CN107362087A - A kind of baby powder that can be breathed and preparation method - Google Patents
A kind of baby powder that can be breathed and preparation method Download PDFInfo
- Publication number
- CN107362087A CN107362087A CN201710694406.8A CN201710694406A CN107362087A CN 107362087 A CN107362087 A CN 107362087A CN 201710694406 A CN201710694406 A CN 201710694406A CN 107362087 A CN107362087 A CN 107362087A
- Authority
- CN
- China
- Prior art keywords
- breathed
- baby powder
- preparation
- chinese medicine
- baby
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Withdrawn
Links
Classifications
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/58—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing atoms other than carbon, hydrogen, halogen, oxygen, nitrogen, sulfur or phosphorus
- A61K8/585—Organosilicon compounds
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q15/00—Anti-perspirants or body deodorants
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q17/00—Barrier preparations; Preparations brought into direct contact with the skin for affording protection against external influences, e.g. sunlight, X-rays or other harmful rays, corrosive materials, bacteria or insect stings
- A61Q17/005—Antimicrobial preparations
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
Landscapes
- Health & Medical Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Public Health (AREA)
- Veterinary Medicine (AREA)
- Animal Behavior & Ethology (AREA)
- General Health & Medical Sciences (AREA)
- Dermatology (AREA)
- Epidemiology (AREA)
- Birds (AREA)
- Engineering & Computer Science (AREA)
- Biotechnology (AREA)
- Botany (AREA)
- Microbiology (AREA)
- Mycology (AREA)
- Medicines Containing Material From Animals Or Micro-Organisms (AREA)
- Pharmaceuticals Containing Other Organic And Inorganic Compounds (AREA)
Abstract
Present invention relates particularly to baby skin protection product technical field, more particularly to a kind of baby powder that can be breathed and preparation method, the preparation method of the baby powder that can be breathed, comprises the following steps：（1）Honeysuckle, Radix Isatidis, chrysanthemum, blackberry lily are extracted, obtain Chinese medicine extract；（2）Chinese medicine extract is reacted with silicon source in a solvent, forms precursor liquid；（3）Added into precursor liquid in the alcoholic solvent of 1~10 times of volume, after stirring 1~120min, separate organic layer, it is then placed in spray dryer, decompression spray drying is carried out to precursor liquid, form the spherical subparticle of aerosil load heat-clearing activating agent, i.e., a kind of baby powder that can be breathed.The baby powder of the present invention not only has good absorbing sweat smoothness, and good with skin compatibility, clearing heat and detoxicating, prevents the sweat breed bacteria of absorption, and aeroge porosity characteristic has good respiratory protection effect to skin, avoids blocked pore.
Description
Technical field
Present invention relates particularly to baby skin protection product technical field, more particularly to a kind of baby powder that can be breathed and
Preparation method.
Background technology
Cosmetics are as the indispensable daily chemical product in life, and development is at full speed in recent years.China's cosmetics scale surpasses within 2015
Cross 150,000,000,000 yuan.China cosmetic foreign trade also develops rapidly, it has also become global cosmetics big trading nation.Working enterprise surpasses
Cross 5000.
With the growth of global Cosmetic Market and the continuous growth of consumer demand, in global cosmetics in the market
There are some new trend：1. environmental protection, with growing to even greater heights for global environmentally friendly cry, consumer is to consumer safety requirement
More and more higher；2. safety, the security of cosmetics is not only related to the physical and mental health of consumer, is also related to enterprise and industry
Final and decisive juncture；3. natural plants especially medicinal herb componentses；4. anti-aging and sun-proof；5. effect cosmetic.China cosmetic city
Field is shown according to employer's organization's statistics, in the coming years speed with annual 15% can be kept to increase.China has turned at present
The most potential Cosmetic Market in the whole world, the quick and sustainable growth of simultaneous China economy, cosmetic industry also turn into
One of industry with fastest developing speed in Chinese national economy.
