CN103948106A - Purification technology and equipment of high-enriched roxburgh rose juice and application thereof - Google Patents
Purification technology and equipment of high-enriched roxburgh rose juice and application thereof Download PDFInfo
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- CN103948106A CN103948106A CN201410178465.6A CN201410178465A CN103948106A CN 103948106 A CN103948106 A CN 103948106A CN 201410178465 A CN201410178465 A CN 201410178465A CN 103948106 A CN103948106 A CN 103948106A
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- juice
- cili juice
- cili
- equipment
- pipe
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- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L2/00—Non-alcoholic beverages; Dry compositions or concentrates therefor; Their preparation
- A23L2/02—Non-alcoholic beverages; Dry compositions or concentrates therefor; Their preparation containing fruit or vegetable juices
- A23L2/08—Concentrating or drying of juices
- A23L2/082—Concentrating or drying of juices by membrane processes
- A23L2/087—Concentrating or drying of juices by membrane processes by ultrafiltration, microfiltration
Abstract
The invention provides a purification technology of high-enriched roxburgh rose juice. The purification technology comprises the following steps: (1) pressing into juice; (2) coarsely filtering; (3) ultrafiltration; (4) concentration. The invention also provides purification equipment of high-enriched roxburgh rose juice. The purification equipment comprises a resin tank, a tubular ultrafiltration membrane and concentration equipment, wherein the resin tank, the tubular ultrafiltration membrane and the concentration equipment are sequentially connected through a pipeline; a large aperture pipe, a medium aperture pipe and a small aperture pipe are sequentially connected through a pipeline inside the tubular ultrafiltration membrane; the apertures of the membranes in the large aperture pipe, the medium aperture pipe and the small aperture pipe are gradually reduced; the concentration equipment is a tri-effect falling film concentration evaporator. The purification technology is applied to purification of the roxburgh rose juice. The purification technology is high in concentration degree, less in loss of effective components, and fewer in residual impurities.
Description
Technical field
The present invention relates to a kind of purifying technique, equipment and application thereof of highly enriched Cili Juice.
Background technology
Superoxide dismutase (SOD) has and suppresses cardiovascular and cerebrovascular disease, anti-ageing, the effect of preventing and treating autoimmune disease, Ribes burejense powder is the important sources of industrial abstract SOD, and the important source material of most enterprises production Ribes burejense powder is exactly Rosa roxburghii inspissated juice, existing Rosa roxburghii concentration technique has following defect: 1. cycles of concentration is low, the Rosa roxburghii inspissated juice cycles of concentration that existing technology is produced, less than 5 times, can not meet the requirement of industrial producing Ribes burejense powder; 2. active ingredient runs off seriously, and existing concentration technology causes the materials such as vitamin C, superoxide dismutase just to decompose in the process of processing mostly; 3. impurity is residual more, Rosa roxburghii inspissated juice inferior quality, and existing technology mostly adopts conventional machining process when filtering, and as gauze, the filter of filter bag is housed, because the aperture of filtration system is larger, filter effect is poor, and impurity is residual more.
As the application number Chinese invention patent that is CN201010151796.2 disclose a kind of can be cordate houttuynia, hoveniae semoveniae semen, Rosa roxburghii, phyllanthus emblica, calabash melon, the Superoxide Dismutase of Higher Purity that the plants such as chocho are suitable for commercial Application proposes technique, this can be cordate houttuynia, hoveniae semoveniae semen, Rosa roxburghii, phyllanthus emblica, calabash melon, the Superoxide Dismutase of Higher Purity that the plants such as chocho are suitable for commercial Application proposes the purification for Rosa roxburghii in technique and adopts first centrifugal, slightly carry, rear ultrafiltration, concentrated mode, but in this technique: 1. centrifugal and slightly put forward process in a lot of active ingredients of Rosa roxburghii run off serious, fail effectively to solve the above-mentioned active ingredient serious problem that runs off, may increase the weight of this problem on the contrary, 2. ultrafiltrate is carried out to not careful selection method for concentration of further concentrated process, and adopt general method for concentration cycles of concentration by 5 times of less thaies, can not meet the demands, fail effectively to solve the low problem of above-mentioned cycles of concentration.
