CN111937913A - Disinfecting and sterilizing aromatic liquid and preparation method thereof - Google Patents
Disinfecting and sterilizing aromatic liquid and preparation method thereof Download PDFInfo
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- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N65/00—Biocides, pest repellants or attractants, or plant growth regulators containing material from algae, lichens, bryophyta, multi-cellular fungi or plants, or extracts thereof
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- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N31/00—Biocides, pest repellants or attractants, or plant growth regulators containing organic oxygen or sulfur compounds
- A01N31/02—Acyclic compounds
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- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N65/00—Biocides, pest repellants or attractants, or plant growth regulators containing material from algae, lichens, bryophyta, multi-cellular fungi or plants, or extracts thereof
- A01N65/08—Magnoliopsida [dicotyledons]
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- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N65/00—Biocides, pest repellants or attractants, or plant growth regulators containing material from algae, lichens, bryophyta, multi-cellular fungi or plants, or extracts thereof
- A01N65/08—Magnoliopsida [dicotyledons]
- A01N65/20—Fabaceae or Leguminosae [Pea or Legume family], e.g. pea, lentil, soybean, clover, acacia, honey locust, derris or millettia
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- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N65/00—Biocides, pest repellants or attractants, or plant growth regulators containing material from algae, lichens, bryophyta, multi-cellular fungi or plants, or extracts thereof
- A01N65/40—Liliopsida [monocotyledons]
- A01N65/42—Aloeaceae [Aloe family] or Liliaceae [Lily family], e.g. aloe, veratrum, onion, garlic or chives
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61L—METHODS OR APPARATUS FOR STERILISING MATERIALS OR OBJECTS IN GENERAL; DISINFECTION, STERILISATION OR DEODORISATION OF AIR; CHEMICAL ASPECTS OF BANDAGES, DRESSINGS, ABSORBENT PADS OR SURGICAL ARTICLES; MATERIALS FOR BANDAGES, DRESSINGS, ABSORBENT PADS OR SURGICAL ARTICLES
- A61L9/00—Disinfection, sterilisation or deodorisation of air
- A61L9/01—Deodorant compositions
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61L—METHODS OR APPARATUS FOR STERILISING MATERIALS OR OBJECTS IN GENERAL; DISINFECTION, STERILISATION OR DEODORISATION OF AIR; CHEMICAL ASPECTS OF BANDAGES, DRESSINGS, ABSORBENT PADS OR SURGICAL ARTICLES; MATERIALS FOR BANDAGES, DRESSINGS, ABSORBENT PADS OR SURGICAL ARTICLES
- A61L9/00—Disinfection, sterilisation or deodorisation of air
- A61L9/01—Deodorant compositions
- A61L9/013—Deodorant compositions containing animal or plant extracts, or vegetable material
Abstract
The invention discloses a disinfection and sterilization aromatic liquid and a preparation method thereof, and the formula comprises: deionized water, aged essence, aged alcohol, oak juice extract, ALOE vera extract, sophora flavescens root extract and ginkgo biloba extract; the invention is prepared by mixing the aged essence and alcohol mixed plant extracts, not only has multiplied disinfection and sterilization effects, but also can form aerosol in the air, effectively kill most common bacteria and viruses, has pleasant fragrance, can customize various different fragrance types, replaces the indoor essential oil fragrance of most public spaces in the prior art, can be used in any public places by matching with a central air conditioner, has wide applicability, adopts pure natural plant components, is nontoxic, harmless, odorless, non-corrosive and high in safety, can be directly used for human bodies, ensures the trip health of people, is colorless and odorless when no aged essence is added, can replace most conventional disinfectants at present, and has better and safer disinfection and sterilization effects.
Description
Technical Field
The invention relates to the technical field of disinfectant, in particular to a disinfecting and sterilizing aromatic liquid and a preparation method thereof.
Background
The public places are dense in space and large in people flow, the public places are always high-incidence areas of infectious diseases, in order to effectively prevent the spread of the infectious diseases and maintain the health of people, managers can spray disinfection products on building facilities to kill germs in the places, and meanwhile, in order to cover up the unpleasant smell of the disinfection products, perfume products can be sprayed, and a more pleasant public environment is created.
