CN106177492A - A kind of method improving Herba Dendrobii fresh goods effective ingredient dissolution - Google Patents
A kind of method improving Herba Dendrobii fresh goods effective ingredient dissolution Download PDFInfo
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- CN106177492A CN106177492A CN201610578900.3A CN201610578900A CN106177492A CN 106177492 A CN106177492 A CN 106177492A CN 201610578900 A CN201610578900 A CN 201610578900A CN 106177492 A CN106177492 A CN 106177492A
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- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Chemical compound O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 15
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- PCHJSUWPFVWCPO-UHFFFAOYSA-N gold Chemical compound [Au] PCHJSUWPFVWCPO-UHFFFAOYSA-N 0.000 description 1
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Classifications
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K36/00—Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
- A61K36/18—Magnoliophyta (angiosperms)
- A61K36/88—Liliopsida (monocotyledons)
- A61K36/898—Orchidaceae (Orchid family)
- A61K36/8984—Dendrobium
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23V—INDEXING SCHEME RELATING TO FOODS, FOODSTUFFS OR NON-ALCOHOLIC BEVERAGES AND LACTIC OR PROPIONIC ACID BACTERIA USED IN FOODSTUFFS OR FOOD PREPARATION
- A23V2002/00—Food compositions, function of food ingredients or processes for food or foodstuffs
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2236/00—Isolation or extraction methods of medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicine
- A61K2236/30—Extraction of the material
- A61K2236/31—Extraction of the material involving untreated material, e.g. fruit juice or sap obtained from fresh plants
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- Health & Medical Sciences (AREA)
- Natural Medicines & Medicinal Plants (AREA)
- Life Sciences & Earth Sciences (AREA)
- Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
- Alternative & Traditional Medicine (AREA)
- Biotechnology (AREA)
- Botany (AREA)
- Medical Informatics (AREA)
- Medicinal Chemistry (AREA)
- Microbiology (AREA)
- Mycology (AREA)
- Pharmacology & Pharmacy (AREA)
- Epidemiology (AREA)
- Animal Behavior & Ethology (AREA)
- General Health & Medical Sciences (AREA)
- Public Health (AREA)
- Veterinary Medicine (AREA)
- Non-Alcoholic Beverages (AREA)
- Coloring Foods And Improving Nutritive Qualities (AREA)
Abstract
The invention discloses a kind of method improving Herba Dendrobii fresh goods effective ingredient dissolution, be with the fresh bar of fresh Herba Dendrobii as raw material, add appropriate amount of purified water, after being then passed through making beating, vacuum outgas, high pressure homogenize, subpackage, sealing, ultra high pressure treatment, obtain finished product.Herba Dendrobii of the present invention fresh squeezing natural juice the most farthest retains " genuine " of new fresh Herba Dendrobii, and have safety and sanitation, effective ingredient dissolution improves, is more conducive to advantages such as digesting and assimilating, and this is significant to the health food development of Herba Dendrobii fresh goods.
Description
One, technical field
The processing method that the present invention relates to a kind of Herba Dendrobii, specifically a kind of Herba Dendrobii fresh goods that improves effectively becomes
The method dividing dissolution, belongs to health product manufacture field.
Two, background technology
Herba Dendrobii (formal name used at school: Dendrobium huoshanense), is commonly called as a meter dry measure used in former times, and main product is in the Anhui Province of Da Bie Mountain area
Huoshan County, is the superfine product in medicinal dendrobium.The record i.e. having Herba Dendrobii to apply in front " Mingyi Bielu " as far back as 1700, goes through
In history, Herba Dendrobii is described as " China nine big Herba mesonae chinensis first of ", " help Herba mesonae chinensis ", modern be respectfully called " China's Herba mesonae chinensis ", " health
Soft gold ".Polysaccharide contained by Herba Dendrobii can increase substantially SOD in human body, in enhancing immunity, resisting fatigue, delays to decline
Aspect of waiting for a long time has obvious effect, thus reaches effect of health-care.
