CN106138266A - Flos Osmanthi Fragrantis is good for tooth buccal tablet and preparation method thereof - Google Patents
Flos Osmanthi Fragrantis is good for tooth buccal tablet and preparation method thereof Download PDFInfo
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- CN106138266A CN106138266A CN201610642990.8A CN201610642990A CN106138266A CN 106138266 A CN106138266 A CN 106138266A CN 201610642990 A CN201610642990 A CN 201610642990A CN 106138266 A CN106138266 A CN 106138266A
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K36/00—Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
- A61K36/18—Magnoliophyta (angiosperms)
- A61K36/185—Magnoliopsida (dicotyledons)
- A61K36/63—Oleaceae (Olive family), e.g. jasmine, lilac or ash tree
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K31/00—Medicinal preparations containing organic active ingredients
- A61K31/045—Hydroxy compounds, e.g. alcohols; Salts thereof, e.g. alcoholates
- A61K31/047—Hydroxy compounds, e.g. alcohols; Salts thereof, e.g. alcoholates having two or more hydroxy groups, e.g. sorbitol
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K36/00—Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
- A61K36/18—Magnoliophyta (angiosperms)
- A61K36/185—Magnoliopsida (dicotyledons)
- A61K36/35—Caprifoliaceae (Honeysuckle family)
- A61K36/355—Lonicera (honeysuckle)
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K36/00—Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
- A61K36/18—Magnoliophyta (angiosperms)
- A61K36/185—Magnoliopsida (dicotyledons)
- A61K36/65—Paeoniaceae (Peony family), e.g. Chinese peony
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K36/00—Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
- A61K36/18—Magnoliophyta (angiosperms)
- A61K36/185—Magnoliopsida (dicotyledons)
- A61K36/71—Ranunculaceae (Buttercup family), e.g. larkspur, hepatica, hydrastis, columbine or goldenseal
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K9/00—Medicinal preparations characterised by special physical form
- A61K9/0012—Galenical forms characterised by the site of application
- A61K9/0053—Mouth and digestive tract, i.e. intraoral and peroral administration
- A61K9/0056—Mouth soluble or dispersible forms; Suckable, eatable, chewable coherent forms; Forms rapidly disintegrating in the mouth; Lozenges; Lollipops; Bite capsules; Baked products; Baits or other oral forms for animals
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K9/00—Medicinal preparations characterised by special physical form
- A61K9/20—Pills, tablets, discs, rods
- A61K9/2004—Excipients; Inactive ingredients
- A61K9/2022—Organic macromolecular compounds
- A61K9/205—Polysaccharides, e.g. alginate, gums; Cyclodextrin
- A61K9/2059—Starch, including chemically or physically modified derivatives; Amylose; Amylopectin; Dextrin
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Abstract
The invention discloses a kind of Flos Osmanthi Fragrantis and be good for tooth buccal tablet, this buccal tablet is made up of following component in parts by weight: Flos Osmanthi Fragrantis 10 25 parts, Flos Lonicerae 5 15 parts, Cortex Moutan 15 parts, xylitol 52 57 parts, maltodextrin 7 15 parts, beta cyclodextrin 48 parts, natural Peppermint essential oil 0.5 1 parts, magnesium stearate 0.4 part.Its preparation method, i.e. prepares this Flos Osmanthi Fragrantis buccal tablet by carrying out the operations such as raw material micronization processes, batch mixing, the soft material of system, pelletize, dry, tabletting successively.Whole invention is used for halitosis, pharyngodynia with dryness, cough dry pharynx, toothache due to dental caries etc., have ward off smelly, promote the production of body fluid, reduce phlegm, the multiple efficacies such as pain relieving, and in good taste, bioavailability is high；Preparation method is simple, it is adaptable to industrialized mass production.
Description
Technical field
The present invention relates to a kind of Flos Osmanthi Fragrantis and be good for tooth buccal tablet and preparation method thereof, belong to medicines and health protection technical field.
Background technology
Halitosis, is the bad breath coming out and making others to be sick of in population, make oneself embarrassment.Slight halitosis hair
Disease, makes us the most worried, and it can make people closely dare not exchange with people, thus produces inferiority complex, affects the most interpersonal, feelings
Sense exchange.