The Chinese invention patent that and for example application number is CN201210265598.8 discloses the extracting method of a kind of SOD, the extracting method of this SOD can adopt full physical method extraction, separated SOD complex enzyme, but still there are the following problems: although 1. the method has adopted the method for three grades of ultrafiltration, but its final SOD solution is but second entrapment liquid and three grades of trapped fluids merges gained, and in its method, also comprise and carry out PH adjusting, add the steps such as sulphur, in final extraction finished product, residual impurity is too much inevitable, fail effectively to solve the residual many problems of above-mentioned impurity; 2. in the method, also have and adopt centrifugation to carry out separation, therefore fail effectively to solve the above-mentioned active ingredient serious problem that runs off.
Summary of the invention
For solving the problems of the technologies described above, the invention provides a kind of purifying technique, equipment and application thereof of highly enriched Cili Juice, the purifying technique of this highly enriched Cili Juice, equipment and application thereof, by adopting successively macroreticular resin, macromolecule tubular type milipore filter, triple effect falling liquid film concentration evaporator to process Cili Juice, have effectively guaranteed that, active ingredient high to the purification cycles of concentration of Cili Juice runs off less, impurity is residual few.
The present invention is achieved by the following technical programs.
The purifying technique of a kind of highly enriched Cili Juice provided by the invention; Comprise the following steps:
1. be pressed into juice: Rosa roxburghii is squeezed into Cili Juice;
2. coarse filtration: with macroreticular resin, Cili Juice is filtered to absorption, the microbe filters such as the mould that may cause in Cili Juice going mouldy and worm's ovum are fallen;
3. ultrafiltration: with polymer ultrafiltration membrane, Cili Juice is filtered, the macromolecular substances such as the brown material in Cili Juice, tannin, white depositions are filtered out;
4. concentrated: Cili Juice to be carried out to vacuum and low temperature evaporation, remove the moisture in Cili Juice, obtain Chen Pin concentrated juice of roxburgh rose.
Described step 2. middle macroreticular resin is compound macroreticular resin.
The described step 2. aperture of middle macroreticular resin is 100～400nm.
An equipment for purifying for highly enriched Cili Juice, comprises resin container, tubular ultra-filtration membrane and concentrator; Described resin container, tubular ultra-filtration membrane and concentrator successively pipeline are connected; In described tubular ultra-filtration membrane, for large-aperture pipe, mesoporous pipe, small-bore, manage pipeline successively and connect, in large-aperture pipe, mesoporous pipe, small-bore pipe, successively decrease successively in the aperture of film; Described concentrator is triple effect falling liquid film concentration evaporator.
Described concentrator is specially low temperature continous way triple effect falling liquid film concentration evaporator.
As a preferred embodiment of the present invention, the described step 2. aperture of middle macroreticular resin is 200nm.
The present invention is applied to the purification to Cili Juice.
Beneficial effect of the present invention is: 1. concentrating degree is high, and the concentration of final finished concentrated juice of roxburgh rose active ingredient reaches the more than 7 times of former Cili Juice active ingredient concentration, the level that the far super prior art of concentrating degree can reach; 2. active ingredient runs off less, and especially the vitamin number of dropouts in Rosa roxburghii significantly reduces in terms of existing technologies, is guaranteeing, on the basis of final finished superoxide dismutase concentration, also to have guaranteed unit volume vitamin content; 3. impurity is residual few, and the microorganism in Cili Juice, brown material, tannin and white depositions etc. all obtain fine removal, make the concentrated degree of purity of high power obtain powerful guarantee.