The skin of infant is more tender and lovely, and thickness only has the 1/10 of adult skin, is rubbed or is easy to when stimulating
Breakage, the immunologic function of skin is also perfect without developing in addition, and resistance is weaker, is upset and is easy to produce inflammation.Baby children
Youngster uses diaper at that time, not to be easy to trigger diaper dermatitis.The red stern of diaper dermatitis, also referred to as diaper rash or baby, table
Now there is flush, fash in the skin for buttocks and diaper contact area, or even occurs festering and infect.In order to maintain Infant
Skin it is dry and comfortable, to prevent diaper dermatitis, generally infant after a bath after, talcum powder is applied to buttocks or the other portions of body
Position.Therefore, during infant is nursed, the use of talcum powder is very universal.
The talcum powder that most of children's talcum powder on the market mainly has talcum powder at present, pearl powder is main body.Its
In, the talcum powder based on talcum powder, its be aided with again zinc stearate, magnesium stearate, lanolin alcohol, glycerin monostearate,
Fibroin, SP, boric acid and essence are made, and this children's talcum powder is product very universal in the market.Talcum powder is by day
A kind of chemical powder that so mineral crystalline substance crushes and screens and air-flow crushing forms, is widely used in environment-friendly type coating, paint, adult
Cosmetics and children's talcum powder.But contain inseparable lead in talcum powder, and talcum powder is easily flown upward, and can be passed through in use
Mouth and nose are sucked, and because infant is weak for the excretory function of lead, lead can not be drained quickly after entering in infants.Infant
The μ g/L of internal blood lead >=100 be lead poisoning, and lead is accumulated when human body for a long time, will endanger neural, hemopoietic system and digestive system,
Have a strong impact on intelligence and the body development of infant.So the body of children's talcum powder based on talcum powder for infant
Body development is harmful.
Children's talcum powder based on pearl powder, it is aided with talcum powder, zinc oxide, zinc stearate, essence, peppermint again
Brain, peppermint oil, camphor, salicylic acid, stephanotis powder, ammonium glycyrrhetate, methyl hydroxybenzoate are made.The main component of pearl powder is carbonic acid
Calcium, respiratory tract is easily invaded, because the respiratory tract development of infant is not perfect, even if soakage can not lean on itself function less
Exclude.If soakage is more, the ciliary movement of bronchial ravages tracheae is invaded, phylactic power defensive power will be reduced, easily induce respiratory tract
Infection.Therefore, body development of children's talcum powder for infant based on pearl powder is still unsafe.
To sum up, above-mentioned talcum powder be by absorbing sweat, it is smooth for the purpose of, it is using that can cause sweat gland of skin to block, even
Breed bacteria, and using excessively, cutaneous respiration functional disturbance can be caused.Therefore, exploitation bioaffinity is good, adjusts skin work(
Energy, absorbing sweat, refreshing body significantly new talcum powder turn into existing talcum powder there is an urgent need to.
The content of the invention
Sweat gland of skin can be caused to block for current talcum powder, or even breed bacteria, and using excessively, skin can be caused to exhale
The deficiency of functional disturbance is inhaled, it is an object of the invention to provide a kind of bioaffinity is good, regulation skin function, absorbing sweat, refreshing body show
The baby powder of the meeting breathing of work.
To solve the above problems, the present invention uses following technical scheme：
A kind of preparation method for the baby powder that can be breathed, comprises the following steps：
（1）Honeysuckle, Radix Isatidis, chrysanthemum, blackberry lily are extracted, obtain Chinese medicine extract；
（2）Chinese medicine extract is reacted with silicon source in a solvent, forms precursor liquid；
（3）Added into precursor liquid in the alcoholic solvent of 1~10 times of volume, after stirring 1~120min, separate organic layer, Ran Houfang
Enter into spray dryer, decompression spray drying is carried out to precursor liquid, form aerosil load heat-clearing activating agent
Spherical subparticle, i.e., a kind of baby powder that can be breathed.
