool 35-45
DEG C, add Octacide 264, stir, be cooled to room temperature, stir 30 minutes, i.e. obtain described synergist;
(3) prepared by soil-repairing agent: the Chinese herbal medicine extract (1) prepared mixes with the Bulbus Allii extract of described part by weight
Close, add the organic solvent of described part by weight, be heated to 60-80 DEG C, fully dissolve, obtain lysate after filtration, add
The synergist of described part by weight, surfactant, emulsifying agent, by lysate water preparation, i.e. obtain described harmful for eliminating
The soil-repairing agent of antibacterial.
The soil-repairing agent using method of the present invention is: broken up by soil loose with rotary cultivator, first sprinkles water to soil so that it is
Humidity is maintained at 50-70%, and it is 30-50ppm that crude drug composition is diluted with water to activity component concentration, is uniformly sprayed at soil
Surface, i.e. can reach soil remediation effect after 20 days.
Compared with prior art, the soil-repairing agent advantage of the present invention is with natural Chinese medicinal herb for Main Function composition, adds
Enter the additive of multiple assosting effect, without any composition being difficult in soil and degrading, to the noxious bacteria reparation in soil
Action effect is notable, and light stability improves, the lasting period is suitable, it is possible to reduce dispenser frequency and cost accounting, to environment after using
Noresidue is polluted, and the vegetation in soil will not be produced untoward reaction, also has the vegetation growth in soil the most anti-simultaneously
Bacterium effect, has fine application and popularization value.
Detailed description of the invention
Embodiment 1:
A kind of soil-repairing agent for eliminating noxious bacteria, described soil-repairing agent mainly includes following weight group
Part: Radix Cissi Kerrii 5%, Radix Seu Folium Ecdysantherae Roseae 4%, Herba Chelidonii 3%, Bulbus Allii extract 2%, synergist 3%, surfactant 1.5%,
Organic solvent 5%, emulsifying agent 5%, surplus are water.
Wherein, described Bulbus Allii extract is allicin, and its preparation method is: smash after unerupted tooth garlic peeling
Broken, it is subsequently adding the ethanol solution that mass concentration is 55% of Bulbus Allii quality 4 times amount, uses ultrasonic extraction 10min, extract temperature
Spending 35 DEG C, after filtration, concentrating under reduced pressure reclaims ethanol, obtains garlic extract, is then loaded by extracting solution in distillator at vacuum bar
Carrying out cold drying under part, described distillator refers to continuous vacuum distilling apparatus, at reduced pressure conditions, can well reduce steaming
Evaporate temperature and improve separation efficiency, enabling allicin degree of depth in extracting solution to purify, when pressure is reduced to the steaming of compound
Vapour pressure, compound begins to boiling, and distillation just can be carried out, and promotes to decompose, and baking temperature is 38 DEG C, and drying time is 5h,
To moisture content≤3% measured, the yellow oily liquid obtained is allicin, and allicin has streptococcus and belongs to bacterium, hidden
The antibacterial actions such as Coccus bacterium and Trichophyton mentagrophytes, can do the renovation agent of plant.Described synergist specifically includes that Octacide 264 5
Part, calcium superphosphate 4 parts, potassium nitrate 1 part, poly-propionic acid amide. 1 part, polypeptide liquid 20 parts, its preparation method is: by described composition by weight
Polypeptide liquid addition reactor is heated to 50 DEG C, adds calcium superphosphate, stir, fully dissolve, be warmed up to 80 DEG C, in stirring
Add potassium nitrate, poly-propionic acid amide. under state, cool 35 DEG C, add Octacide 264, stir, be cooled to room temperature, stir
Mixing 30 minutes, i.e. obtain described synergist, described synergist purity is high, effective, decomposable asymmetric choice net residual pesticide, nitrate,
Agricultural chemicals improve soil environment, purify and rehabilitating soil, strengthen the soil-repairing agent killing effect to noxious bacteria, improve
Ecological environment of soil, decomposes organic matter and improves soil organic matter content, abolish and harden, improve physico shape, culture fertility, make
Thin field becomes fertile soil, improves the sustainable production capacity of soil.Described surfactant is natural coconut oil fatty alcohol ether sulphuric acid
Sodium.Described organic solvent is ethanol.Described emulsifying agent is calcium dodecyl benzene sulfonate.