However, most of the perfumes and aromatherapy essential oils in the current market only have fragrance efficacy, are not enough in safety, and part of the aromatherapy essential oils also have toxicity, while most of disinfection and sterilization products only have disinfection and sterilization functions, have toxicity and pungent odor, cannot be directly used in human bodies and human environments, are limited in use places, and have great potential safety hazards.
Disclosure of Invention
The invention aims to provide a disinfecting and sterilizing aromatic liquid and a preparation method thereof, which aim to solve the problems in the background technology.
In order to solve the technical problems, the invention provides the following technical scheme: the formula of the disinfectant aromatic liquid comprises: deionized water, aged essence, aged alcohol, oak juice extract, ALOE vera extract, sophora flavescens root extract and ginkgo leaf extract, wherein the weight parts of the components are as follows: 70-90 parts of deionized water, 7-9 parts of aging essence, 4-6 parts of aging alcohol, 2-4 parts of oak juice extract, 2-4 parts of ALOE vera extract, 1-2 parts of sophora flavescens root extract and 1-2 parts of ginkgo leaf extract.
A preparation method of a disinfecting and sterilizing aromatic liquid comprises the following steps of firstly, aging with alcohol; step two, aging the essence; step three, water deionization; step four, stirring the raw materials; step five, aging the fragrant liquid; step six, filtering the fragrant liquid; seventhly, toning the fragrant liquid; step eight, filling the fragrant liquid;
injecting a proper amount of alcohol into a purification tower, adding a proper amount of sodium hydroxide, refluxing for a period of time after boiling at high temperature, injecting into a fractionating tower, performing five-time fractionation, taking the part with the most pure fragrance as purified alcohol, injecting the purified alcohol into a paddle stirrer, adding a proper amount of potassium permanganate solution, uniformly mixing and stirring, standing for precipitation, removing precipitates through fine-pore cloth, injecting into a reaction kettle, adding a proper amount of activated carbon, standing for adsorption for a period of time, removing solid impurities through a silica gel filter screen, injecting into a container, adding a proper amount of spice, sealing, and aging at low temperature for a period of time to prepare aged alcohol;
in the second step, a proper amount of essence is put into a container, a proper amount of the aged alcohol prepared in the first step is added, and the aged essence is prepared after sealing and aging for the same time;
in the third step, injecting a proper amount of water into a distillation furnace, distilling and purifying at high temperature, adding a proper amount of sodium citrate, and removing metal ions to prepare deionized water;
in the fourth step, 4-6 parts of aged alcohol, 7-9 parts of aged essence and 70-90 parts of deionized water are respectively selected from the first step, the second step and the third step according to the weight parts of the components and are placed into a silver-lined container, then the silver-lined container is placed on a magnetic stirrer, then 2-4 parts of oak juice extract, 2-4 parts of ALOE vera extract, 1-2 parts of sophora flavescens root extract and 1-2 parts of ginkgo leaf extract are added in parts by weight, and after being uniformly mixed and stirred, the mixture is kept stand for a period of time to prepare a rough aromatic liquid;
in the fifth step, the crude aromatic liquid prepared in the fourth step is filled in a closed container, then a proper amount of oxygen is introduced for full oxidation, then a proper amount of silver chloride is added for full catalysis, then a proper amount of hydrogen is introduced for full reduction, and after full reduction, sealing and aging are carried out for a period of time to prepare refined aromatic liquid;
placing the refined aromatic liquid prepared in the fifth step into a refrigeration house for a period of time, taking out the refined aromatic liquid, heating the refined aromatic liquid to room temperature, then injecting the refined aromatic liquid into a filter press, adding a proper amount of filter aid, adsorbing precipitated particles in the refined aromatic liquid, cooling the refined aromatic liquid to 0 ℃, keeping the temperature for a period of time, heating the refined aromatic liquid to room temperature, and filtering the refined aromatic liquid through a fine-pore cloth to prepare transparent aromatic liquid;
putting the transparent aromatic liquid prepared in the step six into a stirrer, adding a proper amount of toner, and uniformly mixing and stirring to obtain colored aromatic liquid;
and step eight, placing the colored aromatic liquid prepared in the step seven on a quality inspection table, comparing the color and luster, measuring the specific gravity and the refractive index by using an instrument, screening out the colored aromatic liquid with qualified quality, placing the colored aromatic liquid into a filling machine, adding a prefabricated packaging bottle, filling the colored aromatic liquid into the packaging bottle, reserving a proper amount of gaps, and sealing to obtain the sterilizing aromatic liquid.
