CN106106525A - A kind of compositions preventing and treating citrus red mite and preparation method thereof - Google Patents
A kind of compositions preventing and treating citrus red mite and preparation method thereof Download PDFInfo
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- CN106106525A CN106106525A CN201610465453.0A CN201610465453A CN106106525A CN 106106525 A CN106106525 A CN 106106525A CN 201610465453 A CN201610465453 A CN 201610465453A CN 106106525 A CN106106525 A CN 106106525A
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- parts
- acrylonitrile
- sodium hypophosphite
- synergist
- zen
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- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N43/00—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds
- A01N43/90—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having two or more relevant hetero rings, condensed among themselves or with a common carbocyclic ring system
-
- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N37/00—Biocides, pest repellants or attractants, or plant growth regulators containing organic compounds containing a carbon atom having three bonds to hetero atoms with at the most two bonds to halogen, e.g. carboxylic acids
- A01N37/34—Nitriles
-
- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N43/00—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds
- A01N43/34—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having rings with one nitrogen atom as the only ring hetero atom
- A01N43/40—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having rings with one nitrogen atom as the only ring hetero atom six-membered rings
-
- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N59/00—Biocides, pest repellants or attractants, or plant growth regulators containing elements or inorganic compounds
- A01N59/26—Phosphorus; Compounds thereof
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- Life Sciences & Earth Sciences (AREA)
- Agronomy & Crop Science (AREA)
- Pest Control & Pesticides (AREA)
- Plant Pathology (AREA)
- Health & Medical Sciences (AREA)
- Engineering & Computer Science (AREA)
- Dentistry (AREA)
- General Health & Medical Sciences (AREA)
- Wood Science & Technology (AREA)
- Zoology (AREA)
- Environmental Sciences (AREA)
- Chemical & Material Sciences (AREA)
- Inorganic Chemistry (AREA)
- Agricultural Chemicals And Associated Chemicals (AREA)
Abstract
The invention discloses a kind of compositions preventing and treating citrus red mite and preparation method thereof, including the raw material of following weight portion: ZEN 90160,15~25 parts;Cimifugin, 10~20 parts;Ethanol, 120~140 parts;Water, 440~480 parts;Synergist acrylonitrile and sodium hypophosphite totally 7~9 parts, the weight ratio of acrylonitrile and sodium hypophosphite is 6~8:1.The compositions that the present invention provides can prevent and treat citrus red mite, the pesticide of preventing and treating citrus red mite can be developed into, prevention effect is relevant with the weight ratio of synergist acrylonitrile and sodium hypophosphite in raw material, and when the weight ratio of acrylonitrile and sodium hypophosphite is 6~8:1, prevention effect is best.
Description
Technical field
The invention belongs to pesticide field, be specifically related to a kind of compositions preventing and treating citrus red mite and preparation method thereof.
Background technology
ZEN 90160 is systemic fungicide, controlling object wide spectrum, and the foliage disease such as leaf being mainly used in preventing and treating wheat and barley is withered
Disease, leaf rust, glume blight, brown spot, powdery mildew etc., compared with other methoxy acrylic bactericides, ZEN 90160 pair
Wheat leaf blessing disease, net blotch and moire disease have higher therapeutic effect.
Have not yet to see ZEN 90160 and work in coordination with the report preventing and treating citrus red mite with cimifugin.
Summary of the invention
It is an object of the invention to provide a kind of preventing and treating citrus red mite containing ZEN 90160 and cimifugin compositions and
Its application in pesticide.
The above-mentioned purpose of the present invention is achieved by techniques below scheme:
A kind of compositions preventing and treating citrus red mite, including the raw material of following weight portion: ZEN 90160,15~25 parts;Rise
Fiber crops element, 10~20 parts;Ethanol, 120~140 parts;Water, 440~480 parts;Synergist acrylonitrile and sodium hypophosphite totally 7~9 parts, third
The weight ratio of alkene nitrile and sodium hypophosphite is 6~8:1.