A kind of soil-repairing agent for eliminating noxious bacteria, preparation method is:
(1) Chinese herbal medicine effective ingredients extracts: according to described part by weight by Radix Cissi Kerrii, Radix Seu Folium Ecdysantherae Roseae, Herba Chelidonii mixing
Rear pulverizing, adds the water of 8 times amount, is heated to 100 DEG C and decocts 2 hours, filters after extracting decoction liquor, and filtering residue is according still further to aforesaid operations
Extract 2 times, be then combined with the extracting solution of 3 times, be the extractum of d=1.05 by extracting solution concentrating under reduced pressure transpiring moisture to proportion,
Use spray drying tower to carry out spray drying and make extract powder, cross 100 mesh sieves, effective one-tenth of the three kinds of Chinese herbal medicine extracts obtained
Divide mixture;
(2) by being heated to 50 DEG C in the polypeptide liquid addition reactor of described composition by weight, adding calcium superphosphate, stirring is all
Even, fully dissolve, be warmed up to 80 DEG C, under stirring, add potassium nitrate, poly-propionic acid amide., cool 35 DEG C, add
Octacide 264, stirs, and is cooled to room temperature, stirs 30 minutes, i.e. obtains described synergist;
(3) prepared by soil-repairing agent: the Chinese herbal medicine extract (1) prepared mixes with the Bulbus Allii extract of described part by weight
Close, add the organic solvent of described part by weight, be heated to 60 DEG C, fully dissolve, after filtration, obtain lysate, add described
The synergist of part by weight, surfactant, emulsifying agent, by lysate water preparation, i.e. obtain described for eliminating noxious bacteria
Soil-repairing agent.
Embodiment 2:
A kind of soil-repairing agent for eliminating noxious bacteria, described soil-repairing agent mainly includes following weight group
Part: Radix Cissi Kerrii 10%, Radix Seu Folium Ecdysantherae Roseae 6%, Herba Chelidonii 4.5%, Bulbus Allii extract 3%, synergist 4%, surfactant
2.5%, organic solvent 10%, emulsifying agent 7.5%, surplus are water.
Wherein, described Bulbus Allii extract is allicin, and its preparation method is: smash after unerupted tooth garlic peeling
Broken, it is subsequently adding the ethanol solution that mass concentration is 60% of Bulbus Allii quality 5 times amount, uses ultrasonic extraction 12.5min, extract
Temperature 40 DEG C, after filtration, concentrating under reduced pressure reclaims ethanol, obtains garlic extract, then loads in distillator extracting solution in vacuum
Under the conditions of carry out cold drying, described distillator refers to continuous vacuum distilling apparatus, at reduced pressure conditions, can well reduce
Vapo(u)rizing temperature also improves separation efficiency, enables allicin degree of depth in extracting solution to purify, when pressure is reduced to compound
Vapour pressure, compound begins to boiling, and distillation just can be carried out, and promotes decomposition, and baking temperature is 40 DEG C, and drying time is
6.5h, to moisture content≤3% measured, the yellow oily liquid obtained is allicin, and allicin has streptococcus and belongs to
The antibacterial actions such as bacterium, Cryptococcus bacterium and Trichophyton mentagrophytes, can do the renovation agent of plant.Described synergist specifically includes that increasing
Effect amine 7.5 parts, calcium superphosphate 5 parts, potassium nitrate 2 parts, poly-propionic acid amide. 1.5 parts, polypeptide liquid 30 parts, its preparation method is: by described
The polypeptide liquid addition reactor of composition by weight is heated to 52.5 DEG C, adds calcium superphosphate, stir, fully dissolve, heat up
To 82.5 DEG C, adding potassium nitrate, poly-propionic acid amide., cool 40 DEG C under stirring, add Octacide 264, stirring is all
Even, it is cooled to room temperature, stirs 30 minutes, i.e. obtain described synergist, described synergist purity is high, effective, decomposable asymmetric choice net
Residual pesticide, nitrate, agricultural chemicals improve soil environment, purify and rehabilitating soil, strengthen soil-repairing agent to harmful thin
The killing effect of bacterium, improves ecological environment of soil, decomposes organic matter and improves soil organic matter content, abolish and harden, improves physics
Change shape, culture fertility, make thin field become fertile soil, improve the sustainable production capacity of soil.Described surfactant is fat
Alcohol ether sulfosuccinates sodium.Described organic solvent is methanol.Described emulsifying agent is styrylphenol polyoxyethylene ether.
