CN107136133B - A kind of preparation method of aqua type plant electric mosquito repellent liquid - Google Patents
A kind of preparation method of aqua type plant electric mosquito repellent liquid Download PDFInfo
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- CN107136133B CN107136133B CN201710277164.2A CN201710277164A CN107136133B CN 107136133 B CN107136133 B CN 107136133B CN 201710277164 A CN201710277164 A CN 201710277164A CN 107136133 B CN107136133 B CN 107136133B
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- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N65/00—Biocides, pest repellants or attractants, or plant growth regulators containing material from algae, lichens, bryophyta, multi-cellular fungi or plants, or extracts thereof
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- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N25/00—Biocides, pest repellants or attractants, or plant growth regulators, characterised by their forms, or by their non-active ingredients or by their methods of application, e.g. seed treatment or sequential application; Substances for reducing the noxious effect of the active ingredients to organisms other than pests
- A01N25/18—Vapour or smoke emitting compositions with delayed or sustained release
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- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N53/00—Biocides, pest repellants or attractants, or plant growth regulators containing cyclopropane carboxylic acids or derivatives thereof
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- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N65/00—Biocides, pest repellants or attractants, or plant growth regulators containing material from algae, lichens, bryophyta, multi-cellular fungi or plants, or extracts thereof
- A01N65/40—Liliopsida [monocotyledons]
- A01N65/44—Poaceae or Gramineae [Grass family], e.g. bamboo, lemon grass or citronella grass
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- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02A—TECHNOLOGIES FOR ADAPTATION TO CLIMATE CHANGE
- Y02A50/00—TECHNOLOGIES FOR ADAPTATION TO CLIMATE CHANGE in human health protection, e.g. against extreme weather
- Y02A50/30—Against vector-borne diseases, e.g. mosquito-borne, fly-borne, tick-borne or waterborne diseases whose impact is exacerbated by climate change
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- Agronomy & Crop Science (AREA)
- Plant Pathology (AREA)
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- Wood Science & Technology (AREA)
- Pest Control & Pesticides (AREA)
- Natural Medicines & Medicinal Plants (AREA)
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Abstract
The invention discloses a kind of aqua type plant electric mosquito repellent liquids and preparation method thereof, this kind of aqua type plant electric mosquito repellent liquid is made of the raw material below according to mass percent: anophelifuge medicament 0.5 ~ 2.3%, plant extracts 12 ~ 28%, nonionic surfactant 3 ~ 9%, preservative 0.1 ~ 0.8%, ethyl alcohol 20 ~ 50%, surplus are deionized water；Plant extracts is made of following raw material according to parts by weight: 15 ~ 25 parts of lemon grass, 10 ~ 16 parts of Salvia japonica, 8 ~ 13 parts of wild chrysanthemum, 6 ~ 15 parts of aloe, 10 ~ 15 parts of yellow Teng's root, 1 ~ 5 part of tobacco, 18 ~ 26 parts of folium artemisiae argyi, 11 ~ 15 parts of cloves, 3 ~ 9 parts of peppermint, 10 ~ 15 parts of wrinkled giant hyssop, 1 ~ 4 part of radix gentianae.This kind of aqua type plant electric mosquito repellent liquid reduces production cost using deionized water as matrix, safe and non-toxic, the effect of bite by mosquitos can not only be prevented, viral germ is killed, be also equipped with certain tranquilizing the mind, sleeping, raw material is cheap and easy to get, preparation method is simple, is suitable for industrialized production.
Description
Technical field
The present invention relates to hygiene article sectors, and in particular to a kind of aqua type plant electric mosquito repellent liquid and preparation method thereof.
Background technique
Summer is mosquito activity period the most frequent, and people are often bitten by mosquito, allows people to be pestered beyond endurance, sternly
The normal life, work, study of people are affected again, and more seriously bite by mosquitos can also propagate various diseases, to people
Health bring serious threat.Mosquito-repellent incense flies into common people house, wherein electric heating mosquito as a kind of mosquito repellent articles already
The use of fragrant liquid is also more prevalent.Existing mosquito liquid mostly uses alkane solvents as carrier, and alkanes are molten when use
Agent evaporates into the air, spreads effective component as alkane solvent volatilizees, and generates drug effect, this kind of product to contact with target
We can be described as oil-based liquid mosquito-repellent incense, such electric mosquito repellent liquid production cost is higher, be used for a long time hidden in the presence of safety to human health
Suffer from, in addition, mosquito generates certain drug resistance to the effective component of mosquito-repellent incense with the long-time service of mosquito-repellent incense liquid, affects mosquito-repellent incense
The drug effect of liquid.And the present invention replaces partial solvent using water, so that production cost is decreased, in addition, matching using Chinese herbal medicine
Traditional anophelifuge medicament is closed as effective component, user will not be had adverse effect on while improving repelling effect.
