CN106109326A - A kind of anti-bacteria wet keeping facial film containing plant extract and preparation method thereof - Google Patents
A kind of anti-bacteria wet keeping facial film containing plant extract and preparation method thereof Download PDFInfo
- Publication number
- CN106109326A CN106109326A CN201610613223.4A CN201610613223A CN106109326A CN 106109326 A CN106109326 A CN 106109326A CN 201610613223 A CN201610613223 A CN 201610613223A CN 106109326 A CN106109326 A CN 106109326A
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- Prior art keywords
- extract
- plant extract
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- facial film
- film containing
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- 230000000844 anti-bacterial effect Effects 0.000 title claims abstract description 50
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- A61K8/494—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing heterocyclic compounds with more than one nitrogen as the only hetero atom
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- A61K8/34—Alcohols
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- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
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Abstract
The present invention relates to cosmetic technical field, be specifically related to a kind of anti-bacteria wet keeping facial film containing plant extract and preparation method thereof.By plant extract elite, the facial skin for user is brought deep layer to nourish, is recovered to compact, and heavily shine gloss；Use and there is the most antibacterial, the nanometer silver of bactericidal action, complement each other with each component in formula, make product bacteriostasis antibiosis capability improving, and produce synergism with the anti-inflammation components in plant extract fine Central China in this product, make skin acne or inflammation quickly be repaired.
Description
Technical field
The present invention relates to cosmetic technical field, be specifically related to a kind of anti-bacteria wet keeping facial film containing plant extract and system thereof
Make method.
Background technology
One beautiful and charming face, is most can to leave deep primary impression to people.Being full of water profit texture, jade-like stone profit is bright and clean
Facial skin, then allow beautiful and charming face more seem tender, coquettish.How many people seeking beauty, for the maintenance of facial skin, attitude
It is the most all cautiouslyly and deeply concernedly.
In daily life, unavoidable because operating pressure big, cleaning is not focused on, eating and drinking without temperance system, works and rests irregular etc. all
Reason, and cause facial skin occur tarnish, be dried, acne, the skin problem such as lax, use facial film can improve above-mentioned shape
Condition, it is ensured that facial skin water profit, bright and clean, compact, slow down aging.
Use skin care item can improve above-mentioned skin problem, have the skin care item containing plant extract composition the most on the market, as
Aloe face pack, cucumber face pack etc., by plant extract rich in alkaloid, saponin, flavonoid, the different activities such as organic acid
Composition, nourishes bring good effect for facial acne, the reparation of cicatrix, skin moisture-keeping.
At present the facial film adding plant extract the most on the market is of a great variety, but due in plant extract rich in substantial amounts of
Nourish composition, therefore need to add antibacterial, Fungicidal substance in right amount in facial film, to prevent the bacteria breed in facial film, but these
Composition affects facial skin the most to a certain extent, excessively adds the reparation antibacterial, sterilization component easily affects facial acne, and presses down
Bacterium, sterilization component add less, easily make breed bacteria in facial film, are less useful for the reparation of acne, even because of the impact of antibacterial
And make symptom more serious.
Summary of the invention
It is an object of the invention to provide a kind of anti-bacteria wet keeping facial film containing plant extract, by plant extract elite,
Facial skin for user brings deep layer to nourish, and recovers to compact, and heavily shine gloss；Use and there is receiving of the most antibacterial, bactericidal action
Each component in meter Yin, with formula complements each other, and makes product bacteriostasis antibiosis capability improving, and with plant extract fine Central China in this product
Anti-inflammation components produce synergism, make skin acne or inflammation quickly be repaired.
For achieving the above object, the present invention uses techniques below means to be carried out:
A kind of anti-bacteria wet keeping facial film containing plant extract, it is characterised in that total amount ratio meter by weight percent, comprises following one-tenth
Point:
Allantoin and/or glycyrrhizic acid dipotassium 0.1% ~ 0.35%, plant extract 0.3% ~ 0.8%, vitamin E 0.05% ~ 0.3%, card
Ripple nurse 0.05% ~ 0.25%, glycerol 3% ~ 7%, glycerol polymethacrylates 0.5% ~ 2%, hyaluronate sodium 0.005% ~ 0.055%,
Butanediol 0.8% ~ 3.8%, potassium hydroxide 0.008% ~ 0.1%, nano-silver ionic water 28% ~ 35%, remaining deionized water；
Described nano-silver ionic water be mass percent be 0.0001% ~ 0.001% nano oxidized argentum powder, 0.05% ~ 0.15%
Borosilicate, remainder is the dispersed system of deionized water；
Described plant extract is in fermented soybean extract, Herba Visci extract, Rhizoma Imperatae extract, Aloe extract
One or more in any proportion proportioning form.
Matt, be dried, in acne, the multiple facial skin problem such as lax, acne is that impact is particularly evident, for acne
Recovery for, need to kill skin and show antibacterial, accelerate wound healing, horny layer softening cell, prevent pigementation, Fang Keda
To the effect eliminating acne.