A kind of soil-repairing agent for eliminating noxious bacteria, preparation method is:
(1) Chinese herbal medicine effective ingredients extracts: according to described part by weight by Radix Cissi Kerrii, Radix Seu Folium Ecdysantherae Roseae, Herba Chelidonii mixing
Rear pulverizing, adds the water of 10 times amount, is heated to 100 DEG C and decocts 2 hours, filters after extracting decoction liquor, and filtering residue is according still further to above-mentioned behaviour
Make to extract 2 times, be then combined with the extracting solution of 3 times, be the extractum of d=1.1 by extracting solution concentrating under reduced pressure transpiring moisture to proportion,
Use spray drying tower to carry out spray drying and make extract powder, cross 100 mesh sieves, effective one-tenth of the three kinds of Chinese herbal medicine extracts obtained
Divide mixture;
(2) by being heated to 52.5 DEG C in the polypeptide liquid addition reactor of described composition by weight, adding calcium superphosphate, stirring is all
Even, fully dissolve, be warmed up to 82.5 DEG C, under stirring, add potassium nitrate, poly-propionic acid amide., cool 40 DEG C, then add
Enter Octacide 264, stir, be cooled to room temperature, stir 30 minutes, i.e. obtain described synergist;
(3) prepared by soil-repairing agent: the Chinese herbal medicine extract (1) prepared mixes with the Bulbus Allii extract of described part by weight
Close, add the organic solvent of described part by weight, be heated to 70 DEG C, fully dissolve, after filtration, obtain lysate, add described
The synergist of part by weight, surfactant, emulsifying agent, by lysate water preparation, i.e. obtain described for eliminating noxious bacteria
Soil-repairing agent.
Embodiment 3:
A kind of soil-repairing agent for eliminating noxious bacteria, described soil-repairing agent mainly includes following weight group
Part: Radix Cissi Kerrii 15%, Radix Seu Folium Ecdysantherae Roseae 8%, Herba Chelidonii 6%, Bulbus Allii extract 5%, synergist 5%, surfactant
3.5%, organic solvent 15%, emulsifying agent 10%, surplus are water.
Wherein, described Bulbus Allii extract is allicin, and its preparation method is: smash after unerupted tooth garlic peeling
Broken, it is subsequently adding the ethanol solution that mass concentration is 65 of Bulbus Allii quality 6 times amount, uses ultrasonic extraction 15min, Extracting temperature
45 DEG C, after filtration, concentrating under reduced pressure reclaims ethanol, obtains garlic extract, then loads in distillator extracting solution at vacuum condition
Under carry out cold drying, described distillator refers to continuous vacuum distilling apparatus, at reduced pressure conditions, can well reduce distillation
Temperature also improves separation efficiency, enables allicin degree of depth in extracting solution to purify, when pressure is reduced to the steam of compound
Pressure, compound begins to boiling, and distillation just can be carried out, and promotes to decompose, and baking temperature is 42 DEG C, and drying time is 8h, extremely
Moisture content≤3% measured, the yellow oily liquid obtained is allicin, and allicin has streptococcus and belongs to bacterium, hidden ball
The antibacterial actions such as Pseudomonas bacterium and Trichophyton mentagrophytes, can do the renovation agent of plant.Described synergist specifically includes that Octacide 264 10
Part, calcium superphosphate 6 parts, potassium nitrate 3 parts, poly-propionic acid amide. 2 parts, polypeptide liquid 40 parts, its preparation method is: by described composition by weight
Polypeptide liquid addition reactor is heated to 55 DEG C, adds calcium superphosphate, stir, fully dissolve, be warmed up to 85 DEG C, in stirring
Add potassium nitrate, poly-propionic acid amide. under state, cool 45 DEG C, add Octacide 264, stir, be cooled to room temperature, stir
Mixing 30 minutes, i.e. obtain described synergist, described synergist purity is high, effective, decomposable asymmetric choice net residual pesticide, nitrate,
Agricultural chemicals improve soil environment, purify and rehabilitating soil, strengthen the soil-repairing agent killing effect to noxious bacteria, improve
Ecological environment of soil, decomposes organic matter and improves soil organic matter content, abolish and harden, improve physico shape, culture fertility, make
Thin field becomes fertile soil, improves the sustainable production capacity of soil.Described surfactant is polyoxyethylene lauryl ether.Described
Organic solvent is acetone.Described emulsifying agent is NPE.
