CN106923126A - A kind of preparation method of dendrobium stem beverage - Google Patents
A kind of preparation method of dendrobium stem beverage Download PDFInfo
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- CN106923126A CN106923126A CN201710197906.0A CN201710197906A CN106923126A CN 106923126 A CN106923126 A CN 106923126A CN 201710197906 A CN201710197906 A CN 201710197906A CN 106923126 A CN106923126 A CN 106923126A
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- 241001523681 Dendrobium Species 0.000 title claims abstract description 35
- 235000013361 beverage Nutrition 0.000 title claims abstract description 33
- 238000002360 preparation method Methods 0.000 title claims abstract description 19
- 240000004638 Dendrobium nobile Species 0.000 claims abstract description 142
- 239000007788 liquid Substances 0.000 claims abstract description 68
- 235000011389 fruit/vegetable juice Nutrition 0.000 claims abstract description 63
- 239000000463 material Substances 0.000 claims abstract description 49
- 238000007710 freezing Methods 0.000 claims abstract description 12
- 230000008014 freezing Effects 0.000 claims abstract description 12
- 239000002904 solvent Substances 0.000 claims abstract description 12
- 238000010298 pulverizing process Methods 0.000 claims abstract description 8
- 239000002244 precipitate Substances 0.000 claims abstract description 6
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 43
- KRKNYBCHXYNGOX-UHFFFAOYSA-N citric acid Chemical compound OC(=O)CC(O)(C(O)=O)CC(O)=O KRKNYBCHXYNGOX-UHFFFAOYSA-N 0.000 claims description 36
- 238000000034 method Methods 0.000 claims description 22
- 238000004659 sterilization and disinfection Methods 0.000 claims description 18
- 230000001954 sterilising effect Effects 0.000 claims description 16
- 239000002562 thickening agent Substances 0.000 claims description 14
- 238000005406 washing Methods 0.000 claims description 14
- 238000001556 precipitation Methods 0.000 claims description 12
- 238000004140 cleaning Methods 0.000 claims description 11
- 235000013373 food additive Nutrition 0.000 claims description 11
- 239000002778 food additive Substances 0.000 claims description 11
- 235000003599 food sweetener Nutrition 0.000 claims description 10
- 239000003765 sweetening agent Substances 0.000 claims description 10
- 238000001914 filtration Methods 0.000 claims description 9
- 150000004676 glycans Chemical class 0.000 claims description 9
- 229920001282 polysaccharide Polymers 0.000 claims description 9
- 239000005017 polysaccharide Substances 0.000 claims description 9
- 239000004575 stone Substances 0.000 claims description 8
- 229930013930 alkaloid Natural products 0.000 claims description 7
- 150000003797 alkaloid derivatives Chemical class 0.000 claims description 7
- 238000002156 mixing Methods 0.000 claims description 7
- 239000003755 preservative agent Substances 0.000 claims description 7
- 230000002335 preservative effect Effects 0.000 claims description 7
- 238000011049 filling Methods 0.000 claims description 6
- 239000012535 impurity Substances 0.000 claims description 6
- 238000004806 packaging method and process Methods 0.000 claims description 5
- 239000003795 chemical substances by application Substances 0.000 claims description 4
- 238000003756 stirring Methods 0.000 claims description 4
- 239000000203 mixture Substances 0.000 abstract description 5
- 238000004090 dissolution Methods 0.000 abstract description 4
- 230000008901 benefit Effects 0.000 abstract description 3
- 239000003814 drug Substances 0.000 description 32
- 239000000047 product Substances 0.000 description 27
- 238000004519 manufacturing process Methods 0.000 description 17
- CIWBSHSKHKDKBQ-JLAZNSOCSA-N Ascorbic acid Chemical compound OC[C@H](O)[C@H]1OC(=O)C(O)=C1O CIWBSHSKHKDKBQ-JLAZNSOCSA-N 0.000 description 14
- 230000009286 beneficial effect Effects 0.000 description 13
- 229940079593 drug Drugs 0.000 description 10
- 238000007792 addition Methods 0.000 description 9
- 230000000694 effects Effects 0.000 description 8
- 239000000706 filtrate Substances 0.000 description 8
- 230000008569 process Effects 0.000 description 8
- 229920000858 Cyclodextrin Polymers 0.000 description 7
- ZZZCUOFIHGPKAK-UHFFFAOYSA-N D-erythro-ascorbic acid Natural products OCC1OC(=O)C(O)=C1O ZZZCUOFIHGPKAK-UHFFFAOYSA-N 0.000 description 7
- 229930003268 Vitamin C Natural products 0.000 description 7
- 238000001514 detection method Methods 0.000 description 7
- HFHDHCJBZVLPGP-UHFFFAOYSA-N schardinger α-dextrin Chemical group O1C(C(C2O)O)C(CO)OC2OC(C(C2O)O)C(CO)OC2OC(C(C2O)O)C(CO)OC2OC(C(O)C2O)C(CO)OC2OC(C(C2O)O)C(CO)OC2OC2C(O)C(O)C1OC2CO HFHDHCJBZVLPGP-UHFFFAOYSA-N 0.000 description 7
- 235000019154 vitamin C Nutrition 0.000 description 7
- 239000011718 vitamin C Substances 0.000 description 7
- 230000008595 infiltration Effects 0.000 description 6
- 238000001764 infiltration Methods 0.000 description 6
- 239000000843 powder Substances 0.000 description 6
- RYAHJFGVOCZDEI-UFFNCVEVSA-N Dendrobine Chemical compound C([C@H]1CC[C@@H]2[C@@]31C)N(C)[C@@H]3[C@H]1[C@@H](C(C)C)[C@@H]2C(=O)O1 RYAHJFGVOCZDEI-UFFNCVEVSA-N 0.000 description 5
- 241000196324 Embryophyta Species 0.000 description 5
- 229930006000 Sucrose Natural products 0.000 description 5
- CZMRCDWAGMRECN-UGDNZRGBSA-N Sucrose Chemical compound O[C@H]1[C@H](O)[C@@H](CO)O[C@@]1(CO)O[C@@H]1[C@H](O)[C@@H](O)[C@H](O)[C@@H](CO)O1 CZMRCDWAGMRECN-UGDNZRGBSA-N 0.000 description 5
- 238000001816 cooling Methods 0.000 description 5
- RYAHJFGVOCZDEI-CZKZLRAZSA-N dendrobine Natural products O=C1O[C@@H]2[C@H](C(C)C)[C@H]1[C@H]1[C@@]3(C)[C@@H]2N(C)C[C@H]3CC1 RYAHJFGVOCZDEI-CZKZLRAZSA-N 0.000 description 5
