CN106263012B - A kind of low temperature cigarette tobacco material processing method - Google Patents

A kind of low temperature cigarette tobacco material processing method Download PDF

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Publication number
CN106263012B
CN106263012B CN201610807097.6A CN201610807097A CN106263012B CN 106263012 B CN106263012 B CN 106263012B CN 201610807097 A CN201610807097 A CN 201610807097A CN 106263012 B CN106263012 B CN 106263012B
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China
Prior art keywords
tobacco material
tobacco
low temperature
processing method
alkali lye
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CN201610807097.6A
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Chinese (zh)
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CN106263012A (en
Inventor
李朝建
庄亚东
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China Tobacco Jiangsu Industrial Co Ltd
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China Tobacco Jiangsu Industrial Co Ltd
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Priority to CN201610807097.6A priority Critical patent/CN106263012B/en
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    • AHUMAN NECESSITIES
    • A24TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
    • A24BMANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
    • A24B15/00Chemical features or treatment of tobacco; Tobacco substitutes, e.g. in liquid form
    • A24B15/18Treatment of tobacco products or tobacco substitutes
    • A24B15/24Treatment of tobacco products or tobacco substitutes by extraction; Tobacco extracts
    • AHUMAN NECESSITIES
    • A24TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
    • A24BMANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
    • A24B15/00Chemical features or treatment of tobacco; Tobacco substitutes, e.g. in liquid form
    • A24B15/18Treatment of tobacco products or tobacco substitutes
    • A24B15/22Treatment of tobacco products or tobacco substitutes by application of electric or wave energy or particle radiation
    • AHUMAN NECESSITIES
    • A24TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
    • A24BMANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
    • A24B3/00Preparing tobacco in the factory
    • A24B3/04Humidifying or drying tobacco bunches or cut tobacco
    • AHUMAN NECESSITIES
    • A24TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
    • A24BMANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
    • A24B3/00Preparing tobacco in the factory
    • A24B3/12Steaming, curing, or flavouring tobacco

Abstract

The invention discloses a kind of low temperature cigarette tobacco material processing method, comprise the following steps:Alkali lye is added in tobacco material and extracted by step SS1, and progress is ultrasonically treated, is transferred to the step SS2;Step SS2 suction filtrations discard the extraction alkali lye of the step SS1, add pure water by tobacco material quick wash, discard cleaning solution, be transferred to step SS3;Tobacco material low temperature drying made from step SS2 is transferred to step SS4 by step SS3;The tobacco material dried made from step SS3 is placed in balance environment after 24~48h by step SS4, applies the ethanol solution containing flavouring essence for tobacco and polyalcohol thereto, and places 24~48h in sealed states, is transferred to step SS5;Tobacco material made from the step SS4 is placed in balance environment after 48h by step SS5, obtains being applied to the tobacco-containing material of heating non-burning cigarette.Tobacco material after present invention processing, the flue gas concentration that discharges is big under heating non-burning state, smoke alcohol and, soft, excitant is small, and strength is moderate.