In the present invention, Chinese herbal medicine powder is added in talcum powder, makes talcum powder or have have moisturizing, refrigerant effect to skin
's；Or there is antipruritic, anti-inflammatory is antibacterial, it is smelly to dispel and suppress prickly heat regeneration effect；Or with to skin disease have prevention and
Auxiliary treatment functio etc., to meet the needs of infant.
Beneficiating ingredient in Chinese herbal medicine is the Chinese medicine factor for improving talcum powder effect, and the present invention to Chinese herbal medicine to by carrying out
Chinese herbal medicine beneficiating ingredient, is then added in talcum powder by extraction, and the present invention does not have special want to the extracting method of Chinese herbal medicine
Ask, can be such as institute known to one of ordinary skill in the art as long as the efficient extraction of Chinese herbal medicine beneficiating ingredient can be realized
The extracting method for stating Chinese medicine extract is super critical extraction, decocting cooking method, infusion process, percolation, Gelatin improving method, backflow
At least one of method, solvent extraction method, steam distillation and sublimed method.
In order to reduce production cost, the property of medicine of medicine is set to obtain maximum performance, it is preferred that the present invention uses water-boiling method centering
Herbal medicine is extracted, and the technique of the decocting cooking method is：
A, after cleaning up honeysuckle, Radix Isatidis, chrysanthemum, blackberry lily, add in 2 ~ 3 times of water, with 5 ~ 10 DEG C/min speed
80 ~ 100 DEG C are warming up to, after being then incubated 30 ~ 60min, 1 ~ 2 times of water is added, continues 1 ~ 3h of insulation, obtains Chinese medicine mixing
Thing, Traditional Chinese drug mixture is filtered, obtain decoction and the dregs of a decoction；
B, the dregs of a decoction are continued to decoct 2 times according to step A method, merges gained filtrate three times, obtain Chinese medicine extract.
Aerosil is the main component of talcum powder in the present invention, and silica has good bio-compatible
Property, it is the material that can be implanted into human body, therefore it has high security, silicon source is to prepare the important original of silica
Material；Contain substantial amounts of adsorption hole in aeroge, the sweat stain of skin surface can be absorbed, so as to keep skin dry and comfortable.
Preferably, the silicon source be MTMS, ethyl trimethoxy silane, propyl trimethoxy silicane,
Trimethoxysilane, octyl group trimethoxy silane, dimethyldimethoxysil,ne, MTES, ethyl
Triethoxysilane, propyl-triethoxysilicane, isobutyl triethoxy silane, octyltri-ethoxysilane, dodecyl three
Ethoxysilane, trimethylmethoxysilane, tetramethoxy-silicane, tetraethoxysilane, HMDS, hexamethyl two
At least one of siloxanes, VTES.
In the present invention, by the way that Chinese medicine extract is compound with aerosil, assigning silica talcum powder has
Herbal nature, and the content of Chinese herbal medicine is to influence another key factor of talcum powder performance, if Chinese medicine content is too low, is led
Cause the Chinese medicine effect of talcum powder extremely weak, it is impossible to play the effect to skin health care, and Chinese medicine too high levels, not only result in refreshing body
The smell of powder is more unpleasant, prevents infant colony from receiving, and drug effect may be made excessive, and injury is produced to infant, it is preferred that
The weight of the Chinese medicine extract and silicon source ratio is（30~80）：1.
Organic solvent is an important factor for gelation reaction occurs for silicon source, and the species of organic solvent directly determines that gelation is anti-
Whether can should carry out, it is preferred that heretofore described organic solvent is ethyl acetate, dichloromethane, chloroform, four chlorinations
At least one of carbon, tetrahydrofuran, petroleum ether, ether, hexamethylene, toluene, dimethylbenzene, 1,4- dioxane.
Preferably, in step（3）In, the alcoholic solvent is in methanol, ethanol, normal propyl alcohol, isopropanol, butanol and amylalcohol
It is at least one.
Solvent is volatilized by being spray-dried in the present invention, forms dry talcum powder, is spray-dried as the drying of routine
Means, therefore drying process is also for known to the art personnel, it is preferred that the technique of the spray drying is：Temperature is
60 ~ 100 DEG C, pressure -100 ~ 50KPa.