Herba Dendrobii since ancient times, often takes fresh juice and takes, and is particular about " fresh goods is upper ", and fresh juice maintains original property of natural drug
Taste, abnormal smells from the patient is all deposited, and the property moisturized is stronger.Modern pharmacology analysis shows: fresh Herba Dendrobii total alkaloids, polyoses content are above doing
Product, its enhancing immunologic function, also superior to dry medicine, is therefore processed into health food by fresh goods, and under equal conditions, its effect ought to be higher than
Dry product.But fresh goods Herba Dendrobii room temperature place easy dehydration, germinate, rot, use have inconvenience, in native land, existing Herba Dendrobii commodity are several
Being formed by its dry product fabrication and processing, commercial form has Herba Dendrobii extract and coccoid, capsule, soft capsule, oral liquid etc..Dry product exists
In the course of processing, such as dry, pulverize, each link such as mixing, Herba Dendrobii is included active component and the most all produces
Loss, even can produce serious damaging influence to some composition.Therefore, " lossless processing " and the efficiently utilization to fresh Herba Dendrobii
Seem the most urgent and important.
For fresh Herba Dendrobii " lossless processing ", fresh nature of squeezing the juice is a kind of good processing mode, but, owing to not sterilizing, fresh
Squeeze the juice and be limited to existing squeezing now use more, 1-2 days only stored refrigerated phase, simultaneously functional component efficiently to utilize aspect also to have to be added
By force.
Via State Intellectual Property Office's retrieved web, end on July 1st, 2016, process directly related awarding with fresh Herba Dendrobii
Power patent of invention or application mainly have:
1, CN 1552370A discloses a kind of compound fresh dendrobium stem ball and preparation method, including fresh Herba Dendrobii boiling, Radix Puerariae
Radix Notoginseng decoction → collecting decoction filters → is condensed into clear paste → add ethanol precipitation → stand and filters → concentrate the adjuvant that gets dry extract → add
Mixing → pill → be drying to obtain.The fresh Herba Dendrobii ball of the present invention has that drug release rate is fast, bioavailability is high, divided dose is accurate,
Take, the advantage such as easy to carry, good looking appearance.
2, CN 1679856A discloses a kind of fresh Herba Dendrobii processing method, little including whole strain or a length of 1～10cm
Section → Co60Irradiation (dosage is 1-3kGy) or heat treatment (100 DEG C of boiled water blanchings 0.5～2 minutes) → vacuum packaging.During use with
Warm water is soaked to drink or soak with wine and is drunk.The preparation method of the present invention can keep the composition of former plant, does not wastes, does not damages
Lose the main component of Herba Dendrobii, the various convenience of edible way.
3, CN101647593A provides the preparation method of a kind of fresh dendrobe juice, including fresh Herba Dendrobii, Radix Rehmanniae group
Knit smash to pieces → serosity is spray-dried, and obtains ultra-fine particles → add pure water blending → mixing → fill → high temperature sterilization (115-120
DEG C) → check and get final product.Fresh dendrobe juice of the present invention possesses former grass juice factor taste, and under conditions of ultra-fine particles sap-shape, more
It is easy to absorption of human body, improves the absorption rate of Herba Dendrobii Middle nutrition composition.
4, a kind of method that CN 102008654A discloses processing fresh juice stock solution, including: washing and sterilizing → separation of squeezing the juice →
Vacuum outgas → add enzyme hydrolysis → thick micro-filtration → heat sterilization → sterile filling → high temperature sterilize (115-120 DEG C, steam pressure
0.78MPa, high-temperature heating time 4～6 seconds) → finished product.Products obtained therefrom of the present invention at utmost retains the color of Herba Dendrobii natural juice
Pool, local flavor, nutrition and functional component, make product be beneficial to preserve and realize industrialized production simultaneously.
5, CN 102302156 A discloses a kind of method improving Herba Dendrobii finished product effective ingredient blister leaching rate, bag
Including: fresh Herba Dendrobii cleans, dries → shave or Herba Dendrobii section → heating, stir-fry, air blasting breaking cellular wall (air pressure 0.8～0.9MPa) → baking
(100 DEG C, 1h) → sort, select → be vacuum-packed → finished product.The inventive method has that technique is simple and convenient to operate, product is defended
Raw, products obtained therefrom soaks with boiled water when using, and its effective ingredient is easy to leach, improves the health-care effect of Herba Dendrobii.
6, CN 103099285 A discloses composite fresh juice and the systems of oral liquid such as a kind of Herba Dendrobii, money lotus, Fructus Mori
Preparation Method, clean including: raw material dry → grind broken → microwave extracting → enzymolysis → centrifugation → filtering with microporous membrane →
Aseptic canning → flash pasteurization (115-120 DEG C, steam pressure 0.78MPa, time 4～6 seconds) → oral liquid.The present invention
Use microwave extracting and enzyme compounded technology, make intracellular effective ingredient fully be extracted；The centrifugal mocromembrane that adds filters and is not required to
Wanting filter aid, technical process is short, and expense is low, is relatively inexpensive effective health beverage defecation method.