Description

A kind of low temperature cigarette tobacco material processing method
Technical field
The present invention relates to a kind of low temperature cigarette tobacco material processing method, belong to technical field of tobacco processing.
Background technology
With continuing to develop for global Tobacco Control campaign, the World Health Organization and the public for cigarette harmfulness more Concern, the tobacco management and control measures that national governments put into effect in succession are increasingly severe;The development of traditional cigarette, which is encountered, greatly challenges.Grind Consumer's needs can be met by studying carefully exploitation, and the novel tobacco product of energy safety and environmental protection is particularly important.Low temperature cigarette is not required to Burn, only heating pipe tobacco, toasts the demand that nicotine and fragrance matter in tobacco meet smoker.Therefore, low temperature Cigarette reduces the harmful components that the cracking of tobacco high-temp combustion is produced, and substantially reduces main flume chemical constituent burst size, phase It is smaller than traditional cigarette harmfulness;Meanwhile, glowed difference with conventional cigarette, its pipe tobacco when aspirating interval is in non-burning shape State, side-stream smoke and environment flue gas are greatly lowered, and will not produce influence to PE, smoking is alleviated to a certain extent The contradiction banned on opium-smoking and the opium trade with public place.The research and development of low temperature cigarette turn into the focus of attention of current Field of Tobacco.
Be present bigger difference in the aesthetic quality of low temperature cigarette and traditional cigarette, found in experimental study, undressed processing The flue gas of pipe tobacco baking release inhale that taste is strong, excitant is relatively strong, have acid and strong tart flavour, miscellaneous gas heavier.In order to improve Flue gas release performance under tobacco material heating non-burning state, is processed to tobacco material and seems and be even more important.It is existing Some patents are related to the combination to multi-form tobacco-containing material (mainly having pipe tobacco, offal, reconstituted tobacoo), tobacco-containing material are carried out Perfuming handles or carries out performance improvement to tobacco extract.
The content of the invention
The technical problems to be solved by the invention are to overcome the defect of prior art former with tobacco there is provided a kind of low temperature cigarette Expect processing method, after being handled by this method, flue gas release performance of the tobacco material under heating non-burning state is significantly improved, The flue gas aesthetic quality discharged is obviously improved.
The present invention is adopted the following technical scheme that:A kind of low temperature cigarette tobacco material processing method, it is characterised in that including Following steps:
Step SS1 alkali lye is extracted, and is specifically included:Alkali lye is added in tobacco material and extracted, progress is ultrasonically treated, is transferred to institute State step SS2;
Step SS2 suction filtrations, are specifically included:Suction filtration discards the extraction alkali lye of the step SS1, adds pure water by tobacco material Quick wash, discards cleaning solution, is transferred to step SS3;
Step SS3 is dried, and is specifically included:By tobacco material low temperature drying made from step SS2, step SS4 is transferred to;
Step SS4 flavoring and casings, are specifically included:The tobacco material dried made from step SS3 is placed in balance environment After 24~48h, apply the ethanol solution containing flavouring essence for tobacco and polyalcohol thereto, and place 24 in sealed states~ 48h, is transferred to step SS5;
Step SS5 is balanced, and is specifically included:Tobacco material made from the step SS4 is placed in balance environment after 48h, Obtain being applied to the tobacco-containing material of heating non-burning cigarette.
As a kind of preferred embodiment, the tobacco material used in the step SS1 is flue-cured tobacco, Turkish tobaccos, burley tobaccos In any one or a few.
As a kind of preferred embodiment, the alkali lye used in the step SS1 for various concentrations NH4OH solution, NaOH solution, K2CO3Solution, Ca (OH)2Solution, Na2CO3One kind in solution.
As a kind of preferred embodiment, in the step SS1, the applied amount of alkali lye and tobacco material is MPipe tobacco:VAlkali lye= 1.0g:6~20mL.
As a kind of preferred embodiment, in the step SS1, the applied amount of alkali lye and tobacco material is MPipe tobacco:VAlkali lye= 1.0g:8~10mL.
As a kind of preferred embodiment, the ultrasonically treated time in the step SS1 is 5-60min.
As a kind of preferred embodiment, the ultrasonically treated time in the step SS1 is 30-40min.
As a kind of preferred embodiment, in the step SS3, the temperature of tobacco material low temperature drying is 40~70 DEG C.
As a kind of preferred embodiment, the balance environment in the step SS4 is included the tobacco material of drying in temperature Balanced in 22 DEG C of degree, the environment of relative humidity 60%.
As a kind of preferred embodiment, the flavouring essence for tobacco in the step SS4 is eugenol, ethylmaltol, dihydro One or more of mixing in damascenone, 2- acetylpyridines, (2H) furanone of 4- hydroxyl -2,5- dimethyl -3.
As a kind of preferred embodiment, polyalcohol in the step SS4 for propane diols, glycerine any one or Two kinds of mixing.
As a kind of preferred embodiment, the balance environment in the step SS5 includes to add after flavouring essence for tobacco processing Tobacco material is placed in 22 DEG C of temperature, the environment of relative humidity 60% and balanced.