The present invention also provides a kind of baby powder that can be breathed, and is prepared according to above-mentioned preparation method.
The particle diameter of talcum powder is to influence another key factor of talcum powder effect when talcum powder particle diameter is excessive, then talcum powder
It can not adsorb in skin surface, easily be come off from skin, not have the effect of refreshing body, but also pore can be blocked, and refreshing body
The particle diameter of powder is too small, then dramatically increases manufacturing cost again, it is preferred that in the present invention, the particle diameter of the talcum powder is 200 ~ 375
Mesh.
A kind of baby powder that can be breathed of the present invention and preparation method, compared with prior art, the characteristics of it is protruded
It is with excellent effect：
Aerosil is the main component of talcum powder in the present invention, and silica has good biocompatibility, is
The material that can be implanted into human body, therefore it has high security, silicon source is to prepare the important source material of silica；Airsetting
Contain substantial amounts of adsorption hole in glue, the sweat stain of skin surface can be absorbed, so as to keep skin dry and comfortable, in addition, aeroge is porous
Characteristic has good respiratory protection effect to skin, avoids blocked pore.
Chinese herbal medicine powder is added in talcum powder, makes talcum powder or with having moisturizing, refrigerant effect to skin；Or there is town
It is bitterly antipruritic, anti-inflammatory is antibacterial, it is smelly to dispel and suppresses prickly heat regeneration effect；Or with to skin disease have prevention and auxiliary treatment functio
Etc., to meet the needs of infant.
Embodiment
Below by way of embodiment, the present invention is described in further detail, but this should not be interpreted as to the present invention
Scope be only limitted to following example.In the case where not departing from above method thought of the present invention, according to ordinary skill
The various replacements or change that knowledge and customary means are made, should be included in the scope of the present invention.
Embodiment 1
A kind of preparation method for the baby powder that can be breathed, comprises the following steps：
（1）After honeysuckle, Radix Isatidis, chrysanthemum, blackberry lily are cleaned up, add in 2 times of water, heated up with 5 DEG C/min speed
To 80 DEG C, after being then incubated 30min, 1 times of water is added, continues to be incubated 1h, Traditional Chinese drug mixture is obtained, by Traditional Chinese drug mixture mistake
Filter, obtains decoction and the dregs of a decoction；
The dregs of a decoction are continued according to the method described above to decoct 2 times, merges gained filtrate three times, obtains Chinese medicine extract；
（2）Chinese medicine extract is reacted in ethyl acetate with MTMS, forms precursor liquid；
（3）Added into precursor liquid in the methanol of 1 times of volume, after stirring 1min, separate organic layer, be then placed in spray drying
In machine, it is 60 DEG C, decompression spray drying is carried out to precursor liquid under pressure -100KPa in temperature, form aerosil and bear
Carry the spherical subparticle of heat-clearing activating agent, i.e., a kind of baby powder that can be breathed.
A diameter of 200 mesh of the baby powder of meeting breathing prepared by the present embodiment.
Embodiment 2
A kind of preparation method for the baby powder that can be breathed, comprises the following steps：
（1）After honeysuckle, Radix Isatidis, chrysanthemum, blackberry lily are cleaned up, add in 2 times of water, heated up with 5 DEG C/min speed
To 80 DEG C, after being then incubated 30min, 2 times of water is added, continues to be incubated 3h, Traditional Chinese drug mixture is obtained, by Traditional Chinese drug mixture mistake
Filter, obtains decoction and the dregs of a decoction；
The dregs of a decoction are continued according to the method described above to decoct 2 times, merges gained filtrate three times, obtains Chinese medicine extract；
（2）Chinese medicine extract is reacted in ethyl acetate with MTMS, forms precursor liquid；
（3）Added into precursor liquid in the methanol of 2 times of volumes, after stirring 20min, separate organic layer, it is dry to be then placed in spraying
In dry machine, it is 70 DEG C, decompression spray drying is carried out to precursor liquid under pressure -80KPa in temperature, form aerosil and bear
Carry the spherical subparticle of heat-clearing activating agent, i.e., a kind of baby powder that can be breathed.