Argent and oxide thereof are a kind of conventional effective antibacterial.Allantoin has promotion cell growth, accelerates wound
The physiological functions such as mouth heals, horny layer softening albumen, are good consolidant and the antiulcer agents of skin trauma.Can be used as alleviate and
Treatment xeroderma, glycyrrhizic acid dipotassium has the effects such as antiinflammatory, antiallergic, moisturizing.This product passes through nano oxidized argentum powder-allantoin
And/or the material such as Flavonoid substances, chlorogenic acid and the plant polyphenol contained in glycyrrhizic acid dipotassium-plant extract, it is the most collaborative,
Play good antibacterial, sterilization, antiinflammatory, be conducive to acne healing and tissue reconstruction, Herba Visci extract and Rhizoma Imperatae extract
Tryrosinase can also be suppressed to generate, slow down or lower melanic formation；For the acne caused because of endocrine disturbance, rich in
The soybean extract of soybean isoflavone can suppress the regeneration of this acne from source.
Further, this contains the anti-bacteria wet keeping facial film of plant extract, total amount ratio meter by weight percent, comprises following one-tenth
Point:
Allantoin 0.08% ~ 0.3%, glycyrrhizic acid dipotassium 0.01% ~ 0.15%, plant extract 0.4% ~ 0.75%, water soluble vitamins
E0.08% ~ 0.25%, carbomer 0.08% ~ 0.2%, glycerol 4.5% ~ 6.5%, glycerol polymethacrylates 0.6% ~ 1.8%, transparent
Matter acid sodium 0.01% ~ 0.045%, butanediol 1.2% ~ 2.7%, potassium hydroxide 0.02% ~ 0.08%, nano-silver ionic water 29.5% ~
32.5%, remaining deionized water；
Described nano-silver ionic water be mass percent be silver oxide, the borosilicate of 0.07% ~ 0.1% of 0.0003% ~ 0.0015%
Acid sodium and/or calcium borosilicate, remainder is the dispersed system of deionized water；
Described plant extract is in terms of mass fraction, and the powdery Aloe of the enrichment 10 ~ 400:1 containing 12% ~ 20% is extracted
Thing, remaining composition is that Semen sojae atricolor is by the one in the extract of lactic acid bacteria fermentation, Herba Visci extract, Rhizoma Imperatae extract or many
Plant proportioning in any proportion to form.
Aloe has the effects such as sun-proof, moisturizing, analgesia, anti-inflammation, pre-anti-acne, healing shallow wound, by adopting
With the powdery Aloe extract of high concentration, further enhance this product bactericidal antiphlogistic, antiallergic, defying age, promotion damaged skin
Effect of healing, while increasing the damaged skin resistance to alien bacteria, can promote again epidermal cell proliferation, contribute to
The skin regeneration of damaged part；Relative to soybean isoflavone glycoside, soybean isoflavones aglycon has higher physiologically active.
In extract by lactic acid bacteria fermentation Semen sojae atricolor, soybean isoflavones aglycon content can be further enhanced, to anti-acne shape
One-tenth ability is higher.
Further, the enrichment of described powdery Aloe extract is 100 ~ 200:1.
Preferred as one, the described Semen sojae atricolor extract by lactic acid bacteria fermentation: Herba Visci extract: Rhizoma Imperatae extracts
Thing is mixed in the ratio of 1 ~ 5:4 ~ 6:3 ~ 7.
When described hyaluronate sodium can be selected for the hyaluronate sodium wetting agent as this product of two kinds of different molecular weights.
The hyaluronic acid sodium molecule of high molecular can form ventilative hydration shell at skin surface, makes horny layer hydration soft
Change, increase skin and plant extract active substances is absorbed, be suitable for the use of dry skin；Oligomerization hyaluronate sodium
Can directly penetrate into skin corium, expansion blood capillary, increase blood microcirculation, the supply of reinforced nutrition matter, beneficially acne
The reparation at position.Adding and control both ratios in right amount, cooperation can reach more fully jointly, three-dimensional moisturizing is imitated for both
Really, when the ratio of the hyaluronate sodium and oligomerization hyaluronate sodium that control high molecular is 1 ~ 3:1 ~ 2, equal for multiple skin quality
There is good using effect.
Further, this product also can add the essence of total amount percentage ratio 0.005% ~ 0.03%.
Another object of the present invention is to the manufacture method of the anti-bacteria wet keeping facial film providing this to contain plant extract, its feature
It is following steps:
Step (1): silver oxide, borosilicate are proportionally added into deionized water, be kept stirring for shear rate be 10000 ~
Under the rotating speed of 15000r/min, preparation forms the nano-silver ionic water with dispersed system；
Step (2): after the deionized water in agitator tank is heated to 80 ~ 85 DEG C, keeps 10 ~ 20min, stirring with 10 ~ 20r/min
Mix speed, be proportionally added into allantoin, glycyrrhizic acid dipotassium, glycerol polymethacrylates, Aloe extract, hyaluronate sodium,
Carbomer, after stirring is dissolved completely in water to material, keeps the mixing speed of 10 ~ 20r/min and lowers the temperature, being cooled to 38 ~ 45
℃；
Step (3): add potassium hydroxide, fermented soybean extract, Herba Visci extract, Rhizoma Imperatae extraction to agitator tank in proportion
Thing, glycerol, butanediol, vitamin E, after the mixing speed of holding 10 ~ 20r/min to mix homogeneously, be cooled to 28 ~ 37 DEG C；
Step (4): be quickly adding in agitator tank by the nano-silver ionic water maintaining dispersed system, keeps 10 ~ 20r/
The mixing speed stirring 15 ~ 30min of min, prepares finished product.