Halitosis is not a kind of independent disease, but a lot of disease such as oral disease, nasopharyngeal diseases and some general
The symptom that disease is had.Current research finds, the halitosis outpatients of 90% is because what oral problem caused, gingivitis,
Periodontitis, dental caries etc. all may cause the generation of halitosis, and halitosis most commonly encountered diseases is because being periodontitis.Suffer from chronic gingivitis and tooth
The patient of Zhou Yan, due to swelling and aching of gum, hemorrhage, purulent discharge of pocket, dental health are very poor, the bacterial plaque of accumulation, tooth on tooth
Stone and tartar are under the effect of antibacterial and microorganism, and corruption is fermented, and produce niff.
Summary of the invention
For above-mentioned weak point of the prior art, it is desirable to provide a kind of Flos Osmanthi Fragrantis is good for tooth buccal tablet and preparation thereof
Method, it is used for halitosis, pharyngodynia with dryness, cough dry pharynx, toothache due to dental caries etc., have ward off smelly, promote the production of body fluid, reduce phlegm, the multiple merit such as pain relieving
Effect.
To achieve these goals, technical scheme:
A kind of Flos Osmanthi Fragrantis is good for tooth buccal tablet, and this buccal tablet is made up of following component in parts by weight: Flos Osmanthi Fragrantis 10-25 part, mountain
Flos Lonicerae 5-15 part, Cortex Moutan 1-5 part, xylitol 52-57 part, maltodextrin 7-15 part, beta-schardinger dextrin-4-8 part, natural peppermint essence
Oil 0.5-1 part, magnesium stearate 0.4 part.
Further, this buccal tablet is made up of following component the most in parts by weight: Flos Osmanthi Fragrantis 14-17 part, Flos Lonicerae 9-12 part,
Cortex Moutan 2-4 part, xylitol 52-56 part, maltodextrin 10-11 part, beta-schardinger dextrin-5-6 part, natural Peppermint essential oil 0.7-1 part,
Magnesium stearate 0.4 part.
A kind of Flos Osmanthi Fragrantis is good for the preparation method of tooth buccal tablet, and it includes that preparation process has:
S1, each solid material respectively micronizing of component proportion being sieved through by No. 10 pharmacopeia will be pressed filter；
S2, micronizing is filtered the Flos Osmanthi Fragrantis superfine powder of gained, Flos Lonicerae superfine powder, Cortex Moutan superfine powder, xylitol surpass
Micropowder, maltodextrin superfine powder, beta-schardinger dextrin-superfine powder are sufficiently mixed, and are sieved through filter again by No. 10 pharmacopeia, obtain compound；
S3, by compound and mass percentage concentration be 65～70% ethanol mix to obtain soft material, wherein, ethanol and compound
Quality proportioning be 32～35:100, ethanol before mixing with compound, first will by component proportion natural Peppermint essential oil dissolve
In ethanol；
S4, soft material being crossed No. 3 pharmacopeia sieve, be dried after pelletize at 45～55 DEG C, making granule water content is 7～8%；
S5, will be sufficiently mixed with gained granule by the magnesium stearate of component proportion, tabletting obtains Flos Osmanthi Fragrantis buccal tablet.
Further, during described step S4 granulating and drying, gently turn down a layer granule at interval of 15min, make granule materials be heated
Uniformly；It is dried criterion need to meet: one: it is clear-cut, tack-free that hands pinches granule feel, firmly one has pinched and can crumb reluctantly；
Its two: measure granule materials water content, water content is 7～about 8%.
Further, in described step S1, the preparation process of Flos Osmanthi Fragrantis superfine powder includes:
S1-1, fresh Flos Osmanthi Fragrantis is soaked in colour fixative after 1h, takes out, spread and dry；Wherein colour fixative is by following weight
The component composition of part meter: citric acid 2 parts, 1.5 parts of ascorbic acid, ethylenediaminetetraacetic acid 3 parts, 1000 parts of water；
S1-2, colour fixative is processed after Flos Osmanthi Fragrantis at-0.6MPa pressure, under the conditions of 40 DEG C, drying under reduced pressure 4h, make Flos Osmanthi Fragrantis
Water content is down to less than 10%；
S1-3, dried Flos Osmanthi Fragrantis is carried out micronizing 20～30min under the conditions of 10 DEG C, obtain Flos Osmanthi Fragrantis superfine powder.