Summary of the invention
It is an object of that present invention to provide a kind of aqua type plant electric mosquito repellent liquids and preparation method thereof, to solve in above-mentioned background
The problem of mentioning.
To achieve the above object, the invention provides the following technical scheme:
A kind of aqua type plant electric mosquito repellent liquid, is made of the raw material below according to mass percent: anophelifuge medicament 0.5 ~
2.3%, plant extracts 12 ~ 28%, nonionic surfactant 3 ~ 9%, preservative 0.1 ~ 0.8%, ethyl alcohol 20 ~ 50%, surplus is to go
Ionized water.
As a further solution of the present invention: the aqua type plant electric mosquito repellent liquid, by below according to mass percent
Raw material composition: anophelifuge medicament 1.6%, plant extracts 19%, nonionic surfactant 5%, preservative 0.3%, ethyl alcohol 35% are remaining
Amount is deionized water.
As a further solution of the present invention: the aqua type plant electric mosquito repellent liquid plant extracts is by below according to weight
The raw material of number forms: 15 ~ 25 parts of lemon grass, 10 ~ 16 parts of Salvia japonica, and 8 ~ 13 parts of wild chrysanthemum, 6 ~ 15 parts of aloe, yellow Teng's root 10
~ 15 parts, 1 ~ 5 part of tobacco, 18 ~ 26 parts of folium artemisiae argyi, 11 ~ 15 parts of cloves, 3 ~ 9 parts of peppermint, 10 ~ 15 parts of wrinkled giant hyssop, 1 ~ 4 part of radix gentianae.
As a further solution of the present invention: the aqua type plant electric mosquito repellent liquid plant extracts is by below according to weight
The raw material of number forms: 20 parts of lemon grass, 13 parts of Salvia japonica, and 9 parts of wild chrysanthemum, 8 parts of aloe, 14 parts of yellow Teng's root, 2 parts of tobacco,
22 parts of folium artemisiae argyi, 12 parts of cloves, 6 parts of peppermint, 11 parts of wrinkled giant hyssop, 2 parts of radix gentianae.
As a further solution of the present invention: the preparation method of the aqua type plant electric mosquito repellent liquid plant extracts includes
Following steps:
1) ingredient is carried out according to raw material composition and its parts by weight proportion；
2) it is uniformly mixed, obtains after respectively grinding Salvia japonica, wild chrysanthemum, yellow Teng's root, folium artemisiae argyi, cloves, radix gentianae
Mixture A is added to sealed soak 5h in ethyl alcohol, is ultrasonically treated 30min, obtains mixed solution B, will mix molten by mixture A
Liquid B carries out centrifugal treating and takes supernatant, and gained sediment is added centrifugal treating after ethyl alcohol carries out the processing of 20min twice ultrasonic and takes
Clear liquid merges supernatant twice and is concentrated to get concentrate C with Rotary Evaporators, is washed after dry with dehydrated alcohol, is dry
To mixture D；
3) lemon grass, aloe, tobacco, peppermint, wrinkled giant hyssop are distilled with steam method, obtains crystal, crushed 100 mesh
Sieve, obtains mixture E；
4) mixture D and mixture E are mixed, ethyl alcohol is added, stirs evenly, is sealed under the conditions of 0 ~ 5 DEG C of temperature.
As a further solution of the present invention: the aqua type plant electric mosquito repellent liquid anophelifuge medicament is dimefluthrin.
As a further solution of the present invention: the aqua type plant electric mosquito repellent liquid preservative is Kathon CG or Bu Luobo
You.
A kind of preparation method of aqua type plant electric mosquito repellent liquid the following steps are included:
1) anophelifuge medicament and nonionic surfactant are added in deionized water, are stirred under the conditions of 50 DEG C of temperature to complete
Fully dissolved is cooled to room temperature, and filters to take filtrate, obtains solution F；
2) plant extracts is added in deionized water, stirs to being completely dissolved, obtains solution G；
3) solution F, solution G are mixed and preservative is added while stirring, until preservative dissolves, obtain Solution H；
4) into Solution H be added ethyl alcohol to get.