The beneficial effect that the present invention is reached:1st, the present invention is handled tobacco material using alkali lye, can effectively be reduced The content of acid ingredient in tobacco material, makes tobacco material tart flavour in the flue gas discharged under heating non-burning state no longer evident It is aobvious, effectively improve the aesthetic quality of flue gas;2nd, the present invention is former to tobacco using the ethanol solution containing propane diols or glycerine Material carries out charging processing, and flue gas release performance of the increase tobacco material under heating non-burning state improves flue gas concentration;3rd, originally Invention adds eugenol, ethylmaltol, damascone, 2- acetylpyridines, (2H) furans of 4- hydroxyl -2,5- dimethyl -3 The spices such as ketone, can increase tobacco characteristic perfume, increase flue gas richness, improve the organoleptic quality for discharging flue gas;4th, tobacco is former After material is using the method processing of the present invention, its sense organ product for heating the flue gas release performance under non-burning state and discharging flue gas Matter is substantially improved, and flue gas is soft, miscellaneous gas is reduced, exhaust gas volumn is big, excitant and strength are moderate, and flue gas satisfaction is strong, is adding Applicability in hot non-combustion-type tobacco product is remarkably reinforced;4th, operating procedure of the invention is simple, cost is low, with good Industrial prospect.
Brief description of the drawings
Fig. 1 is the flow chart of the present invention.
Embodiment
The invention will be further described below in conjunction with the accompanying drawings.Following examples are only used for clearly illustrating the present invention Technical scheme, and can not be limited the scope of the invention with this.
Embodiment 1:
The present invention proposes a kind of processing method for being applied to heating non-burning cigarette tobacco material, successively including following step Suddenly:
By 3%NH4OH solution presses MPipe tobacco:VAlkali lye=1.0g:10mL ratios are added in tobacco material, ultrasonic 30min;Suction filtration, Leaching liquor is discarded, by MPipe tobacco:VWater=1.0g:10mL ratios add pure water by suction filtration after tobacco material quick wash, discard washing Liquid;By tobacco material in 50 DEG C of drying;The tobacco material of drying is balanced in 22 DEG C of temperature, the environment of relative humidity 60% After 48h, apply the ethanol solution containing flavouring essence for tobacco and polyalcohol thereto, and place 24~48h in sealed states, protect Card tobacco material is fully absorbed to flavouring essence for tobacco and polyalcohol;Tobacco material after perfuming is handled is placed in 22 DEG C of temperature, phase Obtain being applied to the tobacco-containing material of heating non-combustion-type tobacco product to balancing 48h in the environment of humidity 60%.
The present invention does not have special limitation to the species of the flavouring essence for tobacco and source, is known using those skilled in the art Flavouring essence for tobacco.In the present invention, the ethanol solution of the flavouring essence for tobacco and polyalcohol preferentially includes weight percent The following composition of ratio:Eugenol 0.1 ‰, ethylmaltol 0.2 ‰, damascone 0.1 ‰, 2- acetylpyridines 0.2 ‰, 4- Hydroxyl -2,5- dimethyl -3 (2H) furanone 0.2 ‰, glycerine 2%, remaining is absolute ethyl alcohol, and each component summation is 100, is mixed It is made after even.
Embodiment 2:
Be the same as Example 1, difference is that alkali lye is 2%NaOH solution.
Be the same as Example 1, difference is, the ethanol solution of the flavouring essence for tobacco and polyalcohol preferentially includes weight percent The following composition of ratio:Eugenol 0.05 ‰, ethylmaltol 0.2 ‰, damascone 0.1 ‰, 2- acetylpyridines 0.2 ‰, 4- Hydroxyl -2,5- dimethyl -3 (2H) furanone 0.2 ‰, glycerine 2%, remaining is absolute ethyl alcohol, and each component summation is 100, is mixed It is made after even.
Embodiment 3:
Be the same as Example 1, difference is that alkali lye is 2%K2CO3Solution.
Embodiment 4:
Be the same as Example 1, difference is that alkali lye is saturation Ca (OH)2Solution.
Embodiment 5:
Be the same as Example 1, difference is that alkali lye is 1%Na2CO3Solution.
Embodiment 6:
Be the same as Example 1, difference is, the ethanol solution of the flavouring essence for tobacco and polyalcohol preferentially includes weight percent The following composition of ratio:Eugenol 0.1 ‰, ethylmaltol 0.2 ‰, damascone 0.1 ‰, 2- acetylpyridines 0.2 ‰, 4- Hydroxyl -2,5- dimethyl -3 (2H) furanone 0.2 ‰, propane diols 1.5%, remaining is absolute ethyl alcohol, and each component summation is 100, It is mixed evenly to prepare.
Application effect appraisal:
The tobacco prepared using embodiment 1, embodiment 2, embodiment 3, embodiment 4, embodiment 5, the method for embodiment 6 is former Material is added in heating non-burning smoking set with undressed tobacco material (control sample) carries out sensory quality assessment, evaluation result It is shown in Table 1.
Check problem:Sample and check table are provided to 6 experts that smoke panel test, it is desirable to which member of smoking refers to according to form requirement to items Mark is smoked panel test.
The smoking result of the embodiment of the present invention of table 1
As shown in Table 1, released with flue gas of the treated tobacco material of the method for the present invention under heating non-burning state Put performance and discharge flue gas-organoleptic quality substantially improved, by force, comfortableness is good for flue gas satisfaction, is heating non-burning Applicability in type tobacco product is remarkably reinforced.
Described above is only the preferred embodiment of the present invention, it is noted that for the ordinary skill people of the art For member, without departing from the technical principles of the invention, some improvement and deformation can also be made, these improve and deformed Also it should be regarded as protection scope of the present invention.