- 239000000796 flavoring agent Substances 0.000 description 5
- 235000019634 flavors Nutrition 0.000 description 5
- 239000000835 fiber Substances 0.000 description 4
- 239000003205 fragrance Substances 0.000 description 4
- 238000012856 packing Methods 0.000 description 4
- 239000007921 spray Substances 0.000 description 4
- 241000894006 Bacteria Species 0.000 description 3
- 244000248349 Citrus limon Species 0.000 description 3
- 235000005979 Citrus limon Nutrition 0.000 description 3
- NNBFNNNWANBMTI-UHFFFAOYSA-M brilliant green Chemical compound OS([O-])(=O)=O.C1=CC(N(CC)CC)=CC=C1C(C=1C=CC=CC=1)=C1C=CC(=[N+](CC)CC)C=C1 NNBFNNNWANBMTI-UHFFFAOYSA-M 0.000 description 3
- 230000035622 drinking Effects 0.000 description 3
- 235000013305 food Nutrition 0.000 description 3
- 230000036541 health Effects 0.000 description 3
- 235000012907 honey Nutrition 0.000 description 3
- 238000007689 inspection Methods 0.000 description 3
- 238000005070 sampling Methods 0.000 description 3
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- 239000004480 active ingredient Substances 0.000 description 2
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- 239000000725 suspension Substances 0.000 description 2
- 241000331528 Chlorophytum capense Species 0.000 description 1
- 208000015220 Febrile disease Diseases 0.000 description 1
- 241000233855 Orchidaceae Species 0.000 description 1
- 230000002159 abnormal effect Effects 0.000 description 1
- -1 after mixing Substances 0.000 description 1
- 239000003513 alkali Substances 0.000 description 1
- 238000004458 analytical method Methods 0.000 description 1
- 125000003118 aryl group Chemical group 0.000 description 1
- 210000001124 body fluid Anatomy 0.000 description 1
- 239000010839 body fluid Substances 0.000 description 1
- 235000009508 confectionery Nutrition 0.000 description 1
- 239000000470 constituent Substances 0.000 description 1
- 230000007812 deficiency Effects 0.000 description 1
- 201000010099 disease Diseases 0.000 description 1
- 208000037265 diseases, disorders, signs and symptoms Diseases 0.000 description 1
- 238000009826 distribution Methods 0.000 description 1
- 238000001035 drying Methods 0.000 description 1
- 238000005516 engineering process Methods 0.000 description 1
- 239000012530 fluid Substances 0.000 description 1
- 235000011194 food seasoning agent Nutrition 0.000 description 1
- 239000010931 gold Substances 0.000 description 1
- 229910052737 gold Inorganic materials 0.000 description 1
- 239000004615 ingredient Substances 0.000 description 1
- 238000002386 leaching Methods 0.000 description 1
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- 238000012986 modification Methods 0.000 description 1
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- 230000001376 precipitating effect Effects 0.000 description 1
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- 238000004062 sedimentation Methods 0.000 description 1
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- 239000002893 slag Substances 0.000 description 1
- 235000013599 spices Nutrition 0.000 description 1
- 210000002784 stomach Anatomy 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
- 238000006467 substitution reaction Methods 0.000 description 1
- 238000012360 testing method Methods 0.000 description 1
Classifications
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L2/00—Non-alcoholic beverages; Dry compositions or concentrates therefor; Their preparation
- A23L2/38—Other non-alcoholic beverages
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L2/00—Non-alcoholic beverages; Dry compositions or concentrates therefor; Their preparation
- A23L2/42—Preservation of non-alcoholic beverages
- A23L2/44—Preservation of non-alcoholic beverages by adding preservatives
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L2/00—Non-alcoholic beverages; Dry compositions or concentrates therefor; Their preparation
- A23L2/52—Adding ingredients
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L2/00—Non-alcoholic beverages; Dry compositions or concentrates therefor; Their preparation
- A23L2/52—Adding ingredients
- A23L2/60—Sweeteners
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23V—INDEXING SCHEME RELATING TO FOODS, FOODSTUFFS OR NON-ALCOHOLIC BEVERAGES AND LACTIC OR PROPIONIC ACID BACTERIA USED IN FOODSTUFFS OR FOOD PREPARATION
- A23V2002/00—Food compositions, function of food ingredients or processes for food or foodstuffs
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- Health & Medical Sciences (AREA)
- Nutrition Science (AREA)
- Life Sciences & Earth Sciences (AREA)
- Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
- Food Science & Technology (AREA)
- Polymers & Plastics (AREA)
- Non-Alcoholic Beverages (AREA)
Abstract
The present invention provides a kind of preparation method of dendrobium stem beverage, comprises the following steps：1) stem of noble dendrobium is freezed；2) stem of noble dendrobium after freezing is entered into broken wall treatment, obtains stem of noble dendrobium crushed material；3) after stem of noble dendrobium crushed material is mixed with solvent, wet type micronized pulverization is carried out, obtains stem of noble dendrobium liquid；4) will be filtered after stem of noble dendrobium liquid precipitate, obtain stem of noble dendrobium juice；5) stem of noble dendrobium juice is deployed into dendrobium stem beverage.Preparation method of the present invention has dissolution rate high, and effective active composition is easily absorbed by the body, and availability is high, the advantages of relative inexpensiveness.