Beneficial effects of the present invention: for halitosis, pharyngodynia with dryness, cough dry pharynx, toothache due to dental caries etc., wherein, Flos Osmanthi Fragrantis is warm in nature
Acrid in the mouth, has stomach invigorating, reduces phlegm, promotes the production of body fluid, dissipates expectorant, the effect of suppressing the hyperactive liver, can only control abundant expectoration cough, hemorrhoidal hamorrhage dysentery, have a toothache halitosis, appetite
Depressed, amenorrhea stomachache；Flos Lonicerae sugariness is trembled with fear, and has the effect of heat-clearing and toxic substances removing, dispelling wind and heat pathogens, broad-spectrum antiseptic, to aerobic, anaerobism
Bacterium such as gold-coloured staphylococci, escherichia coli, bacillus pyocyaneus have inhibitory action, thus play oral disinfecting, antibacterial effect；Paeonia suffruticosa
Skin bitter in the mouth cold in nature, has the effect of clearing away heat and cooling blood, promoting blood circulation to remove blood stasis, inducing diuresis to remove edema；Xylitol has refrigerant sweet taste, have wet one's whistle, clean
Tooth, pre-anticariogenic effect.Generally speaking, in the present invention buccal tablet have ward off smelly, promote the production of body fluid, reduce phlegm, the multiple efficacies such as pain relieving, and
In good taste, bioavailability is high；Preparation method is simple, it is adaptable to industrialized mass production.
Detailed description of the invention
The present invention is further described below in conjunction with specific embodiment.
A kind of Flos Osmanthi Fragrantis is good for tooth buccal tablet, it is characterised in that this buccal tablet is made up of following component in parts by weight: Flos Osmanthi Fragrantis
10-25 part, Flos Lonicerae 5-15 part, Cortex Moutan 1-5 part, xylitol 52-57 part, maltodextrin 7-15 part, beta-schardinger dextrin-4-8 part,
Natural Peppermint essential oil 0.5-1 part, magnesium stearate 0.4 part.Further, this buccal tablet is by following component group in parts by weight
Become: Flos Osmanthi Fragrantis 14-17 part, Flos Lonicerae 9-12 part, Cortex Moutan 2-4 part, xylitol 52-56 part, maltodextrin 10-11 part, β-ring are stuck with paste
Essence 5-6 part, natural Peppermint essential oil 0.7-1 part, magnesium stearate 0.4 part.
Embodiment 1: Flos Osmanthi Fragrantis is good for the prescription 1 of tooth buccal tablet and includes Flos Osmanthi Fragrantis 14 parts, Flos Lonicerae 12 parts, Cortex Moutan 1 part, xylose
Alcohol 57 parts, maltodextrin 11 parts, beta-schardinger dextrin-5 parts, natural Peppermint essential oil 0.7 part, magnesium stearate 0.4 part.
Embodiment 2: Flos Osmanthi Fragrantis is good for the prescription 2 of tooth buccal tablet and includes Flos Osmanthi Fragrantis 25 parts, Flos Lonicerae 5 parts, Cortex Moutan 2 parts, xylose
Alcohol 52 parts, maltodextrin 7 parts, beta-schardinger dextrin-8 parts, natural Peppermint essential oil 1 part, magnesium stearate 0.4 part.
Embodiment 3: Flos Osmanthi Fragrantis is good for the prescription 3 of tooth buccal tablet and includes Flos Osmanthi Fragrantis 10 parts, Flos Lonicerae 15 parts, Cortex Moutan 4 parts, xylose
Alcohol 52 parts, maltodextrin 15 parts, beta-schardinger dextrin-4 parts, natural Peppermint essential oil 0.5 part, magnesium stearate 0.4 part.
Embodiment 4: Flos Osmanthi Fragrantis is good for the prescription 4 of tooth buccal tablet and includes Flos Osmanthi Fragrantis 17 parts, Flos Lonicerae 9 parts, Cortex Moutan 2 parts, xylose
Alcohol 56 parts, maltodextrin 10 parts, beta-schardinger dextrin-6 parts, natural Peppermint essential oil 0.5 part, magnesium stearate 0.4 part.
