CN106278751A - A kind of organic water-soluble fertilizer utilizing tobacco leftovers to produce - Google Patents
A kind of organic water-soluble fertilizer utilizing tobacco leftovers to produce Download PDFInfo
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- CN106278751A CN106278751A CN201610749092.2A CN201610749092A CN106278751A CN 106278751 A CN106278751 A CN 106278751A CN 201610749092 A CN201610749092 A CN 201610749092A CN 106278751 A CN106278751 A CN 106278751A
- Authority
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- Prior art keywords
- soluble fertilizer
- tobacco
- organic water
- organic
- water
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- 239000003337 fertilizer Substances 0.000 title claims abstract description 82
- 235000002637 Nicotiana tabacum Nutrition 0.000 title claims abstract description 65
- 241000208125 Nicotiana Species 0.000 title claims abstract description 51
- 235000021190 leftovers Nutrition 0.000 title claims abstract description 27
- 239000007788 liquid Substances 0.000 claims abstract description 26
- 238000004519 manufacturing process Methods 0.000 claims abstract description 21
- 239000000758 substrate Substances 0.000 claims abstract description 17
- 244000061176 Nicotiana tabacum Species 0.000 claims abstract description 14
- 229910052700 potassium Inorganic materials 0.000 claims abstract description 14
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims abstract description 12
- 235000019504 cigarettes Nutrition 0.000 claims abstract description 11
- 238000000034 method Methods 0.000 claims abstract description 10
- ZLMJMSJWJFRBEC-UHFFFAOYSA-N Potassium Chemical compound [K] ZLMJMSJWJFRBEC-UHFFFAOYSA-N 0.000 claims abstract description 8
- 239000011591 potassium Substances 0.000 claims abstract description 8
- 238000003756 stirring Methods 0.000 claims abstract description 8
- 229910052698 phosphorus Inorganic materials 0.000 claims abstract description 7
- 230000001954 sterilising effect Effects 0.000 claims abstract description 5
- 238000001914 filtration Methods 0.000 claims abstract description 3
- 238000002156 mixing Methods 0.000 claims abstract description 3
- QGZKDVFQNNGYKY-UHFFFAOYSA-N Ammonia Chemical compound N QGZKDVFQNNGYKY-UHFFFAOYSA-N 0.000 claims description 12
- 239000000126 substance Substances 0.000 claims description 8
- 235000019441 ethanol Nutrition 0.000 claims description 7
- ATRRKUHOCOJYRX-UHFFFAOYSA-N Ammonium bicarbonate Chemical compound [NH4+].OC([O-])=O ATRRKUHOCOJYRX-UHFFFAOYSA-N 0.000 claims description 6
- XSQUKJJJFZCRTK-UHFFFAOYSA-N Urea Chemical group NC(N)=O XSQUKJJJFZCRTK-UHFFFAOYSA-N 0.000 claims description 6
- 229910021529 ammonia Inorganic materials 0.000 claims description 6
- 239000001099 ammonium carbonate Substances 0.000 claims description 6
- 235000012501 ammonium carbonate Nutrition 0.000 claims description 6
- 238000006243 chemical reaction Methods 0.000 claims description 5
- 210000003298 dental enamel Anatomy 0.000 claims description 5
- NLXLAEXVIDQMFP-UHFFFAOYSA-N Ammonia chloride Chemical compound [NH4+].[Cl-] NLXLAEXVIDQMFP-UHFFFAOYSA-N 0.000 claims description 4
- WCUXLLCKKVVCTQ-UHFFFAOYSA-M Potassium chloride Chemical compound [Cl-].[K+] WCUXLLCKKVVCTQ-UHFFFAOYSA-M 0.000 claims description 4
- 238000004090 dissolution Methods 0.000 claims description 4
- 238000004821 distillation Methods 0.000 claims description 4
- FGIUAXJPYTZDNR-UHFFFAOYSA-N potassium nitrate Chemical compound [K+].[O-][N+]([O-])=O FGIUAXJPYTZDNR-UHFFFAOYSA-N 0.000 claims description 4
- OTYBMLCTZGSZBG-UHFFFAOYSA-L potassium sulfate Chemical compound [K+].[K+].[O-]S([O-])(=O)=O OTYBMLCTZGSZBG-UHFFFAOYSA-L 0.000 claims description 4
- 229910052939 potassium sulfate Inorganic materials 0.000 claims description 4
- 235000011151 potassium sulphates Nutrition 0.000 claims description 4
- 230000008569 process Effects 0.000 claims description 4
- 238000011084 recovery Methods 0.000 claims description 4
- 235000013877 carbamide Nutrition 0.000 claims description 3
- 239000004202 carbamide Substances 0.000 claims description 3
- 150000001875 compounds Chemical class 0.000 claims description 3
- 229910000402 monopotassium phosphate Inorganic materials 0.000 claims description 3
- 235000019796 monopotassium phosphate Nutrition 0.000 claims description 3
