CN106209006A - A kind of production technology of quartz-crystal resonator - Google Patents

A kind of production technology of quartz-crystal resonator Download PDF

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Publication number
CN106209006A
CN106209006A CN201610618187.0A CN201610618187A CN106209006A CN 106209006 A CN106209006 A CN 106209006A CN 201610618187 A CN201610618187 A CN 201610618187A CN 106209006 A CN106209006 A CN 106209006A
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China
Prior art keywords
wafer
quartz
crystal resonator
production technology
described step
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Application number
CN201610618187.0A
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Chinese (zh)
Inventor
周淑清
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Anhui Beilai Electronic Technology Co Ltd
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Anhui Beilai Electronic Technology Co Ltd
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Priority to CN201610618187.0A priority Critical patent/CN106209006A/en
Publication of CN106209006A publication Critical patent/CN106209006A/en
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    • HELECTRICITY
    • H03ELECTRONIC CIRCUITRY
    • H03HIMPEDANCE NETWORKS, e.g. RESONANT CIRCUITS; RESONATORS
    • H03H3/00Apparatus or processes specially adapted for the manufacture of impedance networks, resonating circuits, resonators
    • H03H3/007Apparatus or processes specially adapted for the manufacture of impedance networks, resonating circuits, resonators for the manufacture of electromechanical resonators or networks
    • H03H3/02Apparatus or processes specially adapted for the manufacture of impedance networks, resonating circuits, resonators for the manufacture of electromechanical resonators or networks for the manufacture of piezoelectric or electrostrictive resonators or networks

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  • Engineering & Computer Science (AREA)
  • Manufacturing & Machinery (AREA)
  • Piezo-Electric Or Mechanical Vibrators, Or Delay Or Filter Circuits (AREA)

Abstract

The invention discloses the production technology of a kind of quartz-crystal resonator, relate to Electronic Components Manufacturing technical field, comprise the following steps: that (1) quartz wafer grinds successively;(2) polishing;(3) corrosion is cleaned;(4) vacuum coating;(5) glue is shelved;(6) frequency modulation;(7) encapsulation lettering, the present invention is simple and convenient, and utilizes cleaning caustic solution disclosed by the invention, English wafer is corroded, effectively removes destruction layer, improve wafer surface conditions, it is substantially reduced resonator resistance and ageing rate, improves the qualification rate that crystal resonator produces.

