CN106120389A - 一种真丝低温环保染色工艺 - Google Patents

一种真丝低温环保染色工艺 Download PDF

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CN106120389A
CN106120389A CN201610539550.XA CN201610539550A CN106120389A CN 106120389 A CN106120389 A CN 106120389A CN 201610539550 A CN201610539550 A CN 201610539550A CN 106120389 A CN106120389 A CN 106120389A
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real silk
bath raio
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金建国
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Deqing County Xingxinda Silk Pint Co Ltd
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Abstract

本发明公开了一种真丝低温环保染色工艺：以下均为质量百分比；（1）将取真丝织物浸入预处理液中，浴比1：30，保持恒温35℃处理，然后用去离子水清洗干净残留物，40‑45℃烘干；所述预处理液配方为：α‑淀粉酶0.02‑0.04%，木瓜蛋白酶0.8%，甘氨酸0.3‑0.5%，丝素蛋白1%；（2）将预处理后的真丝织物浸入处理液中，浴比1：25，保持恒温35℃处理，然后用去离子水清洗干净残留物，40‑45℃烘干；所述处理液配方为：柠檬酸，海藻糖水溶液；（3）酸性大红3R染色。

Description

一种真丝低温环保染色工艺
技术领域
本发明涉及一种真丝低温环保染色工艺，属于纺织印染领域。
背景技术
真丝织物具有光泽柔和、手感柔滑、吸湿透气等优良的服用性能，特别适宜于制作对抗菌性有较高要求的内衣和婴幼儿服装等产品。蚕丝织物因具有吸湿快干、优雅光泽和滑爽的手感而受到人们的喜爱。理论上蚕丝织物可以用酸性、中性、直接、活性、阳离子、还原、可溶性还原、不溶性偶氮染料染色，但实际应用中，因丝纤维在碱性介质中容易受损，所以一般以酸性染料染色为主一，辅以中性、直接、活性染料染色。蚕丝纤维用匀染性酸性染料染色时湿牢度较差，织物染深性不好，染色脚水对环境污染严重，所以提高蚕丝纤维染色性能具有重要意义。
本发明旨在提供一种真丝低温环保染色工艺，其充分利用多种手段结合，尤其是生物酶的使用，无化学物质残留，天然环保，无需高温，并且染色后的真丝织物具有良好的K/S指，色牢度以及优良的抗菌性能。
发明内容
基于背景技术存在的技术问题，本发明针对背景技术存在的问题，提供一种真丝低温环保染色工艺，其充分利用多种手段结合，尤其是生物酶的使用，无化学物质残留，天然环保，无需高温，并且处理后的真丝具有优异的染色性能以及抗菌性。
本发明的目的通过以下技术方案实现：
一种真丝低温环保染色工艺，其步骤如下：
以下均为质量百分比；
(1)将取真丝织物浸入预处理液中，浴比1：30，保持恒温35℃处理，然后用去离子水清洗干净残留物，40-45℃烘干；
所述预处理液配方为：α-淀粉酶0.02-0.04％，木瓜蛋白酶0.8％，甘氨酸0.3-0.5％，丝素蛋白1％；
(2)将预处理后的真丝织物浸入处理液中，浴比1：25，保持恒温35℃处理，然后用去离子水清洗干净残留物，40-45℃烘干；
所述处理液配方为：柠檬酸1％，海藻糖0.5-0.8％；
(3)酸性大红3R染色：
染色工艺:在50℃入染，10min后以10℃/min升温速度升温至90℃，保温染色60min后降温、排液、后处理。
染色处方:
酸性染料 2％(o.w.f)；
硫酸钠 1g/L；
pH 4.0；
浴比 100:1。
本发明的有益之处在于：
本发明旨在提供一种真丝低温环保染色工艺，其充分利用多种手段结合，尤其是生物酶的使用，无化学物质残留，天然环保，无需高温，并且染色后的真丝织物具有良好的K/S指，色牢度以及优良的抗菌性能。
具体实施方式
本发明所用的真丝织物均为真丝绸14654素绉缎试样。
实施例1：
一种真丝低温环保染色工艺，其步骤如下：
以下均为质量百分比；
(1)将取真丝织物浸入预处理液中，浴比1：30，保持恒温35℃处理，然后用去离子水清洗干净残留物，40℃烘干；
所述预处理液配方为：α-淀粉酶0.04％，木瓜蛋白酶0.8％，甘氨酸0.3％，丝素蛋白1％；
(2)将预处理后的真丝织物浸入处理液中，浴比1：25，保持恒温35℃处理，然后用去离子水清洗干净残留物，45℃烘干；
所述处理液配方为：柠檬酸1％，海藻糖0.5％；
(3)酸性大红3R染色：
染色工艺:在50℃入染，10min后以10℃/min升温速度升温至90℃，保温染色60min后降温、排液、后处理。