Claims (9)

1. a kind of low temperature cigarette tobacco material processing method, it is characterised in that comprise the following steps:
Step SS1 alkali lye is extracted, and is specifically included:Alkali lye is added in tobacco material and extracted, progress is ultrasonically treated, is transferred to the step Rapid SS2;The alkali lye used in the step SS1 for various concentrations NH4OH solution, NaOH solution, K2CO3Solution, Ca (OH)2 Solution, Na2CO3One kind in solution;
Step SS2 suction filtrations, are specifically included:Suction filtration discards the extraction alkali lye of the step SS1, adds pure water tobacco material is quick Washing, discards cleaning solution, is transferred to step SS3;
Step SS3 is dried, and is specifically included:By tobacco material low temperature drying made from step SS2, step SS4 is transferred to;
Step SS4 flavoring and casings, are specifically included:By the tobacco material dried made from step SS3 be placed in balance environment in 24~ After 48h, apply the ethanol solution containing flavouring essence for tobacco and polyalcohol thereto, and place 24~48h in sealed states, turn Enter step SS5;
Step SS5 is balanced, and is specifically included:Tobacco material made from the step SS4 is placed in balance environment after 48h, obtained Tobacco-containing material suitable for heating non-burning cigarette.
2. a kind of low temperature cigarette tobacco material processing method according to claim 1, it is characterised in that the step The tobacco material used in SS1 is any one or a few in flue-cured tobacco, Turkish tobaccos, burley tobaccos.
3. a kind of low temperature cigarette tobacco material processing method according to claim 1, it is characterised in that the step In SS1, the applied amount of alkali lye and tobacco material is MPipe tobacco:VAlkali lye=1.0g:6~20mL.
4. a kind of low temperature cigarette tobacco material processing method according to claim 1, it is characterised in that the step The ultrasonically treated time in SS1 is 5-60min.
5. a kind of low temperature cigarette tobacco material processing method according to claim 1, it is characterised in that the step In SS3, the temperature of tobacco material low temperature drying is 40~70 DEG C.
6. a kind of low temperature cigarette tobacco material processing method according to claim 1, it is characterised in that the step Balance environment in SS4 includes balancing the tobacco material of drying in 22 DEG C of temperature, the environment of relative humidity 60%.
7. a kind of low temperature cigarette tobacco material processing method according to claim 1, it is characterised in that the step Flavouring essence for tobacco in SS4 is eugenol, ethylmaltol, damascone, 2- acetylpyridines, 4- hydroxyl -2,5- dimethyl -3 One or more of mixing in (2H) furanone.
8. a kind of low temperature cigarette tobacco material processing method according to claim 1, it is characterised in that the step Polyalcohol in SS4 for any one or two kinds of propane diols, glycerine mixing.
9. according to a kind of any described low temperature cigarette tobacco material processing methods of claim 1-8, it is characterised in that described Balance environment in step SS5 includes the tobacco material after flavouring essence for tobacco processing will be added to be placed in 22 DEG C of temperature, relative humidity 60% Environment in balance.
CN201610807097.6A 2016-09-06 2016-09-06 A kind of low temperature cigarette tobacco material processing method Active CN106263012B (en)

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Application Number Priority Date Filing Date Title
CN201610807097.6A CN106263012B (en) 2016-09-06 2016-09-06 A kind of low temperature cigarette tobacco material processing method

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CN106263012B true CN106263012B (en) 2017-09-15

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Publication number Priority date Publication date Assignee Title
CN109275943A (en) * 2018-10-08 2019-01-29 浙江中烟工业有限责任公司 A method of moisture in cut tobacco being controlled under not combustion state suitable for heating
CN109275934A (en) * 2018-10-08 2019-01-29 浙江中烟工业有限责任公司 A kind of processing method suitable for heating pipe tobacco under not combustion state
CN111748410A (en) * 2020-07-01 2020-10-09 云南绅博源生物科技有限公司 Sweet essence for adding to tobacco and preparation method thereof

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US20160029689A1 (en) * 2013-03-15 2016-02-04 Philip Morris Products S.A. Methods for reducing one or more tobacco specific nitrosamines in tobacco material
CN105595399B (en) * 2016-02-04 2017-04-12 江苏中烟工业有限责任公司 Treatment method applicable to tobacco raw material of heated non-burning cigarette

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