Further, the compositions of described preventing and treating citrus red mite includes the raw material of following weight portion: ZEN 90160,20
Part;Cimifugin, 15 parts;Ethanol, 130 parts;Water, 460 parts;Synergist acrylonitrile and sodium hypophosphite totally 8 parts, acrylonitrile and hypophosphorous acid
The weight ratio of sodium is 7:1.
Further, the compositions of described preventing and treating citrus red mite includes the raw material of following weight portion: ZEN 90160,15
Part;Cimifugin, 10 parts;Ethanol, 120 parts;Water, 440 parts;Synergist acrylonitrile and sodium hypophosphite totally 7 parts, acrylonitrile and hypophosphorous acid
The weight ratio of sodium is 6:1.
Further, the compositions of described preventing and treating citrus red mite includes the raw material of following weight portion: ZEN 90160,25
Part;Cimifugin, 20 parts;Ethanol, 140 parts;Water, 480 parts;Synergist acrylonitrile and sodium hypophosphite totally 9 parts, acrylonitrile and hypophosphorous acid
The weight ratio of sodium is 8:1.
The preparation method of above-mentioned composition, comprises the steps:
Step S1, by ZEN 90160, cimifugin and synergist acrylonitrile ethanol and water dissolution;
Step S2, by sodium hypophosphite water dissolution;
Step S3, slowly adds the solution of step S1 in the solution of step S2, and interpolation limit, limit is stirred, and to obtain final product.
Advantages of the present invention:
The compositions that the present invention provides can prevent and treat citrus red mite, can develop into the pesticide of preventing and treating citrus red mite.
Detailed description of the invention
Further illustrate the essentiality content of the present invention below in conjunction with embodiment, but do not limit the present invention with this and protect model
Enclose.Although the present invention being explained in detail with reference to preferred embodiment, it will be understood by those within the art that, can be right
Technical scheme is modified or equivalent, without deviating from the spirit and scope of technical solution of the present invention.
Embodiment 1: the preparation of the compositions of preventing and treating citrus red mite
Parts by weight of raw materials compares:
ZEN 90160,20 parts;Cimifugin, 15 parts;Ethanol, 130 parts;Water, 460 parts;Synergist acrylonitrile and sodium hypophosphite
Totally 8 parts, the weight ratio of acrylonitrile and sodium hypophosphite is 7:1.
Preparation method:
Step S1, by ZEN 90160, cimifugin and synergist acrylonitrile ethanol and water dissolution;
Step S2, by sodium hypophosphite water dissolution;
Step S3, slowly adds the solution of step S1 in the solution of step S2, and interpolation limit, limit is stirred, and to obtain final product.
Embodiment 2: the preparation of the compositions of preventing and treating citrus red mite
Parts by weight of raw materials compares:
ZEN 90160,15 parts;Cimifugin, 10 parts;Ethanol, 120 parts;Water, 440 parts;Synergist acrylonitrile and sodium hypophosphite
Totally 7 parts, the weight ratio of acrylonitrile and sodium hypophosphite is 6:1.
Preparation method:
Step S1, by ZEN 90160, cimifugin and synergist acrylonitrile ethanol and water dissolution;
Step S2, by sodium hypophosphite water dissolution;
Step S3, slowly adds the solution of step S1 in the solution of step S2, and interpolation limit, limit is stirred, and to obtain final product.
Embodiment 3: the preparation of the compositions of preventing and treating citrus red mite
Parts by weight of raw materials compares:
ZEN 90160,25 parts;Cimifugin, 20 parts;Ethanol, 140 parts;Water, 480 parts;Synergist acrylonitrile and sodium hypophosphite
Totally 9 parts, the weight ratio of acrylonitrile and sodium hypophosphite is 8:1.
Preparation method:
Step S1, by ZEN 90160, cimifugin and synergist acrylonitrile ethanol and water dissolution;
Step S2, by sodium hypophosphite water dissolution;
Step S3, slowly adds the solution of step S1 in the solution of step S2, and interpolation limit, limit is stirred, and to obtain final product.
