CN106087407B - High-efficiency oil removal agent for textile - Google Patents
High-efficiency oil removal agent for textile Download PDFInfo
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- CN106087407B CN106087407B CN201610422160.4A CN201610422160A CN106087407B CN 106087407 B CN106087407 B CN 106087407B CN 201610422160 A CN201610422160 A CN 201610422160A CN 106087407 B CN106087407 B CN 106087407B
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- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M13/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment
- D06M13/244—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment with compounds containing sulfur or phosphorus
- D06M13/248—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment with compounds containing sulfur or phosphorus with compounds containing sulfur
- D06M13/256—Sulfonated compounds esters thereof, e.g. sultones
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M13/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment
- D06M13/322—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment with compounds containing nitrogen
- D06M13/46—Compounds containing quaternary nitrogen atoms
- D06M13/463—Compounds containing quaternary nitrogen atoms derived from monoamines
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M15/00—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment
- D06M15/19—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment with synthetic macromolecular compounds
- D06M15/37—Macromolecular compounds obtained otherwise than by reactions only involving carbon-to-carbon unsaturated bonds
- D06M15/53—Polyethers
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
- D06P1/00—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed
- D06P1/16—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using dispersed, e.g. acetate, dyestuffs
Abstract
The invention discloses a high-efficiency oil removal agent for a textile. The high-efficiency oil removal agent is prepared from 2-3 parts by weight of iso-tridecanol polyoxyethylene ether 1302, 3-4 parts by weight of iso-tridecanol polyoxyethylene ether 1306, 4-6 parts by weight of iso-tridecanol polyoxyethylene ether 1307, 5-7 parts by weight of iso-tridecanol polyoxyethylene ether 1308, 7-9 parts by weight of iso-tridecanol polyoxyethylene ether 1309, 7-8 parts by weight of a surfactant 1227, 2-3 parts by weight of dodecyl betain BS-12, 10-12 parts by weight of dodecylsulfonic acid, 2-3 parts by weight of a solubiliser S, 8-10 parts by weight of 25% ammonium hydroxide, 5-6 parts by weight of 96% industrial alcohol, 0.1-0.2 parts by weight of an antifoaming agent and 35-40 parts by weight of water. The high-efficiency oil removal agent can remove oil on a textile under the weak acidic condition (of pH=4.5-5.5), guarantee smooth dyeing and provide conditions for one-bath process oil removal/dyeing of a textile in a printing and dyeing enterprise.
Description
Technical field
The present invention relates to textile dyeing and finishing manufacture field, and in particular to be a kind of textile highly effective oil remover.
Background technology
Textile in order to increase the greasy property of yarn, often comes real using substantial amounts of textile finish oil in weaving process
Show, especially the weaving process of knitted fabric.Due to textile finish oil water repellency to textile dyeing and all other after
Arrangement brings greatest trouble, therefore oil removing then seems particular importance as the processing operation before textile dyeing and finishing, oil removing
Whether totally, uniformly directly influence follow-up crudy.
Country's printing and dyeing enterprise is used for all kinds of of the auxiliary agent mainly fats Polyethylene oxide ether structure of textile oil removing at present
Nonionic or the moon/nonionic surfactant, can show to have traditional textile oil preparation under basic or acidic conditions
Preferable emulsifying, peptizaiton.But, on the one hand weaving mill is cost-effective in recent years, begins to use all kinds low cost
Textile finish oil, almost whole body is exited traditional weaving mineral oil oil preparation for being easy to the self emulsifying in water, is replaced
Be the textile finish oil synthesized from various animal and plant oils and fatss from all directions and petrochemical industry；On the other hand, printing and dyeing enterprise is
Reduces cost, shortens technological process, and chemical ＆ blended fabric (especially dacron) has been given up traditional elder generation and removed in the basic conditions
Oil, the technique for then doing Colour Difference again, but employ oil removing, one-pass bath method for dyeing technique, i.e., in solutions of weak acidity (pH=
Also the technique for completing dyeing course under 4.5-5.5) while oil removing, this properties to degreaser propose higher wanting
Ask, complete under 130 DEG C of hot conditionss as dyeing terylene and require that the performances such as the emulsifying of degreaser, dispersion can not be cut
Weak, degreaser can not be on the problems such as the generation impact of the dyeability of dyestuff.