- PJNZPQUBCPKICU-UHFFFAOYSA-N phosphoric acid;potassium Chemical compound [K].OP(O)(O)=O PJNZPQUBCPKICU-UHFFFAOYSA-N 0.000 claims description 3
- 235000019270 ammonium chloride Nutrition 0.000 claims description 2
- LFVGISIMTYGQHF-UHFFFAOYSA-N ammonium dihydrogen phosphate Chemical compound [NH4+].OP(O)([O-])=O LFVGISIMTYGQHF-UHFFFAOYSA-N 0.000 claims description 2
- 229910000387 ammonium dihydrogen phosphate Inorganic materials 0.000 claims description 2
- BFNBIHQBYMNNAN-UHFFFAOYSA-N ammonium sulfate Chemical compound N.N.OS(O)(=O)=O BFNBIHQBYMNNAN-UHFFFAOYSA-N 0.000 claims description 2
- 229910052921 ammonium sulfate Inorganic materials 0.000 claims description 2
- 235000011130 ammonium sulphate Nutrition 0.000 claims description 2
- 235000019837 monoammonium phosphate Nutrition 0.000 claims description 2
- 239000001103 potassium chloride Substances 0.000 claims description 2
- 235000011164 potassium chloride Nutrition 0.000 claims description 2
- 235000010333 potassium nitrate Nutrition 0.000 claims description 2
- 239000004323 potassium nitrate Substances 0.000 claims description 2
- 238000002360 preparation method Methods 0.000 claims description 2
- 238000002386 leaching Methods 0.000 claims 1
- 229910001220 stainless steel Inorganic materials 0.000 claims 1
- 239000010935 stainless steel Substances 0.000 claims 1
- 239000002699 waste material Substances 0.000 abstract description 8
- 230000007613 environmental effect Effects 0.000 abstract description 4
- 238000013459 approach Methods 0.000 abstract description 2
- 239000010865 sewage Substances 0.000 abstract description 2
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 20
- 239000002689 soil Substances 0.000 description 11
- 238000003973 irrigation Methods 0.000 description 10
- 230000002262 irrigation Effects 0.000 description 10
- 239000005416 organic matter Substances 0.000 description 9
- 239000000047 product Substances 0.000 description 7
- 239000007921 spray Substances 0.000 description 7
- 229930091371 Fructose Natural products 0.000 description 6
- RFSUNEUAIZKAJO-ARQDHWQXSA-N Fructose Chemical compound OC[C@H]1O[C@](O)(CO)[C@@H](O)[C@@H]1O RFSUNEUAIZKAJO-ARQDHWQXSA-N 0.000 description 6
- 239000005715 Fructose Substances 0.000 description 6
- 235000001014 amino acid Nutrition 0.000 description 6
- 150000001413 amino acids Chemical class 0.000 description 6
- 238000011161 development Methods 0.000 description 6
- 230000018109 developmental process Effects 0.000 description 6
- 238000005516 engineering process Methods 0.000 description 6
- 235000015097 nutrients Nutrition 0.000 description 6
- 230000000694 effects Effects 0.000 description 5
- 239000002253 acid Substances 0.000 description 4
- 230000004720 fertilization Effects 0.000 description 4
- 235000013619 trace mineral Nutrition 0.000 description 4
- 239000011573 trace mineral Substances 0.000 description 4
- 241000196324 Embryophyta Species 0.000 description 3
- 230000002159 abnormal effect Effects 0.000 description 3
- 230000008859 change Effects 0.000 description 3
- 239000000084 colloidal system Substances 0.000 description 3
- 235000009508 confectionery Nutrition 0.000 description 3
- 238000001514 detection method Methods 0.000 description 3
- 210000003608 fece Anatomy 0.000 description 3
- 239000003205 fragrance Substances 0.000 description 3
- 238000000227 grinding Methods 0.000 description 3
- 230000006872 improvement Effects 0.000 description 3
- 239000010871 livestock manure Substances 0.000 description 3
- 235000016709 nutrition Nutrition 0.000 description 3
- 230000035943 smell Effects 0.000 description 3
- IJGRMHOSHXDMSA-UHFFFAOYSA-N Atomic nitrogen Chemical compound N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 description 2
- 230000008901 benefit Effects 0.000 description 2
- 239000003795 chemical substances by application Substances 0.000 description 2
- 235000013399 edible fruits Nutrition 0.000 description 2
- 239000003344 environmental pollutant Substances 0.000 description 2
- 238000000855 fermentation Methods 0.000 description 2
- 230000004151 fermentation Effects 0.000 description 2
- 239000004021 humic acid Substances 0.000 description 2
- 239000000463 material Substances 0.000 description 2