Nano level argent and oxide thereof are respectively provided with good antibacterial, bactericidal action, but for but certain to having
Viscosity, when the facial film of amorphous state adds nano level argent and oxide thereof, the easily nothing because viscosity is too high
Method mixes, and causes uneven nano level argent and oxide thereof to produce coagulation phenomenon, causes granule to become big, causes sterilization
Effect reduces, and even loses efficacy, so nano level argent and oxide thereof disperse the making of suspension require the highest；Mesh
This type of certain viscosity front, the facial film of amorphous state often adds Methylisothiazolinone, iodo propinyl ammonia butyl formate
Etc. artificial synthetic preservative, it is ensured that sterilization and anticorrosion effect；Or the facial film that part is containing nanometer silver, as CN201310631449.3 is public
" a kind of face mask substrate material non-weaving cloth and preparation method thereof " opened, by by nano level nano level metal silver and oxide thereof
Adding in the spinning solution of base material, nano level metal silver and oxide thereof are fixed in co-blended spinning, it is to avoid nano level
Argent and oxide generation coagulation phenomenon thereof are so that it is guaranteed that sterilization and anticorrosion effect.
In the manufacture method of the anti-bacteria wet keeping facial film containing plant extract that the present invention provides, by first by nano phase ag_2 o
Powder is configured to nano-silver ionic water, by adding borosilicate and nano oxidized argentum powder in the water less to anti-shearing force, and adopts
By the method for 10000 ~ 15000r/min ultrahigh speed stirring, make borosilicate separate nano oxidized argentum powder, and formed dispersed
System, effectively prevent nanometer silver powder generation coagulation phenomenon；By preparation nano-silver ionic water and glycerol polymethacrylates,
After the emulsifyings such as carbomer, glycerol, butanediol, thickening, moisturizing ingredient mixing, it can be ensured that nano oxidized argentum powder is evenly distributed to this product
In the middle of, and due to the emulsifyings such as glycerol polymethacrylates, carbomer, glycerol, butanediol, thickening composition effect under, make to receive
Rice oxidation argentum powder keeps uniform dispersity, coagulation coacervation does not occur, it is ensured that the nano phase ag_2 o composition of this product
Bactericidal effect.Nano oxidized argentum powder-allantoin and/or glycyrrhizic acid dipotassium-plant extract produce mutual synergism, can make to kill
Bacterium effect is greatly promoted.
As the improvement of said method, below the manufacture method of this anti-bacteria wet keeping facial film containing plant extract also can use
Step is carried out:
Step (1): silver oxide, borsal and/or calcium borosilicate are proportionally added into deionized water, is kept stirring for shearing
Speed is under the rotating speed of 10000 ~ 12000r/min, and preparation forms the nano-silver ionic water with dispersed system；
Step (2): after the deionized water in agitator tank is heated to 75 ~ 83 DEG C, with the mixing speed of 13 ~ 18r/min, presses successively
Ratio adds allantoin, glycyrrhizic acid dipotassium, glycerol polymethacrylates, powdery Aloe extract, hyaluronate sodium, card ripple
Nurse, after stirring is dissolved completely in water to material, keeps the mixing speed of 13 ~ 18r/min and lowers the temperature, being cooled to 38 ~ 45 DEG C；
Step (3): in proportion potassium hydroxide is configured to the potassium hydroxide solution that concentration is 85% ~ 95%, the most first to
After agitator tank adds potassium hydroxide solution and mixes, continue to add Semen sojae atricolor and extracted by the extract of lactic acid bacteria fermentation, Herba Visci
Thing, Rhizoma Imperatae extract, glycerol, butanediol, watermiscible vitamin E, holding 13 ~ 18r/min mixing speed to mix homogeneously
After, it is cooled to 28 ~ 37 DEG C；
Step (4): be quickly adding in agitator tank by the nano-silver ionic water maintaining dispersed system, keeps 13 ~ 18r/
The mixing speed stirring 15 ~ 30min of min, prepares finished product.
As improvement, in described step (3), after adding unclassified stores, percentage ratio 0.005% ~ 0.03% in an amount
Ratio add after essence mix homogeneously and complete step (3), add essence and can promote user olfactory sensation in use
Experience, promote the captivation of this product.
Detailed description of the invention
In order to make the purpose of the present invention, technical scheme and advantage be more easily understood, below in conjunction with embodiment, to the present invention
It is further elaborated.Should be appreciated that specific embodiment described herein, only in order to explain the present invention, is not used to
Limit the present invention.