This Flos Osmanthi Fragrantis is good for the preparation method of tooth buccal tablet, has including preparation process:
S1, raw material micronization processes: the compressed tablet slowly dissolved in referring to be contained in oral cavity because of buccal tablet, except meeting tablet
Basic demand outside, it is necessary to possess tempting color, so that the mouthfeel that user has had.When using pressed powder as
When processing raw material, as material particle size is excessive, often will produce harsh feeling in oral cavity, this is owing in tablet, solid particle dissolves
Time occur that trickle friction causes with the contact surface of tongue, therefore will by each solid material of component proportion micronizing respectively also
It is sieved through filter by No. 10 pharmacopeia；
S2, batch mixing: micronizing is filtered the Flos Osmanthi Fragrantis superfine powder of gained, Flos Lonicerae superfine powder, Cortex Moutan superfine powder, xylose
Alcohol superfine powder, maltodextrin superfine powder, beta-schardinger dextrin-superfine powder are sufficiently mixed, and are sieved through filter again by No. 10 pharmacopeia, obtain mixing
Material；
S3, make soft material: by compound and mass percentage concentration be 65～70% ethanol mix to obtain soft material, wherein, ethanol
Being 32～35:100 with the quality proportioning of compound, ethanol is before mixing with compound, first by by the natural Herba Menthae of component proportion
Quintessence oil is dissolved in ethanol；
S4, pelletize, be dried: soft material being crossed No. 3 pharmacopeia sieve, is dried after pelletize at 45～55 DEG C, making granule water content is 7
～8%；Specifically, after granulating and drying a period of time, gently turn down a layer granule at interval of 15min, lower floor's granule is turned to upper strata, makes
Granule materials is heated evenly；Being dried criterion need to meet: one, first carried out sensory judgments, hands is pinched granule feel and is done
Crisp, tack-free, firmly one pinch and can crumb reluctantly；Its two, measure granule materials water content, water content is 7～about 8%.
S5, tabletting: will be sufficiently mixed with gained granule by the magnesium stearate of component proportion, tabletting obtains Flos Osmanthi Fragrantis buccal tablet.
It addition, in step sl, the preparation process of Flos Osmanthi Fragrantis superfine powder includes:
S1-1, fresh Flos Osmanthi Fragrantis is soaked in colour fixative after 1h, takes out, spread and dry；Wherein colour fixative is by following weight
The component composition of part meter: citric acid 2 parts, 1.5 parts of ascorbic acid, ethylenediaminetetraacetic acid 3 parts, 1000 parts of water；
S1-2, colour fixative is processed after Flos Osmanthi Fragrantis at-0.6MPa pressure, under the conditions of 40 DEG C, drying under reduced pressure 4h, make Flos Osmanthi Fragrantis
Water content is down to less than 10%；
S1-3, dried Flos Osmanthi Fragrantis is carried out micronizing 20～30min under the conditions of 10 DEG C, obtain Flos Osmanthi Fragrantis superfine powder.
Because fresh Flos Osmanthi Fragrantis easily occurs oxidizing brown stain in conventional drying, product color is caused to deepen blackening, therefore, newly
Fresh Flos Osmanthi Fragrantis carries out color retention before being dried, rear drying under reduced pressure, then superfine comminution at low temperature, compared with conventional formulation, and bioavailability
Height, and completely remain the intrinsic color and luster of Flos Osmanthi Fragrantis and fragrance, this technique simplifies simultaneously, is lost little.
The technical scheme provided the embodiment of the present invention above is described in detail, specific case used herein
Principle and embodiment to the embodiment of the present invention are set forth, and the explanation of above example is only applicable to help to understand this
The principle of inventive embodiments；Simultaneously for one of ordinary skill in the art, according to the embodiment of the present invention, in specific embodiment party
All will change in formula and range of application, in sum, this specification content should not be construed as limitation of the present invention.
Claims (5)
1. a Flos Osmanthi Fragrantis is good for tooth buccal tablet, it is characterised in that this buccal tablet is made up of following component in parts by weight: Flos Osmanthi Fragrantis
10-25 part, Flos Lonicerae 5-15 part, Cortex Moutan 1-5 part, xylitol 52-57 part, maltodextrin 7-15 part, beta-schardinger dextrin-4-8 part,
Natural Peppermint essential oil 0.5-1 part, magnesium stearate 0.4 part.
Flos Osmanthi Fragrantis the most according to claim 1 is good for tooth buccal tablet, it is characterised in that this buccal tablet by following the most in parts by weight
Component form: Flos Osmanthi Fragrantis 14-17 part, Flos Lonicerae 9-12 part, Cortex Moutan 2-4 part, xylitol 52-56 part, maltodextrin 10-11 part,
Beta-schardinger dextrin-5-6 part, natural Peppermint essential oil 0.7-1 part, magnesium stearate 0.4 part.