Description

A kind of production technology of quartz-crystal resonator
Technical field
The invention belongs to electronic applications, it is more particularly related to the production technology of a kind of quartz-crystal resonator.
Background technology
In recent years, the application in complete electronic set of the quartz crystal components and parts widely, from common toy for children, electronics Clock and watch all be unable to do without it to colour TV, sound equipment, VCD, microprocessor, wireless telecommunications, TV signal relay etc..Along with electronic information is produced The extensive application of developing rapidly of industry, especially digitizer, the market demand of quartz crystal components and parts quickly increases, with Time to its performance, stability, precision it is also proposed that higher requirement.Therefore, development and production high-performance, high stable, high-precision stone English crystal resonator has very important significance and to produce quartz-crystal resonator of good performance, reasonably sets except having Outside meter and excellent raw material, production technology will play a decisive role.
Summary of the invention
Problem to be solved by this invention is to provide the production technology of a kind of quartz-crystal resonator.
To achieve these goals, the technical scheme that the present invention takes is:
The production technology of a kind of quartz-crystal resonator, comprises the steps:
(1) quartz wafer grinds
Being ground wafer, described grinding is divided into corase grind, middle mill and fine grinding, corase grind mainly wafer to be carried out angle and thickness Cutting, middle mill and fine grinding are wafer to carry out fine thickness adjust;
(2) polishing
Utilize buffing machine that the wafer after grinding is polished
(3) corrosion is cleaned
Wafer after polishing is put in corrosive liquid, at 40-60 DEG C, cleans corrosion 5-9min;
(4) vacuum coating
Putting on coater by the most cleaned wafer, reaching in vacuum is 6.7 × 10-3On wafer, plate metal during Pa lead Conductive film;
(5) glue is shelved
The piezoid having plated electrode is slowly put between the two metal sheets of ribbon stent, allow the two metal sheets of slotted hole tightly press from both sides Live piezoid, be then coated with last layer conducting resinl in electrode and sheet metal contact position, make conducting resinl that electrode film passes through on edge with Sheet metal contacts and produces electrical connection, after some glue, toasts about 4 hours in placing a wafer into baking oven at 220 DEG C,;
(6) frequency modulation
Frequency modulation machine is utilized will to plate the aluminium lamination plating 1-3mm on the wafer of electrode again;
(7) encapsulation lettering
Utilizing resistive seal welding machine to be packaged wafer, roasting word at 150 DEG C, the roasting word time is 5-7h.
Preferably, described step (2) is front first by hydrofluoric acid dips 2-4min of wafer concentration 30-40%.
Preferably, described step (3) is clean by wafer cleaning before corrosion, uses chromic acid to be carried out 2-4 time, then Put into deionized water and ultrasound wave carries out super washing, finally use dehydrated alcohol to carry out being dehydrated and in 100-120 DEG C of drying.
Preferably, described step (3) corrosive liquid is formulated by distilled water, ammonium fluoride and Fluohydric acid..
Preferably, in described step (3), the weight ratio of distilled water, ammonium fluoride and Fluohydric acid. is 5:1:1.
Preferably, described step (7) is hunted leak first with leak detector, after confirming to reach leak detection index, then is packaged Lettering.
Preferably, quartz resonator various performance parameters is measured after described step (7) encapsulation lettering.
Beneficial effect: the invention provides the production technology of a kind of quartz-crystal resonator, relate to Electronic Components Manufacturing Technical field, comprises the following steps: that (1) quartz wafer grinds successively;(2) polishing;(3) corrosion is cleaned;(4) vacuum coating;(5) Shelve a glue;(6) frequency modulation;(7) encapsulation lettering, the present invention is simple and convenient, and utilizes cleaning caustic solution disclosed by the invention, English wafer is corroded, effectively removes destruction layer, improve wafer surface conditions, be substantially reduced resonator resistance with old Rate, improves the qualification rate that crystal resonator produces.
Detailed description of the invention
Embodiment 1:
The production technology of a kind of quartz-crystal resonator, comprises the steps:
(1) quartz wafer grinds
Being ground wafer, described grinding is divided into corase grind, middle mill and fine grinding, corase grind mainly wafer to be carried out angle and thickness Cutting, middle mill and fine grinding are wafer to carry out fine thickness adjust;
(2) polishing
First by wafer hydrofluoric acid dips 2min of concentration 30%, the wafer after grinding is polished by recycling buffing machine
(3) corrosion is cleaned
Chromic acid to be used before etching after polishing is carried out 2 times, then puts in ultrasound wave with deionized water and carry out Surpass and wash, finally use dehydrated alcohol to carry out being dehydrated and in 100 DEG C of drying, putting in corrosive liquid, at 40 DEG C, clean corrosion 5min, described corrosive liquid is prepared by distilled water, ammonium fluoride and Fluohydric acid. and is formed by weight for 5:1:1 configuration;
(4) vacuum coating
Putting on coater by the most cleaned wafer, reaching in vacuum is 6.7 × 10-3On wafer, plate metal during Pa lead Conductive film;
(5) glue is shelved
The piezoid having plated electrode is slowly put between the two metal sheets of ribbon stent, allow the two metal sheets of slotted hole tightly press from both sides Live piezoid, be then coated with last layer conducting resinl in electrode and sheet metal contact position, make conducting resinl that electrode film passes through on edge with Sheet metal contacts and produces electrical connection, after some glue, toasts 4h in placing a wafer into baking oven at 220 DEG C;
(6) frequency modulation