染色处方:
酸性染料 2％(o.w.f)；
硫酸钠 1g/L；
pH 4.0；
浴比 100:1。
实施例2：
一种真丝低温环保染色工艺，其步骤如下：
以下均为质量百分比；
(1)将取真丝织物浸入预处理液中，浴比1：30，保持恒温35℃处理，然后用去离子水清洗干净残留物，45℃烘干；
所述预处理液配方为：α-淀粉酶0.02％，木瓜蛋白酶0.8％，甘氨酸0.5％，丝素蛋白1％；
(2)将预处理后的真丝织物浸入处理液中，浴比1：25，保持恒温35℃处理，然后用去离子水清洗干净残留物，40℃烘干；
所述处理液配方为：柠檬酸1％，海藻糖0.8％；
(3)酸性大红3R染色：
染色工艺:在50℃入染，10min后以10℃/min升温速度升温至90℃，保温染色60min后降温、排液、后处理。
染色处方：
酸性染料 2％(o.w.f)；
硫酸钠 1g/L；
pH 4.0；
浴比 100:1。
实施例3：
一种真丝低温环保染色工艺，其步骤如下：
以下均为质量百分比；
(1)将取真丝织物浸入预处理液中，浴比1：30，保持恒温35℃处理，然后用去离子水清洗干净残留物，41℃烘干；
所述预处理液配方为：α-淀粉酶0.03％，木瓜蛋白酶0.8％，甘氨酸0.4％，丝素蛋白1％；
(2)将预处理后的真丝织物浸入处理液中，浴比1∶25，保持恒温35℃处理，然后用去离子水清洗干净残留物，44℃烘干；
所述处理液配方为：柠檬酸1％，海藻糖0.6％；
(3)酸性大红3R染色：
染色工艺:在50℃入染，10min后以10℃/min升温速度升温至90℃，保温染色60min后降温、排液、后处理。
染色处方：
酸性染料 2％(o.w.f)；
硫酸钠 1g/L；
pH 4.0；
浴比 100:1。
实施例4：
一种真丝低温环保染色工艺，其步骤如下：
以下均为质量百分比；
(1)将取真丝织物浸入预处理液中，浴比1∶30，保持恒温35℃处理，然后用去离子水清洗干净残留物，44℃烘干；
所述预处理液配方为：α-淀粉酶0.04％，木瓜蛋白酶0.8％，甘氨酸0.5％，丝素蛋白1％；
(2)将预处理后的真丝织物浸入处理液中，浴比1∶25，保持恒温35℃处理，然后用去离子水清洗干净残留物，41℃烘干；
所述处理液配方为：柠檬酸1％，海藻糖0.7％；
(3)酸性大红3R染色：
染色工艺:在50℃入染，10min后以10℃/min升温速度升温至90℃，保温染色60min后降温、排液、后处理。
染色处方：
酸性染料 2％(o.w.f)；
硫酸钠 1g/L；
pH 4.0；
浴比 100:1。
实施例5：
一种真丝低温环保染色工艺，其步骤如下：
以下均为质量百分比；
(1)将取真丝织物浸入预处理液中，浴比1：30，保持恒温35℃处理，然后用去离子水清洗干净残留物，42℃烘干；
所述预处理液配方为：α-淀粉酶0.02％，木瓜蛋白酶0.8％，甘氨酸0.3％，丝素蛋白1％；
(2)将预处理后的真丝织物浸入处理液中，浴比1：25，保持恒温35℃处理，然后用去离子水清洗干净残留物，43℃烘干；
所述处理液配方为：柠檬酸1％，海藻糖0.5％；
(3)酸性大红3R染色：
染色工艺:在50℃入染，10min后以10℃/min升温速度升温至90℃，保温染色60min后降温、排液、后处理。
染色处方：
酸性染料 2％(o.w.f)；
硫酸钠 1g/L；
pH 4.0；
浴比 100:1。
实施例6：
效果测评：
K/S值测试：织物折叠2层，在DataC olor6 50测色配色仪上测定K/S值，取四个不同的点测定，取平均值。
皂洗牢度的评定：参照G B/T3921.1-1997测试。
评价织物抗菌性能的持久性，主要是对抗菌织物进行抗菌性能的耐洗性试验。抗菌织物洗涤试验参照《FZ/T 73023—2006抗菌针织品》中附录C的简化洗涤条件及程序，对待测织物洗涤50次。
抗菌织物性能测试方法参照《FZ/T 73023—2006抗菌针织品》中附录D的振荡法。振荡法是模仿人体的穿着条件，使细菌在振荡条件下与服装内抗菌剂接触，通过计算细菌减少率，确定抗菌性能大小的一种方法。振荡法测试步骤是：将待测试样放入含有一定浓度的细菌(金黄色葡萄球菌菌种)培养液中，然后把试样置于往复式振荡器上，在(24±1)℃下，以150r/min的速度振荡18h，通过振荡使试样织物与菌液充分接触后，在(37±1)℃生化培养箱中培养24h，测定振荡前后细菌的菌落数，通过菌落计数方法来定量评价抗菌效果。
振荡法测试抗菌性能的计算：
抑菌率(％)＝(A-B)/A×100％
式(1)中：A为标准空白试样振荡18h后菌落数；B为待测试样振荡18h后菌落数。
实验结果如下表所示：
表1
此检测数据只针对上述检测样品。
由此可见，本发明提供了一种真丝低温环保染色工艺，其充分利用多种手段结合，尤其是生物酶的使用，无化学物质残留，天然环保，无需高温，并且染色后的真丝织物具有良好的K/S指，色牢度以及优良的抗菌性能。
以上所述，仅为本发明较佳的具体实施方式，但本发明的保护范围并不局限于此，任何熟悉本技术领域的技术人员在本发明揭露的技术范围内，根据本发明的技术方案及其发明构思加以等同替换或改变，都应涵盖在本发明的保护范围之内。