A diameter of 210 mesh of the baby powder of meeting breathing prepared by the present embodiment.
Embodiment 3
A kind of preparation method for the baby powder that can be breathed, comprises the following steps：
（1）After honeysuckle, Radix Isatidis, chrysanthemum, blackberry lily are cleaned up, add in 2 times of water, heated up with 7 DEG C/min speed
To 85 DEG C, after being then incubated 45min, 2 times of water is added, continues to be incubated 2h, Traditional Chinese drug mixture is obtained, by Traditional Chinese drug mixture mistake
Filter, obtains decoction and the dregs of a decoction；
The dregs of a decoction are continued according to the method described above to decoct 2 times, merges gained filtrate three times, obtains Chinese medicine extract；
（2）Chinese medicine extract is reacted in dichloromethane with ethyl trimethoxy silane, forms precursor liquid；
（3）Added into precursor liquid in the ethanol of 3 times of volumes, after stirring 60min, separate organic layer, it is dry to be then placed in spraying
In dry machine, it is 80 DEG C, decompression spray drying is carried out to precursor liquid under pressure -10KPa in temperature, form aerosil and bear
Carry the spherical subparticle of heat-clearing activating agent, i.e., a kind of baby powder that can be breathed.
A diameter of 220 mesh of the baby powder of meeting breathing prepared by the present embodiment.
Embodiment 4
A kind of preparation method for the baby powder that can be breathed, comprises the following steps：
（1）After honeysuckle, Radix Isatidis, chrysanthemum, blackberry lily are cleaned up, add in 2 times of water, heated up with 8 DEG C/min speed
To 89 DEG C, after being then incubated 30 ~ 60min, 2 times of water is added, continues to be incubated 1h, obtains Traditional Chinese drug mixture, Chinese medicine is mixed
Thing filters, and obtains decoction and the dregs of a decoction；
The dregs of a decoction are continued according to the method described above to decoct 2 times, merges gained filtrate three times, obtains Chinese medicine extract；
（2）Chinese medicine extract is reacted in dichloromethane with ethyl trimethoxy silane, forms precursor liquid；
（3）Added into precursor liquid in the ethanol of 9 times of volumes, after stirring 118min, separate organic layer, it is dry to be then placed in spraying
In dry machine, it is 99 DEG C, decompression spray drying is carried out to precursor liquid under pressure -36KPa in temperature, form aerosil and bear
Carry the spherical subparticle of heat-clearing activating agent, i.e., a kind of baby powder that can be breathed.
A diameter of 236 mesh of the baby powder of meeting breathing prepared by the present embodiment.
Embodiment 5
A kind of preparation method for the baby powder that can be breathed, comprises the following steps：
（1）After honeysuckle, Radix Isatidis, chrysanthemum, blackberry lily are cleaned up, add in 2 times of water, heated up with 9 DEG C/min speed
To 100 DEG C, after being then incubated 60min, 1 times of water is added, continues to be incubated 3h, Traditional Chinese drug mixture is obtained, by Traditional Chinese drug mixture
Filtering, obtains decoction and the dregs of a decoction；
The dregs of a decoction are continued according to the method described above to decoct 2 times, merges gained filtrate three times, obtains Chinese medicine extract；
（2）Chinese medicine extract is reacted in chloroform with propyl trimethoxy silicane, forms precursor liquid；
（3）Added into precursor liquid in the normal propyl alcohol of 9 times of volumes, after stirring 100min, separate organic layer, be then placed in spraying
In drying machine, it is 90 DEG C, decompression spray drying is carried out to precursor liquid under pressure -1KPa in temperature, form aerosil
Load the spherical subparticle of heat-clearing activating agent, i.e., a kind of baby powder that can be breathed.
A diameter of 300 mesh of the baby powder of meeting breathing prepared by the present embodiment.