Description
Technical field
The invention belongs to technical field of health care, more particularly to a kind of preparation method of dendrobium stem beverage.
Background technology
The stem of noble dendrobium also known as dendrobium, generic name Dendrobium is Greek dendron (trees) and the word knots of bios (life) two
Conjunction is formed, and is meant and is grown nonparasitically upon another plant in the tree.Dendrobium is a category of maximum in orchid, and original producton location is distributed mainly on Asia heat
Band and subtropical zone, Australia and Pacific Islands, the whole world there are about kind more than 1000.China there are about 76 kinds of wherein most distributions
In southwest, south China, Taiwan and other places.
HERBA DENDROBII [Dendrobiumnobilelindl.] alias bracketplant, is rare traditional Chinese medicine conventional simply.Stone
Dry measure used in former times is used as medicine with stem, cold in nature, sweet, the effects such as tool reinforcing stomach reg fluid, nourishing Yin and clearing heat, for treating consumption of body fluid caused by febrile disease, dry polydipsia, after being ill
Abnormal heat, tongue light lack the diseases such as tongue, deficiency of food are retched, mesh is secretly failed to understand.
Only it is not convenient for people to make the drink of health care as the stem of noble dendrobium product of medicine currently on the market, this new product
Product fill up this blank.
The content of the invention
In view of problem existing for prior art, the present invention provides a kind of preparation method of dendrobium stem beverage, high with dissolution rate,
Effective active composition is easily absorbed by the body, and availability is high, the advantages of relative inexpensiveness.
The technical scheme that the present invention solves above-mentioned technical problem is as follows：
A kind of preparation method of dendrobium stem beverage, comprises the following steps：
1) stem of noble dendrobium is freezed；
2) stem of noble dendrobium after freezing is entered into broken wall treatment, obtains stem of noble dendrobium crushed material；
3) after stem of noble dendrobium crushed material is mixed with solvent, wet type micronized pulverization is carried out, obtains stem of noble dendrobium liquid；
4) will be filtered after stem of noble dendrobium liquid precipitate, obtain stem of noble dendrobium juice；
5) stem of noble dendrobium juice is deployed into dendrobium stem beverage.
Active ingredient in beverage can be advantageously ensured that with fresh stem of noble dendrobium of prioritizing selection, i.e., fresh stem of Dendrobium strain in the present invention
Content.
The beneficial effects of the invention are as follows：
Preparation method of the present invention is a kind of production procedure of full wet type, and the fresh of the stem of noble dendrobium is ensure that to greatest extent
The property property of medicine, ensure that the dissolution rate of stem of noble dendrobium active principle to greatest extent.Method of the people using the stem of noble dendrobium is simplified, can be people
A kind of relative moderate is provided, convenient stem of noble dendrobium drink is safely and effectively drunk.
Frozen cell broken wall is smashed and Wet-type wall-breaking smashes two processes and is uninterruptedly carried out continuously.Production procedure is compact.
Whole production process is all carried out in liquid conditions, obtains the product of liquid, saves the process that powder is beaten in drying, greatly
Simplify the production process of stem of noble dendrobium drink product, while avoiding the loss of effective active composition.
On the basis of above-mentioned technical proposal, the present invention can also do following improvement.
Further, step 1) to step 5) control below 4 DEG C.
Beneficial effect using such scheme is：Whole production process is carried out all under conditions of low temperature, to greatest extent
Ensure that the freshness and property of medicine health-care effect of stem of noble dendrobium liquid.
Further, step 1) in, the stem of noble dendrobium is refrigerated to less than -8 DEG C；The stem of noble dendrobium is HERBA DENDROBII.
In the present invention, " less than -8 DEG C " include -8 DEG C and less than -8 DEG C.
Beneficial effect using such scheme is：Powder is carried out under the freezing situation that the strain of HERBA DENDROBII medicine must be below -8 DEG C
Essence, by contrast, especially -8 DEG C be HERBA DENDROBII (especially Chishui HERBA DENDROBII) optimal brittle point, at this moment break essence can reach
Preferable shell-broken effect.
Further, step 2) in, the condition of broken wall treatment is：Temperature control is less than -8 DEG C, is entered using wall-broken grinder
Row broken wall, the rotating speed of the main shaft of broken wall disintegrating machine is 3100r/min.
Beneficial effect using such scheme is：With this understanding, crushing effect can further be improved.
Further, step 3) concrete operations be：Stem of noble dendrobium crushed material feeding wet type micronizer is carried out into breaking-wall cell
Crush, add solvent, the quality of solvent is 7 times of the quality of stem of noble dendrobium crushed material, and stem of noble dendrobium crushed material is mixed with solvent, and wet type surpasses
Temperature is less than 2 DEG C when micro- broken, and solvent is water.
Beneficial effect using such scheme is：Ensure fully broken, active constituent content is higher in stem of noble dendrobium liquid.
Further, step 4) in, the concrete operations of precipitation and filtering are：It is clear by filtering to take by stem of noble dendrobium liquid precipitate 4 hours
Liquid, filters out residue；Residue is added water again, is stirred 30 minutes, stand 8 hours, take clear liquid；The clear liquid mixing that will be taken twice, obtains
To stem of noble dendrobium juice.