Flos Osmanthi Fragrantis the most according to claim 1 or claim 2 is good for the preparation method of tooth buccal tablet, it is characterised in that include that preparation process has:
S1, each solid material respectively micronizing of component proportion being sieved through by No. 10 pharmacopeia will be pressed filter；
S2, micronizing is filtered the Flos Osmanthi Fragrantis superfine powder of gained, Flos Lonicerae superfine powder, Cortex Moutan superfine powder, xylitol superfine powder,
Maltodextrin superfine powder, beta-schardinger dextrin-superfine powder are sufficiently mixed, and are sieved through filter again by No. 10 pharmacopeia, obtain compound；
S3, by compound and mass percentage concentration be 65～70% ethanol mix to obtain soft material, wherein, the matter of ethanol and compound
Amount proportioning is 32～35:100, and ethanol, before mixing with compound, first will be dissolved in second by the natural Peppermint essential oil of component proportion
In alcohol；
S4, soft material being crossed No. 3 pharmacopeia sieve, be dried after pelletize at 45～55 DEG C, making granule water content is 7～8%；
S5, will be sufficiently mixed with gained granule by the magnesium stearate of component proportion, tabletting obtains Flos Osmanthi Fragrantis buccal tablet.
The most according to claim 3, Flos Osmanthi Fragrantis is good for the preparation method of tooth buccal tablet, it is characterised in that: described step S4 granulating and drying
Time, gently turn down a layer granule at interval of 15min, make granule materials be heated evenly；It is dried criterion need to meet: one: hands
Pinch granule feel clear-cut, tack-free, firmly one pinch and can crumb reluctantly；Its two: measure granule materials water content, water content be 7～
About 8%.
The most according to claim 3, Flos Osmanthi Fragrantis is good for the preparation method of tooth buccal tablet, it is characterised in that: in described step S1, Flos Osmanthi Fragrantis
The preparation process of superfine powder includes:
S1-1, fresh Flos Osmanthi Fragrantis is soaked in colour fixative after 1h, takes out, spread and dry；Wherein colour fixative is by following weight portion meter
Component composition: citric acid 2 parts, 1.5 parts of ascorbic acid, ethylenediaminetetraacetic acid 3 parts, 1000 parts of water；
S1-2, colour fixative is processed after Flos Osmanthi Fragrantis at-0.6MPa pressure, under the conditions of 40 DEG C, drying under reduced pressure 4h, make the aqueous of Flos Osmanthi Fragrantis
Amount is down to less than 10%；
S1-3, dried Flos Osmanthi Fragrantis is carried out micronizing 20～30min under the conditions of 10 DEG C, obtain Flos Osmanthi Fragrantis superfine powder.
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| CN201610642990.8A CN106138266A (en) | 2016-08-08 | 2016-08-08 | Flos Osmanthi Fragrantis is good for tooth buccal tablet and preparation method thereof |
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Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN115211485A (en) * | 2022-06-08 | 2022-10-21 | 湖北科技学院 | Sweet osmanthus buccal tablets for clearing heat from throat and moistening lung |
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| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN103250859A (en) * | 2013-05-29 | 2013-08-21 | 崔爱叶 | Osmanthus fragrans chewing gum |
| CN103263588A (en) * | 2013-05-23 | 2013-08-28 | 重庆市中药研究院 | Compound buccal tablet containing dendrobium nobile and honeysuckle and preparation method thereof |
| CN103285242A (en) * | 2013-05-23 | 2013-09-11 | 重庆市中药研究院 | Dendrobium buccal tablets and preparation method for same |
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2016
- 2016-08-08 CN CN201610642990.8A patent/CN106138266A/en active Pending
Patent Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN103263588A (en) * | 2013-05-23 | 2013-08-28 | 重庆市中药研究院 | Compound buccal tablet containing dendrobium nobile and honeysuckle and preparation method thereof |
| CN103285242A (en) * | 2013-05-23 | 2013-09-11 | 重庆市中药研究院 | Dendrobium buccal tablets and preparation method for same |
| CN103250859A (en) * | 2013-05-29 | 2013-08-21 | 崔爱叶 | Osmanthus fragrans chewing gum |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN115211485A (en) * | 2022-06-08 | 2022-10-21 | 湖北科技学院 | Sweet osmanthus buccal tablets for clearing heat from throat and moistening lung |
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