CN106260746A - A kind of preparation method of pet fish special growth conditioning agent - Google Patents
A kind of preparation method of pet fish special growth conditioning agent Download PDFInfo
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- CN106260746A CN106260746A CN201610647995.XA CN201610647995A CN106260746A CN 106260746 A CN106260746 A CN 106260746A CN 201610647995 A CN201610647995 A CN 201610647995A CN 106260746 A CN106260746 A CN 106260746A
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K35/00—Medicinal preparations containing materials or reaction products thereof with undetermined constitution
- A61K35/02—Medicinal preparations containing materials or reaction products thereof with undetermined constitution from inanimate materials
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K31/00—Medicinal preparations containing organic active ingredients
- A61K31/70—Carbohydrates; Sugars; Derivatives thereof
- A61K31/715—Polysaccharides, i.e. having more than five saccharide radicals attached to each other by glycosidic linkages; Derivatives thereof, e.g. ethers, esters
- A61K31/737—Sulfated polysaccharides, e.g. chondroitin sulfate, dermatan sulfate
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K36/00—Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
- A61K36/18—Magnoliophyta (angiosperms)
- A61K36/185—Magnoliopsida (dicotyledons)
- A61K36/73—Rosaceae (Rose family), e.g. strawberry, chokeberry, blackberry, pear or firethorn
- A61K36/738—Rosa (rose)
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- Y02A40/00—Adaptation technologies in agriculture, forestry, livestock or agroalimentary production
- Y02A40/80—Adaptation technologies in agriculture, forestry, livestock or agroalimentary production in fisheries management
- Y02A40/81—Aquaculture, e.g. of fish
- Y02A40/818—Alternative feeds for fish, e.g. in aquacultures
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Abstract
The invention discloses the preparation method of a kind of pet fish special growth conditioning agent, belong to technical field of aquaculture；The method uses the mode that oxidized activating technology, molecular weight cutting technique, ULTRASONIC COMPLEX technology are combined, using meal wheat stone and brown coal as raw material, by Green Oxidant oxidized activating, again through membrane filtration purification enrichment, utilize afterwards and ultrasonic compound with Fructus Rosae Normalis concentrated juice, sulfated fucan etc. obtain a kind of liquid preparation.Said preparation can strengthen immunity and the vigor of fish body, promotes that gastro-intestinal digestion absorbs, has simultaneously and improve water body environment, and antibacterial disease-resistant effect can reduce shoal of fish sickness rate and mortality rate dramatically.Additionally, this product safety environmental protection, non-stimulated, have no side effect, applied widely, continuous large-scale production can be realized.
Description
Technical field
The present invention relates to the preparation method of a kind of pet fish special growth conditioning agent, belong to chemical technology field.
Background technology
Pet fish is liked by people again with prismy color, graceful colourful figure and stroke.According to investigations,
Pet fish has become the third-largest house pet being only second to cat and Canis familiaris L..In recent years, along with the raising day by day of China's people's living standard, see
Reward fish and aquarium have been increasingly becoming the new fashion of new period household consumption；Shop, hotel, tourist attractions, house are come into little
The public places such as district, become beautify the environment, promote quality of life, cultivate the moral character and nourish the nature, one of main contents moulding delight of life.?
In the culture of ornamental fish, dissolved oxygen change, water temperature change, acid-base value change, change of water quality, harmful microorganism invasion and attack etc. all may cause
Stress, this can not only affect the healthy growth of the shoal of fish, and may result in fish body immunity degradation, induces pathological changes the most dead
Die.Therefore, strictly one fine work of breeding fish, every aspect will take the utmost care of.In addition to diet, it is also desirable to some auxiliary are arranged
Execute and improve shoal of fish growing environment.