This contains the anti-bacteria wet keeping facial film of plant extract, and total amount can be by weight percent than meter:
Allantoin and/or glycyrrhizic acid dipotassium 0.1% ~ 0.35%, plant extract 0.3% ~ 0.8%, vitamin E 0.05% ~ 0.3%, card
Ripple nurse 0.05% ~ 0.25%, glycerol 3% ~ 7%, glycerol polymethacrylates 0.5% ~ 2%, hyaluronate sodium 0.005% ~ 0.055%,
Butanediol 0.8% ~ 3.8%, potassium hydroxide 0.008% ~ 0.1%, nano-silver ionic water 28% ~ 35%, remaining deionized water；Wherein, institute
The nano-silver ionic water stated be containing the nano oxidized argentum powder that mass percent is 0.0001% ~ 0.001%, 0.05% ~ 0.15%
Borosilicate, remainder is the dispersed system of deionized water；Plant extract is fermented soybean extract, Herba Visci extraction
One or more in thing, Rhizoma Imperatae extract, Aloe extract proportioning in any proportion forms.
On this basis, this product also can be selected for the hyaluronate sodium polymer hyaluronic acid sodium of two kinds of different molecular weights
And oligomerization hyaluronate sodium can form ventilative aquation at skin surface as wetting agent, the hyaluronic acid sodium molecule of high molecular
Film, makes horny layer hydration soften, increases skin and absorb plant extract active substances；And oligomerization hyaluronate sodium energy
Directly penetrate into skin corium, expansion blood capillary, increase blood microcirculation, the supply of reinforced nutrition matter, being total to by both
With cooperation, reach more fully, three-dimensional moistening effect；
For strengthening the fragrance of this product, can add essence in this product formula in right amount, the corresponding content reducing deionized water, for disappearing
For the person of expense, olfactory sensation has better sensory experience.
By above-mentioned composition proportion, and use following method to prepare this product, all can reach good using effect:
Step (1): silver oxide, borosilicate are proportionally added into deionized water, be kept stirring for shear rate be 10000 ~
Under the rotating speed of 15000r/min, preparation forms the nano-silver ionic water with dispersed system；
Step (2): after the deionized water in agitator tank is heated to 80 ~ 85 DEG C, keeps 10 ~ 20min, stirring with 10 ~ 20r/min
Mix speed, be proportionally added into allantoin, glycyrrhizic acid dipotassium, glycerol polymethacrylates, Aloe extract, hyaluronate sodium,
Carbomer, after stirring is dissolved completely in water to material, keeps the mixing speed of 10 ~ 20r/min and lowers the temperature, it is cooled to 38 ~
Step (3) is carried out, to avoid affecting the performance of follow-up interpolation plant extract active component because temperature is too high when 45 DEG C；
Step (3): add potassium hydroxide, fermented soybean extract, Herba Visci to agitator tank in proportion when being cooled to 38 ~ 45 DEG C
Extract, Rhizoma Imperatae extract, glycerol, butanediol, vitamin E, after the mixing speed of holding 10 ~ 20r/min to mix homogeneously,
It is cooled to 28 ~ 37 DEG C；Potassium hydroxide in proportion is made into the hydrogen-oxygen acid potassium solution of concentration 85% ~ 95%, and first adds in agitator tank
During hydro-oxidation potassium solution and after dispersion, then add remaining material, can further improve the easily disperse of potassium hydroxide, it is to avoid
Because of potassium hydroxide and carbomer exothermic heat of reaction, and affect the performance of the active component of this product plant extract.
Step (4): the nano-silver ionic water maintaining dispersed system is quickly adding in agitator tank, keep 10 ~
The mixing speed stirring 15 ~ 30min of 20r/min, prepares finished product.
Below by specific embodiment, the present invention is further described:
Embodiment 1
Calculate by weight, be equipped with allantoin 100g, glycyrrhizic acid dipotassium 50g, glycerol polymethacrylates 800g, hyaluronate sodium
30g, carbomer 150g, watermiscible vitamin E 100g, glycerol 5kg, butanediol 2kg, hydrogen-oxygen acid potassium 50g, enrichment 200:1
Powdery Aloe extract 100g, Herba Visci extract 100g, Rhizoma Imperatae extract 100g, the Semen sojae atricolor extraction by lactic acid bacteria fermentation
Thing 300g, nano-silver ionic water 30kg, natural essence 10g, remaining deionized water 61.1kg；
Step (1): wherein nano-silver ionic water is with the nano oxidized argentum powder of 0.15g, 29.85g borsal, joins 29.97g and goes
In ionized water and under the rotating speed of 10000 ~ 12000r/min, preparation forms the nano-silver ionic water with dispersed system；
Step (2): after the 61.1kg deionized water in agitator tank is heated to 80 DEG C, keeps 15min, with the stirring of 15r/min
Speed, is proportionally added into allantoin 100g, glycyrrhizic acid dipotassium 50g, glycerol polymethacrylates 800g, enrichment 200:1
Powdery Aloe extract 100g, hyaluronate sodium 30g, carbomer 150g, after stirring is dissolved completely in water to material, keep
The mixing speed of 15r/min is also cooled to 40 DEG C；
Step (3): in proportion 50g potassium hydroxide is configured to the potassium hydroxide solution that concentration is 95%, the most successively to
Agitator tank adds the hydrogen-oxygen acid potassium solution of prepare 95%, Semen sojae atricolor passes through the extract 300g of lactic acid bacteria fermentation, Herba Visci extracts
Thing 100g, Rhizoma Imperatae extract 100g, glycerol 5kg, butanediol 2kg, watermiscible vitamin E 100g, natural essence 10g, keep
The mixing speed of 15r/min, to after mix homogeneously, is cooled to 35 DEG C；
Step (4): be quickly adding in agitator tank by the nano-silver ionic water maintaining dispersed system in step (1), protects
Hold the mixing speed stirring 20min of 15r/min, prepare finished product.