Comparative example 1
A kind of preparation method for the baby powder that can be breathed, comprises the following steps：
It will be reacted in ethyl acetate with MTMS, form precursor liquid；
Added into precursor liquid in the methanol of 1 times of volume, after stirring 1min, separate organic layer, be then placed in spray dryer
In, it is 60 DEG C, decompression spray drying is carried out to precursor liquid under pressure -100KPa in temperature, forms aerosil load
The spherical subparticle of heat-clearing activating agent, i.e., a kind of baby powder that can be breathed.
Comparative example 2
A kind of preparation method for the baby powder that can be breathed, comprises the following steps：
（1）After honeysuckle, Radix Isatidis, chrysanthemum, blackberry lily are cleaned up, add in 2 times of water, heated up with 5 DEG C/min speed
To 80 DEG C, after being then incubated 30min, 1 times of water is added, continues to be incubated 1h, Traditional Chinese drug mixture is obtained, by Traditional Chinese drug mixture mistake
Filter, obtains decoction and the dregs of a decoction；
The dregs of a decoction are continued according to the method described above to decoct 2 times, merges gained filtrate three times, obtains Chinese medicine extract；
（2）Chinese medicine extract is reacted in ethyl acetate with titanium dioxide, forms precursor liquid；
（3）Added into precursor liquid in the methanol of 1 times of volume, after stirring 1min, separate organic layer, be then placed in spray drying
In machine, it is 60 DEG C, decompression spray drying is carried out to precursor liquid under pressure -100KPa in temperature, form talcum powder.
Experiment 1：Water absorption rate test
By CN1946373A methods describeds, the talcum powder of embodiment 1 ~ 5 and comparative example 1 ~ 3 is quantified 0.5 gram respectively and is placed on glass
After on cotton, the closed container containing excess water is placed in, is then placed 24 hours under the conditions of 37 DEG C.By calculating on mineral wool
It is of poor quality before and after sample water suction, the final water absorption rate for obtaining sample, 1 is the results are shown in Table, the calculation formula of wherein water absorption rate is as follows：
Example weight × 100% before water absorption rate=(example weight before example weight-water suction after water suction)/water suction.
The bactericidal effect of experimental example 2 is tested
The talcum powder of embodiment 1 ~ 5 and comparative example 1 ~ 3 is subjected to bactericidal effect test：Random selection 50 plays miliaria degree identical
Volunteer, it is divided into 5 groups, every group of 10 people, same amount of embodiment 1-3 products and reference substance, continuous use is coated in respective affected part
One week, affected part healing state is observed, records patient satisfaction rate.As shown in table 1：
Table 1：
| Test event | Golden grape bacillus bacteriostasis rate（%） | Escherichia coli bacteriostasis rate（%） | Effective time（h） | Water absorption rate % |
| Embodiment 1 | 99.9 | 99.5 | 12 | 578 |
| Embodiment 2 | 99.8 | 99.1 | 12 | 559 |
| Embodiment 3 | 99.6 | 95.6 | 12 | 509 |
| Embodiment 4 | 95.1 | 98.1 | 6 | 498 |
| Embodiment 5 | 91.3 | 91.4 | 6 | 466 |
| Comparative example 1 | 56.3 | 38.1 | 2 | 41% |
| Comparative example 2 | 12.3 | 8.9 | 1.5 | 15% |
Claims (10)
1. a kind of preparation method for the baby powder that can be breathed, it is characterised in that comprise the following steps：
（1）Honeysuckle, Radix Isatidis, chrysanthemum, blackberry lily are extracted, obtain Chinese medicine extract；
（2）Chinese medicine extract is reacted with silicon source in a solvent, forms precursor liquid；
（3）Added into precursor liquid in the alcoholic solvent of 1~10 times of volume, after stirring 1~120min, separate organic layer, Ran Houfang
Enter into spray dryer, decompression spray drying is carried out to precursor liquid, form aerosil load heat-clearing activating agent
Spherical subparticle, i.e., a kind of baby powder that can be breathed.