Therefore, degreaser how is made to have given play to excellent emulsifying, dispersion under high temperature, solutions of weak acidity (pH=4.5-5.5)
Effect, has to be solved while dyeing circumstances being unlikely to generation and changing this problem.
The content of the invention
It is an object of the invention to provide a kind of textile highly effective oil remover, under solutions of weak acidity (pH=4.5-5.5)
Can guarantee that whole dyeing course is smoothly completed again while oil removing being carried out to fabric, be that printing and dyeing enterprise carries out single bath process to fabric
Oil removing/dyeing offer condition.
In order to reach above-mentioned purpose, the solution of the present invention is：
A kind of textile highly effective oil remover, by weight, the composition of each raw material and content are：
After such scheme, in the present invention, isomerous tridecanol polyoxyethylene ether 1302,1306,1307,1308,1309 is
The nonionic surfactant of different EO adduct numbers, the HLB shown due to various materials (close and distant equilibrium valve) are different, have
Various different high performance permeabilitys, washing performance and greasy dirt emulsifying, dispersibility, be very effective emulsifying agent, dispersant and
Wetting agent, to adapt to be fully contacted with a variety of oil preparation surfaces in oil removal process, emulsifying；Surfactant 1227 i.e. 12
Zephiran, is cationic surfactant, with stronger cationic, contains two first in molecule
Base, therefore be also a kind of ideal emulsifying agent and dispersant；Empgen BB BS-12 is amphoteric surfactant,
Its molecular structure has abnormal similarity with surfactant 1227, is a kind of more excellent emulsifying of specific surface activating agent 1227
Agent and dispersant, in this system, moreover it is possible to take on isomerous tridecanol polyoxyethylene ether and the co-melting of surfactant 1227 " is adjusted
Section device "；Dodecyl sodium sulfonate can obtain dodecyl sodium sulfonate ammonia with ammonia reaction, be also a kind of excellent emulsifying agent；Solubilizing agent S
For the compound of various modified nonionic surfactants, with stronger emulsifying, peptizaiton；Industrial alcohol is mainly used in increasing
Plus the water solublity of system of the present invention, it is user-friendly to, defoamer then reduces the foam of system of the present invention, improves product operable
Property.
Under mildly acidic conditions, surfactant 1227 and empgen BB BS-12, dodecyl sodium sulfonate ammonia etc. compared with
Strong cationic properties greatly reduce the surface tension of fiber, define cation group inwardly in fiber surface, nonpolar
The arrangement outwardly of Long carbon chain lipophilic group, the oil stain combined with fiber by script are separated with spot, due to various HLB
The presence of the isomerous tridecanol polyoxyethylene ether of value, carries out emulsifying in aqueous again, perfectly completes whole emulsifying
Journey.Spot on the little particle oil stain separated and fabric is firm with nonpolar Long carbon chain lipophilic group in water solution system
With reference to defining tiny oil stain and spot granule；Due to containing 13 carbon in the molecule of isomerous tridecanol polyoxyethylene ether
Carbon-chain structure, this and surfactant 1227 and empgen BB BS-12,12 carbon carbochains of dodecyl sodium sulfonate ammonia
Structure has abnormal similarity, occurs in aqueous solution between the granule that repulsion effect powerful therebetween causes each tiny
Interior stable " suspension ", is allowed to be dispersed in working solution, so as to completing the emulsifying to fabric face greasy dirt stain and disperseing
Journey.