Beneficial effect using such scheme is：Using the technique for washing infiltration again, it is ensured that active drug composition is most
Good dissolution rate.
Further, step 4) in, in stem of noble dendrobium juice, the content of the stem of noble dendrobium is the 6%-8% of stem of noble dendrobium juice, and the content of dendrobium polysaccharide is not
Less than 0.12%, the content of alkaloid is not less than 0.02%.
Beneficial effect using such scheme is：It is suitable for the concentration that people drink, makes taste flavor be more suitable for drinking.
Further, step 5) concrete operations be：Stem of noble dendrobium juice is mixed with food additives, afterwards sterilization filling, packaging；
The food additives include sweetener, thickener, preservative and citric acid, and sweetener is with the mass percent of stem of noble dendrobium juice
5%-20%, thickener is 1%-3% with the mass percent of stem of noble dendrobium juice, and preservative is with the mass percent of stem of noble dendrobium juice
0.1%-0.3%, citric acid is 0.01%-0.05% with the mass percent of stem of noble dendrobium juice.
Beneficial effect using such scheme is：Be conducive to using the sweetener of above-mentioned mass fraction it is in good taste, using upper
The thickener of mass fraction is stated before product is drunk, it is ensured that the suspension grain in stem of noble dendrobium liquid is not precipitated, adjust mouthfeel；Using above-mentioned
The preservative of mass fraction is conducive to extending the shelf life, and is conducive to using the citric acid of above-mentioned mass fraction fresh-keeping.
Further, in step 1) also include sterilized step before, sterilized method is：The stem of noble dendrobium is utilized into 120 DEG C of steam
Spray 20-50 seconds.
Beneficial effect using such scheme is：Medicine strain 20-50 seconds that individual layers lay is sprayed using 120 DEG C of temperature, favorably
Bacterium and the microorganism pollution that strain brings are administered from during harvesting, transport, hand picking in killing, while contributing in medicine strain
The removing of sheath residue.Meanwhile, it is within 20-50 seconds that the high temperature of short time is conducive to avoiding the loss of the medicine ability property of medicine, it is preferable that 20 seconds
Effect is more preferable.
Further, cleaning is also included before sterilisation step, the method for cleaning is：Using the high pressure water washing stem of noble dendrobium.
Beneficial effect using such scheme is：The stem of noble dendrobium is cleaned as far as possible, while avoiding producing damage to the stem of noble dendrobium.
Further, also include selecting detecting step between cleaning：Remove impurity, fibrous root, leaf and sheath, remove mould
The rotten rotten stem of noble dendrobium.
Beneficial effect using such scheme is：It is further ensured that the quality of prepared dendrobium stem beverage.
Specific embodiment
Principle of the invention and feature are described below, example is served only for explaining the present invention, is not intended to limit
Determine the scope of the present invention.
A kind of preparation method of HERBA DENDROBII beverage, comprises the following steps：
1) the fresh stem of noble dendrobium selects detection (artificial):
The standard of detection is：Remove impurity, fibrous root, leaf and sheath, remove the rotten plant that goes rotten.
2) cleaning and sterilization：Sprayed 20-50 seconds with 120 DEG C of steam after high pressure water washing.The parameter of high pressure water washing can be with
It is second 1-2 kilograms of water under high pressure every square centimeter, washing time 1-2 minutes or is totally defined to range estimation.Using 120 DEG C of spray individual layers
The medicine strain of laying 20-50 seconds, is conducive to killing bacterium and the micro- life for being administered that strain brings from during harvesting, transport, hand picking
Thing pollutes, and is within 20-50 seconds that the high temperature of short time is conducive to avoiding the medicinal material property of medicine while contributing to the removing of the upper sheath residue of medicine strain
Loss.
3) freeze：The stem of noble dendrobium after cleaning sterilization is sent into cool chamber, less than -8 DEG C are refrigerated to, is at this temperature HERBA DENDROBII
The optimal brittle point of (especially Chishui HERBA DENDROBII), is conducive to improving the quality that next step broken wall is smashed, and is also beneficial in medicine
Guaranteeing the quality during material deposit, especially when control is at -8 DEG C, effect is more preferable.
4) broken wall is crushed：HERBA DENDROBII feeding freezing wall-broken grinder after freezing is crushed, crushed material is obtained.Gold
The strain of hairpin stem of noble dendrobium medicine must be smashed under not higher than -8 DEG C of freezing situation, and by contrast, -8 DEG C is Chishui HERBA DENDROBII
Optimal brittle point, at this moment breaking essence can reach more preferable shell-broken effect compared to other temperature.Freezing broken wall smashes owner's rotating speed
3100r/min, with type, 500 kilograms of speed of the stem of noble dendrobium of broken wall are carried out per hour.
In a particular embodiment, pulverizer primary election Jiangyin Yongchang RM -50 type, production capacity 500 kilograms, motor per hour
Power 45 (KW).
5) Wet-type wall-breaking is crushed：By step 4) crushed material that obtains subsequently enters wet type micronizer and carries out breaking-wall cell
Crush.When breaking-wall cell is crushed, to 7 times of water of weight of fresh stem of noble dendrobium weight are added in crushed material, after mixing, essence is carried out brokenly,
(broken abundant to ensure) is carried out to crush 60 kilograms of speed of crushed material per hour, stem of noble dendrobium liquid is obtained.By HERBA DENDROBII liquid
The mass fraction of middle crushed material is controlled to 12%-16%, and it is HERBA DENDROBII liquid that the quality of material is now smashed in HERBA DENDROBII liquid
12.5%.