Embodiment 2
Calculating by weight, outfit allantoin 120g, glycyrrhizic acid dipotassium 70g, glycerol polymethacrylates 850g, macromolecule are transparent
Matter acid sodium 35g, carbomer 150g, watermiscible vitamin E 120g, glycerol 5kg, butanediol 2kg, hydrogen-oxygen acid potassium 50g, enrichment
The powdery Aloe extract 100g of 50:1, Herba Visci extract 100g, Rhizoma Imperatae extract 150g, Semen sojae atricolor pass through lactic acid bacteria fermentation
Extract 250g, nano-silver ionic water 30kg, remaining deionized water 60.996kg；
Step (1): wherein nano-silver ionic water is with the nano oxidized argentum powder of 0.2g, 29.8g calcium borosilicate, join 29.97g go from
In sub-water and under the rotating speed of 12000 ~ 14000r/min, preparation forms the nano-silver ionic water with dispersed system；
Step (2): after the 60.996kg deionized water in agitator tank is heated to 80 DEG C, keeps 15min, stirring with 15r/min
Mix speed, be proportionally added into allantoin 120g, glycyrrhizic acid dipotassium 70g, glycerol polymethacrylates 850g, enrichment 100:1
Powdery Aloe extract 100g, polymer hyaluronic acid sodium 35g, carbomer 150g, stir to material and be dissolved completely in water
After, keep the mixing speed of 15r/min and be cooled to 42 DEG C；
Step (3): add hydrogen-oxygen acid potassium 50g to agitator tank in proportion, Semen sojae atricolor is posted by the extract 250g of lactic acid bacteria fermentation, Mongolian oak
Raw extract 100g, Rhizoma Imperatae extract 150g, glycerol 5kg, butanediol 2kg, watermiscible vitamin E 120g, keep 15r/min
Mixing speed to after mix homogeneously, be cooled to 30 DEG C；
Step (4): be quickly adding in agitator tank by the nano-silver ionic water maintaining dispersed system in step (1), protects
Hold the mixing speed stirring 20min of 15r/min, prepare finished product.
Embodiment 3
Calculating by weight, outfit allantoin 110g, glycyrrhizic acid dipotassium 75g, glycerol polymethacrylates 1000g, macromolecule are saturating
Bright matter acid sodium 15g, oligomerization hyaluronate sodium 15g, carbomer 200g, vitamin E2 00g, glycerol 5.5kg, butanediol 2.5kg, hydrogen
Oxygen acid potassium 50g, the powdery Aloe extract 100g of enrichment 100:1, Herba Visci extract 250g, Rhizoma Imperatae extract 150g,
Semen sojae atricolor passes through the extract 100g of lactic acid bacteria fermentation, nano-silver ionic water 30kg, natural essence 10g, remaining deionized water
59.725kg；
Step (1): wherein nano-silver ionic water is with the nano oxidized argentum powder of 0.2g, 29.8g borsal, join 29.97g go from
In sub-water and under the rotating speed of 12000 ~ 14000r/min, preparation forms the nano-silver ionic water with dispersed system；
Step (2): after the 60.995kg deionized water in agitator tank is heated to 80 DEG C, keeps 15min, stirring with 15r/min
Mix speed, be proportionally added into allantoin 110g, glycyrrhizic acid dipotassium 75g, glycerol polymethacrylates 1000g, enrichment 100:1
Powdery Aloe extract 100g, polymer hyaluronic acid sodium 15g, oligomerization hyaluronate sodium 15g, carbomer 200g, stirring extremely
After material is dissolved completely in water, keeps the mixing speed of 15r/min and be cooled to 40 DEG C；
Step (3): in proportion 50g potassium hydroxide is configured to the potassium hydroxide solution that concentration is 95%, the most in proportion to stirring
Tank adds the hydrogen-oxygen acid potassium solution of prepare 95% and after stirring, and continuously adds the Semen sojae atricolor extraction by lactic acid bacteria fermentation
Thing 100g, Herba Visci extract 250g, Rhizoma Imperatae extract 150g, glycerol 5.5kg, butanediol 2.5kg, vitamin E2 00g, sky
So essence 10g, after the mixing speed of holding 15r/min to mix homogeneously, is cooled to 30 DEG C；
Step (4): be quickly adding in agitator tank by the nano-silver ionic water maintaining dispersed system in step (1), protects
Hold the mixing speed stirring 20min of 15r/min, prepare finished product.