Frequency modulation machine is utilized will to plate the aluminium lamination plating 1mm on the wafer of electrode again;
(7) encapsulation lettering
Hunt leak first with leak detector, confirm to reach to hunt leak after index, utilize resistive seal welding machine that wafer is packaged, with Roasting word at 150 DEG C, the roasting word time is 5h, measures quartz resonator various performance parameters after encapsulation lettering.
Embodiment 2:
The production technology of a kind of quartz-crystal resonator, comprises the steps:
(1) quartz wafer grinds
Being ground wafer, described grinding is divided into corase grind, middle mill and fine grinding, corase grind mainly wafer to be carried out angle and thickness Cutting, middle mill and fine grinding are wafer to carry out fine thickness adjust;
(2) polishing
First by wafer hydrofluoric acid dips 3min of concentration 35%, the wafer after grinding is polished by recycling buffing machine
(3) corrosion is cleaned
Chromic acid to be used before etching after polishing is carried out 3 times, then puts in ultrasound wave with deionized water and carry out Surpass and wash, finally use dehydrated alcohol to carry out being dehydrated and in 110 DEG C of drying, putting in corrosive liquid, at 50 DEG C, clean corrosion 7min, described corrosive liquid is prepared by distilled water, ammonium fluoride and Fluohydric acid. and is formed by weight for 5:1:1 configuration;
(4) vacuum coating
Putting on coater by the most cleaned wafer, reaching in vacuum is 6.7 × 10-3On wafer, plate metal during Pa lead Conductive film;
(5) glue is shelved
The piezoid having plated electrode is slowly put between the two metal sheets of ribbon stent, allow the two metal sheets of slotted hole tightly press from both sides Live piezoid, be then coated with last layer conducting resinl in electrode and sheet metal contact position, make conducting resinl that electrode film passes through on edge with Sheet metal contacts and produces electrical connection, after some glue, toasts 4.5h in placing a wafer into baking oven at 230 DEG C;
(6) frequency modulation
Frequency modulation machine is utilized will to plate the aluminium lamination plating 2mm on the wafer of electrode again;
(7) encapsulation lettering
Hunt leak first with leak detector, confirm to reach to hunt leak after index, utilize resistive seal welding machine that wafer is packaged, with Roasting word at 150 DEG C, the roasting word time is 6h, measures quartz resonator various performance parameters after encapsulation lettering.
Embodiment 3:
The production technology of a kind of quartz-crystal resonator, comprises the steps:
(1) quartz wafer grinds
Being ground wafer, described grinding is divided into corase grind, middle mill and fine grinding, corase grind mainly wafer to be carried out angle and thickness Cutting, middle mill and fine grinding are wafer to carry out fine thickness adjust;
(2) polishing
First by wafer hydrofluoric acid dips 4min of concentration 40%, the wafer after grinding is polished by recycling buffing machine
(3) corrosion is cleaned
Chromic acid to be used before etching after polishing is carried out 4 times, then puts in ultrasound wave with deionized water and carry out Surpass and wash, finally use dehydrated alcohol to carry out being dehydrated and in 120 DEG C of drying, putting in corrosive liquid, at 60 DEG C, clean corrosion 9min, described corrosive liquid is prepared by distilled water, ammonium fluoride and Fluohydric acid. and is formed by weight for 5:1:1 configuration;
(4) vacuum coating
Putting on coater by the most cleaned wafer, reaching in vacuum is 6.7 × 10-3On wafer, plate metal during Pa lead Conductive film;
(5) glue is shelved
The piezoid having plated electrode is slowly put between the two metal sheets of ribbon stent, allow the two metal sheets of slotted hole tightly press from both sides Live piezoid, be then coated with last layer conducting resinl in electrode and sheet metal contact position, make conducting resinl that electrode film passes through on edge with Sheet metal contacts and produces electrical connection, after some glue, toasts 5h in placing a wafer into baking oven at 240 DEG C;
(6) frequency modulation
Frequency modulation machine is utilized will to plate the aluminium lamination plating 3mm on the wafer of electrode again;
(7) encapsulation lettering
Hunt leak first with leak detector, confirm to reach to hunt leak after index, utilize resistive seal welding machine that wafer is packaged, with Roasting word at 150 DEG C, the roasting word time is 7h, measures quartz resonator various performance parameters after encapsulation lettering.
After process above, taking out sample respectively, measurement result is as follows:
Detection project Embodiment 1 Embodiment 2 Embodiment 3 Prior art index
Qualification rate (%) 93 95 94 90
Resistivity (Ω) 14 12 15 20
Ageing rate % 3 2 3 5
Can draw according to above table data, the quartz-crystal resonator produced than prior art when embodiment 2 parameter Resistance and ageing rate low, and improve crystal resonator produce qualification rate.
The invention provides the production technology of a kind of quartz-crystal resonator, relate to Electronic Components Manufacturing technical field, Comprise the following steps: that (1) quartz wafer grinds successively;(2) polishing;(3) corrosion is cleaned;(4) vacuum coating;(5) glue is shelved; (6) frequency modulation;(7) encapsulation lettering, the present invention is simple and convenient, and utilizes cleaning caustic solution disclosed by the invention, to English wafer Corrode, effectively remove destruction layer, improve wafer surface conditions, be substantially reduced resonator resistance and ageing rate, carry The qualification rate that high crystal resonator produces.
The foregoing is only embodiments of the invention, not thereby limit the scope of the claims of the present invention, every utilize this Equivalent structure or equivalence flow process that bright description is made convert, or are directly or indirectly used in other relevant technology necks Territory, is the most in like manner included in the scope of patent protection of the present invention.