According to the technical scheme, the oak juice extract, the ALOE vera extract ALOE, the sophora flavescens root extract and the ginkgo leaf extract are respectively selected from the oak juice extract with the concentration of 3.5 percent, the ALOE vera extract with the concentration of 1.5 percent, the sophora flavescens root extract with the concentration of 0.5 percent and the ginkgo leaf extract with the concentration of 0.5 percent.
According to the technical scheme, in the first step, the boiling temperature of the purification tower is 75-85 ℃, and the reflux time is 3-4 hours.
According to the technical scheme, in the first step, the stirring speed of the paddle stirrer is 40-60 r/min, and the stirring time is 5-15 s.
According to the technical scheme, in the first step, the adsorption time is 5-7 d, the aging temperature is 13-17 ℃, and the aging time is 30-40 d.
According to the technical scheme, in the fourth step, the stirring speed of the magnetic stirrer paddle is 60-120 r/min, the stirring time is 30-50 s, and the standing time is 3-5 d.
According to the technical scheme, in the fifth step, the closed container is provided with a safety valve, and the aging time is 90-100 days.
According to the technical scheme, in the sixth step, the filter press adopts plate-and-frame filter pressing, and the filter aid adopts diatomite.
Compared with the prior art, the invention has the following beneficial effects: the invention is prepared by mixing deionized water, aging essence, aging alcohol, oak juice extract, ALOE vera extract, sophora flavescens root extract and ginkgo leaf extract, not only has multiplied disinfection and sterilization effects, but also can form aerosol in the air, effectively kill most common bacteria and viruses, has pleasant fragrance, can customize various different fragrance types, replaces the indoor essential oil fragrance of most public spaces, is matched with a central air conditioner, can be used in any public places, and has wide applicability; the oak juice extract, the ALOE vera extract, the sophora flavescens root extract and the ginkgo leaf extract are all pure natural plant components, are non-toxic, harmless, odorless, non-corrosive and high in safety, can be directly used for a human body to guarantee the trip health of people, are colorless and tasteless when aging essence is not added, can replace most conventional disinfectants at present, such as 84 disinfectant, alcohol, chlorine dioxide and the like, and are better and safer in disinfection and sterilization effects.
Drawings
The accompanying drawings, which are included to provide a further understanding of the invention and are incorporated in and constitute a part of this specification, illustrate embodiments of the invention and together with the description serve to explain the principles of the invention and not to limit the invention. In the drawings:
FIG. 1 is a flow chart of the method of the present invention.
Detailed Description
The technical solutions in the embodiments of the present invention will be clearly and completely described below with reference to the drawings in the embodiments of the present invention, and it is obvious that the described embodiments are only a part of the embodiments of the present invention, and not all of the embodiments. All other embodiments, which can be derived by a person skilled in the art from the embodiments given herein without making any creative effort, shall fall within the protection scope of the present invention.
Referring to fig. 1, the present invention provides a technical solution:
example 1:
the formula of the disinfectant aromatic liquid comprises: deionized water, aged essence, aged alcohol, oak juice extract, ALOE vera extract, sophora flavescens root extract and ginkgo leaf extract, wherein the weight parts of the components are as follows: 70-90 parts of deionized water, 7-9 parts of aging essence, 4-6 parts of aging alcohol, 2-4 parts of oak juice extract, 2-4 parts of ALOE vera extract, 1-2 parts of sophora flavescens ait root extract and 1-2 parts of ginkgo leaf extract, wherein the oak juice extract, the ALOE vera extract ALOE, the sophora flavescens ait root extract and the ginkgo leaf extract are respectively selected from 3.5% oak juice extract, 1.5% ALOE vera extract, 0.5% sophora flavescens ait root extract and 0.5% ginkgo leaf extract.
