CN106268553A - A kind of quintessence oil microsphere for mask filter disc and preparation method thereof - Google Patents
A kind of quintessence oil microsphere for mask filter disc and preparation method thereof Download PDFInfo
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- CN106268553A CN106268553A CN201610671671.XA CN201610671671A CN106268553A CN 106268553 A CN106268553 A CN 106268553A CN 201610671671 A CN201610671671 A CN 201610671671A CN 106268553 A CN106268553 A CN 106268553A
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- microsphere
- oil
- quintessence oil
- filter disc
- mask filter
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J13/00—Colloid chemistry, e.g. the production of colloidal materials or their solutions, not otherwise provided for; Making microcapsules or microballoons
- B01J13/02—Making microcapsules or microballoons
- B01J13/025—Applications of microcapsules not provided for in other subclasses
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- Organic Chemistry (AREA)
- Dispersion Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Treatments For Attaching Organic Compounds To Fibrous Goods (AREA)
- Respiratory Apparatuses And Protective Means (AREA)
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Abstract
The present invention relates to a kind of quintessence oil microsphere for mask filter disc and preparation method thereof.Material for the quintessence oil microsphere of mask filter disc of the present invention is sodium alginate or gelatin, wraps up common several plant quintessence oil in microsphere.Its preparation technology is simple and easy to do, and cost is relatively low, is suitable for industrialized great production.Quintessence oil microsphere purposes of the present invention, for being placed in mask filter disc, distributes fragrance, has refreshment, refrigerant effect releived.
Description
Technical field
The invention belongs to Microspheres Technique field, relate to a kind of quintessence oil microsphere for mask filter disc and preparation method thereof.
Background technology
Mask is a kind of hygienic article, refers generally to the air being worn over nose and mouth for filtering entrance mouth and nose, to reach resistance
Gas that gear is harmful, abnormal smells from the patient, the apparatus of spittle turnover wearer's mouth and nose, make with gauze or paper etc..Mask is to entering pulmonary
Air has certain filtration, and when respiratory infectious disease is popular, in the environment that dust etc. pollutes during operation, wear masks tool
There is extraordinary effect.Universal due to industrial expansion and automobile, air quality declines year by year, the most annual heating period
In, owing to using fire coal, in air, discharge a large amount of nuisance, the most in recent years by the PM2.5 granule of public attention.By
In the development of science and technology and popularizing of network, increasing people recognize the harm of harmful substance in air, the most various mouths
The use of cover is the most increasing.In conventional mask type, protection PM2.5 is maximally effective is specialty protective mask, the most often
The mask of N95, N90 model seen, but the obturation effect of this kind of mask is very good, to such an extent as to the air capacity that can pass through also is subject to
The biggest impact, can not wear for a long time, is not particularly suitable for the crowd that child, old people or Respiratory ft tive resistance are poor.And wear
Comfort level and protection effect all preferably mask is the cotton mask of replaceable filter disc, and is easy to clean, so being also major part
Consumer's selection when buying mask.
Quintessence oil is from the flower of plant, leaf, stem, root or fruit, by steam distillation, squeezing and pressing method, cold-maceration or molten
Agent extraction method refines the volatile flavor of extraction.Quintessence oil is made up of chemical moleculars such as terpenes, aldehydes, esters, alcohols.Cause
For high fluidity, so being referred to as " oily ", but there is this qualitative difference with the daily vegetable oil seen.Plant main body of oil is
Triglyceride and fatty acid composition.The present invention have selected several frequently seen plants essential oil, its effect is summarized as follows: Camellia sinensis
Quintessence oil has bactericidal antiphlogistic, restrains pore, treats Common Cold, cough, rhinitis, asthma, improves dysmenorrhea, menoxenia and reproduction
The effects such as device infection.Fructus Citri Limoniae quintessence oil can help to refresh oneself spirit, alleviate irritated, also have the most positive tune for skin and health
Reason effect.Grapefruit essential oil energy nurse tissue cell, increases muscle power, bronchitis of releiving, diuresis, improves fat, edema and pouring
The disease of bar glandular system, infection.Grapefruit essential oil can also resist melancholy, the melancholy that especially occurs in winter or drowsy etc.