Broken wall is directly transferred to Wet-type wall-breaking machine advantage after smashing is that stem of noble dendrobium spice is put into breaking again without any treatment
Under wall-like state with solvent (for example：Water) contact, so as to obtain the high dissolved efficiency of active drug composition in the stem of noble dendrobium.Simplify
Production procedure, it is to avoid the loss of effective ingredient in production link.Improve productivity effect.Water cryogenic pulverization is added, it is wet
The full machine jacket cooling system of formula micronizer is cooled to less than 2 DEG C.
By the regulation of Wet-type wall-breaking disintegrating machine jacket cooling system, make in whole production process all in the state of low temperature
Carry out, low-temperature condition is avoided that the volatilization and destruction of aromatic substance in fresh HERBA DENDROBII, its intrinsic fresh fragrance can be retained.
Drink middle energy product and go out the unique delicate fragrance of HERBA DENDROBII, the local flavor of its unique pleasant is formed, rather than flavour of a drug.Meanwhile,
The emerald green color of stem of noble dendrobium drink is ensure that, beautiful outward appearance is formed.This is the key for ensureing product quality.
In a particular embodiment, the machine choosing of wet type micronizer can reach micro-, model XDW --- F100J for Jinan, raw
Production capacity power is 60 kilograms, power of motor 15 (KW) per hour.
6) precipitation filtering, the step is controlled below 4 DEG C, and the concrete operations for precipitating filtering are：By step 5) obtained by stone
Dry measure used in former times liquid enters tapered settling vessel, and the sedimentation time can be 4 hours, after precipitation, take clear liquid, as first time clear liquid, filter out residual
Slag.Residue is added water washing, specific washing methods is：Residue is entered into tank, the water of same weight (is smashed when adding wet type to smash
Expect weight 7 times of water of weight) stirring infiltration 30 minutes, then stand 8 hours after, first extract out top liquid, then by remaining
Filtering, collects filtrate, and liquid and the filtrate sum on top are second clear liquid.
7) by step 6) in the stem of noble dendrobium twice clear liquid mixing, obtain 6%-8%'s containing crushed material (mass percent)
Stem of noble dendrobium juice.Inspection by sampling in the process, controls requisite quality.Stem of noble dendrobium juice viscosity now is small, is easy to precipitation to filter.
In stem of noble dendrobium juice, the content of crushed material is 6%-8% (mass percent).Now, in stem of noble dendrobium juice, dendrobium polysaccharide contains
Amount is not less than 0.12% (mass percent), and alkaloid (with dendrobine as representative) content is not less than 0.02% (quality percentage
Than), the stem of noble dendrobium juice for meeting the standard is product up to standard.
The standard for controlling requisite quality is：In stem of noble dendrobium juice, the content of dendrobium polysaccharide is not less than 0.12%.Alkaloid is (with stone
Dry measure used in former times alkali is representative) not less than 0.02% (mass percent), the stem of noble dendrobium juice for meeting the standard is product up to standard to content.
8) by food additives seasoning in stem of noble dendrobium juice：Qualified stem of noble dendrobium juice is squeezed into storage tank, various food additions are conducted batch-wise
The addition of agent, obtains differently flavoured beverage products in batches.
For example：Beverage products can be using stem of noble dendrobium liquid and sweetener (for example：White sugar or honey) it is made into, in beverage products
Stem of noble dendrobium juice accounts for 80%-95% (mass percent), and white sugar or honey account for 5%-20% (mass percent).
For example：Numerous food additive can also be added, food additives include sweetener, preservative, thickener, lemon
One or more in acid etc., storage tank is squeezed into by qualified stem of noble dendrobium juice, and various sweeteners, preservative, thickener and lemon is conducted batch-wise
The addition of lemon acid, obtains differently flavoured beverage products in batches.
Sweetener can be white sugar, and addition is the 5%-20% (mass percent) of stem of noble dendrobium juice quality, can be according to city
Depending on the demand of field.Sweetener can also use honey, and addition is the 5%-15% (mass percent) of stem of noble dendrobium juice quality, also root
Depending on the market demand.
Thickener is cyclodextrin, and addition is the 1%-3% (mass percent) of stem of noble dendrobium juice.Before product is drunk, it is ensured that
Suspension grain in stem of noble dendrobium liquid is not precipitated, and adjusts mouthfeel.
It is vitamin C to protect color antistaling agent (preservative), and addition is the 0.1%-0.3% (mass percent) of stem of noble dendrobium juice.
The addition of citric acid is percent 0.01%-0.05% (mass percent) of stem of noble dendrobium juice.
9) quality is detected:
Detect quality standard be：It is more than 0.02% containing dendrobine in stem of noble dendrobium liquid, dendrobium polysaccharide is more than 0.12%.Perception without
Precipitation, color is emerald green transparent.
10) sterilization filling：General drinking bottle mouth ultraviolet sterilization is taken to pack.
11) finished product packing：Overall process is all carried out in closed machinery and pipeline, to ensure that canned rear product does not receive other
Pollution.Finally, sterilization packaging is carried out into liquid beverage flow package, obtains commercially available finished product.
Introduced in more detail below by specific embodiment.
Embodiment 1
1) fresh HERBA DENDROBII (preferably, originating in the HERBA DENDROBII of Chishui Area) of detection is selected, specific method is：Manually
Remove impurity, fibrous root, leaf and sheath, remove the rotten plant that goes rotten.
2) cleaning sterilization：After with fresh stem of noble dendrobium of high pressure water washing, the fresh stem of noble dendrobium laid to individual layer using 120 DEG C of steam
Spray 20 seconds, natural airing.
3) HERBA DENDROBII is refrigerated to -8 DEG C；
4) broken wall is crushed：The HERBA DENDROBII feeding wall-broken grinder of freezing is crushed, crushed material is obtained.Broken wall treatment
Condition be：Temperature control is that, less than -8 DEG C, the rotating speed of the main shaft of broken wall disintegrating machine is 3100r/min.