Fulvic acid is that humic acids middle-molecular-weihydroxyethyl is minimum, dissolubility is the highest, biological activity The cream of the crop, easily by people with dynamic
Thing absorbs.In recent years, many reports have affirmed that fulvic acid and salt thereof are exempted from antibacterial, antiinflammatory, antiviral, antiulcer, regulation
Epidemic disease system, the remarkable result of the aspect such as aid digestion, represent its wide application prospect in the field such as medical, agriculture.The present inventor
Team is devoted for years in the biologic applications basic research of fulvic acid (and salt), understands that fulvic acid (and salt) is because of raw material group deeply
Become different, processing technique different or even enriched composition different and cause it that finally the physicochemical property including biological activity is not
With.It is true that along with the understanding of fulvic acid (and salt) is deepened continuously by we, it is pressed the pin of molecular size range cutting classification
Property is utilized and has had become as a new trend.Particularly, the wherein substance bioactivity of molecular weight this sight best
Point is proved by substantial amounts of test.Meanwhile, the humic acids (fulvic acid) after peroxide degradation activates is more than primary humic acids
The active component of (fulvic acid) is much more, merges " molecular weight cutting classification technique " hence with " oxidative degradation activating technology " again
High bioactivity and chemically active fulvic acid and salt thereof can be extracted, it addition, implementing " molecular weight cutting classification technique "
While can realize the purpose of purifying products.And based on this be processed further utilize, progressively become fulvic acid and
The important breakthrough mouth of the related industry grafting upgrading and transformation such as salt and big medicine, multi-form agriculture.
Therefore, we are summing up forefathers' fulvic acid and the successful experience of technology of threonates thereof and the basis of problem defect
On, innovated the core process of fulvic acid and salt thereof, improve dramatically fulvic acid and the purity of salt thereof, biological activity,
And safety.And be combined with the Pharmaceutical ingredients such as Fructus Rosae Normalis extract, sulfated fucan based on this, prepare one
The special growth conditioning agent of Novel ornamental fish, for ensureing that growing up healthy and sound of the shoal of fish provides a kind of new adjuvant to select.
Summary of the invention
It is an object of the invention to provide the preparation method of a kind of pet fish special growth conditioning agent, it uses brand-new work
Technology prepares that a kind of function is many, usefulness fast, low cost, the fish built agent that has no side effect, carries for the culture of ornamental fish
A kind of reliable healthy adjuvant has been supplied to select.
The preparation method step of pet fish of the present invention special growth conditioning agent is as follows:
(1) being dried by brown coal to moisture is 15-20%, crosses 80-100 mesh sieve, obtain brown coal powder, then by meal wheat stone powder after pulverizing
Broken, also cross 80-100 mesh sieve, obtain meal wheat stone powder, then be that 1:500-800 carried out with brown coal powder according to weight ratio by meal wheat stone powder
Mixing, obtains mixed powder, standby；
(2) sodium hydroxide solution is pressed: peracetic acid soln: three is premixed by the mass ratio of hydrogenperoxide steam generator=1:1-3:50-80
Even, obtain oxidation solution, standby, wherein sodium hydroxide solution be mass fraction be 20-30%, peracetic acid in peracetic acid soln
Mass percent concentration be 20-30%, in hydrogenperoxide steam generator, the mass percent concentration of hydrogen peroxide is 20-30%；
(3) emulsified silicone oil is pressed: the two is mixed by the mass ratio of rhamnolipid=1:2-4 in advance, obtains oxidation promoter, standby；
(4) by oxidation promoter: mixed powder: three is inserted instead by the mass ratio of oxidation solution=1:1000-1500:2000-3000 successively
Answering still, be stirred under the condition of normal pressure of 50-60 DEG C, speed of agitator is 80-100r/min, and mixing time is 40-60min,
Adding the deionized water that weight is oxidation solution 3-5 times afterwards, and temperature of reaction kettle rises to 60-70 DEG C, speed of agitator is adjusted to
60-80r/min, continues stirring 10-15min, is subsequently added into the sodium hydroxide solution regulation that mass percent concentration is 20-30%
PH value is to 7-8, and stirring reaction 15-20min under the conditions of 70-80 DEG C, is finally cooled to 30-40 DEG C, after standing 20-30min,
Take standing liquid, standby；
(5) liquid centrifugal 10-15min under the conditions of 3000-5000r/min will be stood, obtain supernatant, then carry out vacuum mistake
Filter, then vacuum filtrate is inserted molecular cut off is that the daltonian film filter of 500-1000 filters, and obtains fulvic acid
Saline solution, standby；
(6) sulfated fucan is pressed: Fructus Rosae Normalis concentrated juice: the mass ratio of Xanthohumate solution=1:5-10:800-1000 is by three
Insert the ultrasonic response still that supersonic frequency is 30-40kHz successively, and be 40-50 DEG C and speed of agitator is 80-in temperature
Under the conditions of 100r/min, compound 20-30min, is finally cooled to 20-30 DEG C, and the mixed solution obtained is the special growth of pet fish
Conditioner.
