CN106220433A - A kind of high activity little molecule richness carbon is fertile and preparation method thereof - Google Patents
A kind of high activity little molecule richness carbon is fertile and preparation method thereof Download PDFInfo
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- CN106220433A CN106220433A CN201610615283.XA CN201610615283A CN106220433A CN 106220433 A CN106220433 A CN 106220433A CN 201610615283 A CN201610615283 A CN 201610615283A CN 106220433 A CN106220433 A CN 106220433A
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- C—CHEMISTRY; METALLURGY
- C05—FERTILISERS; MANUFACTURE THEREOF
- C05G—MIXTURES OF FERTILISERS COVERED INDIVIDUALLY BY DIFFERENT SUBCLASSES OF CLASS C05; MIXTURES OF ONE OR MORE FERTILISERS WITH MATERIALS NOT HAVING A SPECIFIC FERTILISING ACTIVITY, e.g. PESTICIDES, SOIL-CONDITIONERS, WETTING AGENTS; FERTILISERS CHARACTERISED BY THEIR FORM
- C05G3/00—Mixtures of one or more fertilisers with additives not having a specially fertilising activity
- C05G3/80—Soil conditioners
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- C—CHEMISTRY; METALLURGY
- C05—FERTILISERS; MANUFACTURE THEREOF
- C05D—INORGANIC FERTILISERS NOT COVERED BY SUBCLASSES C05B, C05C; FERTILISERS PRODUCING CARBON DIOXIDE
- C05D9/00—Other inorganic fertilisers
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- Chemical & Material Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Organic Chemistry (AREA)
- Soil Sciences (AREA)
- Pest Control & Pesticides (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Inorganic Chemistry (AREA)
- Fertilizers (AREA)
Abstract
The present invention relates to novel organic fertilizer material field, the invention discloses a kind of high activity little molecule richness carbon fertilizer and preparation method thereof；Contained by described high activity little molecule richness carbon fertilizer, raw material and weight proportion thereof are: organic solid waste: straw: kieselguhr: Concha Ostreae: wood flour is 1:(0.6～0.9): (0.04～0.1): (0.01～0.1): (0.1～0.5).Compared with prior art, high activity of the present invention little molecule richness carbon fertilizer contains abundant aminoacid, dipeptides and polypeptide, little molecule organic matter, without heavy metal, hormone, worm's ovum, pathogenic bacterium etc., there is the features such as molecule innoxious, little, high activity, low dose, less manpower, proportion is little, more loose.Have simultaneously and significantly improve soil, promote plant growing and strengthen plant resistance to environment stress, suppression effect such as plant pathogen, thoroughly solve the series of agricultural problem brought because of the use of chemical pesticide and chemical fertilizer.
Description
Technical field
The invention belongs to organic solid waste process and the technical field of organic fertilizer production, be that a kind of high activity little molecule richness carbon is fertile
And preparation method thereof, it is specifically related to a kind of method utilizing organic waste to produce little molecule richness carbon fertilizer, particularly to a kind of base
In subcritical hydrolysis method, organic waste is utilized to produce the fertile technology of high activity little molecule richness carbon and production method.
Background technology
Organic waste includes that plant garbage (such as agricultural crop straw, branch etc.), animal class garbage are (such as manure of livestock and poultry
Just), processing class garbage and life kind garbage are (such as the kitchen such as dining table, food market excess, foodstuff processing factory leftover bits and pieces, life dirt
Mud etc.).Organic waste has the features of pollution that quantity is big, kind is many, harm is many, and the annual organic waste number produced is with hundred million
Meter, simultaneous contamination accident is also increasing year by year.These organic wastes should return with carbon or Organic substance form
Go back to farmland to complete the circulation of whole material, but due in garbage beneficiating ingredient content low, available article position is the highest, and is harmful to
Component content is high, such as contains the poisonous and harmful substances such as antibiotic, aromatic hydrocarbon, heavy metal, adds municipal sludge and feces of livestock and poultry
The factors such as stench is difficult to, and crop material volume is big, fertilizer efficiency is low, cause making full use of these garbages and must carry out harmless
Change processes, and therefore cost improves.Carry out for many years although reclaiming organic waste utilizes, also achieved some achievements, but
At present the utilization rate of China's organic waste does not only improve with comparing several years ago, decreases on the contrary, crop straw burning and intensive
The pollution of environment is on the rise by the fowl and animal excrement that change cultivation brings, and soil organic matter content is more and more lower, and carbon element content is more
Coming the fewest, and carbon can not complete the loop jump at nature, therefore farmland quality is deteriorated year by year, have impact on China's agriculture
The sustainable development of industry.