Embodiment 4: the preparation of the compositions of preventing and treating citrus red mite
Parts by weight of raw materials compares:
ZEN 90160,20 parts;Cimifugin, 15 parts;Ethanol, 130 parts;Water, 460 parts;Synergist acrylonitrile and sodium hypophosphite
Totally 8 parts, the weight ratio of acrylonitrile and sodium hypophosphite is 6:1.
Preparation method:
Step S1, by ZEN 90160, cimifugin and synergist acrylonitrile ethanol and water dissolution;
Step S2, by sodium hypophosphite water dissolution;
Step S3, slowly adds the solution of step S1 in the solution of step S2, and interpolation limit, limit is stirred, and to obtain final product.
Embodiment 5: the preparation of the compositions of preventing and treating citrus red mite
Parts by weight of raw materials compares:
ZEN 90160,20 parts;Cimifugin, 15 parts;Ethanol, 130 parts;Water, 460 parts;Synergist acrylonitrile and sodium hypophosphite
Totally 8 parts, the weight ratio of acrylonitrile and sodium hypophosphite is 8:1.
Preparation method:
Step S1, by ZEN 90160, cimifugin and synergist acrylonitrile ethanol and water dissolution;
Step S2, by sodium hypophosphite water dissolution;
Step S3, slowly adds the solution of step S1 in the solution of step S2, and interpolation limit, limit is stirred, and to obtain final product.
The weight ratio of embodiment 6: comparative example, acrylonitrile and sodium hypophosphite is 5:1
Parts by weight of raw materials compares:
ZEN 90160,20 parts;Cimifugin, 15 parts;Ethanol, 130 parts;Water, 460 parts;Synergist acrylonitrile and sodium hypophosphite
Totally 8 parts, the weight ratio of acrylonitrile and sodium hypophosphite is 5:1.
Preparation method:
Step S1, by ZEN 90160, cimifugin and synergist acrylonitrile ethanol and water dissolution;
Step S2, by sodium hypophosphite water dissolution;
Step S3, slowly adds the solution of step S1 in the solution of step S2, and interpolation limit, limit is stirred, and to obtain final product.
The weight ratio of embodiment 7: comparative example, acrylonitrile and sodium hypophosphite is 9:1
Parts by weight of raw materials compares:
ZEN 90160,20 parts;Cimifugin, 15 parts;Ethanol, 130 parts;Water, 460 parts;Synergist acrylonitrile and sodium hypophosphite
Totally 8 parts, the weight ratio of acrylonitrile and sodium hypophosphite is 9:1.
Preparation method:
Step S1, by ZEN 90160, cimifugin and synergist acrylonitrile ethanol and water dissolution;
Step S2, by sodium hypophosphite water dissolution;
Step S3, slowly adds the solution of step S1 in the solution of step S2, and interpolation limit, limit is stirred, and to obtain final product.
Embodiment 8: effect example
The compositions of the testing example 1~7 preparation preventing and treating effective percentage (%) to citrus red mite respectively.
When field test uses, present composition water carries out 40 times of dilutions, and fountain height is 40 liters/mu.
Result such as following table.
Preventing and treating effective percentage (%) | |
Embodiment 1 | 100 |
Embodiment 4 | 98 |
Embodiment 5 | 98 |
Embodiment 6 | 73 |
Embodiment 7 | 72 |
The effect of embodiment 2,3 is basically identical with embodiment 4,5.
The above results shows, the compositions that the present invention provides can prevent and treat citrus red mite, can develop into preventing and treating Citrus
The pesticide of red spider, prevention effect is relevant with the weight ratio of synergist acrylonitrile and sodium hypophosphite in raw material, acrylonitrile and
When the weight ratio of sodium hypophosphite is 6~8:1, prevention effect is best.
The effect of above-described embodiment indicates that the essentiality content of the present invention, but does not limit the protection of the present invention with this
Scope.It will be understood by those within the art that, technical scheme can be modified or equivalent,
Essence and protection domain without deviating from technical solution of the present invention.