- 230000035764 nutrition Effects 0.000 description 2
- 230000008635 plant growth Effects 0.000 description 2
- 231100000719 pollutant Toxicity 0.000 description 2
- 238000012545 processing Methods 0.000 description 2
- 239000002994 raw material Substances 0.000 description 2
- 238000004064 recycling Methods 0.000 description 2
- SNICXCGAKADSCV-JTQLQIEISA-N (-)-Nicotine Chemical compound CN1CCC[C@H]1C1=CC=CN=C1 SNICXCGAKADSCV-JTQLQIEISA-N 0.000 description 1
- PAWQVTBBRAZDMG-UHFFFAOYSA-N 2-(3-bromo-2-fluorophenyl)acetic acid Chemical compound OC(=O)CC1=CC=CC(Br)=C1F PAWQVTBBRAZDMG-UHFFFAOYSA-N 0.000 description 1
- PUKLDDOGISCFCP-JSQCKWNTSA-N 21-Deoxycortisone Chemical compound C1CC2=CC(=O)CC[C@]2(C)[C@@H]2[C@@H]1[C@@H]1CC[C@@](C(=O)C)(O)[C@@]1(C)CC2=O PUKLDDOGISCFCP-JSQCKWNTSA-N 0.000 description 1
- QJZYHAIUNVAGQP-UHFFFAOYSA-N 3-nitrobicyclo[2.2.1]hept-5-ene-2,3-dicarboxylic acid Chemical compound C1C2C=CC1C(C(=O)O)C2(C(O)=O)[N+]([O-])=O QJZYHAIUNVAGQP-UHFFFAOYSA-N 0.000 description 1
- 241000894006 Bacteria Species 0.000 description 1
- 108010082495 Dietary Plant Proteins Proteins 0.000 description 1
- FCYKAQOGGFGCMD-UHFFFAOYSA-N Fulvic acid Natural products O1C2=CC(O)=C(O)C(C(O)=O)=C2C(=O)C2=C1CC(C)(O)OC2 FCYKAQOGGFGCMD-UHFFFAOYSA-N 0.000 description 1
- OAICVXFJPJFONN-UHFFFAOYSA-N Phosphorus Chemical compound [P] OAICVXFJPJFONN-UHFFFAOYSA-N 0.000 description 1
- 229910000831 Steel Inorganic materials 0.000 description 1
- YUWBVKYVJWNVLE-UHFFFAOYSA-N [N].[P] Chemical compound [N].[P] YUWBVKYVJWNVLE-UHFFFAOYSA-N 0.000 description 1
- 238000010521 absorption reaction Methods 0.000 description 1
- 239000000783 alginic acid Substances 0.000 description 1
- 235000010443 alginic acid Nutrition 0.000 description 1
- 229960001126 alginic acid Drugs 0.000 description 1
- 229920000615 alginic acid Polymers 0.000 description 1
- 150000004781 alginic acids Chemical class 0.000 description 1
- 150000001412 amines Chemical class 0.000 description 1
- 229940024606 amino acid Drugs 0.000 description 1
- 230000001580 bacterial effect Effects 0.000 description 1
- 230000015572 biosynthetic process Effects 0.000 description 1
- 239000003575 carbonaceous material Substances 0.000 description 1
- 238000004140 cleaning Methods 0.000 description 1
- 238000010668 complexation reaction Methods 0.000 description 1
- 239000002131 composite material Substances 0.000 description 1
- 230000003750 conditioning effect Effects 0.000 description 1
- 238000010276 construction Methods 0.000 description 1
- 230000002079 cooperative effect Effects 0.000 description 1
- 230000000875 corresponding effect Effects 0.000 description 1
- 230000003247 decreasing effect Effects 0.000 description 1
- 238000013461 design Methods 0.000 description 1
- 238000000605 extraction Methods 0.000 description 1
- 238000009313 farming Methods 0.000 description 1
- 230000035558 fertility Effects 0.000 description 1
- 239000000706 filtrate Substances 0.000 description 1
- 229960002737 fructose Drugs 0.000 description 1
- 239000002509 fulvic acid Substances 0.000 description 1
- 229940095100 fulvic acid Drugs 0.000 description 1
- 230000012010 growth Effects 0.000 description 1
- 229910001385 heavy metal Inorganic materials 0.000 description 1
- 230000010354 integration Effects 0.000 description 1
- 238000012423 maintenance Methods 0.000 description 1
- 238000005259 measurement Methods 0.000 description 1
- 230000000813 microbial effect Effects 0.000 description 1
- 239000000203 mixture Substances 0.000 description 1
- 229960002715 nicotine Drugs 0.000 description 1
- SNICXCGAKADSCV-UHFFFAOYSA-N nicotine Natural products CN1CCCC1C1=CC=CN=C1 SNICXCGAKADSCV-UHFFFAOYSA-N 0.000 description 1
- 229910052757 nitrogen Inorganic materials 0.000 description 1
- 239000003895 organic fertilizer Substances 0.000 description 1
- 238000002161 passivation Methods 0.000 description 1
- 239000011574 phosphorus Substances 0.000 description 1
- 230000003389 potentiating effect Effects 0.000 description 1
- 230000001737 promoting effect Effects 0.000 description 1
- 238000004080 punching Methods 0.000 description 1
- 230000007261 regionalization Effects 0.000 description 1
- 229930000044 secondary metabolite Natural products 0.000 description 1
- 238000000926 separation method Methods 0.000 description 1