The processing method processing these rubbish the most frequently used at present has landfill method, burning method and composting process.These three method is again
There are some drawbacks, such as landfill method, floor space is big, and soil, subsoil water and air are easily caused secondary by the rubbish after landfill
Polluting, surrounding enviroment easily grow mosquito, emitting offensive odor, simultaneously serious waste resource；Burning method: burn remaining slag and also to fill out
Burying, cause secondary pollution, seriously in burning process, easily generation two English, Mercury in Battery steam cause atmospheric pollution, money
Source can not get recycling；Although composting process obtains resource reutilization, but heavy metal can not get controlling, and impurity is more, processes the time
Very long, place is big.In a word, current organic solid waste treatment technology level is relatively low, is difficulty with innoxious, the resource of rubbish,
Let alone industrialization.
Subcritical water often refers to temperature compressed liquid water between 180 DEG C-350 DEG C, the H in water+And OHˉClose to weak acid and
Weak base, has the function of acid catalysis and base catalysis, and the dielectric constant of subcritical water is substantially reduced and has super ionization property, polarity
Reduce, there is dissolved organic matter and the super dissolution characteristics of inorganic matter simultaneously, additionally there is excellent mass-transfer performance and environmental protection
Etc. advantage.Utilize subcritical water can make the cellulose family in rubbish, lignin, starch based, oils, organic toxic substance and
Partly plastics etc. decompose, and make macromolecular substances be degraded to crop easily by the little molecules of fatty acids of crop utilization, protein, ammonia
The Organic substance such as base acid, polypeptide and oligosaccharide, therefore subcritical water technology utilize fertilizer efficiency obtained by the organic waste of town and country and
Activity is higher.
Currently for subcritical water treatment technology, corresponding patent documentation also has certain report, such as Chinese patent application
Number being CN201510147287, title is " Semen Maydis grit subcritical hydrolysis prepares the method for Semen Maydis polypeptide " and Chinese Patent Application No.
For CN201510411800, title is " one utilizes subcritical water to produce oligopeptide and amino acid whose method from high temperature grouts ",
I.e. by being heated to reflux reclaiming the residual oils and fats in high temperature grouts, use subsequently subcritical water hydrolysis grouts, by centrifugation, decolouring,
Ultrafiltration, nanofiltration separation, spray drying obtain oligopeptide and aminoacid respectively.This method needs heating due to preamble processing, follow-up
Add work step be also performed to be centrifuged, decolour, ultrafiltration, nanofiltration separation, the tedious steps such as spray drying, therefore energy consumption is relatively big, relatively costly.
China Patent No. is CN201520050669, and title is " the subcritical water reaction unit preparing fertilizer " and Chinese patent application
Number being CN201520051115, title is " using feces of livestock and poultry to prepare the subcritical water reaction unit of fertilizer ", this method
Disclose a kind of subcritical water reaction unit using feces of livestock and poultry to prepare fertilizer, but the method processing equipment is single, only
Processed by reactor connection, and only add simple churned mechanically mode by being passed through high-temperature steam when processing, have
Machine thing processes not thorough, and the product of post processing does not carry out follow-up utilization；China Patent No. is CN201510155926,
Title is " the Subcritical Water Extraction agent of polyphenols and extracting process in a kind of lotus solid waste ", and this method is to utilize
Subcritical water makes extractant, extractant by water, citric acid or malic acid or both mixing, Vc, sodium sulfite by certain weight
Amount number composition, enriches the content of extractant, and processing cost is higher.Additionally also have some patent literatures by subcritical
Organic solid waste is processed as the method for imflammable gas or other liquid by water.
Above-mentioned document is not the most reported about the method being added follow-up aerobic fermentation by subcritical water organic waste is raw
Produce into a whole set of processing procedure that high activity little molecule richness carbon is fertile；And want intelligent processing method in processing procedure, reduce cost, fertilizer
The multipurpose of material converts, and is all to use subcritical water to process organic waste to add the problem that aerobic fermentation needs solve.