Aqua type plant electric mosquito repellent liquid of the invention reduces production cost using deionized water as matrix, safe and non-toxic,
The effect of bite by mosquitos can not only be prevented, viral germ is killed, be also equipped with certain tranquilizing the mind, sleeping, raw material is cheap and easy to get, system
Preparation Method is simple, is suitable for industrialized production.
Specific embodiment
Below in conjunction with the embodiment of the present invention, technical scheme in the embodiment of the invention is clearly and completely described,
Obviously, described embodiments are only a part of the embodiments of the present invention, instead of all the embodiments.Based in the present invention
Embodiment, every other embodiment obtained by those of ordinary skill in the art without making creative efforts, all
Belong to the scope of protection of the invention.
Embodiment 1
In the embodiment of the present invention, a kind of aqua type plant electric mosquito repellent liquid is made of the raw material below according to mass percent:
Anophelifuge medicament 0.5%, plant extracts 12%, nonionic surfactant 3%, preservative 0.1%, ethyl alcohol 20%, surplus are deionization
Water.
Aqua type plant electric mosquito repellent liquid plant extracts is made of following raw material according to parts by weight: lemon grass 15
Part, 10 parts of Salvia japonica, 8 parts of wild chrysanthemum, 6 parts of aloe, 10 parts of yellow Teng's root, 1 part of tobacco, 18 parts of folium artemisiae argyi, 11 parts of cloves, 3 parts of peppermint,
10 parts of wrinkled giant hyssop, 1 part of radix gentianae.
The preparation method of aqua type plant electric mosquito repellent liquid plant extracts the following steps are included:
1) ingredient is carried out according to raw material composition and its parts by weight proportion；
2) it is uniformly mixed, obtains after respectively grinding Salvia japonica, wild chrysanthemum, yellow Teng's root, folium artemisiae argyi, cloves, radix gentianae
Mixture A is added to sealed soak 5h in ethyl alcohol, is ultrasonically treated 30min, obtains mixed solution B, will mix molten by mixture A
Liquid B carries out centrifugal treating and takes supernatant, and gained sediment is added centrifugal treating after ethyl alcohol carries out the processing of 20min twice ultrasonic and takes
Clear liquid merges supernatant twice and is concentrated to get concentrate C with Rotary Evaporators, is washed after dry with dehydrated alcohol, is dry
To mixture D；
3) lemon grass, aloe, tobacco, peppermint, wrinkled giant hyssop are distilled with steam method, obtains crystal, crushed 100 mesh
Sieve, obtains mixture E；
4) mixture D and mixture E are mixed, ethyl alcohol is added, stirs evenly, is sealed under the conditions of 0 ~ 5 DEG C of temperature.
The preparation method of aqua type plant electric mosquito repellent liquid the following steps are included:
1) anophelifuge medicament and nonionic surfactant are added in deionized water, are stirred under the conditions of 50 DEG C of temperature to complete
Fully dissolved is cooled to room temperature, and filters to take filtrate, obtains solution F；
2) plant extracts is added in deionized water, stirs to being completely dissolved, obtains solution G；
3) solution F, solution G are mixed and preservative is added while stirring, until preservative dissolves, obtain Solution H；
4) into Solution H be added ethyl alcohol to get.
Embodiment 2
In the embodiment of the present invention, a kind of aqua type plant electric mosquito repellent liquid is made of the raw material below according to mass percent:
Anophelifuge medicament 2.3%, plant extracts 28%, nonionic surfactant 9%, preservative 0.8%, ethyl alcohol 50%, surplus are deionization
Water.
Aqua type plant electric mosquito repellent liquid plant extracts is made of following raw material according to parts by weight: lemon grass 25
Part, 16 parts of Salvia japonica, 13 parts of wild chrysanthemum, 15 parts of aloe, 15 parts of yellow Teng's root, 5 parts of tobacco, 26 parts of folium artemisiae argyi, 15 parts of cloves, peppermint 9
Part, 15 parts of wrinkled giant hyssop, 4 parts of radix gentianae.
The preparation method is the same as that of Example 1.
Embodiment 3
In the embodiment of the present invention, a kind of aqua type plant electric mosquito repellent liquid is made of the raw material below according to mass percent:
Anophelifuge medicament 1.6%, plant extracts 19%, nonionic surfactant 5%, preservative 0.3%, ethyl alcohol 35%, surplus are deionization
Water.