Test case
Using embodiment 1 as the present invention in-vitro simulated bactericidal assay method, the test example of skin anti-acne method of testing and following
Method is prepared:
Test example 1
Choose in embodiment 1 facial mask liquid as experimental raw；
Test example 2
By production method in embodiment 1, in step (4), directly add and embodiment 1 moderate nano-silver ionic powder, borosilicate
Acid sodium, the mode of deionized water carry out facial film production；
Test example 3
By production method in embodiment 1, omit step (4), in the way of without nano-silver ionic water, use instead equivalent go from
Sub-water carries out facial film production.
Test example 4
By the production method in embodiment 1, and extract without allantoin, Radix Glycyrrhizae oxalic acid dipotassium, Aloe extract, Herba Visci
Thing, Rhizoma Imperatae extract, replace above-mentioned substance to carry out facial film production with aliquots of deionized water.
Test example 5
According to the production method of embodiment 1 nano-silver ionic water, prepared nano-silver ionic water is joined in deionized water also
It is formulated into 100kg.
In-vitro simulated bactericidal assay method:
By normal bacterial (Pseudomonas aeruginosa, staphylococcus aureus, escherichia coli, propionibacterium acnes), standard mycete (in vain
Color candidiasis, aspergillus niger, Aspergillus citrimum) inoculate cultured solution of broth respectively, at 37 DEG C, cultivate 24h, be configured to certain mass concentration
Bacteria suspension.
Test method 1:
Culture bottle is divided into five groups, in culture bottle, adds the trial target of test example 1 ~ 5 equivalent respectively；And in five groups of culture bottles
Inoculation 1.0 × 106The normal bacterial of cfu/g, each group culture bottle antibacterial situation of change in observing 28 days.
Test method 2:
Culture bottle is divided into five groups, in culture bottle, adds the trial target of test example 1 ~ 5 equivalent respectively；And in five groups of culture bottles
Inoculation 1.0 × 106The standard mycete of cfu/g, each group culture bottle antibacterial situation of change in observing 28 days.
Result of the test: be shown in Table 1, table 2.
Table 1 normal bacterial experimental group
Table 2 standard mycete experimental group
Conclusion (of pressure testing):
The product obtained in test example 1, at nano oxidized argentum powder-allantoin and/or glycyrrhizic acid dipotassium-plant extract objects system
Under effect, bactericidal property is efficient and bactericidal effect is obvious；Within in test example 2 the 7th day, there is increasing antibacterial phenomenon, but follow-up natural law is sent out
Existing total number of bacterial colonies declines, and result is combined knowable to judgement in test example 5, is likely to be due to nano oxidized argentum powder generation coagulation existing
As, cause sterilizing ability to decline；In test example 3, total plate count downward trend is more mild, and in test example 4, bacterium in early days
The sum downward trend that falls is fast, but later stage total plate count has risen, and fungicidal effectiveness is for test example 1, and test example 4 is relative
More weak, result is combined and makes supposition in test example 2, test example 5, uses merely the bactericidal action of allantoin-plant extract
Relatively slow, use merely nano-silver ionic water then bactericidal effect more weak, both combine formation composite antibacterial system and then can
Make antibacterial, bactericidal effect have to be obviously improved.In test method 2, same acquisition is similar to conclusion.
After testing, this product has the characteristic of broad-spectrum antiseptic, is respectively provided with good antibacterial effect for multiple mushroom, employing
Antibacterial, mycete, as the brief introduction of two kinds of simulation bactericidal assay method test cases, are only used as verifying that the example of this product effect is made,
Not the range of application of the present invention is limited.
Skin anti-acne is tested
Method of testing:
Choosing the age at 18 years old to 25 years old, face has the volunteer of moderate acne acne, each 60 of men and women volunteer, with
Machine is divided into four groups, often group each 15 people of men and women, and the facial film being respectively adopted in test example 1-4 preparation is tested.
Volunteer does not allows to use other cosmetics during testing, simultaneously must not Exposure to Sunlight for a long time, reduce edible easy on
Fire food, holding are normally worked and rested, are not scratched and grab acne spots.
Use the mode of volunteer's self evaluation facial acne situation, allow volunteer feel after each group of facial film of use
The improvement situation of portion's acne.Evaluation result is divided into no effect, effective fine with effect.
Test result:
Using facial film after one month, test group 1-4 volunteer's evaluation effect is as follows:
Test group 1 volunteer's evaluation effect is 2 people very well, and having certain effect is 10 people, do not have effect or inconspicuous be 18 people, examination
Testing group effective percentage is 40%；
Test group 2 volunteer's evaluation effect is 2 people very well, and having certain effect is 8 people, do not have effect or inconspicuous be 20 people, examination
Testing group 2 effective percentage is 33.3%；
Test group 3 volunteer's evaluation effect is 0 people very well, and having certain effect is 5 people, do not have effect or inconspicuous be 25 people, examination
Testing group 2 effective percentage is 16.7%；
Test group 4 volunteer's evaluation effect is 1 people very well, and having certain effect is 5 people, do not have effect or inconspicuous be 24 people, examination
Testing group effective percentage is 20%.
