CN110339099A - A kind of perfume that aesthetics is good - Google Patents

A kind of perfume that aesthetics is good Download PDF

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Publication number
CN110339099A
CN110339099A CN201910771082.2A CN201910771082A CN110339099A CN 110339099 A CN110339099 A CN 110339099A CN 201910771082 A CN201910771082 A CN 201910771082A CN 110339099 A CN110339099 A CN 110339099A
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CN
China
Prior art keywords
parts
perfume
ethyl alcohol
oil
water
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Pending
Application number
CN201910771082.2A
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Chinese (zh)
Inventor
楼炳吐
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Story Of Love Cosmetic Co Ltd
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Story Of Love Cosmetic Co Ltd
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Priority to CN201910771082.2A priority Critical patent/CN110339099A/en
Publication of CN110339099A publication Critical patent/CN110339099A/en
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    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/19Cosmetics or similar toiletry preparations characterised by the composition containing inorganic ingredients
    • A61K8/26Aluminium; Compounds thereof
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/92Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof
    • A61K8/922Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof of vegetable origin
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61QSPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q13/00Formulations or additives for perfume preparations

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  • Life Sciences & Earth Sciences (AREA)
  • Health & Medical Sciences (AREA)
  • Veterinary Medicine (AREA)
  • Animal Behavior & Ethology (AREA)
  • General Health & Medical Sciences (AREA)
  • Public Health (AREA)
  • Birds (AREA)
  • Epidemiology (AREA)
  • Chemical & Material Sciences (AREA)
  • Inorganic Chemistry (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Cosmetics (AREA)
  • Medicines Containing Plant Substances (AREA)

Abstract

A kind of perfume that aesthetics is good, the Lavender that the present invention is added has soothes the spirit well, it is with all worries set aside, help sleep, it releives pressure, gentle mood, there is sedation effect to heart, hypertension can be reduced, pacify palpitaition, analgesic, promote cytothesis, enhance memory, improve congested, edema, antibacterial, antirheumatic, analgesic, tighten skin, stimulate the effect of hair growth, Peppermint essential oil has cool refreshing, pacify soul, it relieves fatigue, beneficial to respiratory disease, tea tree ethereal oil, which has, refreshes oneself, aligning border, bactericidal antiphlogistic, treat acne, shrinkable pore, Bergamot Mint Extract, clean skin, eucalyptus quintessence oil has restoring consciouness, refresh oneself, it focuses on, synthetic fluorophlogopite can increase cosmetics brightness, it will increase skin texture and sense of touch after use, it will not be absorbed by the skin, skin will not be caused due to being minerals What injury, primarily to the visual effect that enhancing cosmetics are glittering.