Claims (3)

1.一种真丝低温环保染色工艺，其步骤如下：
以下均为质量百分比；
（1）将取真丝织物浸入预处理液中，浴比1：30，保持恒温35℃处理，然后用去离子水清洗干净残留物，40-45℃烘干；
所述预处理液配方为：α-淀粉酶0.02-0.04%，木瓜蛋白酶0.8%，甘氨酸0.3-0.5%，丝素蛋白1%；
（2）将预处理后的真丝织物浸入处理液中，浴比1：25，保持恒温35℃处理，然后用去离子水清洗干净残留物，40-45℃烘干；
所述处理液配方为：柠檬酸，海藻糖水溶液；
（3）酸性大红3R染色：
染色工艺：在50℃入染，10m in后以10℃/min升温速度升温至90℃，保温染色60 min后降温、排液、后处理。
2.权利要求1所述的真丝低温环保染色工艺，其特征在于：
染色处方：
酸性染料 2% （o.w.f）；
硫酸钠 1g /L；
pH 4 .0；
浴 比 100:1。
3.权利要求1-2所述的权利要求1所述的真丝低温环保染色工艺，其特征在于：
所述处理液配方为：柠檬酸1%，海藻糖0.5-0.8%。
CN201610539550.XA 2016-07-06 2016-07-06 一种真丝低温环保染色工艺 Pending CN106120389A (zh)

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Application publication date: 20161116