Using facial film after two months, test group 1-4 volunteer's evaluation effect is as follows:
Test group 1 volunteer's evaluation effect is 4 people very well, and having certain effect is 17 people, do not have effect or inconspicuous be 9 people, examination
Testing group effective percentage is 70%；
Test group 2 volunteer's evaluation effect is 2 people very well, and having certain effect is 12 people, do not have effect or inconspicuous be 16 people, examination
Testing group 2 effective percentage is 46.7%；
Test group 3 volunteer's evaluation effect is 1 people very well, and having certain effect is 9 people, do not have effect or inconspicuous be 20 people, examination
Testing group 2 effective percentage is 33.3%；
Test group 4 volunteer's evaluation effect is 0 people very well, and having certain effect is 7 people, do not have effect or inconspicuous be 23 people, examination
Testing group effective percentage is 23.3%.
From skin anti-acne test result it can be seen that the most persistently use test example 1-4, skin acne situation all by
Step is improved；
The product effect of test group 1 is relative to other three groups, and effect obtains the satisfaction of volunteer and has higher rating；The product of test example 2
Using, effect in early days is similar to test group 1, but is persistently using after two months, and the product effect of test group 1 is relative to test
Organize 2 effects to become apparent from；And test group 1 and test group 3 contrast, effect then becomes apparent from.Visible test example 1 has and uniformly divides
The nano-silver ionic water of prose style free from parallelism system, functional for product, and the lasting effectiveness of function have good lifting effect；
Test group 3 finds with test group 4 contrast, and test group 3 uses on effective percentage relatively low relative to test group 4 at first month,
For the most nano oxidized argentum powder of short time sterilizing ability, plant extract sterilizing ability is more weak, but persistently makes
With after two months, effect relative test group 3 becomes apparent from, because of antiinflammatory, effect of promotion cytothesis of plant extract composition,
Acne is made gradually to be repaired.
The above, the only present invention preferably detailed description of the invention, but protection scope of the present invention is not limited thereto,
Any those familiar with the art in the technical scope that the invention discloses, the change that can readily occur in or replacement,
All should contain within protection scope of the present invention.Therefore, protection scope of the present invention should be with scope of the claims
It is as the criterion.
Claims (10)
1. the anti-bacteria wet keeping facial film containing plant extract, it is characterised in that total amount ratio meter by weight percent, comprises following
Composition:
Allantoin and/or glycyrrhizic acid dipotassium 0.1% ~ 0.35%, plant extract 0.3% ~ 0.8%, vitamin E 0.05% ~ 0.3%, card
Ripple nurse 0.05% ~ 0.25%, glycerol 3% ~ 7%, glycerol polymethacrylates 0.5% ~ 2%, hyaluronate sodium 0.005% ~ 0.055%,
Butanediol 0.8% ~ 3.8%, potassium hydroxide 0.008% ~ 0.1%, nano-silver ionic water 28% ~ 35%, remaining deionized water；
Described nano-silver ionic water be containing the nano oxidized argentum powder that mass percent is 0.0001% ~ 0.001%, 0.05% ~
The borosilicate of 0.15%, remainder is the dispersed system of deionized water；
Described plant extract is in fermented soybean extract, Herba Visci extract, Rhizoma Imperatae extract, Aloe extract
One or more in any proportion proportioning form.
A kind of anti-bacteria wet keeping facial film containing plant extract, it is characterised in that total amount presses quality
Percent, than meter, comprises following component:
Allantoin 0.08% ~ 0.3%, glycyrrhizic acid dipotassium 0.01% ~ 0.15%, plant extract 0.4% ~ 0.75%, water soluble vitamins
E0.08% ~ 0.25%, carbomer 0.08% ~ 0.2%, glycerol 4.5% ~ 6.5%, glycerol polymethacrylates 0.6% ~ 1.8%, transparent
Matter acid sodium 0.01% ~ 0.045%, butanediol 1.2% ~ 2.7%, potassium hydroxide 0.02% ~ 0.08%, nano-silver ionic water 29.5% ~
32.5%, remaining deionized water；
Described nano-silver ionic water be mass percent be 0.0003% ~ 0.0015% nanometer level silver oxide, 0.07% ~ 0.1%
Borsal and/or calcium borosilicate, remainder is the dispersed system of deionized water；
Described plant extract is in terms of mass fraction, and the powdery Aloe of the enrichment 10 ~ 400:1 containing 12% ~ 20% is extracted
Thing, remaining composition is that Semen sojae atricolor is by the one in the extract of lactic acid bacteria fermentation, Herba Visci extract, Rhizoma Imperatae extract or many
Plant proportioning in any proportion to form.