Description

A kind of perfume that aesthetics is good
Technical field
The present invention relates to show device field, the good perfume of specially a kind of aesthetics.
Background technique
Perfume is a kind of liquid for being mixed with essential oil, fixative and alcohol or ethyl acetate, for allow object (usually Human body) possess the smell of lasting and happy people.Essential oil is taken from flowers and plants plant, inhales method extraction with the way of distillation or rouge, can also make With fragrant organic matter.Time immemorial people just uses fragrance to change human scent, and fragrance uses and uses and unite as upper layer The patent for the person of controlling.People constantly create more novel more unique essence, so that a part in the perfume world is constituted, this tide Stream has become the mark in the epoch of our lives.
There are certain unicity for existing perfume performance, have been unable to satisfy the demand of people, while being transparency liquid Or colored liquid, it is more dull, it has been unable to satisfy pursuit of the people to beauty.
Summary of the invention
For above situation, to overcome the shortcomings of existing technologies, the present invention provides a kind of perfume that aesthetics is good, effectively It solves the problems, such as to propose in technical background.
To achieve the above object, the invention provides the following technical scheme: the present invention perfume by following weight proportion original Material is made: 45-50 parts of ethyl alcohol, 9-10 parts of water, 6-7 parts of essence, 0.6-1 parts of propylene glycol, 0.5-1 parts of sodium citrate, hydrogenated castor 0.2-0.3 parts oily, 0.08-0.1 parts of synthetic fluorophlogopite, 3-11 parts of Peppermint essential oil, 1-5 parts of citric acid, smokes clothing at 2-10 parts of glycerol Careless essential oil 3-5 parts, 4-5 parts of Rosemary Oil, 5-6 parts of tea tree ethereal oil and 3-5 parts of eucalyptus quintessence oil;
The perfume the preparation method comprises the following steps: 1) alcohol pre-treatment, pre-processes ethyl alcohol using method of purification and ageing method;
2) water is distilled in water pretreatment, and temperature is controlled at 100 degrees Celsius, and sodium citrate is added into water, distills Bacterium in water is removed, the sodium citrate of addition removes the metal ion in water;
3) essence pre-processes, and a small amount of pretreated ethyl alcohol is added in essence, and ageing uses after one month;
4) it mixes, takes 45-50 parts of ethyl alcohol, 9-10 parts of water, 6-7 parts of essence, 0.6-1 parts of propylene glycol, rilanit special 0.2- 0.3 part, 0.08-0.1 parts of synthetic fluorophlogopite, 2-10 parts of glycerol, 3-11 parts of Peppermint essential oil, 1-5 parts of citric acid, Lavender 3-5 parts, 4-5 parts of Rosemary Oil, 5-6 parts of tea tree ethereal oil and 3-5 parts of eucalyptus quintessence oil are put into stainless steel and are stirred container Interior, revolving speed control is stirred 30 minutes in 200r/min, and stands 3 hours, and the clear mixture in static back upper place is poured out;
5) it is aged, 4) clarified mixture poured out is poured into stirring container, for control revolving speed in 400r/min, stirring 2 is small When, stop stirring, pours into closed container and be aged 3 months;
6) it filters, the liquid after ageing is poured into filter press, finished product can be obtained after the sediment after ageing is filtered out.
According to the above technical scheme: the purification process of the ethyl alcohol are as follows: add alkali circumfluence method and potassium permanganate oxidation in ethyl alcohol Method removes impurity, then sodium hydroxide is added into ethyl alcohol, after boiling reflux a few hours, then through one or many fractionation, after collection It can be used to prepare perfume.
According to the above technical scheme: the operating method of the potassium permanganate oxidation method are as follows: potassium permanganate is added into ethyl alcohol Solution, stirring is stood after five minutes rapidly, filters off precipitating, adds active carbon, after placing a couple of days, is filtered using silica gel, into one Step absorbs impurity, can be used to prepare perfume after the completion of processing.
According to the above technical scheme: the method for the ageing are as follows: be put into a small amount of essence in ethyl alcohol after purification, taken the photograph 15 Sealing placement 2 months can be spare under family name's degree.
According to the above technical scheme: diatomite being added into filter press when the step 6) filters pressing.