Claims (7)

1. the production technology of a quartz-crystal resonator, it is characterised in that: comprise the steps:
(1) quartz wafer grinds
Being ground wafer, described grinding is divided into corase grind, middle mill and fine grinding, corase grind mainly wafer to be carried out angle and thickness Cutting, middle mill and fine grinding are wafer to carry out fine thickness adjust;
(2) polishing
Utilize buffing machine that the wafer after grinding is polished;
(3) corrosion is cleaned
Wafer after polishing is put in corrosive liquid, at 40-60 DEG C, cleans corrosion 5-9min;
(4) vacuum coating
Putting on coater by the most cleaned wafer, reaching in vacuum is 6.7 × 10-3On wafer, metallic conduction is plated during Pa Thin film;
(5) glue is shelved
The piezoid having plated electrode is slowly put between the two metal sheets of ribbon stent, allow the two metal sheets of slotted hole tightly press from both sides Live piezoid, be then coated with last layer conducting resinl in electrode and sheet metal contact position, make conducting resinl that electrode film passes through on edge with Sheet metal contacts and produces electrical connection, after some glue, toasts about 4 hours in placing a wafer into baking oven at 220 DEG C,;
(6) frequency modulation
Frequency modulation machine is utilized will to plate the aluminium lamination plating 1-3mm on the wafer of electrode again;
(7) encapsulation lettering
Utilizing resistive seal welding machine to be packaged wafer, roasting word at 150 DEG C, the roasting word time is 5-7h.
2. according to the production technology of a kind of quartz-crystal resonator described in claim 1, it is characterised in that: described step (2) Front first by hydrofluoric acid dips 2-4min of wafer concentration 30-40%.
3. according to the production technology of a kind of quartz-crystal resonator described in claim 2, it is characterised in that: described step (3) By wafer cleaning totally to use chromic acid to be carried out 2-4 time, then to put in ultrasound wave with deionized water and carry out before corrosion Surpass and wash, finally use dehydrated alcohol to carry out being dehydrated and in 100-120 DEG C of drying.
4. according to the production technology of a kind of quartz-crystal resonator described in claim 1, it is characterised in that: described step (3) Corrosive liquid is formulated by distilled water, ammonium fluoride and Fluohydric acid..
5. according to the production technology of a kind of quartz-crystal resonator described in claim 4, it is characterised in that: described step (3) The weight ratio of middle distilled water, ammonium fluoride and Fluohydric acid. is 5:1:1.
6. according to the production technology of a kind of quartz-crystal resonator described in claim 1, it is characterised in that: described step (7) Hunt leak first with leak detector, after confirming to reach leak detection index, then be packaged lettering.
7. according to the production technology of a kind of quartz-crystal resonator described in claim 1, it is characterised in that: described step (7) Quartz resonator various performance parameters is measured after encapsulation lettering.
CN201610618187.0A 2016-08-01 2016-08-01 A kind of production technology of quartz-crystal resonator Withdrawn CN106209006A (en)