Pulverizer primary election Jiangyin Yongchang RM-50 types, 500 kilograms per hour of production capacity, power of motor 45 (KW).
5) Wet-type wall-breaking is crushed：The crushed material that upper step is obtained is subsequently entered into wet type micronizer carries out breaking-wall cell powder
It is broken.Less than 2 DEG C are cooled to water cryogenic pulverization, full machine jacket cooling system is added in crushed material.The quality for adding water is crushed material
7 times of amounts of quality, 60 kilograms of speed is smashed per hour, and HERBA DENDROBII liquid is obtained after crushing, and now HERBA DENDROBII liquid contains
The mass fraction of crushed material is 12%-16%.Now, crushed material includes two parts, and a part can be dissolved in water, another part
Water, such as crude fibre etc. can not be dissolved in.
Machine selects Jinan up to micro-, model XDW-F100J, and production capacity is 60 kilograms, power of motor 15 (KW) per hour.
6) precipitation filtering：Making step 5) into tapered settling vessel, precipitation 4 hours takes clear liquid, as first to gained stem of noble dendrobium liquid
The secondary clear liquid for taking, (residue is part water insoluble in crushed material, for example to filter out residue：Crude fibre etc.).Residue is added again
Water washing, the concrete operations of washing are：Residue is entered into tank, the infiltration that adds water is extracted, the weight of water is smash material weight 7 times, to
Crushed material is stirred 30 minutes after adding water, and stands 8 hours, takes the liquid on upper strata, and the liquid remaining part that will take upper strata away was carried out
Filter, takes filtrate, the liquid on upper strata is mixed with filtrate, as the clear liquid for taking for the second time.
7) by step 6) the middle clear liquid of the stem of noble dendrobium twice mixing for obtaining, stem of noble dendrobium juice is obtained, the matter containing crushed material in stem of noble dendrobium juice
Amount fraction is 6%-8%.Inspection by sampling in the process.
Now：In stem of noble dendrobium juice, the content of dendrobium polysaccharide is 0.12%.The content of alkaloid (with dendrobine as representative) is
0.02%.
8) HERBA DENDROBII juice is deployed into HERBA DENDROBII beverage together with food additives.Food additives include white sand
Sugar, thickener, vitamin C and citric acid.White granulated sugar is the 5% of stem of noble dendrobium juice, and used as thickener, cyclodextrin is stone to selection cyclodextrin
The 1% of dry measure used in former times juice, vitamin C is the 0.1% of stem of noble dendrobium juice, and citric acid is the 0.01% of stem of noble dendrobium juice, and every percentage is quality hundred
Divide ratio.
9) sterilization filling.
10) finished product packing：Sterilization packaging is carried out into liquid beverage flow package, finished product is obtained
Embodiment 2
1) fresh HERBA DENDROBII selects detection (by the way of hand picking detection).The standard of detection is：Remove impurity,
Fibrous root, leaf and sheath, remove the rotten plant that goes rotten, it is preferable that using the HERBA DENDROBII for originating in Chishui Area.
2) cleaning sterilization：With fresh stem of noble dendrobium of high pressure water washing, the fresh of individual layers laying is sprayed using 120 DEG C of vapor (steam) temperatures afterwards
The strain of stem of noble dendrobium medicine, is conducive to killing from plucking, transport, bacterium and the microorganism pollution that strain brings is administered during hand picking,
Contribute to the removing of the upper sheath residue of medicine strain simultaneously.It is within 20 seconds that the high temperature of short time is conducive to avoiding the loss of the medicine ability property of medicine.
3) freeze：The stem of noble dendrobium after cleaning sterilization is sent into cool chamber, -8 DEG C are refrigerated to, is at this temperature Chishui HERBA DENDROBII
Optimal brittle point, be conducive to improving the quality that next step broken wall is smashed, be also beneficial to guaranteeing the quality during medicinal material reserve.
4) broken wall is crushed：HERBA DENDROBII feeding freezing wall-broken grinder after freezing is crushed, crushed material is obtained.Powder
Broken condition is：Temperature control is at -8 DEG C.It is 3100r that broken wall smashes the agent speed of mainshaft | min.
Pulverizer primary election Jiangyin Yongchang RM-50 types, 500 kilograms per hour of production capacity, power of motor 45 (KM).
5) Wet-type wall-breaking is crushed：By step 4) crushed material that obtains subsequently enters wet type micronizer and carries out breaking-wall cell
Crush.Less than 2 DEG C are cooled to water cryogenic pulverization, full machine jacket cooling system is added in crushing.The quality for adding water is golden hairpin stone
7 times of the quality of dry measure used in former times crushed material.HERBA DENDROBII liquid is obtained after broken.Now the mass percent of crushed material is in HERBA DENDROBII liquid
12%-16%.
Now, crushed material includes two parts, and a part can be dissolved in water, and another part can not be dissolved in water, such as thick fine
Dimension etc..
Wet type micronizer machine selects Jinan up to micro-, model XDW-F100J, and production capacity is 60 kilograms, motor per hour
Power 15 (KW).
6) precipitation filtering：By step 5) stem of noble dendrobium liquid that obtains enters tapered settling vessel, precipitates 4 hours, afterwards, as first
The secondary clear liquid for taking, filters out residue (residue is water insoluble part in crushed material, such as crude fibre etc.).Residue is added water and is washed
Infiltration is washed, water (smashing 7 times of water of weight of material weight) stirring of same weight 30 minutes, Ran Houjing when adding wet type to smash
After putting 8 hours, take the liquid on upper strata, the liquid remaining part that will take upper strata away is filtered, and takes filtrate, by the liquid on upper strata with
Filtrate mixes, used as the clear liquid for taking for the second time；
7) by step 6) in obtain twice the stem of noble dendrobium clear liquid mixing, obtain HERBA DENDROBII juice, obtain HERBA DENDROBII
The mass fraction of crushed material is 6%-8% in juice.Now the content of important active ingredient is respectively in stem of noble dendrobium juice：In stem of noble dendrobium juice,
The content of dendrobium polysaccharide is 0.14%, and the content of alkaloid is 0.024%, is mass percent.