The Lavender that the present invention is added, which has, soothes the spirit well, sets aside all worries, helping sleep, and pressure of releiving, gentle mood are right Heart has sedation effect, can reduce hypertension, pacifies palpitaition, analgesic, promotes cytothesis, balances sebum secretion, treatment scald And bite by mosquitos, Rosemary Oil, which has, adjusts psychosoma, and restoring consciouness enhances memory, improve congested, edema, antibacterial, antirheumatic, Skin is tightened in analgesic, stimulates the effect of hair growth, and Peppermint essential oil has cool refreshing, pacifies soul, relieve fatigue, beneficial to Respiratory disease, analgesia are alleviated limb swelling, are helped digest, toxin expelling decontamination, and blackhead is removed, and sebum secretion is adjusted, and fit For oily skin, tea tree ethereal oil have refresh oneself, aligning border, bactericidal antiphlogistic, treat acne, shrinkable pore, Sage Extract point It secretes, clean skin, eucalyptus quintessence oil has restoring consciouness, refreshes oneself, and focuses on, and promotes vigor, can alleviate arthritis and rheumatalgia, has There is the effects of eliminating the phlegm, hypoglycemic, antipyretic, toxin expelling, promote wound healing, treats skin infection, improve the effect of the skin of obstruction, Synthetic fluorophlogopite can increase cosmetics brightness, will increase skin texture and sense of touch after use, will not be absorbed by the skin, due to It is that minerals will not cause anything to injure skin, primarily to the visual effect that enhancing cosmetics are glittering.
Detailed description of the invention
Attached drawing is used to provide further understanding of the present invention, and constitutes part of specification, with reality of the invention It applies example to be used to explain the present invention together, not be construed as limiting the invention.In the accompanying drawings:
Fig. 1 is flow diagram of the present invention.
Specific embodiment
1 pair of a specific embodiment of the invention is described in further details with reference to the accompanying drawing.
Embodiment one, is provided by Fig. 1, and the present invention provides a kind of perfume that aesthetics is good, and the perfume is by following weight proportion Raw material be made: 45-50 parts of ethyl alcohol, 9-10 parts of water, 6-7 parts of essence, 0.6-1 parts of propylene glycol, 0.5-1 parts of sodium citrate, hydrogenation 0.2-0.3 parts of castor oil, 0.08-0.1 parts of synthetic fluorophlogopite, 2-10 parts of glycerol, 3-11 parts of Peppermint essential oil, 1-5 parts of citric acid, 3-5 parts of Lavender, 4-5 parts of Rosemary Oil, 5-6 parts of tea tree ethereal oil and 3-5 parts of eucalyptus quintessence oil;
The perfume the preparation method comprises the following steps: 1) alcohol pre-treatment, pre-processes ethyl alcohol using method of purification and ageing method;
2) water is distilled in water pretreatment, and temperature is controlled at 100 degrees Celsius, and sodium citrate is added into water, distills Bacterium in water is removed, the sodium citrate of addition removes the metal ion in water;
3) essence pre-processes, and a small amount of pretreated ethyl alcohol is added in essence, and ageing uses after one month;
4) it mixes, takes 45 parts of ethyl alcohol, 9 parts of water, 6 parts of essence, 0.6 part of propylene glycol, 0.2 part of rilanit special, synthesis fluorine gold 0.08 part of mica, 2 parts of glycerol, 3 parts of Peppermint essential oil, 1 part of citric acid, 3 parts of Lavender, 4 parts of Rosemary Oil, tea tree ethereal oil 5 parts and 3 parts of eucalyptus quintessence oil are put into stainless steel and are stirred in container, and revolving speed control is stirred 30 minutes in 200r/min, And 3 hours are stood, the clear mixture in static back upper place is poured out;
5) it is aged, 4) clarified mixture poured out is poured into stirring container, for control revolving speed in 400r/min, stirring 2 is small When, stop stirring, pours into closed container and be aged 3 months;
6) it filters, the liquid after ageing is poured into filter press, finished product can be obtained after the sediment after ageing is filtered out.
The purification process of the ethyl alcohol are as follows: add alkali circumfluence method and potassium permanganate oxidation method in ethyl alcohol, remove impurity, then Xiang Yi Sodium hydroxide is added in alcohol, after boiling reflux a few hours, then through one or many fractionation, can be used to prepare perfume after collection.