Symptom, can make people refresh, and is the regulator of seasonal psychataxia.Rosemary ethereal oil is the most helpful to respiratory system,
The respiratory system diseases such as flu, bronchitis, can use Herba Rosmarini Officinalis.Foremost effect of Herba Rosmarini Officinalis, it is simply that memory can be promoted
Power, makes that people is clearheaded, has clear presentation, and the people being best suitable for examinee or brain overwork uses.Peppermint essential oil taste is clearly cooled off oneself,
The mind, cleaning throat and moistening larynx can be rouse oneself, offset antihalitosis and there is good effect, and have unique curative effect of body and mind of releiving.
Summary of the invention
It is an object of the invention to overcome the deficiencies in the prior art, it is provided that a kind of preparation technology is relatively simple, lower cost
A kind of preparation method of the quintessence oil microsphere for mask filter disc.
Second object of the present invention is to provide a kind of quintessence oil microsphere for mask filter disc.
Technical scheme is summarized as follows:
A kind of quintessence oil microsphere for mask filter disc, is characterized by that the material of microsphere is sodium alginate or gelatin.
A kind of quintessence oil microsphere for mask filter disc, is characterized by that the quintessence oil that microsphere wraps up is natural plant essential oils, including
But it is not limited in tea tree ethereal oil, rosemary ethereal oil, Fructus Citri Limoniae quintessence oil, Peppermint essential oil, grapefruit essential oil, eucalyptus oil, Flos Rosae Rugosae quintessence oil
One or more.
The preparation method of a kind of quintessence oil microsphere for mask filter disc, is characterized in that comprising the steps:
(1) by 4%(w/v) sodium alginate soln, at 70 DEG C, add appropriate 0.1% CaCl2Cross-linking agent, after chelating 24-48h, in
121 DEG C of pyrolysis processing, survey its viscosity about 800-1500mpa.s under 30 DEG C of water-baths；
(2) in stirring, in sodium alginate glue, pigment solution and plants essential oil it are sequentially added into；
(3) using coaxial air-flow method to prepare microsphere, regulation air pressure is 0.01-0.05Mpa, and air-flow velocity is 4.0-8.0L/min,
After solidification, collect microsphere, drying and get final product.
The preparation method of a kind of quintessence oil microsphere for mask filter disc, is characterized in that comprising the steps:
(1) by gelatin and appropriate plasticizer (glycerol or sorbitol), it is completely dissolved in 60 DEG C of water-baths, obtained solution A；
(2) under fast stirring, in solution A, pigment solution and plants essential oil it are sequentially added into, obtained solution B after homogenizing；
(3) under 60 DEG C of water bath condition, solution B is poured slowly in the liquid paraffin that stirred, after stirring a period of time, ice bath
Reduce temperature, be stirred for, keep constant rotational speed according to required microsphere size, stand, settle microsphere, remove oil phase, with acetone or
Ethanol or ethyl acetate cyclic washing microsphere, leach microsphere, drying and get final product.
A kind of quintessence oil microsphere for mask filter disc, is characterized by that the purposes of described quintessence oil microsphere is for being placed on mask filter
In sheet, distribute fragrance, have refreshment, refrigerant effect releived.
Advantages of the present invention:
The present invention provides a kind of quintessence oil microsphere for mask filter disc, and its preparation technology is simple and easy to do, and cost is relatively low, is suitable for industry
Change big production.Quintessence oil microsphere purposes of the present invention, for being placed in mask filter disc, distributes fragrance, has refreshment, refrigerant
The effect releived.
Detailed description of the invention
The present invention is further elaborated by following example, but the scope of the present invention is not limited to these embodiments.Institute
With, under the method premise of the present invention, the simple modifications of the present invention is all belonged to the scope of protection of present invention.
Embodiment 1
The preparation technology of the Peppermint essential oil microsphere using sodium alginate to be material is as follows:
(1) by 4%(w/v) sodium alginate soln, at water-bath 70 DEG C, add 0.1% CaCl2Appropriate (the 1000ml Sargassum of cross-linking agent
Acid sodium solution adds 40ml), after chelating 24h, under 121 DEG C of pyrolysis processing 15min, 30 DEG C of water-baths, survey its viscosity about
900mpa.s；
(2) under electric stirring, in sodium alginate glue, add pigment solution 15ml, add Peppermint essential oil 12ml；
(3) using coaxial air-flow method to prepare microsphere, air pressure is 0.020Mpa, and air-flow velocity is 5.0L/min, solidifies 0.5 hour,
Collecting microsphere, drying i.e. obtains Peppermint essential oil.