- 239000002893 slag Substances 0.000 description 1
- 239000010959 steel Substances 0.000 description 1
- 239000013589 supplement Substances 0.000 description 1
- 238000010189 synthetic method Methods 0.000 description 1
- 238000012360 testing method Methods 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C05—FERTILISERS; MANUFACTURE THEREOF
- C05G—MIXTURES OF FERTILISERS COVERED INDIVIDUALLY BY DIFFERENT SUBCLASSES OF CLASS C05; MIXTURES OF ONE OR MORE FERTILISERS WITH MATERIALS NOT HAVING A SPECIFIC FERTILISING ACTIVITY, e.g. PESTICIDES, SOIL-CONDITIONERS, WETTING AGENTS; FERTILISERS CHARACTERISED BY THEIR FORM
- C05G3/00—Mixtures of one or more fertilisers with additives not having a specially fertilising activity
- C05G3/80—Soil conditioners
-
- C—CHEMISTRY; METALLURGY
- C05—FERTILISERS; MANUFACTURE THEREOF
- C05B—PHOSPHATIC FERTILISERS
- C05B7/00—Fertilisers based essentially on alkali or ammonium orthophosphates
-
- C—CHEMISTRY; METALLURGY
- C05—FERTILISERS; MANUFACTURE THEREOF
- C05C—NITROGENOUS FERTILISERS
- C05C1/00—Ammonium nitrate fertilisers
-
- C—CHEMISTRY; METALLURGY
- C05—FERTILISERS; MANUFACTURE THEREOF
- C05C—NITROGENOUS FERTILISERS
- C05C9/00—Fertilisers containing urea or urea compounds
-
- C—CHEMISTRY; METALLURGY
- C05—FERTILISERS; MANUFACTURE THEREOF
- C05F—ORGANIC FERTILISERS NOT COVERED BY SUBCLASSES C05B, C05C, e.g. FERTILISERS FROM WASTE OR REFUSE
- C05F5/00—Fertilisers from distillery wastes, molasses, vinasses, sugar plant or similar wastes or residues, e.g. from waste originating from industrial processing of raw material of agricultural origin or derived products thereof
- C05F5/006—Waste from chemical processing of material, e.g. diestillation, roasting, cooking
-
- C—CHEMISTRY; METALLURGY
- C05—FERTILISERS; MANUFACTURE THEREOF
- C05G—MIXTURES OF FERTILISERS COVERED INDIVIDUALLY BY DIFFERENT SUBCLASSES OF CLASS C05; MIXTURES OF ONE OR MORE FERTILISERS WITH MATERIALS NOT HAVING A SPECIFIC FERTILISING ACTIVITY, e.g. PESTICIDES, SOIL-CONDITIONERS, WETTING AGENTS; FERTILISERS CHARACTERISED BY THEIR FORM
- C05G3/00—Mixtures of one or more fertilisers with additives not having a specially fertilising activity
-
- C—CHEMISTRY; METALLURGY
- C05—FERTILISERS; MANUFACTURE THEREOF
- C05G—MIXTURES OF FERTILISERS COVERED INDIVIDUALLY BY DIFFERENT SUBCLASSES OF CLASS C05; MIXTURES OF ONE OR MORE FERTILISERS WITH MATERIALS NOT HAVING A SPECIFIC FERTILISING ACTIVITY, e.g. PESTICIDES, SOIL-CONDITIONERS, WETTING AGENTS; FERTILISERS CHARACTERISED BY THEIR FORM
- C05G5/00—Fertilisers characterised by their form
- C05G5/20—Liquid fertilisers
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02A—TECHNOLOGIES FOR ADAPTATION TO CLIMATE CHANGE
- Y02A40/00—Adaptation technologies in agriculture, forestry, livestock or agroalimentary production
- Y02A40/10—Adaptation technologies in agriculture, forestry, livestock or agroalimentary production in agriculture
- Y02A40/20—Fertilizers of biological origin, e.g. guano or fertilizers made from animal corpses
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Life Sciences & Earth Sciences (AREA)
- Pest Control & Pesticides (AREA)
- Soil Sciences (AREA)
- Engineering & Computer Science (AREA)
- Botany (AREA)
- Environmental & Geological Engineering (AREA)
- Fertilizers (AREA)
Abstract
The invention discloses a kind of organic water-soluble fertilizer utilizing tobacco leftovers to produce, make by the following method: the collection of the Nicotiana tabacum L. ethanol leachate produced in production of cigarettes and filtration；(2) formed after tobacco leachate being used sterilizing under 100 120 DEG C of high temperature, concentration rich in organic and containing potassium substrate liquid；(3) substrate liquid temp is cooled to 40 50 DEG C, then adds N P and K source, stir to being completely dissolved chelating, mixing speed 480r/min 560r/min, adjust pH value；(4) grind, stand de-soak, obtain organic water-soluble fertilizer.Novel organic water-soluble fertilizer produced by tobacco leachate leftover bits and pieces by the present invention, fundamentally solves the environmental issue in tobacco leaf production, stops sewage discharge, and tobacco leftovers of turning waste into wealth develops new higher value application approach.