Summary of the invention
For defect of the prior art, it is an object of the invention to provide a kind of high activity little molecule richness carbon fertilizer and preparation thereof
Method；Described preparation method specifically from utilize subcritical water process organic solid waste to process product, to making good use of aerobe fermentation process
Carry out tail product After-ripening, be prepared as fully to supplement organic matter for soil, improving soil aggregate, loose activated soil
Earth, the high activity little molecule richness carbon fertilizer of recovery soil health vigor；Whole process energy conservation is efficient, compact in design, Environmental Safety,
Fertilizer activity is high.
The present invention is to be realized by following technical scheme:
First aspect, the present invention provides a kind of high activity little molecule richness carbon fertile, and contained raw material and weight proportion thereof be: organic
Solid waste: straw: kieselguhr: Concha Ostreae: wood flour is 1:(0.6～0.9): (0.04～0.1): (0.01～0.1): (0.1～0.5)
Preferably, described organic solid waste includes changing food waste etc..
Preferably, the length of described straw, the particle diameter of wood flour are respectively less than 5cm.
Second aspect, the present invention provides the preparation method that a kind of described high activity little molecule richness carbon is fertile, comprises the steps:
Step one, according to the above ratio by organic solid waste, straw, kieselguhr, Concha Ostreae, wood flour mixing, obtains pending organic
Solid waste；
Step 2, carries out subcritical water reaction to described pending organic solid waste, obtains process product；
Step 3, carries out aerobic fermentation, Aging storage to described process product, obtains high activity little molecule richness carbon fertile.
Preferably, in step one, described addition straw, kieselguhr, Concha Ostreae, the amount of wood flour are according to described organic solid waste
Water content depending on.Preferably, in step one, described organic solid waste needs sorting to remove impurity therein before use, and right
It is pulverized.
Preferably, in step 2, described reaction betides in subcritical water processing equipment, uses Based Intelligent Control means, logical
Cross primary response still and the accumulator still of some parallel connections, carry out sequence and criticize the subcritical water organic solid waste process of column reaction, product must be processed
Thing；The method of the present invention can complete on the equipment described in patent ZL 2,010 1 0580486.2.
Preferably, in step 3, before described aerobic fermentation, need that described process product is carried out dewatering and be dried so that it is contain
Water weight is maintained at 45～65%.
Preferably, in step 3, described aerobic fermentation is at the bar adding microbe leaven in described process product
Complete under part；Described microbe leaven is commercially available prod, such as Gymboree bio-fermentation agent, and Beijing China Kang Yuan science and technology has
Limit company.
Preferably, the consumption of described microbe leaven is: process product per ton adds 3kg microbe leaven.
Preferably, described aerobic fermentation, Aging storage, particularly as follows: stand 2 days, carry out turning when temperature is increased to 65 DEG C
Stirring, then stand 2～3 days, when temperature is increased to about 65 DEG C, carry out secondary turning, be repeated in this process, until processing
Product moisture content is down to less than 30%.
Preferably, described preparation method also include the product after aerobic fermentation, Aging storage is pulverized, sieve, measure and
The step of pack.
The third aspect, the present invention provides a kind of described high activity little molecule richness carbon fertile at promotion plant growth, raising fruit
Application in quality.
Preferably, described crop specifically includes Fructus Pruni pseudocerasi.
In the high activity little molecule richness carbon fertilizer of the present invention, Concha Ostreae can neutralize the portion that subcritical water decomposing organic matter produces
Divide organic acid, adjust fertilizer pH value to 5.5～8；Concha Ostreae can fully discharge calcium constituent therein in the reaction so that calcareous fertilisers
Effectiveness increase substantially, supplement the big moderate-element such as phosphorus, calcium, magnesium simultaneously；The kieselguhr added reacts through subcritical water, its
In mineral element will be chelated by Organic substance, improve effectiveness and the utilization rate of element.Add wood flour or the effect of straw
Plastic degradation speed in the moisture of changing food waste, the most beneficially rubbish can be reduced improve.