7, CN 103300450 B discloses the preparation method of a kind of raw dendrobium officinale pulp beverage, including: the baking of fresh bar →
Making beating → first the serosity that adds water boils, filtration → filtering residue, repeat to process (pull an oar, boil, filter) secondary serosity → serosity enzymolysis,
Repeat process → merging filtrate → boil sterilization → primary pulp drink.Filtering residue, by toasting Herba Dendrobii, is entered by the present invention
Row enzymolysis processing, not only increases the extraction ratio of function polysaccharide, flavone, and dietary fiber content increases, and beverage color is fresh
Gorgeous, stable.
8, CN 105029439 A discloses a kind of blood sugar lowering fresh Herba Dendrobii mouth being made up of Herba Dendrobii, Aloe, Fructus Lycii, Semen Fagopyri Esculenti
Taking liquid, preparation process is as follows: broken, pulverizing → enzymolysis 2h → color fixative seasoning → centrifugation → homogenizing degassing → blood sugar lowering is administered orally
Liquid.The present invention had both retained the natural juice local flavor of Herba Dendrobii, the most conveniently takes and has function of blood sugar reduction.
9, CN 105077272A discloses the preparation method of a kind of Herba Dendrobii oleo stock oral liquid, including: rinsing dries → 100
DEG C water blancing → saline solution color fixative, making beating → double gauze filtration → filtering residue making beating → serosity merges, enzymolysis → color fixative, seasoning
→ centrifugation → filtering with microporous membrane → homogenizing degassing → oral liquid.The present invention is by adding green apple concentrated juice, malic acid
With and Essential Oil From Citrus Grandis Peel, reach antibacterial, color fixative and cover the miscellaneous taste that Herba Dendrobii is original, it is ensured that the optimal mouthfeel of oral liquid.
10, CN 103549411 A discloses a kind of synchronous production technique making Herba Dendrobii oral liquid, decoction piece beverage,
Including: clean just disconnected (0.5-20mm) → making beating → serosity dilute → supertension circulation pressurization (450～550MPa pressurize,
Decompression cycles 3 times) → supersonic speed spiral water jet (2 Mach) → ceramic membrane filter → filtrate sterile filling obtains oral liquid；Filtering residue
Tabletting obtains healthcare decoction pieces.The present invention makes plant thin by low-temperature ultrahigh-pressure circulation pressurization with supersonic speed spiral water jet cell breakage
Born of the same parents' moment explosion discharges, and the peptidoglycan being difficult in Herba Dendrobii extract is discharged dissolving completely, synchronizes to refine into oral liquid, beverage drink
Sheet；Low-temperature ultrahigh-pressure (less than 20 DEG C) avoids the destroyed of heat-sensitive substance simultaneously, improves Herba Dendrobii oral liquid quality.
In sum, at present to the processing of fresh Herba Dendrobii mainly by the following manner: (1) Herba Dendrobii fresh bar high temperature decocts and extracts effectively
Composition (CN 1552370A)；(2) fresh bar irradiation or burn (CN 1679856A) are beneficial to preserve for a long time；(3) fresh bar room temperature (or
Burn) pulverize after use be spray dried to ultramicro powder (CN101647593 A) or extraction (microwave extracting such as CN
103099285A, heated and boiled are extracted such as CN 103300450 B)；(4) cell wall breaking of fresh bar or serosity is accelerated, as fresh bar dries
Air-flow explosion (CN 102302156 A) after roasting, serosity add enzyme hydrolysis (CN 102008654A, CN 103099285 A, CN
105029439 A, CN 105077272A), circulation pressurization combine with spiral water jet (CN 103549411 A) etc., these
Processing technique the most more or less relates to higher temperature and processes, as decocted, toast air blasting, spray drying, enzymolysis (50-60 DEG C), height
Temperature sterilizing (115-120 DEG C) etc., heat-sensitive ingredients and character flavor compound to fresh Herba Dendrobii have loss in various degree, because of
This, it is necessary to develop the processing technique of a kind of fresh Herba Dendrobii, so that it retains the local flavor of new fresh Herba Dendrobii, nutrition and effect to greatest extent
Composition, makes product be beneficial to preserve and realize industrialized production simultaneously.