The operating method of the potassium permanganate oxidation method are as follows: liquor potassic permanganate is added into ethyl alcohol, rapidly stirring 5 minutes After stand, filter off precipitating, add active carbon, after placing a couple of days, filtered using silica gel, further absorb impurity, handled At it is rear i.e. can be used to prepare perfume.
The method of the ageing are as follows: a small amount of essence is put into ethyl alcohol after purification, sealing places 2 under 15 degrees Celsius The moon can be spare.
Diatomite is added into filter press when the step 6) filters pressing.
Embodiment two, is provided by Fig. 1, and the present invention provides a kind of perfume that aesthetics is good, and the perfume is by following weight proportion Raw material be made: 45-50 parts of ethyl alcohol, 9-10 parts of water, 6-7 parts of essence, 0.6-1 parts of propylene glycol, 0.5-1 parts of sodium citrate, hydrogenation 0.2-0.3 parts of castor oil, 0.08-0.1 parts of synthetic fluorophlogopite, 2-10 parts of glycerol, 3-11 parts of Peppermint essential oil, 1-5 parts of citric acid, 3-5 parts of Lavender, 4-5 parts of Rosemary Oil, 5-6 parts of tea tree ethereal oil and 3-5 parts of eucalyptus quintessence oil;
The perfume the preparation method comprises the following steps: 1) alcohol pre-treatment, pre-processes ethyl alcohol using method of purification and ageing method;
2) water is distilled in water pretreatment, and temperature is controlled at 100 degrees Celsius, and sodium citrate is added into water, distills Bacterium in water is removed, the sodium citrate of addition removes the metal ion in water;
3) essence pre-processes, and a small amount of pretreated ethyl alcohol is added in essence, and ageing uses after one month;
4) it mixes, perfume is prepared from the following raw materials in parts by weight: 47 parts of ethyl alcohol, 9.5 parts of water, 6.5 parts of essence, propylene glycol 0.8 part, 0.25 part of rilanit special, 0.09 part of synthetic fluorophlogopite, 6 parts of glycerol, 7 parts of Peppermint essential oil, 3.5 parts of citric acid, smoke 4 parts of clothing grass essential oil, 4.5 parts of Rosemary Oil, 5.5 parts of tea tree ethereal oil and 4 parts of eucalyptus quintessence oil are put into stainless steel and are stirred In container, revolving speed control is stirred 30 minutes in 200r/min, and stands 3 hours, and the clear mixture in static back upper place is fallen Out;
5) it is aged, 4) clarified mixture poured out is poured into stirring container, for control revolving speed in 400r/min, stirring 2 is small When, stop stirring, pours into closed container and be aged 3 months;
6) it filters, the liquid after ageing is poured into filter press, finished product can be obtained after the sediment after ageing is filtered out.
The purification process of the ethyl alcohol are as follows: add alkali circumfluence method and potassium permanganate oxidation method in ethyl alcohol, remove impurity, then Xiang Yi Sodium hydroxide is added in alcohol, after boiling reflux a few hours, then through one or many fractionation, can be used to prepare perfume after collection.
The operating method of the potassium permanganate oxidation method are as follows: liquor potassic permanganate is added into ethyl alcohol, rapidly stirring 5 minutes After stand, filter off precipitating, add active carbon, after placing a couple of days, filtered using silica gel, further absorb impurity, handled At it is rear i.e. can be used to prepare perfume.
The method of the ageing are as follows: a small amount of essence is put into ethyl alcohol after purification, sealing places 2 under 15 degrees Celsius The moon can be spare.
Diatomite is added into filter press when the step 6) filters pressing.
Embodiment three, is provided by Fig. 1, and the present invention provides a kind of perfume that aesthetics is good, and the perfume is by following weight proportion Raw material be made: 45-50 parts of ethyl alcohol, 9-10 parts of water, 6-7 parts of essence, 0.6-1 parts of propylene glycol, 0.5-1 parts of sodium citrate, hydrogenation 0.2-0.3 parts of castor oil, 0.08-0.1 parts of synthetic fluorophlogopite, 2-10 parts of glycerol, 3-11 parts of Peppermint essential oil, 1-5 parts of citric acid, 3-5 parts of Lavender, 4-5 parts of Rosemary Oil, 5-6 parts of tea tree ethereal oil and 3-5 parts of eucalyptus quintessence oil;
The perfume the preparation method comprises the following steps: 1) alcohol pre-treatment, pre-processes ethyl alcohol using method of purification and ageing method;
2) water is distilled in water pretreatment, and temperature is controlled at 100 degrees Celsius, and sodium citrate is added into water, distills Bacterium in water is removed, the sodium citrate of addition removes the metal ion in water;