Description
Technical field
The present invention relates to fertilizer field, specifically, relate to a kind of organic water-soluble fertilizer utilizing tobacco leftovers to produce.
Background technology
The cultivated area of China Nicotiana tabacum L. and the yield Jun Ju world are the first, also along with producing about in annual Nicotiana tabacum L. processing
The leftover bits and pieces such as inapplicable offal, tobacco rod and the tobacco leachate of 25% (901,500,000 tons), if dealt with improperly, not only can give ring
Bring serious pollution and harm in border, and will also result in the waste of resource.These leftover bits and pieces cannot be used for production of cigarettes, generally
In the case of all arbitrarily abandoned, burned and discharged；Some enterprise uses extraction nicotine, Salanesol, vegetable protein, ethanol or cigarette phthalein
Its garbage is recycled by the methods such as amine, but these methods all majorities rest on the experimental stage, are produced widely
Industryization is promoted；Owing to tobacco waste containing fructose, amino acid whose biological organic principle and secondary metabolite, contain simultaneously
The nutrients such as substantial amounts of nitrogen, phosphorus, potassium and trace element, therefore, are applied to organic agriculture and produce value higher for tool.
China is now with ploughing 1.3 hundred million hectares, and farmland under irrigation accounts for the gross area 56% in arable land, fills according to China's water saving
Irrigating development plan, it is contemplated that to the year two thousand thirty, China's population is up to 1,900,000,000, about more than 800,000,000,000,000 kilogram of required grain, increases than current
More than adding 2,500 hundred million kilograms, for the area of this agricultural irrigation, need substantial increase.Even if traditional fertilization mode, such as broadcast application, if
Not having rainfall, do not irrigate, crop cannot absorb.Therefore water soluble fertilizer combines Irrigation farming, accomplishes liquid manure one, tool
There is water saving, save fertilizer, the feature of saving of work and time.It was verified that the fertilization mode of water-fertilizer integral is compared with tradition watering, fertilizing, joint
Water reaches more than 50%, and have even can reach 90%." in the case of water resource supply can not be fully solved, irrigated area
Expansion, water-saving irrigation region will be relied primarily on." the Chinese Academy of Agricultural Sciences's agricultural resource and agricultural regionalization director of the Institute's kingly way dragon
Say.
Therefore, water-fertilizer integral just becomes the topic that brainstrust is discussed warmly and advocated in recent years, just when coming to see, and its prospect
The most wide.Mentioning the market trend of water-fertilizer integral, it has to carry is exactly water-soluble fertilizer, it is the guiding of water-fertilizer integral
Main product.
The trend of Developing Water-saving Agriculture is not only the development of water soluble fertilizer and creates condition, simultaneously to water soluble fertilizer yet
Development propose new demand.With regard to China's water-fertilizer integral development status and trend, USDA National agricultural technology center saves
At water, director Du Sen points out, through for many years it was verified that water-fertilizer integral is the critical path of " control water fat-reducing ", current liquid manure
Integration popularizing area, probably at more than 4,670,000 hectares, is disposed according to the Ministry of Agriculture, to the year two thousand twenty, is promoted by newly-increased water-fertilizer integral
Area more than 5,330,000 hectare, tomorrow requirement amount increases severely.
At present, the water-soluble fertilizer one having obtained Ministry of Agriculture's registration card has 6602, wherein a great number of elements water-soluble fertilizer
1494, trace element water-soluble fertilizer 1714, aminoacid water-soluble fertilizer 1679, humic acid water-soluble fertilizer 1615, and have
Machine water-soluble fertilizer only has 100, it is seen that organic water-soluble fertilizer product still compares shortcoming, and it is organic to use tobacco leachate to be used as
Raw material production Water soluble fertilizer is the most pioneering.