Accompanying drawing explanation
Fig. 1 is the structural representation of equipment in the present invention;
In figure: 1-resin container, 2-tubular ultra-filtration membrane, 21-large-aperture pipe, 22-mesoporous pipe, 23-small-bore pipe, 3-concentrator, 41-Cili Juice, 42-finished product concentrated juice of roxburgh rose, 43-condensed water.
The specific embodiment
Further describe technical scheme of the present invention below, but described in claimed scope is not limited to.
A kind of purifying technique of highly enriched Cili Juice; Comprise the following steps:
1. be pressed into juice: Rosa roxburghii is squeezed into Cili Juice;
2. coarse filtration: with macroreticular resin, Cili Juice is filtered to absorption, the microbe filters such as the mould that may cause in Cili Juice going mouldy and worm's ovum are fallen;
3. ultrafiltration: with polymer ultrafiltration membrane, Cili Juice is filtered, the macromolecular substances such as the brown material in Cili Juice, tannin, white depositions are filtered out;
4. concentrated: Cili Juice to be carried out to vacuum and low temperature evaporation, remove the moisture in Cili Juice, obtain Chen Pin concentrated juice of roxburgh rose.
Described step 2. middle macroreticular resin is compound macroreticular resin.
The described step 2. aperture of middle macroreticular resin is 100～400nm.
The equipment for purifying of a kind of highly enriched Cili Juice as shown in Figure 1, comprises resin container 1, tubular ultra-filtration membrane 2 and concentrator 3; Described resin container 1, tubular ultra-filtration membrane 2 and concentrator 3 successively pipeline are connected; In described tubular ultra-filtration membrane 2, be large-aperture pipe 21, mesoporous pipe 22, small-bore pipe 23 pipeline connection successively, in large-aperture pipe 21, mesoporous pipe 22, small-bore pipe 23, successively decrease successively in the aperture of film; Described concentrator 3 is triple effect falling liquid film concentration evaporator.
Described concentrator 3 is specially low temperature continous way triple effect falling liquid film concentration evaporator.
That in resin container 1, fills is macroreticular resin, and optimal selection is that aperture is the compound macroreticular resin of 200nm.
The condensed water 43 of discharging in concentrator 3 also can be used as plant area's undrinkable water and uses.
The present invention is applied to the purification to Cili Juice.
Claims (7)
1. a purifying technique for highly enriched Cili Juice, is characterized in that: comprise the following steps:
1. be pressed into juice: Rosa roxburghii is squeezed into Cili Juice;
2. coarse filtration: with macroreticular resin, Cili Juice is filtered to absorption, the microbe filters such as the mould that may cause in Cili Juice going mouldy and worm's ovum are fallen;
3. ultrafiltration: with polymer ultrafiltration membrane, Cili Juice is filtered, the macromolecular substances such as the brown material in Cili Juice, tannin, white depositions are filtered out;
4. concentrated: Cili Juice to be carried out to vacuum and low temperature evaporation, remove the moisture in Cili Juice, obtain Chen Pin concentrated juice of roxburgh rose.
2. the purifying technique of highly enriched Cili Juice as claimed in claim 1, is characterized in that: described step 2. middle macroreticular resin is compound macroreticular resin.
3. the purifying technique of highly enriched Cili Juice as claimed in claim 1 or 2, is characterized in that: the described step 2. aperture of middle macroreticular resin is 100～400nm.
4. the purifying technique of highly enriched Cili Juice as claimed in claim 1 or 2, is characterized in that: the described step 2. aperture of middle macroreticular resin is 200nm.
5. the equipment for purifying of a highly enriched Cili Juice, it is characterized in that: comprise resin container (1), tubular ultra-filtration membrane (2) and concentrator (3), described resin container (1), tubular ultra-filtration membrane (2) and concentrator (3) successively pipeline are connected; In described tubular ultra-filtration membrane (2), be the pipeline connection successively of large-aperture pipe (21), mesoporous pipe (22), small-bore pipe (23), in large-aperture pipe (21), mesoporous pipe (22), small-bore pipe (23), successively decrease successively in the aperture of film; Described concentrator (3) is triple effect falling liquid film concentration evaporator.