2. the preparation method of the baby powder according to claim 1 that can be breathed, it is characterised in that the Chinese medicine carries
The extracting method for taking liquid is super critical extraction, decocting cooking method, infusion process, percolation, Gelatin improving method, circumfluence method, solvent carry
Follow the example of, at least one of steam distillation and sublimed method.
3. the preparation method of the baby powder according to claim 2 that can be breathed, it is characterised in that the decocting is boiled
The technique of method is：
A, after cleaning up honeysuckle, Radix Isatidis, chrysanthemum, blackberry lily, add in 2 ~ 3 times of water, with 5 ~ 10 DEG C/min speed
80 ~ 100 DEG C are warming up to, after being then incubated 30 ~ 60min, 1 ~ 2 times of water is added, continues 1 ~ 3h of insulation, obtains Chinese medicine mixing
Thing, Traditional Chinese drug mixture is filtered, obtain decoction and the dregs of a decoction；
B, the dregs of a decoction are continued to decoct 2 times according to step A method, merges gained filtrate three times, obtain Chinese medicine extract.
4. the preparation method of the baby powder according to claim 1 that can be breathed, it is characterised in that the silicon source is
MTMS, ethyl trimethoxy silane, propyl trimethoxy silicane, trimethoxysilane, octyl group three
Methoxy silane, dimethyldimethoxysil,ne, MTES, ethyl triethoxysilane, propyl triethoxy
Silane, isobutyl triethoxy silane, octyltri-ethoxysilane, dodecyl triethoxysilane, trimethyl methoxy silicon
Alkane, tetramethoxy-silicane, tetraethoxysilane, HMDS, HMDO, VTES
At least one of.
5. the preparation method of the baby powder according to claim 1 that can be breathed, it is characterised in that the Chinese medicine carries
The weight of the liquid and silicon source ratio is taken to be（30~80）：1.
6. the preparation method of the baby powder according to claim 1 that can be breathed, it is characterised in that described organic molten
Agent is ethyl acetate, dichloromethane, chloroform, carbon tetrachloride, tetrahydrofuran, petroleum ether, ether, hexamethylene, toluene, diformazan
At least one of benzene, 1,4- dioxane.
7. the preparation method of the baby powder according to claim 1 that can be breathed, it is characterised in that in step（3）
In, the alcoholic solvent is at least one of methanol, ethanol, normal propyl alcohol, isopropanol, butanol and amylalcohol.
8. the preparation method of the baby powder according to claim 7 that can be breathed, it is characterised in that the spraying is dry
Dry technique is：Temperature is 60 ~ 100 DEG C, pressure -100 ~ 50KPa.
9. a kind of baby powder that can be breathed, it is characterised in that according to the preparation side described in claim 1 ~ 8 any one
Method is prepared.
10. the baby powder according to claim 9 that can be breathed, it is characterised in that its particle diameter is 200 ~ 375 mesh.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201710694406.8A CN107362087A (en) | 2017-08-15 | 2017-08-15 | A kind of baby powder that can be breathed and preparation method |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201710694406.8A CN107362087A (en) | 2017-08-15 | 2017-08-15 | A kind of baby powder that can be breathed and preparation method |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN107362087A true CN107362087A (en) | 2017-11-21 |
Family
ID=60309683
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201710694406.8A Withdrawn CN107362087A (en) | 2017-08-15 | 2017-08-15 | A kind of baby powder that can be breathed and preparation method |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN107362087A (en) |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN108309823A (en) * | 2018-03-22 | 2018-07-24 | 徐增强 | A kind of baby talcum powder and preparation method thereof |
Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1569033A (en) * | 2003-04-28 | 2005-01-26 | 莱雅公司 | Cosmetic composition comprising a sebum-absorbing powder and a powder with a low critical surface energy |
| CN101652320A (en) * | 2007-03-30 | 2010-02-17 | 株式会社高丝 | Granulated silica particle, composite powder, their production methods, and cosmetic preparation containing them |