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Application Number Priority Date Filing Date Title
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Cited By (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN106826408A (en) * 2017-02-09 2017-06-13 同济大学 A kind of lbo crystal polishing method based on crystal oxidant
CN106877833A (en) * 2016-12-29 2017-06-20 北京晨晶电子有限公司 A kind of processing method of quartz-crystal resonator
CN107453726A (en) * 2017-08-08 2017-12-08 随州泰华电子科技有限公司 A kind of technique for lifting tuning fork crystal oscillation ion(ic) etching speed
CN108346737A (en) * 2018-02-08 2018-07-31 嘉兴晶控电子有限公司 Piezoelectric quartz process for preparing substrate
CN109639254A (en) * 2018-11-28 2019-04-16 江苏海德频率科技有限公司 A kind of resonator manufacturing process of SMD3225 chip
CN110798164A (en) * 2019-10-25 2020-02-14 苏师大半导体材料与设备研究院(邳州)有限公司 Method for manufacturing electronic component

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* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN103208973A (en) * 2013-04-23 2013-07-17 铜陵市海德电子有限公司 Method for producing column type third overtone crystal resonator
CN103684318A (en) * 2013-12-04 2014-03-26 铜陵迈维电子科技有限公司 Method for manufacturing quartz-crystal resonator with silver-gilt surface
CN103684315A (en) * 2013-12-04 2014-03-26 铜陵迈维电子科技有限公司 Processing technique of quartz-crystal resonator
CN103684313A (en) * 2013-12-04 2014-03-26 铜陵迈维电子科技有限公司 Technology for manufacturing quartz crystal resonator

Patent Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN103208973A (en) * 2013-04-23 2013-07-17 铜陵市海德电子有限公司 Method for producing column type third overtone crystal resonator
CN103684318A (en) * 2013-12-04 2014-03-26 铜陵迈维电子科技有限公司 Method for manufacturing quartz-crystal resonator with silver-gilt surface
CN103684315A (en) * 2013-12-04 2014-03-26 铜陵迈维电子科技有限公司 Processing technique of quartz-crystal resonator
CN103684313A (en) * 2013-12-04 2014-03-26 铜陵迈维电子科技有限公司 Technology for manufacturing quartz crystal resonator

Cited By (8)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN106877833A (en) * 2016-12-29 2017-06-20 北京晨晶电子有限公司 A kind of processing method of quartz-crystal resonator
CN106877833B (en) * 2016-12-29 2020-04-14 北京晨晶电子有限公司 Processing method of quartz crystal resonator
CN106826408A (en) * 2017-02-09 2017-06-13 同济大学 A kind of lbo crystal polishing method based on crystal oxidant
CN107453726A (en) * 2017-08-08 2017-12-08 随州泰华电子科技有限公司 A kind of technique for lifting tuning fork crystal oscillation ion(ic) etching speed
CN108346737A (en) * 2018-02-08 2018-07-31 嘉兴晶控电子有限公司 Piezoelectric quartz process for preparing substrate
CN109639254A (en) * 2018-11-28 2019-04-16 江苏海德频率科技有限公司 A kind of resonator manufacturing process of SMD3225 chip
CN109639254B (en) * 2018-11-28 2023-05-09 江苏浩都频率科技有限公司 Manufacturing process of resonator of SMD3225 wafer
CN110798164A (en) * 2019-10-25 2020-02-14 苏师大半导体材料与设备研究院(邳州)有限公司 Method for manufacturing electronic component

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Application publication date: 20161207