A kind of soil-repairing agent for eliminating noxious bacteria, preparation method is:
(1) Chinese herbal medicine effective ingredients extracts: according to described part by weight by Radix Cissi Kerrii, Radix Seu Folium Ecdysantherae Roseae, Herba Chelidonii mixing
Rear pulverizing, adds the water of 12 times amount, is heated to 100 DEG C and decocts 2 hours, filters after extracting decoction liquor, and filtering residue is according still further to above-mentioned behaviour
Make to extract 2 times, be then combined with the extracting solution of 3 times, be the leaching of d=1.15 by extracting solution concentrating under reduced pressure transpiring moisture to proportion
Cream, uses spray drying tower to carry out spray drying and makes extract powder, cross 100 mesh sieves, having of the three kinds of Chinese herbal medicine extracts obtained
Effect constituents mixt;
(2) by being heated to 55 DEG C in the polypeptide liquid addition reactor of described composition by weight, adding calcium superphosphate, stirring is all
Even, fully dissolve, be warmed up to 85 DEG C, under stirring, add potassium nitrate, poly-propionic acid amide., cool 45 DEG C, add
Octacide 264, stirs, and is cooled to room temperature, stirs 30 minutes, i.e. obtains described synergist;
(3) prepared by soil-repairing agent: the Chinese herbal medicine extract (1) prepared mixes with the Bulbus Allii extract of described part by weight
Close, add the organic solvent of described part by weight, be heated to 80 DEG C, fully dissolve, after filtration, obtain lysate, add described
The synergist of part by weight, surfactant, emulsifying agent, by lysate water preparation, i.e. obtain described for eliminating noxious bacteria
Soil-repairing agent.
Concrete verification experimental verification:
1. experimental subject: take four pieces of experimental field of wheat containing noxious bacteria respectively, wherein comprises multiple pollution pathogenic bacteria, such as sand
Door Bordetella, Shigella, bacillus, Bacteroides, fusobacterium, pseudomonas, Bacterionema, streptococcus
Genus, Mycobacterium etc., be divided into three groups of experimental plots, one group of comparison field, often group area 16 square metres, noxious bacteria content and affiliated
Environment zero difference, has comparability.
2. experimental technique: use soil remediation prepared by embodiment 1, embodiment 2, embodiment 3 respectively to three groups of experimental plots
Agent, breaks up loose with rotary cultivator by soil, first sprinkles water to soil so that it is humidity is maintained at 50-70%, is added water by crude drug composition
Being diluted to activity component concentration is 30-50ppm, is uniformly sprayed at soil surface, carries out wheat planting after 20 days;Comparison field is not done
Any process, directly carries out wheat planting;All experimental plots wheat density and kind are identical without significant difference, observe all
The growing state of experimental plot Semen Tritici aestivi record.
3. experimental data statistics:
4. experimental result: as seen from the above table, soil-repairing agent prepared by embodiments of the invention is in crops field test
In, all show preferable repairing effect, the fast growth of plant compared with comparison field, and disease does not occurs, compare field
Owing to not doing any repair process so that it is plant growing rate is low, the speed of growth is slow, and occurs in that head blight, the therefore present invention
The soil-repairing agent effect of preparation is notable, has the biggest application and popularization value.
Last it is noted that above example is only in order to illustrate technical scheme, it is not intended to limit;Although
With reference to previous embodiment, the present invention is described in detail, it will be understood by those within the art that: it still may be used
So that the technical scheme described in previous embodiment to be modified, or wherein portion of techniques feature is carried out equivalent;And
These amendments or replacement, do not make the essence of appropriate technical solution depart from spirit and the model of embodiment of the present invention technical scheme
Enclose.
Claims (8)
1. one kind for eliminating the soil-repairing agent of noxious bacteria, it is characterised in that described soil-repairing agent mainly include with
Lower composition by weight: Radix Cissi Kerrii 5-15%, Radix Seu Folium Ecdysantherae Roseae 4-8%, Herba Chelidonii 3-6%, Bulbus Allii extract 2-5%, synergist 3-
5%, surfactant 1.5-3.5%, organic solvent 5-15%, emulsifying agent 5-10%, surplus are water.