Beneficial effects of the present invention:
(1) agent of pet fish provided by the present invention special growth conditioning can strengthen immunity and the vigor of fish body, promotes that gastrointestinal disappears
Change and absorb；
(2) agent of pet fish provided by the present invention special growth conditioning has and improves water body environment, and antibacterial disease-resistant effect can pole
Big degree ground reduces shoal of fish sickness rate and mortality rate；
(3) pet fish provided by the present invention special growth conditioning agent safety and environmental protection, non-stimulated, have no side effect, applied widely；
(4) preparation method provided by the present invention operation is relatively easy, and cost relative reduction can realize continuous large-scale production.
Detailed description of the invention
Below by embodiment, the present invention is described in further detail, but scope is not limited to described content.
Embodiment 1:
The preparation method of the special growth conditioning agent of pet fish described in the present embodiment, specifically comprises the following steps that
(1) being dried by brown coal to moisture is 15%, crosses 80 mesh sieves, obtains brown coal powder, then pulverized by meal wheat stone, also mistake after pulverizing
80 mesh sieves, obtain meal wheat stone powder, then are that 1:500 mix with brown coal powder according to weight ratio by meal wheat stone powder, obtain mixed powder,
Standby；
(2) by sodium hydroxide solution: peracetic acid soln: three is mixed by the mass ratio of hydrogenperoxide steam generator=1:1:50 in advance,
To oxidation solution, standby, wherein sodium hydroxide solution be mass fraction be 20%, the quality hundred of peracetic acid in peracetic acid soln
Proportion by subtraction concentration is 20%, and in hydrogenperoxide steam generator, the mass percent concentration of hydrogen peroxide is 30%；
(3) emulsified silicone oil is pressed: the two is mixed by the mass ratio of rhamnolipid=1:2 in advance, obtains oxidation promoter, standby；
(4) by oxidation promoter: mixed powder: three is inserted reactor by the mass ratio of oxidation solution=1:1000:2000 successively, 50
DEG C condition of normal pressure under be stirred, speed of agitator is 80r/min, and mixing time is 60min, add afterwards weight for oxidation
The deionized water that liquid is 3 times, and temperature of reaction kettle is risen to 60 DEG C, speed of agitator is adjusted to 60r/min, continues stirring 15min, then
Add mass percent concentration be 20% sodium hydroxide solution regulation pH value to 7, and under the conditions of 70 DEG C stirring reaction 20min,
It is finally cooled to 30 DEG C, after standing 20min, takes standing liquid, standby；
(5) liquid centrifugal 15min under the conditions of 3000r/min will be stood, obtain supernatant, then carry out vacuum filtration, then will be true
It is that 500 daltonian film filters filter that air filter liquid inserts molecular cut off, obtains Xanthohumate solution, standby；
(6) by sulfated fucan: Fructus Rosae Normalis concentrated juice: three is inserted by the mass ratio of Xanthohumate solution=1:5:800 successively
Supersonic frequency is the ultrasonic response still of 30kHz, and compound under the conditions of temperature is 40 DEG C and speed of agitator is 100r/min
20min, is finally cooled to 20 DEG C, and the mixed solution obtained is pet fish special growth conditioning agent.
The pet fish special growth conditioning agent that the present embodiment prepares specifically apply effect:
Test with fish be on market buy view and admire Cyprinus carpio, about body weight 200g, test respectively three aquariums (1096mm ×
470mm × 670mm) in carry out, matched group is taked normally to raise, and test group 1 is 1(every liter in proportion on the basis of normal raising
Cultivation water adds 0.1 milliliter of conditioner) add conditioner, test group 2 is 2(every liter cultivation in proportion on the basis of normal raising
Water adds 0.2 milliliter of conditioner) add conditioner.Each aquarium is put 30 in a suitable place to breed and is viewed and admired Cyprinus carpio, and test group is adjusted every dropping in 5 days
Reason agent once, is changed water 1 time simultaneously, is changed water 30% every time, and long run test stopped after 1 month, and recorded every inspection target, result
As shown in table 1.