Compared with prior art, the present invention has a following beneficial effect:
1, fully process the Concha Ostreae that coastal area is discarded, reduce Concha Ostreae and arbitrarily abandon and heap is rivals in a contest the danger that environment causes
Evil；
2, processing product calcium content is 19.6mol/kg, fully can provide sufficient calcium constituent for crop；
3, process product to be 85% containing little molecule (molecular weight the is less than 500) content of organic matter and be high activity, plant absorption
Utilizing usefulness is 2～3 times of common fertilizer；
4, the nutrient substance that process product contains is concentrated type, and consumption is the 15～30% of common fertilizer；
5, after aerobic After-ripening, product characteristics are stable, commodity shelf life extension；
6, product of the present invention can improve Available phosphorus enzymatic activity 83%, makes effective bacterial number in soil improve
68.92%；
7, product of the present invention can make strawberry fruit sugariness increase by 14.2%, and single fruit weight increases by 18.8%；
8, product of the present invention can make cherry fruit hardness improve 0.08, and keeping quality strengthens, and soluble solid improves
0.94%.
Accompanying drawing explanation
By the detailed description non-limiting example made with reference to the following drawings of reading, the further feature of the present invention,
Purpose and advantage will become more apparent upon:
Fig. 1 is the fertile and conventional fertilizer using effect local contrast figure of the present invention；
Fig. 2 is the fertile and conventional fertilizer using effect overall contrast figure of the present invention；
Wherein, " use ring to cultivate fertilizer " to be and use fertilizer of the present invention.
Detailed description of the invention
Below in conjunction with specific embodiment, the present invention is described in detail.Following example will assist in the technology of this area
Personnel are further appreciated by the present invention, but limit the present invention the most in any form.It should be pointed out that, the ordinary skill to this area
For personnel, without departing from the inventive concept of the premise, it is also possible to make some deformation and improvement.These broadly fall into the present invention
Protection domain.
The preparation method that the little molecule richness carbon of high activity described in following embodiment 1 to 3 is fertile, comprises the steps:
Step one, according to the above ratio by organic solid waste, straw, kieselguhr, Concha Ostreae, wood flour mixing, obtains pending organic
Solid waste；
Step 2, carries out subcritical water reaction to described pending organic solid waste, obtains process product；
Step 3, carries out aerobic fermentation, Aging storage to described process product, obtains high activity little molecule richness carbon fertile.
In step one, described addition straw, kieselguhr, Concha Ostreae, the amount of wood flour are aqueous according to described organic solid waste
Depending on amount；Described organic solid waste needs sorting to remove impurity therein before use, and pulverizes it.
In step 2, described reaction betides in subcritical water processing equipment, uses Based Intelligent Control means, if by dry doubling
The primary response still of connection and accumulator still, carry out sequence and criticize the subcritical water organic solid waste process of column reaction, obtain process product；The present invention
Method can complete on the equipment described in patent ZL 2,010 1 0580486.2.
In step 3, before described aerobic fermentation, need that described process product is carried out dewatering and be dried so that it is wet weight is protected
Hold 45～65%；Described aerobic fermentation completes under conditions of adding microbe leaven in described process product；
Described microbe leaven is commercially available prod, such as Gymboree bio-fermentation agent, Kang Yuan Science and Technology Ltd. of Beijing China；Described
The consumption of microbe leaven is: process product per ton adds 3kg microbe leaven；Described aerobic fermentation, Aging storage have
Body is: stand 2 days, carries out turning stirring, then stands 2～3 days, treat that temperature is increased to about 65 DEG C when temperature is increased to 65 DEG C
Shi Jinhang secondary turning, is repeated in this process, until processing product moisture content to be down to less than 30%.
Further, described preparation method also includes the product after aerobic fermentation, Aging storage is pulverized, sieves, measured
And the step of pack.
Embodiment 1
The present embodiment provides a kind of high activity little molecule richness carbon fertile, and the organic solid waste of employing is changing food waste, described straw
Length and the particle diameter of wood flour less than 5cm；The weight ratio of each component is changing food waste: straw: kieselguhr: Concha Ostreae: wood flour=1
∶0.8:0.05:0.1:0.3。
Said components is processed through aerobic fermentation and get final product again after sub-critical treatment technique.
Usage amount is 100kg/ mu.
Embodiment 2
The present embodiment provides a kind of high activity little molecule richness carbon fertile, and the organic solid waste of employing is changing food waste, described straw
Length and the particle diameter of wood flour less than 5cm；The weight ratio of each component is changing food waste: straw: kieselguhr: Concha Ostreae: wood flour=1
∶0.6:0.05:0.1:0.5。
Said components is processed through aerobic fermentation and get final product again after sub-critical treatment technique.