8) stem of noble dendrobium juice is squeezed into storage tank, addition white sugar, thickener cyclodextrin, vitamin C and citric acid are deployed into beverage
Product.In beverage products, white sugar is the 5% of stem of noble dendrobium juice, and thickener cyclodextrin is the 1% of stem of noble dendrobium juice, and vitamin C is stem of noble dendrobium juice
0.1%, citric acid for stem of noble dendrobium juice 0.01%, each percentage is mass percent.
9) quality is detected.
10) sterilization filling.
11) finished product packing.
Embodiment 3
1) fresh HERBA DENDROBII (preferably, originating in the HERBA DENDROBII of Chishui Area) of detection is selected, specific method is：Manually
Remove impurity, fibrous root, leaf and sheath, remove the rotten plant that goes rotten.
2) cleaning sterilization：After with fresh stem of noble dendrobium of high pressure water washing, the fresh stem of noble dendrobium laid to individual layer using 120 DEG C of steam
Spray 50 seconds, natural airing.
3) HERBA DENDROBII is refrigerated to less than -8 DEG C；
4) broken wall is crushed：The HERBA DENDROBII feeding wall-broken grinder of freezing is crushed, crushed material is obtained.Broken wall treatment
Condition be：Temperature control is that, less than -8 DEG C, the rotating speed of the main shaft of broken wall disintegrating machine is 3100r/min.
Pulverizer primary election Jiangyin Yongchang RM-50 types, 500 kilograms per hour of production capacity, power of motor 45 (KW).
5) Wet-type wall-breaking is crushed：The crushed material that upper step is obtained is subsequently entered into wet type micronizer carries out breaking-wall cell powder
It is broken.Less than 2 DEG C are cooled to water cryogenic pulverization, full machine jacket cooling system is added in crushed material.The quality for adding water is crushed material
7 times of amounts of quality, 60 kilograms of speed is smashed per hour, HERBA DENDROBII liquid is obtained after crushing, now in HERBA DENDROBII liquid
The mass fraction of crushed material is 12%-16%.
Now, crushed material includes two parts, and a part can be dissolved in water, and another part can not be dissolved in water, such as thick fine
Dimension etc..
Machine selects Jinan up to micro-, model XDW-F100J, and production capacity is 60 kilograms, power of motor 15 (KW) per hour.
6) precipitation filtering：Making step 5) into tapered settling vessel, precipitation 4 hours takes clear liquid, as first to gained stem of noble dendrobium liquid
The secondary clear liquid for taking, filters out residue (residue is that can not be dissolved in the part of water, such as crude fibre etc. in crushing).Residue is added water again
Wash, the concrete operations of washing are：Residue is entered into tank, the infiltration that adds water is extracted, the weight of water is smash material weight 7 times, stirring
30 minutes.8 hours are stood afterwards, the liquid on upper strata is taken, the liquid remaining part that will take upper strata away is filtered, and takes filtrate, will
The liquid on upper strata mixes with filtrate, used as the clear liquid for taking for the second time.
7) by step 6) the middle clear liquid of the stem of noble dendrobium twice mixing for obtaining, stem of noble dendrobium juice is obtained, the quality of crushed material point in stem of noble dendrobium juice
Number is 6%-8%.Inspection by sampling in the process.
Now：In stem of noble dendrobium juice, the content of dendrobium polysaccharide is more than 0.12%.The content of alkaloid (with dendrobine as representative)
It is more than 0.02%.
8) HERBA DENDROBII juice is deployed into HERBA DENDROBII beverage together with food additives.Food additives include white sand
Sugar, thickener, vitamin C and citric acid.White granulated sugar is the 5% of stem of noble dendrobium juice, and used as thickener, cyclodextrin is stone to selection cyclodextrin
The 1% of dry measure used in former times juice, vitamin C is the 0.1% of stem of noble dendrobium juice, and citric acid is the 0.01% of stem of noble dendrobium juice, and every percentage is quality hundred
Divide ratio.
9) sterilization filling.
10) finished product packing：Sterilization packaging is carried out into liquid beverage flow package, finished product is obtained
Through experiment, it is chilled to the smashing of brittle point broken wall and is compared with the smashing of normal temperature broken wall, the active drug content in stem of noble dendrobium liquid
Dendrobium polysaccharide improves 16%.Dendrobine improves 20%, illustrates that the broken wall for being chilled to brittle point is smashed and is effectively improved stone
The leaching rate of dry measure used in former times drug ingedient.
The stem of noble dendrobium is chilled to optimal brittle point, full wet type broken wall is smashed, and broken wall is smashed and is carried out continuously twice, infiltration twice is carried
Take, an a kind of technical scheme for the excellent of relative ease of flow production.
The present invention is directly to be chilled to -8 DEG C or less than -8 DEG C of optimal brittle point with the fresh stem of noble dendrobium (to be tested by test of many times
Card, with HERBA DENDROBII as raw material, under other conditions same case, -8 DEG C of condition obtains the content highest of active drug) enter
After row broken wall is smashed, Wet-type wall-breaking smashing is subsequently entered, be made stem of noble dendrobium liquid.Thereafter merely through extracting twice, precipitation, at separation
Reason.Feature is that whole process is completed all under conditions of low temperature, ensure that to most successful the genuine of fresh HERBA DENDROBII and
The property of medicine.Through experiment, it is chilled to the smashing of brittle point broken wall and is compared with the smashing of normal temperature broken wall, the active drug content in stem of noble dendrobium liquid is improved
More than 15%.Analysis data explanation extracted amount has reached more than the 95% of theoretical content.