Table 1 result of the test
Embodiment 2:
The preparation method of the special growth conditioning agent of pet fish described in the present embodiment, specifically comprises the following steps that
(1) being dried by brown coal to moisture is 18%, crosses 90 mesh sieves, obtains brown coal powder, then pulverized by meal wheat stone, also mistake after pulverizing
90 mesh sieves, obtain meal wheat stone powder, then are that 1:650 mix with brown coal powder according to weight ratio by meal wheat stone powder, obtain mixed powder,
Standby；
(2) by sodium hydroxide solution: peracetic acid soln: three is mixed by the mass ratio of hydrogenperoxide steam generator=1:2:65 in advance,
To oxidation solution, standby, wherein sodium hydroxide solution be mass fraction be 25%, the quality hundred of peracetic acid in peracetic acid soln
Proportion by subtraction concentration is 25%, and in hydrogenperoxide steam generator, the mass percent concentration of hydrogen peroxide is 25%；
(3) emulsified silicone oil is pressed: the two is mixed by the mass ratio of rhamnolipid=1:3 in advance, obtains oxidation promoter, standby；
(4) by oxidation promoter: mixed powder: three is inserted reactor by the mass ratio of oxidation solution=1:1200:2500 successively, 55
DEG C condition of normal pressure under be stirred, speed of agitator is 90r/min, and mixing time is 50min, add afterwards weight for oxidation
The deionized water that liquid is 4 times, and temperature of reaction kettle is risen to 65 DEG C, speed of agitator is adjusted to 70r/min, continues stirring 12min, then
Add mass percent concentration be 25% sodium hydroxide solution regulation pH value to 7.5, and under the conditions of 75 DEG C stirring reaction
18min, is finally cooled to 35 DEG C, after standing 25min, takes standing liquid, standby；
(5) liquid centrifugal 12min under the conditions of 4000r/min will be stood, obtain supernatant, then carry out vacuum filtration, then will be true
It is that 800 daltonian film filters filter that air filter liquid inserts molecular cut off, obtains Xanthohumate solution, standby；
(6) by sulfated fucan: Fructus Rosae Normalis concentrated juice: three is inserted by the mass ratio of Xanthohumate solution=1:8:900 successively
Supersonic frequency is the ultrasonic response still of 35kHz, and compound under the conditions of temperature is 45 DEG C and speed of agitator is 90r/min
25min, is finally cooled to 25 DEG C, and the mixed solution obtained is pet fish special growth conditioning agent.
The pet fish special growth conditioning agent that the present embodiment prepares specifically apply effect:
Test method: as described in Example 1, result is as shown in table 2.
Table 2 result of the test
Embodiment 3:
The preparation method of the special growth conditioning agent of pet fish described in the present embodiment, specifically comprises the following steps that
(1) being dried by brown coal to moisture is 20%, crosses 100 mesh sieves, obtains brown coal powder, then pulverized by meal wheat stone, also mistake after pulverizing
100 mesh sieves, obtain meal wheat stone powder, then are that 1:800 mix with brown coal powder according to weight ratio by meal wheat stone powder, are mixed
Powder, standby；
(2) by sodium hydroxide solution: peracetic acid soln: three is mixed by the mass ratio of hydrogenperoxide steam generator=1:3:80 in advance,
To oxidation solution, standby, wherein sodium hydroxide solution be mass fraction be 30%, the quality hundred of peracetic acid in peracetic acid soln
Proportion by subtraction concentration is 30%, and in hydrogenperoxide steam generator, the mass percent concentration of hydrogen peroxide is 20%；
(3) emulsified silicone oil is pressed: the two is mixed by the mass ratio of rhamnolipid=1:4 in advance, obtains oxidation promoter, standby；
(4) by oxidation promoter: mixed powder: three is inserted reactor by the mass ratio of oxidation solution=1:1500:3000 successively, 60
DEG C condition of normal pressure under be stirred, speed of agitator is 100r/min, and mixing time is 40min, and adding weight afterwards is oxygen
Changing the deionized water of liquid 5 times, and temperature of reaction kettle rises to 70 DEG C, speed of agitator is adjusted to 80r/min, continues stirring 10min, connects
Add mass percent concentration be 30% sodium hydroxide solution regulation pH value to 8, and under the conditions of 80 DEG C stirring reaction
15min, is finally cooled to 40 DEG C, after standing 30min, takes standing liquid, standby；
(5) liquid centrifugal 10min under the conditions of 5000r/min will be stood, obtain supernatant, then carry out vacuum filtration, then will be true
It is that 1000 daltonian film filters filter that air filter liquid inserts molecular cut off, obtains Xanthohumate solution, standby；
(6) by sulfated fucan: Fructus Rosae Normalis concentrated juice: three is put by the mass ratio of Xanthohumate solution=1:10:1000 successively
Enter the ultrasonic response still that supersonic frequency is 40kHz, and compound under the conditions of temperature is 50 DEG C and speed of agitator is 80r/min
30min, is finally cooled to 30 DEG C, and the mixed solution obtained is pet fish special growth conditioning agent.