Water soluble fertilizer is a kind of polyelement composite fertilizer that can be completely soluble, and it can promptly be dissolved in the water, more
The most absorbed by crops, and its absorption rate is of a relatively high, does not has organic principle in general chemical fertilizer type Water soluble fertilizer.And
" organic water-soluble fertilizer ", the national standard that there is presently no authority named, but the most commonly used be organic substance+change
Learn the solution that fertilizer+water is formed.Wherein, organic substance can include any have chemical fertilizer potentiating effect and complexation (chelating) effect
Soluble organic matter, the humic acids existed the most separately or together, fulvic acid, aminoacid, fructose, alginic acid etc..Come
Come from plant and animal, fermented, become thoroughly decomposed, extract or activate after to impose on soil to provide plant nutrient be containing of its primary efficacy
Carbon material is organic.
The advantage of organic water-soluble fertilizer: one, employing water, fertilizer are with executing, fertile with water band, it is achieved that water-fertilizer integral, and fertilising is imitated
Rate is high, it is possible to reduce total fertilization amount, plays rich water cooperative effect, makes fertile and water utilization ratio all significantly improve.Its two, fertile
Effect is fast, it is possible to resolve the nutritional need of high-yield crop fast growing period.Can be applicable to spray, spray, drip irrigation, it is achieved liquid manure one
Change, water-saving, province's fertilizer, less manpower.
The organic substances such as aminoacid that the organic water-soluble fertilizer that this technology is produced leaches rich in Nicotiana tabacum L. and fructose and crop are raw
Nutrient substance needed for length, and dissolve and chelated n p k nutrition, this fertilizer of abundant Appropriate application can not only provide plant growth
Required nutrient, improves soil, partly or entirely substitutes chemical fertilizer and can improve soil environment and build up fertility, improves the micro-life of soil
State environment, improves crop yield, it is also possible to improve crops quality, can improve utilization rate of fertilizer simultaneously, reduces production cost.
This technology is for the purpose of focus utilization tobacco leftovers is for development of raw materials Eco-fertilizer also field, i.e. to make ecological fertilizer
For tie, tobacco and agricultural planting are optimized combination, accomplish that energy multi-level utilizes, material circulates benignly, formed " zero "
Polluting the Agro-ecological System of sustainable development, the most perfect industrial chain of Nicotiana tabacum L., for promoting environmental protection to discharge portion
Strength.
This technology is with the tobacco rod offal produced in tobacco leaf production, and the filter collected after tobacco leachate solid-liquid separation
Slag, filtrate, for processing object, utilize biological bacteria orientation fermentation technology that material carries out fermentation maturity weight gaining process, multiple by adding
Close microbial bacterial agent or select desired passivation agent the heavy metal in tobacco waste to be carried out harmless treatment, by tobacco waste
The series ecological fertilizer such as biological organic fertilizer, organic water-soluble fertilizer is developed in comprehensive utilization, it is achieved environmental conservation and waste material
Higher value application.The equipment used due to the project implementation is home equipment, and Construction and operation maintenance cost is relatively low, adds resource
Change high treating effect, it is possible to the garbage produced during production of cigarettes is accomplished 100% recycling, " zero " can be reached again dirty
Dye is discharged thus is realized cleaning and produce, and therefore has highly application value.
To sum up, the present invention has good novelty and feasibility, utilizes process technology of the present invention, utilizes tobacco leftovers raw
Produce the product of novel organic water-soluble fertilizer, on the basis of meeting China's water-soluble fertilizer standard corresponding index, it is also possible to freely regulate
Ratio between n p k nutrition, to adapt to the requirement of different soil and crop, can meet the needs of fertilization compositions based on earth measurement,
Both can spray, spray, again can drip irrigation and foliage spray, application is very strong, and market demand average annual growth, and the coming five years turns over
, therefore, this patent product has huge value space at modern fertilizer industry.
Summary of the invention
It is an object of the invention to the pollution disaster problem solving current tobacco leftovers during production of cigarettes, stop
Disposal of pollutants, turns waste into wealth, and improves the industrial chain of Nicotiana tabacum L. further, solves current China soil present stage urgent need and supplements organic matter
Present situation with a great number of elements, it is provided that a kind of organic water-soluble fertilizer utilizing tobacco leftovers to produce.
To achieve these goals, the present invention adopts the following technical scheme that
A kind of organic water-soluble fertilizer utilizing tobacco leftovers to produce, makes by the following method:
(1) collection of Nicotiana tabacum L. ethanol leachate produced in production of cigarettes and filtration；
(2) formed rich in organic matter with containing potassium after tobacco leachate being used sterilizing under 100-120 DEG C of high temperature, concentration
Substrate liquid；
(3) substrate liquid temp being cooled to 40-50 DEG C, then add N P and K source, stirring, to being completely dissolved chelating, is stirred
Speed 480r/min-560r/min, adjusts pH value；
(4) grind, stand de-soak, obtain organic water-soluble fertilizer.