A preparation method of a disinfecting and sterilizing aromatic liquid comprises the following steps of firstly, aging with alcohol; step two, aging the essence; step three, water deionization; step four, stirring the raw materials; step five, aging the fragrant liquid; step six, filtering the fragrant liquid; seventhly, toning the fragrant liquid; step eight, filling the fragrant liquid;
wherein in the first step, injecting a proper amount of alcohol into a purification tower, boiling the purification tower at 75-85 ℃ for 3-4 h, adding a proper amount of sodium hydroxide, boiling at high temperature, refluxing for a period of time, injecting into a fractionating tower, performing five-time fractionation, taking the part with the highest fragrance as the purified alcohol, then injecting the purified alcohol into a paddle stirrer at a stirring speed of 40-60 r/min for 5-15 s, adding a proper amount of potassium permanganate solution, mixing, stirring uniformly, standing for precipitation, removing precipitates through fine pore cloth, injecting into a reaction kettle, adding a proper amount of activated carbon, standing for adsorption for a period of time, adsorbing for 5-7 d, removing solid impurities through a silica gel filter screen, injecting into a container, adding a proper amount of perfume, sealing, performing low-temperature aging for a period of time, aging at the temperature of 13-17 ℃ for 30-40 d to obtain aged alcohol;
in the second step, a proper amount of essence is put into a container, a proper amount of the aged alcohol prepared in the first step is added, and the aged essence is prepared after sealing and aging for the same time;
in the third step, injecting a proper amount of water into a distillation furnace, distilling and purifying at high temperature, adding a proper amount of sodium citrate, and removing metal ions to prepare deionized water;
in the fourth step, 4 parts of aged alcohol, 7 parts of aged essence and 70 parts of deionized water are respectively selected from the first step, the second step and the third step according to the weight parts of the components and are placed into a silver-lined container, the silver-lined container is placed on a magnetic stirrer, the stirring speed of a magnetic stirrer paddle is 60-120 r/min, the stirring time is 30-50 s, the standing time is 3-5 d, then 2 parts of oak juice extract, 2 parts of ALOE vera extract, 1 part of sophora flavescens ait root extract and 1 part of ginkgo leaf extract are respectively added, and after uniform mixing and stirring, the mixture is kept standing for a period of time to prepare a crude aromatic liquid;
in the fifth step, the crude aromatic liquid prepared in the fourth step is filled in a closed container, the closed container is provided with a safety valve, a proper amount of oxygen is introduced for full oxidation, a proper amount of silver chloride is added for full catalysis, a proper amount of hydrogen is introduced for full reduction, and after the reduction, the sealed aging is carried out for a period of time, wherein the aging time is 90-100 days, so as to prepare the refined aromatic liquid;
placing the refined aromatic liquid prepared in the fifth step into a refrigeration house for a period of time, taking out, heating to room temperature, injecting into a filter press, adding a proper amount of filter aid, wherein the filter press is a plate-and-frame filter press, the filter aid is diatomite, adsorbing precipitated particles in the refined aromatic liquid, cooling to 0 ℃, keeping the temperature for a period of time, heating to room temperature, and filtering through a fine-pore cloth to prepare transparent aromatic liquid;
putting the transparent aromatic liquid prepared in the step six into a stirrer, adding a proper amount of toner, and uniformly mixing and stirring to obtain colored aromatic liquid;
and step eight, placing the colored aromatic liquid prepared in the step seven on a quality inspection table, comparing the color and luster, measuring the specific gravity and the refractive index by using an instrument, screening out the colored aromatic liquid with qualified quality, placing the colored aromatic liquid into a filling machine, adding a prefabricated packaging bottle, filling the colored aromatic liquid into the packaging bottle, reserving a proper amount of gaps, and sealing to obtain the sterilizing aromatic liquid.
Example 2:
the formula of the disinfectant aromatic liquid comprises: deionized water, aged essence, aged alcohol, oak juice extract, ALOE vera extract, sophora flavescens root extract and ginkgo leaf extract, wherein the weight parts of the components are as follows: 70-90 parts of deionized water, 7-9 parts of aging essence, 4-6 parts of aging alcohol, 2-4 parts of oak juice extract, 2-4 parts of ALOE vera extract, 1-2 parts of sophora flavescens ait root extract and 1-2 parts of ginkgo leaf extract, wherein the oak juice extract, the ALOE vera extract ALOE, the sophora flavescens ait root extract and the ginkgo leaf extract are respectively selected from 3.5% oak juice extract, 1.5% ALOE vera extract, 0.5% sophora flavescens ait root extract and 0.5% ginkgo leaf extract.