The pet fish special growth conditioning agent that the present embodiment prepares specifically apply effect:
Test method: as described in Example 1, result is as shown in table 3.
Table 3 result of the test
Claims (1)
1. the preparation method of a pet fish special growth conditioning agent, it is characterised in that carry out as follows:
(1) being dried by brown coal to moisture is 15-20%, crosses 80-100 mesh sieve, obtain brown coal powder, then by meal wheat stone powder after pulverizing
Broken, also cross 80-100 mesh sieve, obtain meal wheat stone powder, then be that 1:500-800 carried out with brown coal powder according to weight ratio by meal wheat stone powder
Mixing, obtains mixed powder, standby；
(2) sodium hydroxide solution is pressed: peracetic acid soln: three is premixed by the mass ratio of hydrogenperoxide steam generator=1:1-3:50-80
Even, obtain oxidation solution, standby；Wherein sodium hydroxide solution be mass fraction be 20-30%, peracetic acid in peracetic acid soln
Mass percent concentration be 20-30%, in hydrogenperoxide steam generator, the mass percent concentration of hydrogen peroxide is 20-30%；
(3) emulsified silicone oil is pressed: the two is mixed by the mass ratio of rhamnolipid=1:2-4 in advance, obtains oxidation promoter, standby；
(4) by oxidation promoter: mixed powder: three is inserted instead by the mass ratio of oxidation solution=1:1000-1500:2000-3000 successively
Answering still, be stirred under the condition of normal pressure of 50-60 DEG C, speed of agitator is 80-100r/min, and mixing time is 40-60min,
Adding the deionized water that weight is oxidation solution 3-5 times afterwards, and temperature of reaction kettle rises to 60-70 DEG C, speed of agitator is adjusted to
60-80r/min, continues stirring 10-15min, is subsequently added into the sodium hydroxide solution regulation that mass percent concentration is 20-30%
PH value is to 7-8, and stirring reaction 15-20min under the conditions of 70-80 DEG C, is finally cooled to 30-40 DEG C, after standing 20-30min,
Take standing liquid, standby；
(5) liquid centrifugal 10-15min under the conditions of 3000-5000r/min will be stood, obtain supernatant, then carry out vacuum mistake
Filter, then vacuum filtrate is inserted molecular cut off is that the daltonian film filter of 500-1000 filters, and obtains fulvic acid
Saline solution, standby；
(6) sulfated fucan is pressed: Fructus Rosae Normalis concentrated juice: the mass ratio of Xanthohumate solution=1:5-10:800-1000 is by three
Insert the ultrasonic response still that supersonic frequency is 30-40kHz successively, and be 40-50 DEG C and speed of agitator is 80-in temperature
Under the conditions of 100r/min, compound 20-30min, is finally cooled to 20-30 DEG C, and the mixed solution obtained is the special growth of pet fish
Conditioner.
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Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101423536A (en) * | 2008-12-02 | 2009-05-06 | 昆明理工大学 | Method for preparing humic acid and salt thereof by oxidation and degradation of brown coal |
| CN103749538A (en) * | 2014-01-07 | 2014-04-30 | 昆明理工大学 | Production method and application of low-rack coal degradation liquid |
| CN103948106A (en) * | 2014-04-30 | 2014-07-30 | 贵州金维宝刺梨开发有限公司 | Purification technology and equipment of high-enriched roxburgh rose juice and application thereof |
| CN104431170A (en) * | 2014-11-18 | 2015-03-25 | 杜小岗 | Marine bioactive polysaccharide or oligosaccharide granular tea drink for improving metabolic syndrome (six highs and one lipid) |
-
2016
- 2016-08-10 CN CN201610647995.XA patent/CN106260746A/en active Pending
Patent Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101423536A (en) * | 2008-12-02 | 2009-05-06 | 昆明理工大学 | Method for preparing humic acid and salt thereof by oxidation and degradation of brown coal |
| CN103749538A (en) * | 2014-01-07 | 2014-04-30 | 昆明理工大学 | Production method and application of low-rack coal degradation liquid |
| CN103948106A (en) * | 2014-04-30 | 2014-07-30 | 贵州金维宝刺梨开发有限公司 | Purification technology and equipment of high-enriched roxburgh rose juice and application thereof |
| CN104431170A (en) * | 2014-11-18 | 2015-03-25 | 杜小岗 | Marine bioactive polysaccharide or oligosaccharide granular tea drink for improving metabolic syndrome (six highs and one lipid) |
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