The present invention can retain the intrinsic fresh fragrance of HERBA DENDROBII by dendrobium stem beverage prepared by the above method.In drinking
Energy product go out the unique delicate fragrance of HERBA DENDROBII, the local flavor of its unique pleasant are formed, rather than flavour of a drug.Meanwhile, also ensure that
The emerald green color of stem of noble dendrobium drink, forms beautiful outward appearance, is more suitable for people and drinks.
The present invention is farthest extracted and make use of pharmaceutical compositions.The drug resource of preciousness is not wasted.The stem of noble dendrobium is used as medicine
Thing, always just there is raw and dry two kinds of food methods, the fresh raw stem of noble dendrobium health beverages that the present invention provides a convenient.By fresh stone
Dry measure used in former times spreads to the area for not producing the stem of noble dendrobium.
Technological process of the invention is fairly simple, eliminates the complex steps processed as powder medicaments, thus can be big
Big reduces cost, can provide high-quality cheap dendrobium health-care product.Valuable medicine is allowed to come into daily life,
The foregoing is only presently preferred embodiments of the present invention, be not intended to limit the invention, it is all it is of the invention spirit and
Within principle, any modification, equivalent substitution and improvements made etc. should be included within the scope of the present invention.
Claims (10)
1. a kind of preparation method of dendrobium stem beverage, it is characterised in that comprise the following steps：
1) stem of noble dendrobium is freezed；
2) stem of noble dendrobium after freezing is entered into broken wall treatment, obtains stem of noble dendrobium crushed material；
3) after stem of noble dendrobium crushed material is mixed with solvent, wet type micronized pulverization is carried out, obtains stem of noble dendrobium liquid；
4) will be filtered after stem of noble dendrobium liquid precipitate, obtain stem of noble dendrobium juice；
5) stem of noble dendrobium juice is deployed into dendrobium stem beverage.
2. a kind of preparation method of dendrobium stem beverage according to claim 1, it is characterised in that step 1) to step 5) control
Below 4 DEG C；Step 1) in, the stem of noble dendrobium is refrigerated to less than -8 DEG C；The stem of noble dendrobium is HERBA DENDROBII.
3. a kind of preparation method of dendrobium stem beverage according to claim 1, it is characterised in that step 2) in, broken wall treatment
Condition is：Temperature control is less than -8 DEG C, and broken wall is carried out using wall-broken grinder, and the rotating speed of the main shaft of broken wall disintegrating machine is
3100r/min。
4. a kind of preparation method of dendrobium stem beverage according to claim 1, it is characterised in that step 3) concrete operations be：
Stem of noble dendrobium crushed material feeding wet type micronizer is carried out into breaking-wall cell crushing, solvent is added, the quality of solvent is stem of noble dendrobium crushing
7 times of the quality of material, stem of noble dendrobium crushed material is mixed with solvent, and temperature is less than 2 DEG C during wet type micronized pulverization, and solvent is water.
5. a kind of preparation method of dendrobium stem beverage according to claim 1, it is characterised in that step 4) in, precipitation and filter
Concrete operations be：By stem of noble dendrobium liquid precipitate 4 hours, by filtering to take clear liquid, residue is filtered out；Residue is added water again, stirring 30
Minute, 8 hours are stood, take clear liquid；The clear liquid mixing that will be taken twice, obtains stem of noble dendrobium juice.
6. a kind of preparation method of dendrobium stem beverage according to claim 1, it is characterised in that step 4) in, in stem of noble dendrobium juice, stone
The content of dry measure used in former times is the 6%-8% of stem of noble dendrobium juice, and the content of dendrobium polysaccharide is not less than 0.12%, and the content of alkaloid is not less than
0.02%.
7. a kind of preparation method of dendrobium stem beverage according to claim 1, it is characterised in that step 5) concrete operations be：
Stem of noble dendrobium juice is mixed with food additives, afterwards sterilization filling, packaging；The food additives include sweetener, thickener, prevent
Rotten agent and citric acid, sweetener and the mass percent that the mass percent of stem of noble dendrobium juice is 5%-20%, thickener and stem of noble dendrobium juice
It is 1%-3%, preservative and the mass percent that the mass percent of stem of noble dendrobium juice is 0.1%-0.3%, citric acid and stem of noble dendrobium juice
It is 0.01%-0.05%.
8. a kind of preparation method of dendrobium stem beverage according to claim any one of 1-7, it is characterised in that in step 1) before
Also include sterilized step, sterilized method is：The stem of noble dendrobium is sprayed 20-50 seconds using 120 DEG C of steam.
9. a kind of preparation method of dendrobium stem beverage according to claim 8, it is characterised in that also include before sterilisation step clear
Clean step, the method for cleaning is：Using the high pressure water washing stem of noble dendrobium.
10. a kind of preparation method of dendrobium stem beverage according to claim 9, it is characterised in that also wrapped between cleaning
Include and select detecting step：Remove impurity, fibrous root, leaf and sheath, remove the rotten stem of noble dendrobium that goes rotten.
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| CN108244433A (en) * | 2018-01-26 | 2018-07-06 | 合肥工业大学 | A kind of preparation method for improving the fresh middle total alkaloid stripping quantity of squeezing the juice of the stem of noble dendrobium |
| CN109007498A (en) * | 2018-07-28 | 2018-12-18 | 普定县真源农业开发有限公司 | A kind of preparation method of mulberry juice |
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Application publication date: 20170707 |