Three, summary of the invention
It is an object of the invention to provide a kind of method improving Herba Dendrobii fresh goods effective ingredient dissolution, this method can
Retain the fresh clear hay-scented taste squeezed the juice of Herba Dendrobii, improve fresh middle effective ingredient dissolution of squeezing the juice simultaneously, and conveniently take, technique letter
Single, environmental protection.This method processing gained Herba Dendrobii fresh goods natural juice absorption easy to digest, health-care effect is strong.
The present invention improves the method for Herba Dendrobii fresh goods effective ingredient dissolution, comprises the steps:
1, fresh for the Herba Dendrobii of harvesting bar cleaned and drained surface moisture, being cut into the Herba Dendrobii section of a length of 1-2cm；
2, described Herba Dendrobii section is put in beater or colloid mill, add the pure water of 25-50 mass times, make after crushing
The Herba Dendrobii fresh squeezing natural juice of uniform and smooth；The Herba Dendrobii fresh squeezing natural juice that this step obtains is without screen filtration or centrifuging treatment；
3, by fresh for described Herba Dendrobii squeezing natural juice vacuum outgas high pressure homogenize, it is subsequently added in high pressure resistant plastic bottle or freshness protection package
Subpackage, sealing；
4, fresh for the Herba Dendrobii after step 3 encapsulates juice is placed in ultra-high-pressure processing equipment, pressurize 5-under 300-400MPa
15min, gets product.
Grain graininess≤50 μm of the Herba Dendrobii fresh squeezing natural juice obtained after crushing in step 2.
Vacuum outgas described in step 3 is holding 2-3min under vacuum 0.08-0.1MPa.
Homogenization pressure is controlled during high pressure homogenize at 20-30MPa described in step 3.
In step 3, subpackage uses high pressure resistant packaging material, can be PE or PA vacuum fresh-keeping bag or for PE or PET bottle.
Gained finished product of the present invention needs cold preservation (0-4 DEG C) or freezing (-18 DEG C) storage.
Advantages of the present invention and good effect are as follows:
1, compared with fresh squeezing the juice, in dendrobe fresh product natural juice of the present invention, the dissolution of effective ingredient improves, and is more conducive to digest and assimilate.
The present invention is for realizing this effect, and its granularity less (below 50 μm) when fresh Herba Dendrobii crushes, this is conducive to the fresh squeezing of Herba Dendrobii former
Polysaccharide and the preliminary dissolution of alkaloid in juice；Fresh squeezing natural juice is without filtering or centrifugal treating, for smudge cells not yet completely, its
Effective ingredient is through ultra high pressure treatment again to be fully dissolved out, and the fresh of HIGH PRESSURE TREATMENT is squeezed the juice due to historrhexis simultaneously, is more conducive to
Digest and assimilate.
2, compared with now using with the fresh existing squeezing squeezed the juice, dendrobe fresh product natural juice of the present invention is effectively killed through ultra high pressure treatment
Bacterium, its finished product can preserve the long period under refrigeration or freezing, if stored refrigerated was up to 2 months, can under freezing conditions
Reach more than 6 months.
3, dendrobe fresh product natural juice of the present invention preferably retains the clear hay-scented taste of new fresh Herba Dendrobii, and heat-sensitive ingredients loss simultaneously also obtains
To reduce.The present invention is for realizing this effect, and when Herba Dendrobii fresh juice degassing homogenizing, the vacuum of vacuum outgas selects 0.08-
The 0.1MPa time is 2-3min, and homogenization pressure 20-30MPa is advisable；It is simultaneously introduced superhigh pressure technique and processes Herba Dendrobii fresh squeezing natural juice,
Processing pressure 300-400MPa, can realize polysaccharide, the fully extraction of alkaloid and effectively sterilize under the conditions of pressurize 5-15min,
Thus avoid traditional enzymolysis (about 60 DEG C) or high temperature to decoct and the high temperature sterilization (115-120 DEG C) damage to heat-sensitive ingredients
Lose.
Four, detailed description of the invention
Below by specific embodiment, the invention will be further described, and following example are illustrative, is not limit
Qualitatively, it is impossible to limit protection scope of the present invention with this.