Usage amount is 150kg/ mu.
Embodiment 3
The present embodiment provides a kind of high activity little molecule richness carbon fertile, and the organic solid waste of employing is changing food waste, described straw
Length and the particle diameter of wood flour less than 5cm；The weight ratio of each component is changing food waste: straw: kieselguhr: Concha Ostreae: wood flour=1
∶0.9:0.05:0.1:0.1。
Said components is processed through aerobic fermentation and get final product again after sub-critical treatment technique.
Usage amount is 200kg/ mu.
Comparative example 1
This comparative example is the comparative example of above-described embodiment, is in place of contrast, does not uses fertilizer of the present invention to sample plot, and
It is to use chicken manure, 3 cubes of chicken manure/mus.
Comparative example 2
This comparative example is the comparative example of above-described embodiment, is in place of contrast, does not uses fertilizer of the present invention to sample plot, and
It is to use commercially available common fertilizer.
Comparative example 3
This comparative example provides a kind of high activity little molecule richness carbon fertile, and the organic solid waste of employing is changing food waste, described straw
Length and the particle diameter of wood flour less than 5cm；The weight ratio of each component is changing food waste: straw: kieselguhr: Concha Ostreae: wood flour=1
∶0.3:0.05:0.1:0.3。
Said components is processed through aerobic fermentation and get final product again after sub-critical treatment technique.
Usage amount is 100kg/ mu.
Comparative example 4
This comparative example provides a kind of high activity little molecule richness carbon fertile, and the organic solid waste of employing is changing food waste, described straw
Length and the particle diameter of wood flour less than 5cm；Each component and weight ratio are changing food waste: straw: kieselguhr: Concha Ostreae: wood flour=1
: 0.6:0.05:0.1:0.05 adds straw.
Said components processes through aerobic fermentation after sub-critical treatment technique again.
Usage amount is 150kg/ mu.
Comparative example 5
This comparative example provides a kind of high activity little molecule richness carbon fertile, and the organic solid waste of employing is changing food waste, described straw
Length and the particle diameter of wood flour less than 5cm；Each component and weight ratio thereof are changing food waste: straw: kieselguhr: Concha Ostreae: wood flour
=1: 0.9:0.2:0.1:0.1.
Said components processes through aerobic fermentation after sub-critical treatment technique again.
Usage amount is 200kg/ mu.
Field efficacy
Select the cherry orchard of JIUYUE Fertilizer In Autumn base fertilizer as experimental subject.
Design with randomized block experiment, three repetitions are set every community.Process is provided that
By comparative example 1, the product that embodiment 1～3 obtains is spreading fertilizer over the fields under tree tries to get to the heart of a matter by the end of September, uniformly ploughs under soil with hoe rake
Under.After process, Second Year measures sweet cherry leaves size, leaf color and chlorophyll relative content spring.After fruit harvesting, survey
Determine fruit single fruit weight, the hardness of fruit and soluble solid content.
Using excel2013 and DPS7.05 statistical software to carry out, multiple comparisons uses Duncan duncan's new multiple range method.
Table 1 different disposal measurement result (detection method is this area conventional method) to Physiological Index in Leaves
The physiological index determining result of different disposal blade is as shown in table 1.As it can be seen from table 1 embodiment 1～2 with than
Relatively example 1 is compared: can significantly improve Fructus Pruni pseudocerasi tree vigo(u)r, increases leaf blade size, and leaf color is more dark green, and chlorophyll content significantly improves.With
Upper result shows, high activity little molecule richness carbon fertilizer ratio in terms of improving cherry fruit single fruit weight, soluble solid content is common
Chicken manure effect becomes apparent from.
Table 2 different disposal fruit quality index determining result (detection method is this area conventional method)
The index of quality measurement result of different disposal fruit is as shown in table 2:
Embodiment 1 is compared with comparative example 3, and single fruit weight significantly improves, and the hardness of fruit improves 0.08, and keeping quality strengthens, solvable
Property solid content improve 0.94%, difference is more significant.
Embodiment 2 is compared with comparative example 4, and single fruit weight difference is not notable, and soluble solid content difference is not notable, but fruit
Real hardness improves 0.075, and keeping quality improves.
Embodiment 3 is compared with comparative example 5, and single fruit weight significantly improves, and soluble solid content significantly improves.