Embodiment 2
The preparation technology of the grapefruit essential oil microsphere using sodium alginate to be material is as follows:
(1) by 4%(w/v) sodium alginate soln, at water-bath 70 DEG C, add 0.1% CaCl2Appropriate (the 1000ml Sargassum of cross-linking agent
Acid sodium solution adds 50ml), after chelating 48h, under 121 DEG C of pyrolysis processing 15min, 30 DEG C of water-baths, survey its viscosity about
1400mpa.s；
(2) under electric stirring, in sodium alginate glue, add pigment solution 20ml, add grapefruit essential oil 15ml；
(3) using coaxial air-flow method to prepare microsphere, air pressure is 0.040Mpa, and air-flow velocity is 7.0L/min, solidifies 0.5 hour,
Collecting microsphere, drying i.e. obtains grapefruit essential oil microsphere.
Embodiment 3
The preparation technology of the Fructus Citri Limoniae quintessence oil microsphere using sodium alginate to be material is as follows:
(1) by 3%(w/v) sodium alginate soln, at water-bath 70 DEG C, add 0.1% CaCl2Appropriate (the 1000ml Sargassum of cross-linking agent
Acid sodium solution adds 45ml), after chelating 36h, under 30 DEG C of water-baths, survey its viscosity about 1500mpa.s；
(2) under electric stirring, in sodium alginate glue, add pigment solution 18ml, add Fructus Citri Limoniae quintessence oil 18ml；
(3) using coaxial air-flow method to prepare microsphere, air pressure is 0.030Mpa, and air-flow velocity is 6.0L/min, solidifies 0.5 hour,
Collecting microsphere, drying i.e. obtains Fructus Citri Limoniae quintessence oil microsphere.
Embodiment 4
The preparation technology of the Peppermint essential oil microsphere using gelatin to be material is as follows:
(1) by 25g gelatin, 50g water, 12.5g glycerol, it is completely dissolved in 60 DEG C of water-baths, obtained solution A；
(2) under fast stirring, in solution A, pigment solution 5g, Peppermint essential oil 3ml, obtained solution B after homogenizing are added；
(3) under 60 DEG C of water bath condition, solution B is poured slowly in the liquid paraffin that stirred, after stirring 10min, ice bath
Reducing temperature, be stirred for 30min, rotating speed is always maintained at 300rpm, stands, and settles microsphere, removes oil phase, with acetone repeatedly
Washing microsphere 2-3 time, leaches microsphere, and drying i.e. obtains Peppermint essential oil microsphere.
Embodiment 5
The preparation technology of the tea tree ethereal oil microsphere using gelatin to be material is as follows:
(1) by 25g gelatin, 50g water, 15g sorbitol, it is completely dissolved in 60 DEG C of water-baths, obtained solution A；
(2) under fast stirring, in solution A, pigment solution 4g, tea tree ethereal oil 5ml, obtained solution B after homogenizing are added；
(3) under 60 DEG C of water bath condition, solution B is poured slowly in the liquid paraffin that stirred, after stirring 10min, ice bath
Reducing temperature, be stirred for 30min, rotating speed is always maintained at 400rpm, stands, and settles microsphere, removes oil phase, with ethanol repeatedly
Washing microsphere 2-3 time, leaches microsphere, and drying i.e. obtains tea tree ethereal oil microsphere.
Embodiment 6
The preparation technology of the rosemary ethereal oil microsphere using gelatin to be material is as follows:
(1) by 25g gelatin, 50g water, 12.5g glycerol, it is completely dissolved in 60 DEG C of water-baths, obtained solution A；
(2) under fast stirring, in solution A, pigment solution 6g, rosemary ethereal oil 6ml, obtained solution B after homogenizing are added；
(3) under 60 DEG C of water bath condition, solution B is poured slowly in the liquid paraffin that stirred, after stirring 10min, ice bath
Reducing temperature, be stirred for 30min, rotating speed is always maintained at 500rpm, stands, and settles microsphere, removes oil phase, uses ethyl acetate
Cyclic washing microsphere 2-3 time, leaches microsphere, and drying i.e. obtains rosemary ethereal oil microsphere.
Quintessence oil microsphere embodiment 1-6 prepared is placed on wherein it is possible to slowly discharge quintessence oil when producing mask filter disc
Fragrance, there is refreshment, refrigerant effect releived.