A kind of soil-repairing agent for eliminating noxious bacteria, it is characterised in that described Bulbus Allii
Extract is allicin, and its preparation method is: smash to pieces after unerupted tooth garlic peeling, is subsequently adding Bulbus Allii quality 4-6 times
The ethanol solution that mass concentration is 55-65% of amount, uses ultrasonic extraction 10-15min, and Extracting temperature 35-45 DEG C, after filtration
Concentrating under reduced pressure reclaims ethanol, obtains garlic extract, is then loaded by extracting solution and carry out low temperature in distillator under vacuum
Being dried, baking temperature is 40 ± 2 DEG C, and drying time is 5-8h, to moisture content≤3% measured, the yellow oily liquid obtained
For allicin.
A kind of soil-repairing agent for eliminating noxious bacteria, it is characterised in that described potentiation
Agent specifically includes that Octacide 264 5-10 part, calcium superphosphate 4-6 part, potassium nitrate 1-3 part, poly-propionic acid amide. 1-2 part, polypeptide liquid 20-40
Part, its preparation method is: the polypeptide liquid of described composition by weight is added in reactor and is heated to 50-55 DEG C, adds calcium superphosphate,
Stirring, fully dissolve, be warmed up to 80-85 DEG C, add potassium nitrate, poly-propionic acid amide. under stirring, cool 35-
45 DEG C, add Octacide 264, stir, be cooled to room temperature, stir 30 minutes, i.e. obtain described synergist.
A kind of soil-repairing agent for eliminating noxious bacteria, it is characterised in that described surface
Activating agent be natural coconut oil fatty alcohol-ether sodium sulfate, fatty alcohol ether sulfosuccinate sodium, polyoxyethylene lauryl ether wherein
One or several mixture.
A kind of soil-repairing agent for eliminating noxious bacteria, it is characterised in that described is organic
Solvent is ethanol, methanol, acetone one or several mixture therein.
A kind of soil-repairing agent for eliminating noxious bacteria, it is characterised in that described emulsifying
Agent is calcium dodecyl benzene sulfonate, styrylphenol polyoxyethylene ether, NPE, aliphatic acid polyethenoxy base
Ester one or several mixture therein.
7. a kind of soil-repairing agent for eliminating noxious bacteria as described in claim 1-6 any one, it is characterised in that
Preparation method is:
(1) Chinese herbal medicine effective ingredients extracts: according to described part by weight by powder after Radix Cissi Kerrii, Radix Seu Folium Ecdysantherae Roseae, Herba Chelidonii mixing
Broken, add the water of 8-12 times amount, be heated to 100 DEG C and decoct 2 hours, filter after extracting decoction liquor, filtering residue is according still further to aforesaid operations
Extract 2 times, be then combined with the extracting solution of 3 times, be d=1.05-1.15's by extracting solution concentrating under reduced pressure transpiring moisture to proportion
Extractum, uses spray drying tower to carry out spray drying and makes extract powder, cross 100 mesh sieves, the three kinds of Chinese herbal medicine extracts obtained
Effective ingredient mixture;
(2) prepared by synergist: the polypeptide liquid of described composition by weight is added in reactor and is heated to 50-55 DEG C, adds peroxophosphoric acid
Calcium, stirs, and fully dissolves, and is warmed up to 80-85 DEG C, adds potassium nitrate, poly-propionic acid amide., cool under stirring
35-45 DEG C, add Octacide 264, stir, be cooled to room temperature, stir 30 minutes, i.e. obtain described synergist.
(3) prepared by soil-repairing agent: mixed with the Bulbus Allii extract of described part by weight by the Chinese herbal medicine extract that (1) prepares,
Add the organic solvent of described part by weight, be heated to 60-80 DEG C, fully dissolve, after filtration, obtain lysate, add described
The synergist of part by weight, surfactant, emulsifying agent, make water preparation by lysate, i.e. obtains described harmful for eliminating
The soil-repairing agent of antibacterial.
A kind of soil-repairing agent for eliminating noxious bacteria, it is characterised in that described soil
During renovation agent application, the activity component concentration being diluted with water to count with crude drug weight is as 30-50ppm.
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CN107197718A (en) * | 2017-06-28 | 2017-09-26 | 铜仁市绿缘生态农林发展有限公司 | A kind of pest control method of peach |
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CN105165491A (en) * | 2015-07-28 | 2015-12-23 | 魏琦 | Method for comprehensive control of papaya anthracnose |
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