A preparation method of a disinfecting and sterilizing aromatic liquid comprises the following steps of firstly, aging with alcohol; step two, aging the essence; step three, water deionization; step four, stirring the raw materials; step five, aging the fragrant liquid; step six, filtering the fragrant liquid; seventhly, toning the fragrant liquid; step eight, filling the fragrant liquid;
wherein in the first step, injecting a proper amount of alcohol into a purification tower, boiling the purification tower at 75-85 ℃ for 3-4 h, adding a proper amount of sodium hydroxide, boiling at high temperature, refluxing for a period of time, injecting into a fractionating tower, performing five-time fractionation, taking the part with the highest fragrance as the purified alcohol, then injecting the purified alcohol into a paddle stirrer at a stirring speed of 40-60 r/min for 5-15 s, adding a proper amount of potassium permanganate solution, mixing, stirring uniformly, standing for precipitation, removing precipitates through fine pore cloth, injecting into a reaction kettle, adding a proper amount of activated carbon, standing for adsorption for a period of time, adsorbing for 5-7 d, removing solid impurities through a silica gel filter screen, injecting into a container, adding a proper amount of perfume, sealing, performing low-temperature aging for a period of time, aging at the temperature of 13-17 ℃ for 30-40 d to obtain aged alcohol;
in the second step, a proper amount of essence is put into a container, a proper amount of the aged alcohol prepared in the first step is added, and the aged essence is prepared after sealing and aging for the same time;
in the third step, injecting a proper amount of water into a distillation furnace, distilling and purifying at high temperature, adding a proper amount of sodium citrate, and removing metal ions to prepare deionized water;
in the fourth step, 5 parts of aged alcohol, 8 parts of aged essence and 80 parts of deionized water are respectively selected from the first step, the second step and the third step according to the weight parts of the components and are placed into a silver-lined container, the silver-lined container is placed on a magnetic stirrer, the stirring speed of a magnetic stirrer paddle is 60-120 r/min, the stirring time is 30-50 s, the standing time is 3-5 d, then 3 parts of oak juice extract, 3 parts of ALOE vera extract, 1.5 parts of sophora flavescens root extract and 1.5 parts of ginkgo leaf extract are respectively added, and after uniform mixing and stirring, the mixture is stood for a period of time to prepare a crude aromatic liquid;
in the fifth step, the crude aromatic liquid prepared in the fourth step is filled in a closed container, the closed container is provided with a safety valve, a proper amount of oxygen is introduced for full oxidation, a proper amount of silver chloride is added for full catalysis, a proper amount of hydrogen is introduced for full reduction, and after the reduction, the sealed aging is carried out for a period of time, wherein the aging time is 90-100 days, so as to prepare the refined aromatic liquid;
placing the refined aromatic liquid prepared in the fifth step into a refrigeration house for a period of time, taking out, heating to room temperature, injecting into a filter press, adding a proper amount of filter aid, wherein the filter press is a plate-and-frame filter press, the filter aid is diatomite, adsorbing precipitated particles in the refined aromatic liquid, cooling to 0 ℃, keeping the temperature for a period of time, heating to room temperature, and filtering through a fine-pore cloth to prepare transparent aromatic liquid;
putting the transparent aromatic liquid prepared in the step six into a stirrer, adding a proper amount of toner, and uniformly mixing and stirring to obtain colored aromatic liquid;
and step eight, placing the colored aromatic liquid prepared in the step seven on a quality inspection table, comparing the color and luster, measuring the specific gravity and the refractive index by using an instrument, screening out the colored aromatic liquid with qualified quality, placing the colored aromatic liquid into a filling machine, adding a prefabricated packaging bottle, filling the colored aromatic liquid into the packaging bottle, reserving a proper amount of gaps, and sealing to obtain the sterilizing aromatic liquid.