Aqua type plant electric mosquito repellent liquid plant extracts is made of following raw material according to parts by weight: lemon grass 20
Part, 13 parts of Salvia japonica, 9 parts of wild chrysanthemum, 8 parts of aloe, 14 parts of yellow Teng's root, 2 parts of tobacco, 22 parts of folium artemisiae argyi, 12 parts of cloves, 6 parts of peppermint,
11 parts of wrinkled giant hyssop, 2 parts of radix gentianae.
The preparation method is the same as that of Example 1.
The method for examining above-mentioned aqua type plant electric mosquito repellent liquid is as follows.
Test 1: indoor harmacological effect
1) odor detection: faint scent has no irritating odor.
2) it Composition analyzed: is tested using GB 18418-2001 domestic sanitary desinsection articles electric liquid device standard.
In the standard, KT50 value (boxing method) ￡ 10 minutes as qualification, mosquito-repellent incense liquid indoor harmacological effect tables are shown in Table 1.
Table 1
| Embodiment 1 | Embodiment 2 | Embodiment 3 | |
| KT50 value | 7 points 40 seconds | 8 points 10 seconds | 6 points 30 seconds |
Test 2: safety
1) acute oral toxicity detects
The mosquito-repellent incense liquid of above-mentioned 3 embodiments is subjected to stomach-filling to 3 white mouse respectively, paradoxical reaction is no different after 30min, does not go out
Existing slow in reacting, diarrhea, it is dull situations such as, no white mouse is dead, LD50Greater than 5000mg/kg, it is grouped and is marked according to pesticide acute oral
Toxicity and the classer's description judgement of standard, the Ministry of Agriculture 1.2,1.1.8G product belong to nontoxic grade.
2) acute inhalation toxicity detects
The mosquito-repellent incense liquid for taking above-mentioned 3 embodiments is respectively placed in static exposure cabinet and is powered on volatilization, is then respectively put into 3
White mouse carries out, examination according to white mouse acute inhalation toxicity test related in GB15670-1995 agriculture chemical registration toxicology test method
It is as follows to test result: it is dead not occur symptoms, no white mouse such as perspire, the deep slow, activity of breathing reduces, is slow in reacting for white mouse after contamination
It dies, LD50Greater than 10g/m3, according to pesticide acute inhalation toxicity grade scale, the Ministry of Agriculture 1.2, the toxicity of 1.1.8G product and point
Grade mark judgement belongs to nontoxic grade.
Test 3: sleeping effect
The effect of in terms of tranquilizing the mind, sleeping is proved by following implementation method: main method is mosquito-repellent incense user volunteer
Experiment, totally 100 people passes through SCL-90 questionnaire (i.e. " Self-reporting inventory-respectively using the mosquito-repellent incense liquid in above-mentioned 3 embodiments
SCL90 ", be one of foremost Mental health test scale in the world) and PSQL(Pittsburgh Sleep Quality Index) investigation asks
Volume is tracked by continuous use in 2 weeks, to determine actual efficacy effect of the invention.
It assesses there are sleep disturbance [ Pittsburgh Sleep Quality Index (PSQL) scores 7-19 points ] 100, wherein male 45,
Female 55, the age 15-65 years old；Schooling: 10, primary school, 30, middle school, special secondary school 40,20, university；The sleep disturbance course of disease
0.5-7；It difficulty falling asleep 67, easily wakes up 13, early awakening 20；Daily sleeping time < 4h 15,4-5h 36,5-6h 49
Example, and sedative hypnotic drug is not used in the proximal segment time, is randomly divided into control group and observation group, two groups of genders, years by registration order
Age, culture procedure, sleep degree compare, no significant difference (> P0.05), using Wilcoxon rank sum test, inspection
Level a=0.05 is tested, sleep disturbance improves statistical result and is shown in Table 2.
Table 2
| Number of cases | It is basic to cure | It is effective | It improves | In vain | It is efficient |
| 100 | 7 | 56 | 35 | 2 | 98% |
It is obvious to a person skilled in the art that invention is not limited to the details of the above exemplary embodiments, Er Qie
In the case where without departing substantially from spirit or essential attributes of the invention, the present invention can be realized in other specific forms.Therefore, no matter
From the point of view of which point, the present embodiments are to be considered as illustrative and not restrictive, and the scope of the present invention is by appended power
Benefit requires rather than above description limits, it is intended that all by what is fallen within the meaning and scope of the equivalent elements of the claims
Variation is included within the present invention.
In addition, it should be understood that although this specification is described in terms of embodiments, but not each embodiment is only wrapped
Containing an independent technical solution, this description of the specification is merely for the sake of clarity, and those skilled in the art should
It considers the specification as a whole, the technical solutions in the various embodiments may also be suitably combined, forms those skilled in the art
The other embodiments being understood that.