3) essence pre-processes, and a small amount of pretreated ethyl alcohol is added in essence, and ageing uses after one month;
4) it mixes, takes 50 parts of ethyl alcohol, 10 parts of water, 7 parts of essence, 1 part of propylene glycol, 0.3 part of rilanit special, synthesis fluorine gold cloud Female 0.1 part, 10 parts of glycerol, 11 parts of Peppermint essential oil, 5 parts of citric acid, 5 parts of Lavender, 5 parts of Rosemary Oil, tea tree ethereal oil 6 Part is put into stainless steel with 5 parts of eucalyptus quintessence oil and is stirred in container, and revolving speed control is stirred 30 minutes in 200r/min, And 3 hours are stood, the clear mixture in static back upper place is poured out;
5) it is aged, 4) clarified mixture poured out is poured into stirring container, for control revolving speed in 400r/min, stirring 2 is small When, stop stirring, pours into closed container and be aged 3 months;
6) it filters, the liquid after ageing is poured into filter press, finished product can be obtained after the sediment after ageing is filtered out.
The purification process of the ethyl alcohol are as follows: add alkali circumfluence method and potassium permanganate oxidation method in ethyl alcohol, remove impurity, then Xiang Yi Sodium hydroxide is added in alcohol, after boiling reflux a few hours, then through one or many fractionation, can be used to prepare perfume after collection.
The operating method of the potassium permanganate oxidation method are as follows: liquor potassic permanganate is added into ethyl alcohol, rapidly stirring 5 minutes After stand, filter off precipitating, add active carbon, after placing a couple of days, filtered using silica gel, further absorb impurity, handled At it is rear i.e. can be used to prepare perfume.
The method of the ageing are as follows: a small amount of essence is put into ethyl alcohol after purification, sealing places 2 under 15 degrees Celsius The moon can be spare.
Diatomite is added into filter press when the step 6) filters pressing.
Experimental example:
Experimental subjects: referring to the required standard of QB/T 1858-93 standard index, respectively to one institute of the embodiment of the present invention Perfume obtained, perfume obtained by embodiment two, perfume obtained by embodiment three carry out performance detection
Experiment purpose: under the same conditions, the performance of each group perfume is tested, testing standard is all satisfied.
The Lavender that the present invention is added, which has, soothes the spirit well, sets aside all worries, helping sleep, and pressure of releiving, gentle mood are right Heart has sedation effect, can reduce hypertension, pacifies palpitaition, analgesic, promotes cytothesis, balances sebum secretion, treatment scald And bite by mosquitos, Rosemary Oil, which has, adjusts psychosoma, and restoring consciouness enhances memory, improve congested, edema, antibacterial, antirheumatic, Skin is tightened in analgesic, stimulates the effect of hair growth, and Peppermint essential oil has cool refreshing, pacifies soul, relieve fatigue, beneficial to Respiratory disease, analgesia are alleviated limb swelling, are helped digest, toxin expelling decontamination, and blackhead is removed, and sebum secretion is adjusted, and fit For oily skin, tea tree ethereal oil have refresh oneself, aligning border, bactericidal antiphlogistic, treat acne, shrinkable pore, Sage Extract point It secretes, clean skin, eucalyptus quintessence oil has restoring consciouness, refreshes oneself, and focuses on, and promotes vigor, can alleviate arthritis and rheumatalgia, has There is the effects of eliminating the phlegm, hypoglycemic, antipyretic, toxin expelling, promote wound healing, treats skin infection, improve the effect of the skin of obstruction, Synthetic fluorophlogopite can increase cosmetics brightness, will increase skin texture and sense of touch after use, will not be absorbed by the skin, due to It is that minerals will not cause anything to injure skin, primarily to the visual effect that enhancing cosmetics are glittering.
Finally, it should be noted that the foregoing is only a preferred embodiment of the present invention, it is not intended to restrict the invention, Although the present invention is described in detail referring to the foregoing embodiments, for those skilled in the art, still may be used To modify the technical solutions described in the foregoing embodiments or equivalent replacement of some of the technical features. All within the spirits and principles of the present invention, any modification, equivalent replacement, improvement and so on should be included in of the invention Within protection scope.