Example 3:
the formula of the disinfectant aromatic liquid comprises: deionized water, aged essence, aged alcohol, oak juice extract, ALOE vera extract, sophora flavescens root extract and ginkgo leaf extract, wherein the weight parts of the components are as follows: 70-90 parts of deionized water, 7-9 parts of aging essence, 4-6 parts of aging alcohol, 2-4 parts of oak juice extract, 2-4 parts of ALOE vera extract, 1-2 parts of sophora flavescens ait root extract and 1-2 parts of ginkgo leaf extract, wherein the oak juice extract, the ALOE vera extract ALOE, the sophora flavescens ait root extract and the ginkgo leaf extract are respectively selected from 3.5% oak juice extract, 1.5% ALOE vera extract, 0.5% sophora flavescens ait root extract and 0.5% ginkgo leaf extract.
A preparation method of a disinfecting and sterilizing aromatic liquid comprises the following steps of firstly, aging with alcohol; step two, aging the essence; step three, water deionization; step four, stirring the raw materials; step five, aging the fragrant liquid; step six, filtering the fragrant liquid; seventhly, toning the fragrant liquid; step eight, filling the fragrant liquid;
wherein in the first step, injecting a proper amount of alcohol into a purification tower, boiling the purification tower at 75-85 ℃ for 3-4 h, adding a proper amount of sodium hydroxide, boiling at high temperature, refluxing for a period of time, injecting into a fractionating tower, performing five-time fractionation, taking the part with the highest fragrance as the purified alcohol, then injecting the purified alcohol into a paddle stirrer at a stirring speed of 40-60 r/min for 5-15 s, adding a proper amount of potassium permanganate solution, mixing, stirring uniformly, standing for precipitation, removing precipitates through fine pore cloth, injecting into a reaction kettle, adding a proper amount of activated carbon, standing for adsorption for a period of time, adsorbing for 5-7 d, removing solid impurities through a silica gel filter screen, injecting into a container, adding a proper amount of perfume, sealing, performing low-temperature aging for a period of time, aging at the temperature of 13-17 ℃ for 30-40 d to obtain aged alcohol;
in the second step, a proper amount of essence is put into a container, a proper amount of the aged alcohol prepared in the first step is added, and the aged essence is prepared after sealing and aging for the same time;
in the third step, injecting a proper amount of water into a distillation furnace, distilling and purifying at high temperature, adding a proper amount of sodium citrate, and removing metal ions to prepare deionized water;
in the fourth step, 6 parts of aged alcohol, 9 parts of aged essence and 90 parts of deionized water are respectively selected from the first step, the second step and the third step according to the weight parts of the components and are placed into a silver-lined container, the silver-lined container is placed on a magnetic stirrer, the stirring speed of a magnetic stirrer paddle is 60-120 r/min, the stirring time is 30-50 s, the standing time is 3-5 d, then 4 parts of oak juice extract, 4 parts of ALOE vera extract, 2 parts of sophora flavescens ait root extract and 2 parts of ginkgo leaf extract are respectively added, and after uniform mixing and stirring, the mixture is kept standing for a period of time to prepare a crude aromatic liquid;
in the fifth step, the crude aromatic liquid prepared in the fourth step is filled in a closed container, the closed container is provided with a safety valve, a proper amount of oxygen is introduced for full oxidation, a proper amount of silver chloride is added for full catalysis, a proper amount of hydrogen is introduced for full reduction, and after the reduction, the sealed aging is carried out for a period of time, wherein the aging time is 90-100 days, so as to prepare the refined aromatic liquid;
placing the refined aromatic liquid prepared in the fifth step into a refrigeration house for a period of time, taking out, heating to room temperature, injecting into a filter press, adding a proper amount of filter aid, wherein the filter press is a plate-and-frame filter press, the filter aid is diatomite, adsorbing precipitated particles in the refined aromatic liquid, cooling to 0 ℃, keeping the temperature for a period of time, heating to room temperature, and filtering through a fine-pore cloth to prepare transparent aromatic liquid;
putting the transparent aromatic liquid prepared in the step six into a stirrer, adding a proper amount of toner, and uniformly mixing and stirring to obtain colored aromatic liquid;
and step eight, placing the colored aromatic liquid prepared in the step seven on a quality inspection table, comparing the color and luster, measuring the specific gravity and the refractive index by using an instrument, screening out the colored aromatic liquid with qualified quality, placing the colored aromatic liquid into a filling machine, adding a prefabricated packaging bottle, filling the colored aromatic liquid into the packaging bottle, reserving a proper amount of gaps, and sealing to obtain the sterilizing aromatic liquid.