As preferably, in the above-mentioned organic water-soluble fertilizer utilizing tobacco leftovers to produce, described N P and K source is
Carbamide, potassium sulfate, potassium nitrate, ammonium sulfate, ammonium carbonate, potassium dihydrogen phosphate, ammonium dihydrogen phosphate, potassium chloride, ammonium chloride and Nitrogen-and Phosphorus-containing
The compound fertilizer of potassium, addition is the 10-20% of substrate liquid quality.
As preferably, in the above-mentioned organic water-soluble fertilizer utilizing tobacco leftovers to produce, described adjustment pH value is
Use ammonium carbonate or ammonia, adjust between pH5-9.As preferably, at the above-mentioned organic water utilizing tobacco leftovers to produce
In molten fertilizer, the equipment that step (2) described sterilizing and concentration process are used be the enamel reaction still of band high pressure or rustless steel anti-
Answer still.
Compared with prior art, there is advantages that
(1) tobacco leachate leftover bits and pieces is produced novel organic water-soluble fertilizer by the present invention, fundamentally solves tobacco leaf production
In environmental issue, stop sewage discharge, and tobacco leftovers of turning waste into wealth develop new higher value application approach.
(2) organic water-soluble fertilizer that the present invention obtains can be used for concentrated fertilizer and agricultural high-effiency soil improvement, decreasing
Fertile amount of application, improves current China soil and owes the organic and present situation of nutrient, and product is water solublity, the shape of Chelating state
State is present in product and can effectively be absorbed by plant completely, is suitable for the water-fertilizer integral modern agriculture such as drip irrigation and spray irrigation.Utilize this
Fertilizer, every mu of ground uses 2-10kg, and improvement is hardened, acidified soil, and crop yield can improve 20-30%, and improve crops
Quality.
(3) this patent preparation method is simple to operate, uses " a still synthetic method " to prepare the organic a great number of elements of high concentration fertile,
And same method can compound the polynary organic water-soluble fertilizer of more than ternary and ternary, and nutrient ratio is controlled.Can be right
100% recycling accomplished by the leftover bits and pieces produced during production of cigarettes, can reach again " zero " disposal of pollutants.
(4) organic water-soluble fertilizer China is temporarily without working standard, first with amino-acid trace element water-soluble fertilizer (NY1429-
2010) comparing with a great number of elements microelement type water-soluble fertilizer standard (NY1107-2010), organic index shows excellent.
Detailed description of the invention
Embodiment 1: the production stage utilizing tobacco leftovers production organic water-soluble fertilizer is as follows:
(1) collection of tobacco leachate: having an operation in production of cigarettes is first to use alcohol-pickled Nicotiana tabacum L., dissolution fructose and ammonia
The organic matters such as base acid, then recovery of alcohol distillation, remaining is i.e. tobacco leachate；
(2) tobacco leachate is used 100 DEG C of high temperature sterilize concentration time 3h of enamel reaction still, is formed after concentration rich in having
Machine matter and the substrate liquid containing potassium, moisture is 60%；
(3) lower the temperature 40-50 DEG C at substrate liquid temp, add quality 5% carbamide and potassium sulfate 5%, stirring speed by substrate liquid
Degree 480r/min, stirring 2h are completely dissolved chelating；
(4) pH value determination, adjusts acid-base value to pH equal to 6.8 with ammonium carbonate；
(5) grinding by colloid mill, filter 100 mesh filters, and is finally putting into reserve pool and stands froth breaking, detection conjunction in 24 hours
Lattice, canned dispatch from the factory.
Gained organic water-soluble fertilizer outward appearance is brown color liquid, and abnormal smells from the patient is tobacco sweet fragrance, and the content of organic matter is more than 180g/
L, N-P-K content is more than 100g/L, and insoluble matter is less than 50g/L, is highly suitable as agricultural drop irrigation punching fertilising.Consumption is every mu
Use 3-10kg, make crop turn rapidly green, promote plant growth, improve yield and crop quality sweetness potency is obvious.
Embodiment 2: the production stage utilizing tobacco leftovers production organic water-soluble fertilizer is as follows:
(1) collection of tobacco leachate: having an operation in production of cigarettes is first to use alcohol-pickled Nicotiana tabacum L., dissolution fructose and ammonia
The organic matters such as base acid, then recovery of alcohol distillation, remaining is i.e. tobacco leachate；
(2) tobacco leachate is used 121 DEG C of high temperature sterilize 2h of enamel reaction still, declines formation richness after temperature continuous concentration
Containing organic and containing potassium substrate liquid, reaching moisture is 70%；
(3) lower the temperature 50-55 DEG C at substrate liquid temp, add quality 10% potassium dihydrogen phosphate 5%, mixing speed by substrate liquid
560r/min, stirs and is completely dissolved chelating in 2 hours；
(4) pH value determination, adjusts acid-base value to pH equal to 6.5 with ammonium carbonate；
(5) grinding by colloid mill, filter 100 mesh filters, and is finally putting into reserve pool and stands de-soak, detection conjunction in 24 hours
Lattice, canned dispatch from the factory.