| CN101690503A (en) * | 2009-10-12 | 2010-04-07 | 何丹凤 | Chinese herbal medicine health-care joss stick |
| CN102167337A (en) * | 2011-03-21 | 2011-08-31 | 冷水江三A化工有限责任公司 | Silicon dioxide aerogel and preparation method thereof |
-
2017
- 2017-08-15 CN CN201710694406.8A patent/CN107362087A/en not_active Withdrawn
Patent Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1569033A (en) * | 2003-04-28 | 2005-01-26 | 莱雅公司 | Cosmetic composition comprising a sebum-absorbing powder and a powder with a low critical surface energy |
| CN101652320A (en) * | 2007-03-30 | 2010-02-17 | 株式会社高丝 | Granulated silica particle, composite powder, their production methods, and cosmetic preparation containing them |
| CN101690503A (en) * | 2009-10-12 | 2010-04-07 | 何丹凤 | Chinese herbal medicine health-care joss stick |
| CN102167337A (en) * | 2011-03-21 | 2011-08-31 | 冷水江三A化工有限责任公司 | Silicon dioxide aerogel and preparation method thereof |
Non-Patent Citations (2)
| Title |
|---|
| 米歇尔•安德烈•埃杰尔特: "《气凝胶手册》", 31 December 2014 * |
| 陈照峰: "《无机非金属材料学》", 31 March 2010 * |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN108309823A (en) * | 2018-03-22 | 2018-07-24 | 徐增强 | A kind of baby talcum powder and preparation method thereof |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| CN104530777A (en) | Healthcare interior wall coating material and preparation method thereof | |
| CN102935245A (en) | Wind-cold dispelling incense | |
| CN105030016A (en) | Chinaberry bark carpet with air purifying function | |
| CN102817091A (en) | Nanometer selenium germanium negative-ion far-infrared anti-mite electromagnetic-shielding fabric clothes for treating apoplectic hemiplegia | |
| CN108403589A (en) | Natural plants face cream | |
| KR101854342B1 (en) | Manufacturing method of mask pack for blocking and removing ultra-fine particles and the mask pack produced therefrom | |
| CN108142986A (en) | A kind of Chinese herbal medicine composite extract, preparation method and its application in cigarette | |
| CN107362087A (en) | A kind of baby powder that can be breathed and preparation method | |
| CN103027881A (en) | Daily use chemical article with antibacterial and calleidic efficacies | |
| CN101836920A (en) | Far infrared active oxygen & anion sanitary towel and sanitary pad | |
| CN104188872A (en) | Environmental protection moisture type water-based nail polish and preparation method thereof | |
| CN104547682B (en) | A kind of composition of effect of relievining asthma that wet one's whistle with removing heat from the lung and relieving sorethroat | |
| CN105726363A (en) | Plant care composition and preparation method thereof | |
| CN105250385A (en) | Nasal drops for treating infant nasal obstruction | |
| CN104957952B (en) | There is the rhamnus crenata sieb.et zucc. carpet of health care function of driving mosquitoes | |
| CN105435275A (en) | Combined formula of lemon blended fragrant essential oil | |
| CN114515324A (en) | Traditional Chinese medicine epidemic prevention aromatherapy composition and product thereof | |
| CN105687353A (en) | Pharmaceutical composition for infantile erythema glutealis and preparation method thereof | |
| CN110179718A (en) | A kind of anthosin droplet dew for purifying skin of refreshing oneself and preparation method thereof | |
| CN104957950B (en) | Novel desmodium triquetrum anion health care type carpet | |
| CN109288762A (en) | A kind of baby's peach leaf is felt well body dew and preparation method thereof | |
| CN104274856A (en) | Incense for improving haze air and preparation method thereof | |
| CN108096491A (en) | It is a kind of using borneol cinnamomum camphora as the fragrant plant stacte and its preparation process of monarch | |
| KR102266870B1 (en) | A relax doll | |
| CN106563143A (en) | Environment-friendly air freshener |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| PB01 | Publication | ||
| PB01 | Publication | ||
| SE01 | Entry into force of request for substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| WW01 | Invention patent application withdrawn after publication | ||
| WW01 | Invention patent application withdrawn after publication |
Application publication date: 20171121 |