The disinfectant aromatic liquid obtained in the above examples was compared with the ordinary 84 disinfectant liquid, and the following results were obtained:
| smell(s) | For human body | |
| 84 sterilizing liquid | Offensive smell | Toxic and harmful |
| Example 1 | Fragrant and pleasant | Non-toxic and harmless |
| Example 2 | Fragrant and pleasant | Non-toxic and harmless |
| Example 3 | Fragrant and pleasant | Non-toxic and harmless |
Compared with the prior art, the invention has the following beneficial effects: the aromatic liquid is prepared by mixing the oak juice extract, the ALOE vera extract, the sophora flavescens root extract and the ginkgo leaf extract with deionized water, aging essence and aging alcohol, so that the sterilizing effect is multiplied, aerosol can be formed in the air, most common bacterial viruses can be effectively killed, the fragrance is pleasant, various different fragrance types can be customized, the indoor essential oil fragrance of most public spaces in the prior art is replaced, and the aromatic liquid is matched with a central air conditioner to be used in any public places, so that the applicability is wide; the oak juice extract, the ALOE vera extract, the sophora flavescens root extract and the ginkgo leaf extract which are all natural plant components are utilized to sterilize, are non-toxic, harmless, free of peculiar smell and corrosion, high in safety, can be directly used for a human body to guarantee the trip health of people, are colorless and tasteless when aging essence is not added, can replace most conventional disinfectants at present, such as 84 disinfectant, alcohol, chlorine dioxide and the like, and are better and safer in sterilization effect.
It is noted that, herein, relational terms such as first and second, and the like may be used solely to distinguish one entity or action from another entity or action without necessarily requiring or implying any actual such relationship or order between such entities or actions. Also, the terms "comprises," "comprising," or any other variation thereof, are intended to cover a non-exclusive inclusion, such that a process, method, article, or apparatus that comprises a list of elements does not include only those elements but may include other elements not expressly listed or inherent to such process, method, article, or apparatus.
Finally, it should be noted that: although the present invention has been described in detail with reference to the foregoing embodiments, it will be apparent to those skilled in the art that changes may be made in the embodiments and/or equivalents thereof without departing from the spirit and scope of the invention. Any modification, equivalent replacement, or improvement made within the spirit and principle of the present invention should be included in the protection scope of the present invention.
Claims (9)
1. The formula of the disinfectant aromatic liquid comprises: deionized water, aged essence, aged alcohol, oak juice extract, ALOE vera extract ALOE, sophora flavescens root extract and ginkgo leaf extract, and is characterized in that: the weight parts of the components are respectively as follows: 70-90 parts of deionized water, 7-9 parts of aging essence, 4-6 parts of aging alcohol, 2-4 parts of oak juice extract, 2-4 parts of ALOE vera extract, 1-2 parts of sophora flavescens root extract and 1-2 parts of ginkgo leaf extract.