Embodiment 1: the preparation of Herba Dendrobii fresh goods natural juice
The method improving Herba Dendrobii fresh goods effective ingredient dissolution in the present embodiment, comprises the steps:
1, select the fresh bar of fresh Herba Dendrobii, remove earth and impurity, drain after clear water rinsing, the Huoshan of moisture will be drained
Herba Dendrobii fresh bar 50g is cut into the Herba Dendrobii section of a length of 1-2cm；
2, described Herba Dendrobii section is put in breaking cellular wall beater, add the pure water of 40 mass times, pull an oar 2-3 minute, make
The Herba Dendrobii fresh squeezing natural juice of uniform and smooth；The Herba Dendrobii fresh squeezing natural juice that this step obtains is without screen filtration or centrifuging treatment；
3, by the fresh squeezing natural juice vacuum outgas of step 2 gained Herba Dendrobii, 2-3min under vacuum 0.08-0.1MPa, is kept；Subsequently
High pressure homogenize under 25MPa, is distributed into PE/PA combined package bag, every bag of 50ml by fresh for the Herba Dendrobii after homogenizing juice, and evacuation seals
Mouthful；
4, fresh for the Herba Dendrobii after step 3 encapsulates juice is placed in ultra-high-pressure processing equipment, pressurize 15min under 300MPa, release
After get product.Finished product is in 0-4 DEG C of cold preservation or-18 DEG C of refrigerated storages.
Embodiment 2: polysaccharide and the mensuration of total alkaloids in Herba Dendrobii fresh goods natural juice
In Herba Dendrobii, polysaccharide determination is carried out by 2015 official methods, and Determination of Total Alkaloid uses bromocresol green acidity dye
Material-ultraviolet spectrophotometry is carried out.Measure the fresh bar of Herba Dendrobii, the fresh bar of 10g Herba Dendrobii to add 40 times of water and directly squeeze the juice (fresh squeezing
Juice) and dendrobium polysaccharide, total alkaloid content or the dissolution rate of embodiment 1 gained Herba Dendrobii fresh goods natural juice, the results are shown in Table 1 institute
Show.
Under table 1 Herba Dendrobii Different treatments, effective ingredient dissolution is compared
From table 1 it follows that the fresh juice of Herba Dendrobii after ultra high pressure treatment is compared with fresh squeezing the juice, its effective ingredient polysaccharide
Dissolution rate improves 44% (54.19% → 78.04%), and total alkaloids dissolution rate improves 58% (40.96% → 64.86%).
Claims (5)
1. the method improving Herba Dendrobii fresh goods effective ingredient dissolution, it is characterised in that comprise the steps:
(1) fresh for the Herba Dendrobii of harvesting bar cleaned and drained surface moisture, being cut into the Herba Dendrobii section of a length of 1-2cm；
(2) described Herba Dendrobii section is put in beater or colloid mill, add the pure water of 25-50 mass times, make uniform and smooth
Herba Dendrobii fresh squeezing natural juice；
(3) by fresh for described Herba Dendrobii squeezing natural juice vacuum outgas high pressure homogenize, it is subsequently added in high pressure resistant plastic bottle or freshness protection package and divides
Dress, sealing；
(4) the fresh juice of Herba Dendrobii after step (3) encapsulates is placed in ultra-high-pressure processing equipment, pressurize 5-15min under 300-400MPa,
Get product.
Method the most according to claim 1, it is characterised in that:
Grain graininess≤50 μm of the Herba Dendrobii fresh squeezing natural juice obtained after crushing in step (2).
Method the most according to claim 1, it is characterised in that:
Vacuum outgas described in step (3) is holding 2-3min under vacuum 0.08-0.1MPa.
Method the most according to claim 1, it is characterised in that:
Homogenization pressure is controlled during high pressure homogenize at 20-30MPa described in step (3).
Method the most according to claim 1, it is characterised in that:
Gained finished product needs 0-4 DEG C of cold preservation or-18 DEG C of refrigerated storages.
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| CN112076286A (en) * | 2020-08-10 | 2020-12-15 | 安徽大别山霍斛科技有限公司 | Dendrobium huoshanense stock solution extraction process and dendrobium huoshanense beverage |
| CN112206282A (en) * | 2020-10-13 | 2021-01-12 | 安徽霍山县药王谷林农科技有限公司 | Pure dendrobium huoshanense ultramicro wall-broken buccal tablet |
| CN116035145A (en) * | 2022-12-30 | 2023-05-02 | 安徽迎驾山泉股份有限公司 | Dendrobium huoshanense beverage and preparation method thereof |
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| Publication number | Priority date | Publication date | Assignee | Title |
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| CN112206282A (en) * | 2020-10-13 | 2021-01-12 | 安徽霍山县药王谷林农科技有限公司 | Pure dendrobium huoshanense ultramicro wall-broken buccal tablet |
| CN116035145A (en) * | 2022-12-30 | 2023-05-02 | 安徽迎驾山泉股份有限公司 | Dendrobium huoshanense beverage and preparation method thereof |
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