Gained organic water-soluble fertilizer outward appearance is brown color liquid, and abnormal smells from the patient is tobacco sweet fragrance, and the content of organic matter is more than 150g/
L, N-P-K content is more than 100g/L, and insoluble matter is less than 50g/L, is highly suitable as agricultural and sprays and use foliage fertilizer.Consumption is every
Mu uses 3-5kg, improves percentage of fertile fruit, prevents dehiscent fruit, promotes quality of agricultural product effect obvious.
Embodiment 3: the production stage utilizing tobacco leftovers production organic water-soluble fertilizer is as follows:
(1) collection of tobacco leachate: having an operation in production of cigarettes is first to use alcohol-pickled Nicotiana tabacum L., dissolution fructose and ammonia
The organic matters such as base acid, then recovery of alcohol distillation, remaining is i.e. tobacco leachate；
(2) formed rich in organic matter after tobacco leachate is used 110 DEG C of high temperature sterilize 2h of enamel reaction still, concentration and contain
The substrate liquid of potassium, moisture is 65%；
(3) lower the temperature 35-45 DEG C at substrate liquid temp, add quality 15% ammonium nitrate and 5% potassium sulfate, stirring by substrate liquid
Speed 560r/min, stirring 2h is completely dissolved chelating；
(4) pH value determination, adjusts acid-base value to pH equal to 8.5 with ammonia；
(5) grinding by colloid mill, filter 100 mesh filters, and is finally putting into reserve pool and stands de-soak, detection conjunction in 24 hours
Lattice, canned dispatch from the factory.
Gained organic water-soluble fertilizer outward appearance is brown color liquid, and abnormal smells from the patient is tobacco sweet fragrance, and the content of organic matter is more than 160g/
L, N-P-K content is more than 100g/L, and insoluble matter is less than 50g/L, is highly suitable as the drip irrigation of soil conditioning function and rushes fertilising and make
With.Consumption is every mu and uses 5-10kg, notable to acid soil improvement, crop green effect again.
Data test: organic water-soluble fertilizer China is temporarily without working standard, first with amino-acid trace element water-soluble fertilizer
(NY1429-2010) comparing with a great number of elements microelement type water-soluble fertilizer standard (NY1107-2010), result shows three
The most single insoluble matter of embodiment and acid-base value Ph value all meet the requirement of two national standards of comparison, and three embodiments is organic
Matter content is more than 150g/L, and the content of organic matter compareing two standards is all 0.Design parameter is shown in Table 1:
Table 1
Claims (5)
1. the organic water-soluble fertilizer utilizing tobacco leftovers to produce, it is characterised in that make by the following method:
(1) collection of Nicotiana tabacum L. ethanol leachate produced in production of cigarettes and filtration；
(2) formed after tobacco leachate being used sterilizing under 100-121 DEG C of high temperature, concentration rich in organic and containing potassium substrate
Liquid；
(3) substrate liquid temp is cooled to 40-55 DEG C, then interpolation N P and K source, mixing speed 480r/min-560r/min,
Stirring, to being completely dissolved chelating, adjusts pH value；
(4) grind, stand de-soak, obtain organic water-soluble fertilizer.
Utilize the organic water-soluble fertilizer that tobacco leftovers produces the most as claimed in claim 1, it is characterised in that described Nicotiana tabacum L. is soaked
The preparation method going out liquid is: first using alcohol-pickled Nicotiana tabacum L., recovery of alcohol distillation after dissolution Organic substance, remaining is i.e. Nicotiana tabacum L. leaching
Liquid.
Utilize the organic water-soluble fertilizer that tobacco leftovers produces the most as claimed in claim 1, it is characterised in that described N P and K
Source is carbamide, potassium sulfate, potassium nitrate, ammonium sulfate, ammonium carbonate, potassium dihydrogen phosphate, ammonium dihydrogen phosphate, potassium chloride, ammonium chloride and contains
The solubility compound fertilizer of N P and K, addition is the 10-20% of substrate liquid quality.
Utilize the organic water-soluble fertilizer that tobacco leftovers produces the most as claimed in claim 1, it is characterised in that described adjustment pH
Value is to use ammonium carbonate or ammonia, adjusts between pH5-9.
Utilize the organic water-soluble fertilizer that tobacco leftovers produces the most as claimed in claim 1, it is characterised in that step (2) institute
State sterilizing and equipment that concentration process is used is enamel reaction still or the stainless steel cauldron of band high pressure.
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Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN110915596A (en) * | 2019-09-30 | 2020-03-27 | 中国烟草总公司河南省公司 | Planting method and fertilizer for six tobacco leaves on flue-cured tobacco |
| CN111170792A (en) * | 2020-02-21 | 2020-05-19 | 中化（烟台）作物营养有限公司 | Organic water-soluble fertilizer containing water-soluble carbon compound and preparation method and application thereof |
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