Fig. 1 is the fertile and conventional fertilizer using effect local contrast figure of the present invention；Fig. 2 is the fertile and conventional fertilizer of the present invention
Using effect overall contrast figure；Wherein, " use ring to cultivate fertilizer " to be and use fertilizer of the present invention.As seen from Figure 1, Figure 2, the present invention produces
Thing can significantly improve Fructus Pruni pseudocerasi tree vigo(u)r, increases leaf blade size, and leaf color is more dark green, and chlorophyll content significantly improves.
Above the specific embodiment of the present invention is described.It is to be appreciated that the invention is not limited in above-mentioned
Particular implementation, those skilled in the art can make various deformation or amendment within the scope of the claims, this not shadow
Ring the flesh and blood of the present invention.
Claims (10)
1. a high activity little molecule richness carbon is fertile, it is characterised in that contained raw material and weight proportion thereof be: organic solid waste: straw:
Kieselguhr: Concha Ostreae: wood flour is 1:(0.6～0.9): (0.04～0.1): (0.01～0.1): (0.1～0.5).
High activity the most according to claim 1 little molecule richness carbon is fertile, it is characterised in that described organic solid waste includes kitchen rubbish
Rubbish.
High activity the most according to claim 1 little molecule richness carbon is fertile, it is characterised in that the length of described straw, wood flour
Particle diameter is respectively less than 5cm.
4. one kind according to the fertile preparation method of high activity little molecule richness carbon described in any one of claims 1 to 3, it is characterised in that
Comprise the steps:
Step one, according to the above ratio by organic solid waste, straw, kieselguhr, Concha Ostreae, wood flour mixing, obtains pending organic solid waste；
Step 2, carries out subcritical water reaction to described pending organic solid waste, obtains process product；
Step 3, carries out aerobic fermentation, Aging storage to described process product, obtains high activity little molecule richness carbon fertile.
The preparation method that high activity the most according to claim 4 little molecule richness carbon is fertile, it is characterised in that in step one, step
In rapid one, described organic solid waste needs sorting to remove impurity therein before use, and pulverizes it.
The preparation method that high activity the most according to claim 4 little molecule richness carbon is fertile, it is characterised in that in step 3, institute
Before stating aerobic fermentation, need that described process product is carried out dewatering and be dried.
The preparation method that high activity the most according to claim 4 little molecule richness carbon is fertile, it is characterised in that in step 3, institute
State aerobic fermentation to complete under conditions of adding microbe leaven in described process product.
The preparation method that high activity the most according to claim 7 little molecule richness carbon is fertile, it is characterised in that described microorganism is sent out
The consumption of ferment agent is: process product per ton adds 3kg microbe leaven.
The preparation method that high activity the most according to claim 4 little molecule richness carbon is fertile, it is characterised in that described aerobic
Ferment, Aging storage, particularly as follows: stand 2 days, carry out turning stirring when temperature is increased to 65 DEG C, then stand 2-3 days, treat temperature liter
Carry out secondary turning when height is to about 65 DEG C, be repeated in this process, until processing product moisture content to be down to less than 30%.
10. one kind is promoting plant growth according to high activity little molecule richness carbon described in any one of claims 1 to 3 is fertile, is improving fruit
Application in real quality.
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Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
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| CN107759400A (en) * | 2017-09-13 | 2018-03-06 | 郭成东 | A kind of organic carbon fertilizer and preparation method thereof |
| CN107857674A (en) * | 2017-11-07 | 2018-03-30 | 厦门康浩生态农业有限公司 | Oyster shell soil-repairing agent and preparation method thereof |
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| CN105967926A (en) * | 2016-04-07 | 2016-09-28 | 铜陵家宴生态农业发展有限公司 | Fertilizer for boosting yield of fruits and vegetables and preparation method thereof |
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| CN1548404A (en) * | 2003-05-13 | 2004-11-24 | 上海汇仁复合有机肥料有限公司 | Production process of microbial organic composite fertilizer |
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| Publication number | Priority date | Publication date | Assignee | Title |
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| CN107759400A (en) * | 2017-09-13 | 2018-03-06 | 郭成东 | A kind of organic carbon fertilizer and preparation method thereof |
| CN107857674A (en) * | 2017-11-07 | 2018-03-30 | 厦门康浩生态农业有限公司 | Oyster shell soil-repairing agent and preparation method thereof |
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Application publication date: 20161214 |