Claims (5)
1., for a quintessence oil microsphere for mask filter disc, it is characterized by that the material of microsphere is sodium alginate or gelatin.
2., for the quintessence oil microsphere of mask filter disc, it is characterized by that the quintessence oil that microsphere wraps up is natural plant essential oils, including but
It is not limited in tea tree ethereal oil, rosemary ethereal oil, Fructus Citri Limoniae quintessence oil, Peppermint essential oil, grapefruit essential oil, eucalyptus oil, Flos Rosae Rugosae quintessence oil
One or more.
3. it is used for a preparation method for the quintessence oil microsphere of mask filter disc, it is characterized in that comprising the steps:
(1) by 4%(w/v) sodium alginate soln, at 70 DEG C, add appropriate 0.1% CaCl2Cross-linking agent, after chelating 24-48h, in
121 DEG C of pyrolysis processing, survey its viscosity about 800-1500mpa.s under 30 DEG C of water-baths；
(2) in stirring, in sodium alginate glue, pigment solution and plants essential oil it are sequentially added into；
(3) using coaxial air-flow method to prepare microsphere, regulation air pressure is 0.01-0.05Mpa, and air-flow velocity is 4.0-8.0L/min,
After solidification, collect microsphere, drying and get final product.
4. it is used for a preparation method for the quintessence oil microsphere of mask filter disc, it is characterized in that comprising the steps:
(1) by gelatin and appropriate plasticizer (glycerol or sorbitol), it is completely dissolved in 60 DEG C of water-baths, obtained solution A；
(2) under fast stirring, in solution A, pigment solution and plants essential oil it are sequentially added into, obtained solution B after homogenizing；
(3) under 60 DEG C of water bath condition, solution B is poured slowly in the liquid paraffin that stirred, after stirring a period of time, ice bath
Reduce temperature, be stirred for, keep constant rotational speed according to required microsphere size, stand, settle microsphere, remove oil phase, with acetone or
Ethanol or ethyl acetate cyclic washing microsphere, leach microsphere, drying and get final product.
5., for a quintessence oil microsphere for mask filter disc, it is characterized by that the purposes of described quintessence oil microsphere is for being placed on mask filter disc
In, distribute fragrance, have refreshment, refrigerant effect releived.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201610671671.XA CN106268553A (en) | 2016-08-16 | 2016-08-16 | A kind of quintessence oil microsphere for mask filter disc and preparation method thereof |
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| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201610671671.XA CN106268553A (en) | 2016-08-16 | 2016-08-16 | A kind of quintessence oil microsphere for mask filter disc and preparation method thereof |
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| CN106268553A true CN106268553A (en) | 2017-01-04 |
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| Application Number | Title | Priority Date | Filing Date |
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| CN201610671671.XA Pending CN106268553A (en) | 2016-08-16 | 2016-08-16 | A kind of quintessence oil microsphere for mask filter disc and preparation method thereof |
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Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN109567288A (en) * | 2018-12-18 | 2019-04-05 | 四川省乐至贵均卫生材料有限公司 | A kind of essential oil mask |
| CN110279178A (en) * | 2019-07-12 | 2019-09-27 | 广州禾安化工有限公司 | A kind of manufacture craft and application method of solid champignon essence oil mask |
| CN114515306A (en) * | 2022-03-23 | 2022-05-20 | 常州美杰医疗用品有限公司 | Nose-clearing essential oil patch and preparation method thereof |
-
2016
- 2016-08-16 CN CN201610671671.XA patent/CN106268553A/en active Pending
Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN109567288A (en) * | 2018-12-18 | 2019-04-05 | 四川省乐至贵均卫生材料有限公司 | A kind of essential oil mask |
| CN110279178A (en) * | 2019-07-12 | 2019-09-27 | 广州禾安化工有限公司 | A kind of manufacture craft and application method of solid champignon essence oil mask |
| CN114515306A (en) * | 2022-03-23 | 2022-05-20 | 常州美杰医疗用品有限公司 | Nose-clearing essential oil patch and preparation method thereof |
| CN114515306B (en) * | 2022-03-23 | 2023-03-10 | 常州美杰医疗用品有限公司 | Nose-clearing essential oil patch and preparation method thereof |
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Application publication date: 20170104 |
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| WD01 | Invention patent application deemed withdrawn after publication |