Claims (5)

1. a kind of good perfume of aesthetics, it is characterised in that: the perfume is prepared from the following raw materials in parts by weight: ethyl alcohol 45-50 Part, 9-10 parts of water, 6-7 parts of essence, 0.6-1 parts of propylene glycol, 0.5-1 parts of sodium citrate, 0.2-0.3 parts of rilanit special, synthesis 0.08-0.1 parts of fluorophologopite, 2-10 parts of glycerol, 3-11 parts of Peppermint essential oil, 1-5 parts of citric acid, 3-5 parts of Lavender, fan change 4-5 parts of essential oil, 5-6 parts of tea tree ethereal oil and 3-5 parts of eucalyptus quintessence oil;
The perfume the preparation method comprises the following steps: 1) alcohol pre-treatment, pre-processes ethyl alcohol using method of purification and ageing method;
2) water is distilled in water pretreatment, and temperature is controlled at 100 degrees Celsius, and sodium citrate is added into water, distills water In bacterium remove, the sodium citrate of addition removes the metal ion in water;
3) essence pre-processes, and a small amount of pretreated ethyl alcohol is added in essence, and ageing uses after one month;
4) it mixes, takes 45-50 parts of ethyl alcohol, 9-10 parts of water, 6-7 parts of essence, 0.6-1 parts of propylene glycol, rilanit special 0.2-0.3 Part, 0.08-0.1 parts of synthetic fluorophlogopite, 2-10 parts of glycerol, 3-11 parts of Peppermint essential oil, 1-5 parts of citric acid, Lavender 3-5 Part, 4-5 parts of Rosemary Oil, 5-6 parts of tea tree ethereal oil and 3-5 parts of eucalyptus quintessence oil are put into stainless steel and are stirred in container, Revolving speed control is stirred 30 minutes in 200r/min, and stands 3 hours, and the clear mixture in static back upper place is poured out;
5) it being aged, 4) clarified mixture poured out is poured into stirring container, control revolving speed stirred 2 as a child in 400r/min, Stop stirring, pours into closed container and be aged 3 months;
6) it filters, the liquid after ageing is poured into filter press, finished product can be obtained after the sediment after ageing is filtered out.
2. a kind of good perfume of aesthetics according to claim 1, which is characterized in that the purification process of the ethyl alcohol are as follows: Add alkali circumfluence method and potassium permanganate oxidation method in ethyl alcohol, removes impurity, then sodium hydroxide is added into ethyl alcohol, boiling reflux number is small Shi Hou, then through one or many fractionation, can be used to prepare perfume after collection.
3. a kind of good perfume of aesthetics according to claim 2, which is characterized in that the behaviour of the potassium permanganate oxidation method Make method are as follows: liquor potassic permanganate is added into ethyl alcohol, stirring is stood after five minutes rapidly, and precipitating is filtered off, active carbon is added, It after placing a couple of days, is filtered using silica gel, further absorbs impurity, can be used to prepare perfume after the completion of processing.
4. a kind of good perfume of aesthetics according to claim 1, which is characterized in that the method for the ageing are as follows: pure A small amount of essence is put into ethyl alcohol after change, sealing placement 2 months can be spare under 15 degrees Celsius.
5. a kind of good perfume of aesthetics according to claim 1, which is characterized in that filters pressing when the step 6) filters pressing Diatomite is added in machine.
CN201910771082.2A 2019-08-20 2019-08-20 A kind of perfume that aesthetics is good Pending CN110339099A (en)

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Application Number Priority Date Filing Date Title
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Application Number Priority Date Filing Date Title
CN201910771082.2A CN110339099A (en) 2019-08-20 2019-08-20 A kind of perfume that aesthetics is good

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Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN111937913A (en) * 2020-08-24 2020-11-17 广州艺境环保科技有限公司 Disinfecting and sterilizing aromatic liquid and preparation method thereof
CN112438909A (en) * 2020-12-08 2021-03-05 黄精钢 Perfume with small skin irritation and long persistence time and preparation process thereof

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN111937913A (en) * 2020-08-24 2020-11-17 广州艺境环保科技有限公司 Disinfecting and sterilizing aromatic liquid and preparation method thereof
CN112438909A (en) * 2020-12-08 2021-03-05 黄精钢 Perfume with small skin irritation and long persistence time and preparation process thereof

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Application publication date: 20191018