Claims (5)
1. the compositions preventing and treating citrus red mite, it is characterised in that include the raw material of following weight portion: ZEN 90160,15
~25 parts;Cimifugin, 10~20 parts;Ethanol, 120~140 parts;Water, 440~480 parts;Synergist acrylonitrile and sodium hypophosphite are altogether
7~9 parts, the weight ratio of acrylonitrile and sodium hypophosphite is 6~8:1.
The compositions of preventing and treating citrus red mite the most according to claim 1, it is characterised in that include the former of following weight portion
Material: ZEN 90160,20 parts;Cimifugin, 15 parts;Ethanol, 130 parts;Water, 460 parts;Synergist acrylonitrile and sodium hypophosphite totally 8 parts,
The weight ratio of acrylonitrile and sodium hypophosphite is 7:1.
The compositions of preventing and treating citrus red mite the most according to claim 1, it is characterised in that include the former of following weight portion
Material: ZEN 90160,15 parts;Cimifugin, 10 parts;Ethanol, 120 parts;Water, 440 parts;Synergist acrylonitrile and sodium hypophosphite totally 7 parts,
The weight ratio of acrylonitrile and sodium hypophosphite is 6:1.
The compositions of preventing and treating citrus red mite the most according to claim 1, it is characterised in that include the former of following weight portion
Material: ZEN 90160,25 parts;Cimifugin, 20 parts;Ethanol, 140 parts;Water, 480 parts;Synergist acrylonitrile and sodium hypophosphite totally 9 parts,
The weight ratio of acrylonitrile and sodium hypophosphite is 8:1.
5. the preparation method of the arbitrary described compositions of Claims 1 to 4, it is characterised in that comprise the steps:
Step S1, by ZEN 90160, cimifugin and synergist acrylonitrile ethanol and water dissolution;
Step S2, by sodium hypophosphite water dissolution;
Step S3, slowly adds the solution of step S1 in the solution of step S2, and interpolation limit, limit is stirred, and to obtain final product.
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CN201610465453.0A CN106106525A (en) | 2016-06-22 | 2016-06-22 | A kind of compositions preventing and treating citrus red mite and preparation method thereof |
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CN201610465453.0A CN106106525A (en) | 2016-06-22 | 2016-06-22 | A kind of compositions preventing and treating citrus red mite and preparation method thereof |
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Citations (4)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN102017960A (en) * | 2011-01-01 | 2011-04-20 | 陕西上格之路生物科学有限公司 | Acaricidal composition containing etoxazole and pyridaben |
CN103563904A (en) * | 2013-11-11 | 2014-02-12 | 陕西农心作物科技有限公司 | Acaricidal composition containing pyriminostrobin and tebufenpyrad |
CN104488916A (en) * | 2014-11-28 | 2015-04-08 | 许冠安 | Pharmaceutical composition for preventing and treating citrus red mites |
CN104872164A (en) * | 2015-05-29 | 2015-09-02 | 杨新兰 | Method for preventing citrus red mites |
-
2016
- 2016-06-22 CN CN201610465453.0A patent/CN106106525A/en active Pending
Patent Citations (4)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN102017960A (en) * | 2011-01-01 | 2011-04-20 | 陕西上格之路生物科学有限公司 | Acaricidal composition containing etoxazole and pyridaben |
CN103563904A (en) * | 2013-11-11 | 2014-02-12 | 陕西农心作物科技有限公司 | Acaricidal composition containing pyriminostrobin and tebufenpyrad |
CN104488916A (en) * | 2014-11-28 | 2015-04-08 | 许冠安 | Pharmaceutical composition for preventing and treating citrus red mites |
CN104872164A (en) * | 2015-05-29 | 2015-09-02 | 杨新兰 | Method for preventing citrus red mites |
Non-Patent Citations (1)
Title |
---|
刘长令: "《世界农药大全 杀菌剂卷》", 31 January 2006, 化学工业出版社 * |
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