6. the purifying technique of highly enriched Cili Juice as claimed in claim 5, equipment and application thereof, is characterized in that: described concentrator (3) is specially low temperature continous way triple effect falling liquid film concentration evaporator.
7. the purifying technique of a kind of highly enriched Cili Juice as described in claim 1 or 5 or equipment, is characterized in that: be applied to the purification to Cili Juice.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201410178465.6A CN103948106A (en) | 2014-04-30 | 2014-04-30 | Purification technology and equipment of high-enriched roxburgh rose juice and application thereof |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201410178465.6A CN103948106A (en) | 2014-04-30 | 2014-04-30 | Purification technology and equipment of high-enriched roxburgh rose juice and application thereof |
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| Publication Number | Publication Date |
|---|---|
| CN103948106A true CN103948106A (en) | 2014-07-30 |
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| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201410178465.6A Pending CN103948106A (en) | 2014-04-30 | 2014-04-30 | Purification technology and equipment of high-enriched roxburgh rose juice and application thereof |
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Cited By (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN104643061A (en) * | 2015-01-20 | 2015-05-27 | 乐业县高野刺梨有限公司 | Preparation process for concentrated roxburgh rose essence |
| CN106036301A (en) * | 2016-06-01 | 2016-10-26 | 贵州宝寿生物科技有限公司 | Processing method of protecting SOD of concentrated rosa roxburghii juice |
| CN106036270A (en) * | 2016-06-01 | 2016-10-26 | 贵州宝寿生物科技有限公司 | Method for concentrating natural vitamin C of rosa roxburghii |
| CN106260746A (en) * | 2016-08-10 | 2017-01-04 | 云南尚呈生物科技有限公司 | A kind of preparation method of pet fish special growth conditioning agent |
| CN107223826A (en) * | 2017-06-27 | 2017-10-03 | 杭州瑞纳膜工程有限公司 | A kind of Rosa roxburghi Juice film concentration technology and concentration systems |
| CN113647536A (en) * | 2021-08-09 | 2021-11-16 | 贵州金维宝生物技术有限公司 | Preparation method of roxburgh rose juice |
| CN115399422A (en) * | 2022-08-24 | 2022-11-29 | 杭州科膜水处理工程有限公司 | Rosa roxburghii powder preparation process and equipment |
-
2014
- 2014-04-30 CN CN201410178465.6A patent/CN103948106A/en active Pending
Cited By (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN104643061A (en) * | 2015-01-20 | 2015-05-27 | 乐业县高野刺梨有限公司 | Preparation process for concentrated roxburgh rose essence |
| CN106036301A (en) * | 2016-06-01 | 2016-10-26 | 贵州宝寿生物科技有限公司 | Processing method of protecting SOD of concentrated rosa roxburghii juice |
| CN106036270A (en) * | 2016-06-01 | 2016-10-26 | 贵州宝寿生物科技有限公司 | Method for concentrating natural vitamin C of rosa roxburghii |
| CN106260746A (en) * | 2016-08-10 | 2017-01-04 | 云南尚呈生物科技有限公司 | A kind of preparation method of pet fish special growth conditioning agent |
| CN107223826A (en) * | 2017-06-27 | 2017-10-03 | 杭州瑞纳膜工程有限公司 | A kind of Rosa roxburghi Juice film concentration technology and concentration systems |
| CN113647536A (en) * | 2021-08-09 | 2021-11-16 | 贵州金维宝生物技术有限公司 | Preparation method of roxburgh rose juice |
| CN115399422A (en) * | 2022-08-24 | 2022-11-29 | 杭州科膜水处理工程有限公司 | Rosa roxburghii powder preparation process and equipment |
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| C06 | Publication | ||
| PB01 | Publication | ||
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Application publication date: 20140730 |