2. A preparation method of a disinfecting and sterilizing aromatic liquid comprises the following steps of firstly, aging with alcohol; step two, aging the essence; step three, water deionization; step four, stirring the raw materials; step five, aging the fragrant liquid; step six, filtering the fragrant liquid; seventhly, toning the fragrant liquid; step eight, filling the fragrant liquid; the method is characterized in that:
injecting a proper amount of alcohol into a purification tower, adding a proper amount of sodium hydroxide, refluxing for a period of time after boiling at high temperature, injecting into a fractionating tower, performing five-time fractionation, taking the part with the most pure fragrance as purified alcohol, injecting the purified alcohol into a paddle stirrer, adding a proper amount of potassium permanganate solution, uniformly mixing and stirring, standing for precipitation, removing precipitates through fine-pore cloth, injecting into a reaction kettle, adding a proper amount of activated carbon, standing for adsorption for a period of time, removing solid impurities through a silica gel filter screen, injecting into a container, adding a proper amount of spice, sealing, and aging at low temperature for a period of time to prepare aged alcohol;
in the second step, a proper amount of essence is put into a container, a proper amount of the aged alcohol prepared in the first step is added, and the aged essence is prepared after sealing and aging for the same time;
in the third step, injecting a proper amount of water into a distillation furnace, distilling and purifying at high temperature, adding a proper amount of sodium citrate, and removing metal ions to prepare deionized water;
in the fourth step, 4-6 parts of aged alcohol, 7-9 parts of aged essence and 70-90 parts of deionized water are respectively selected from the first step, the second step and the third step according to the weight parts of the components and are placed into a silver-lined container, then the silver-lined container is placed on a magnetic stirrer, then 2-4 parts of oak juice extract, 2-4 parts of ALOE vera extract, 1-2 parts of sophora flavescens root extract and 1-2 parts of ginkgo leaf extract are added in parts by weight, and after being uniformly mixed and stirred, the mixture is kept stand for a period of time to prepare a rough aromatic liquid;
in the fifth step, the crude aromatic liquid prepared in the fourth step is filled in a closed container, then a proper amount of oxygen is introduced for full oxidation, then a proper amount of silver chloride is added for full catalysis, then a proper amount of hydrogen is introduced for full reduction, and after full reduction, sealing and aging are carried out for a period of time to prepare refined aromatic liquid;
placing the refined aromatic liquid prepared in the fifth step into a refrigeration house for a period of time, taking out the refined aromatic liquid, heating the refined aromatic liquid to room temperature, then injecting the refined aromatic liquid into a filter press, adding a proper amount of filter aid, adsorbing precipitated particles in the refined aromatic liquid, cooling the refined aromatic liquid to 0 ℃, keeping the temperature for a period of time, heating the refined aromatic liquid to room temperature, and filtering the refined aromatic liquid through a fine-pore cloth to prepare transparent aromatic liquid;
putting the transparent aromatic liquid prepared in the step six into a stirrer, adding a proper amount of toner, and uniformly mixing and stirring to obtain colored aromatic liquid;
and step eight, placing the colored aromatic liquid prepared in the step seven on a quality inspection table, comparing the color and luster, measuring the specific gravity and the refractive index by using an instrument, screening out the colored aromatic liquid with qualified quality, placing the colored aromatic liquid into a filling machine, adding a prefabricated packaging bottle, filling the colored aromatic liquid into the packaging bottle, reserving a proper amount of gaps, and sealing to obtain the sterilizing aromatic liquid.
3. The aromatic liquid for disinfection and sterilization as claimed in claim 1, wherein: the oak juice extract, ALOE vera extract, sophora flavescens root extract and ginkgo leaf extract are respectively selected from oak juice extract with the concentration of 3.5%, ALOE vera extract with the concentration of 1.5%, sophora flavescens root extract with the concentration of 0.5% and ginkgo leaf extract with the concentration of 0.5%.
4. The preparation method of the sterilizing aromatic liquid according to claim 2, characterized in that: in the first step, the boiling temperature of the purification tower is 75-85 ℃, and the reflux time is 3-4 h.
5. The preparation method of the sterilizing aromatic liquid according to claim 2, characterized in that: in the first step, the stirring speed of the blade stirrer is 40-60 r/min, and the stirring time is 5-15 s.
6. The preparation method of the sterilizing aromatic liquid according to claim 2, characterized in that: in the first step, the adsorption time is 5-7 days, the aging temperature is 13-17 ℃, and the aging time is 30-40 days.
7. The preparation method of the sterilizing aromatic liquid according to claim 2, characterized in that: in the fourth step, the stirring speed of the magnetic stirrer paddle is 60-120 r/min, the stirring time is 30-50 s, and the standing time is 3-5 d.
8. The preparation method of the sterilizing aromatic liquid according to claim 2, characterized in that: in the fifth step, the closed container is provided with a safety valve, and the aging time is 90-100 days.
9. The preparation method of the sterilizing aromatic liquid according to claim 2, characterized in that: in the sixth step, the filter press adopts a plate and frame filter press, and the filter aid adopts diatomite.
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