A kind of anti-bacteria wet keeping facial film containing plant extract, it is characterised in that described powdery
The enrichment of Aloe extract is 100 ~ 200:1.
A kind of anti-bacteria wet keeping facial film containing plant extract, it is characterised in that described Semen sojae atricolor
By the extract of lactic acid bacteria fermentation: Herba Visci extract: Rhizoma Imperatae extract is mixed in the ratio of 1 ~ 5:4 ~ 6:3 ~ 7.
5. a kind of anti-bacteria wet keeping facial film containing plant extract as described in claim 1 ~ 4 any one, it is characterised in that
Described hyaluronate sodium is polymer hyaluronic acid sodium and/or oligomerization hyaluronate sodium.
A kind of anti-bacteria wet keeping facial film containing plant extract, it is characterised in that hyaluronate sodium
It is 1 ~ 3:1 ~ 2 with the ratio of oligomerization hyaluronate sodium.
7. a kind of anti-bacteria wet keeping facial film containing plant extract as described in claim 1 ~ 4 any one, it is characterised in that
Also comprise the essence of total amount percentage ratio 0.005% ~ 0.03%.
8. the manufacture method of the anti-bacteria wet keeping facial film containing plant extract as claimed in claim 1, it is characterised in that walk below
Rapid:
Step (1): silver oxide, borosilicate are proportionally added into deionized water, be kept stirring for shear rate be 10000 ~
Under the rotating speed of 15000r/min, preparation forms the nano-silver ionic water with dispersed system；
Step (2): after the deionized water in agitator tank is heated to 80 ~ 85 DEG C, keeps 10 ~ 20min, stirring with 10 ~ 20r/min
Mix speed, be proportionally added into allantoin, glycyrrhizic acid dipotassium, glycerol polymethacrylates, Aloe extract, hyaluronate sodium,
Carbomer, after stirring is dissolved completely in water to material, keeps the mixing speed of 10 ~ 20r/min and lowers the temperature, being cooled to 38 ~ 45
℃；
Step (3): add potassium hydroxide, fermented soybean extract, Herba Visci extract, Rhizoma Imperatae extraction to agitator tank in proportion
Thing, glycerol, butanediol, vitamin E, after the mixing speed of holding 10 ~ 20r/min to mix homogeneously, be cooled to 28 ~ 37 DEG C；
Step (4): be quickly adding in agitator tank by the nano-silver ionic water maintaining dispersed system, keeps 10 ~ 20r/
The mixing speed stirring 15 ~ 30min of min, prepares finished product.
9. the manufacture method of the anti-bacteria wet keeping facial film containing plant extract as described in claim 2 ~ 7 any one, it is special
Levy and be following steps:
Step (1): silver oxide, borsal and/or calcium borosilicate are proportionally added into deionized water, is kept stirring for shearing
Speed is under the rotating speed of 10000 ~ 12000r/min, and preparation forms the nano-silver ionic water with dispersed system；
Step (2): after the deionized water in agitator tank is heated to 75 ~ 83 DEG C, with the mixing speed of 13 ~ 18r/min, presses successively
Ratio adds allantoin, glycyrrhizic acid dipotassium, glycerol polymethacrylates, powdery Aloe extract, hyaluronate sodium, card ripple
Nurse, after stirring is dissolved completely in water to material, keeps the mixing speed of 13 ~ 18r/min and lowers the temperature, being cooled to 38 ~ 45 DEG C
Time；
Step (3): in proportion potassium hydroxide is configured to the potassium hydroxide solution that concentration is 85% ~ 95%, the most first to
After agitator tank adds potassium hydroxide solution and mixes, continue to add Semen sojae atricolor and extracted by the extract of lactic acid bacteria fermentation, Herba Visci
Thing, Rhizoma Imperatae extract, glycerol, butanediol, watermiscible vitamin E, holding 13 ~ 18r/min mixing speed to mix homogeneously
After, it is cooled to 28 ~ 37 DEG C；
Step (4): be quickly adding in agitator tank by the nano-silver ionic water maintaining dispersed system, keeps 13 ~ 18r/
The mixing speed stirring 15 ~ 30min of min, prepares finished product.
10. contain the manufacture method of the anti-bacteria wet keeping facial film of plant extract as claimed in claim 8 or 9, it is characterised in that: institute
In the step (3) stated, after adding unclassified stores, after the ratio of percentage ratio 0.005% ~ 0.03% adds essence in an amount, mixing is all
Even and complete step (3).
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| CN107412053A (en) * | 2017-07-25 | 2017-12-01 | 苏州凌科特新材料有限公司 | A kind of acne scars repair surface film dressing and preparation method thereof |
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Denomination of invention: Antibacterial and moisturizing facial mask containing plant extracts and its preparation method Effective date of registration: 20231009 Granted publication date: 20190212 Pledgee: Shantou Chaonan sub branch of industrial and Commercial Bank of China Ltd. Pledgor: GUANGDONG YALGET FINE CHEMICAL Co.,Ltd. Registration number: Y2023980060314 |