Claims (5)
1. a kind of preparation method of aqua type plant electric mosquito repellent liquid, which is characterized in that the aqua type plant electric mosquito repellent liquid by
It is formed below according to the raw material of mass percent: anophelifuge medicament 0.5 ~ 2.3%, plant extracts 12 ~ 28%, non-ionic surface active
Agent 3 ~ 9%, preservative 0.1 ~ 0.8%, ethyl alcohol 20 ~ 50%, surplus are deionized water；
The plant extracts is made of following raw material according to parts by weight: 15 ~ 25 parts of lemon grass, Salvia japonica 10 ~ 16
Part, it is 8 ~ 13 parts of wild chrysanthemum, 6 ~ 15 parts of aloe, 10 ~ 15 parts of yellow Teng's root, 1 ~ 5 part of tobacco, 18 ~ 26 parts of folium artemisiae argyi, 11 ~ 15 parts of cloves, thin
3 ~ 9 parts of lotus, 10 ~ 15 parts of wrinkled giant hyssop, 1 ~ 4 part of radix gentianae；
Plant extracts is prepared as follows:
1) ingredient is carried out according to raw material composition and its parts by weight proportion；
2) it is uniformly mixed, is mixed after respectively grinding Salvia japonica, wild chrysanthemum, yellow Teng's root, folium artemisiae argyi, cloves, radix gentianae
Mixture A is added to sealed soak 5h in ethyl alcohol, is ultrasonically treated 30min, obtains mixed solution B by object A, by mixed solution B into
Row centrifugal treating takes supernatant, and gained sediment is added centrifugal treating after ethyl alcohol carries out the processing of 20min twice ultrasonic and takes supernatant,
Merge supernatant twice and be concentrated to get concentrate C with Rotary Evaporators, is washed after dry with dehydrated alcohol, is dried to obtain mixing
Object D；
3) lemon grass, aloe, tobacco, peppermint, wrinkled giant hyssop to be distilled with steam method, obtains crystal, crushing sieves with 100 mesh sieve,
Obtain mixture E；
4) mixture D and mixture E are mixed, ethyl alcohol is added, stirs evenly, is sealed under the conditions of 0 ~ 5 DEG C of temperature；
Aqua type plant electric mosquito repellent liquid is prepared as follows:
1) anophelifuge medicament and nonionic surfactant are added in deionized water, are stirred under the conditions of 50 DEG C of temperature to completely molten
Solution, is cooled to room temperature, filters to take filtrate, obtain solution F；
2) plant extracts is added in deionized water, stirs to being completely dissolved, obtains solution G；
3) solution F, solution G are mixed and preservative is added while stirring, until preservative dissolves, obtain Solution H；
4) into Solution H be added ethyl alcohol to get.
2. the preparation method of aqua type plant electric mosquito repellent liquid according to claim 1, which is characterized in that by below according to matter
The raw material for measuring percentage forms: anophelifuge medicament 1.6%, plant extracts 19%, nonionic surfactant 5%, preservative 0.3%,
Ethyl alcohol 35%, surplus are deionized water.
3. the preparation method of aqua type plant electric mosquito repellent liquid according to claim 1, which is characterized in that plant extracts by
Raw material according to parts by weight forms below: 20 parts of lemon grass, 13 parts of Salvia japonica, and 9 parts of wild chrysanthemum, 8 parts of aloe, yellow Teng's root 14
Part, 2 parts of tobacco, 22 parts of folium artemisiae argyi, 12 parts of cloves, 6 parts of peppermint, 11 parts of wrinkled giant hyssop, 2 parts of radix gentianae.
4. the preparation method of aqua type plant electric mosquito repellent liquid according to claim 1, which is characterized in that anophelifuge medicament four
Fluorine methothrin.
5. the preparation method of aqua type plant electric mosquito repellent liquid according to claim 1, which is characterized in that preservative is Kathon CG
Or Bronopol.
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| CN111771921A (en) * | 2019-12-09 | 2020-10-16 | 湖南省九喜日化有限公司 | Electric heating mosquito-repellent incense liquid and preparation method thereof |
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| CN114403142A (en) * | 2022-01-19 | 2022-04-29 | 福建省欧赛加日用品有限公司 | Strong-effect odorless chlorofluoroether pyrethrin electric heating mosquito-repellent incense tablet and preparation method thereof |
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