Due to the ionic category nonionic of the disperse dyes of dyeing system, its water solublity is relatively low, in outstanding in dyeing system
Floating state, easily assembles at high temperature and causes the inhomogeneities for dyeing, the textile highly effective oil remover is applied to dye
Cheng Zhong, while oil removing, due to the good dispersion that isomerous tridecanol polyoxyethylene ether has in itself, along with due to isomery
Tridecanol polyoxyethylene ether and surfactant 1227 and empgen BB BS-12, dodecyl sodium sulfonate ammonia have abnormal
Similar carbon-chain structure, forms therebetween powerful repulsion effect so that the suspended state of the molecule of disperse dyes is more
Plus it is stable, that is, the high temperature dispersibility of dyestuff is increased, the dyeing for disperse dyes in fabric single bath process oil removing/dyeing course is carried
More preferable environment has been supplied, the process time has been greatlyd save, the stability and repeatability of dyeing has been improve.
Therefore, a kind of textile highly effective oil remover of the invention, can enter to fabric under solutions of weak acidity (pH=4.5-5.5)
Can guarantee that while row oil removing that whole dyeing course is smoothly completed again, be that printing and dyeing enterprise carries out single bath process oil removing/dyeing to fabric
Offer condition.
In addition, the raw material adopted in the present invention is environmentally friendly machine, meet 100 Hes of European Union Oeko-Tex Standard
The requirements of REACH regulations, i.e. the textile highly effective oil remover are that a kind of environment-friendly type removes oil assistant, will not in dyeing and finishing technology
To environment, be conducive to environmental conservation.
Specific embodiment
In order to technical scheme is explained further, the present invention is explained in detail below by specific embodiment
State.
A kind of textile highly effective oil remover, by weight, the composition of each raw material and content are：
Above-mentioned raw materials are prepared as follows method enforcement：
(1) dodecyl sodium sulfonate and 8- of 10-12 weight portions are slowly added in the deionized water of 35-40 weight portions successively
25% ammonia of 10 weight portions, room temperature are sufficiently stirred for 50-60 minutes；
(2) isomerous tridecanol polyoxyethylene ether 1302, the isomery of 3-4 weight portions of 2-3 weight portions are slowly added into again successively
Tridecanol polyoxyethylene ether 1306, the isomerous tridecanol polyoxyethylene ether 1307 of 4-6 weight portions, the isomery 13 of 5-7 weight portions
Polyoxyethylenated alcohol 1308, the isomerous tridecanol polyoxyethylene ether 1309 of 7-9 weight portions, the surfactant of 7-8 weight portions
1227th, the solubilizing agent S of the empgen BB BS-12 and 2-3 weight portion of 2-3 weight portions, is sufficiently stirred for 15-20 minutes；
(3) 50 DEG C are slowly ramped to and 96% industrial wine of 5-6 weight portions after continuing to stir 80-90 minutes, is slowly added to
Essence, continues stirring 15-20 minutes；
(4) defoamer that foam situation adds 0.1-0.2 weight portions as one sees fit is produced according to solution, continues stirring 20 minutes,
Obtain final product the textile highly effective oil remover.
Embodiment one
Textile highly effective oil remover of the present invention, is specifically prepared from by the raw material of following weight portion：The isomery ten of 3 weight portions
Three polyoxyethylenated alcohol 1302, the isomerous tridecanol polyoxyethylene ether 1306 of 3 weight portions, the isomerous tridecanol polyoxy of 6 weight portions
Vinyl Ether 1307, the isomerous tridecanol polyoxyethylene ether 1308 of 5 weight portions, the isomerous tridecanol polyoxyethylene ether of 9 weight portions
1309th, the surfactant 1227 of 7 weight portions, the empgen BB BS-12 of 2 weight portions, the dodecyl of 10 weight portions
Sulfonic acid, the solubilizing agent S of 2 weight portions, 25% ammonia of 8 weight portions, the defoamer of 0.1-0.2 weight portions, 95% work of 5 weight portions
The deionized water of industry ethanol and 40 weight portions.
The preparation method of the textile highly effective oil remover in the present embodiment, is realized according to the following steps：
(1) dodecyl sodium sulfonate and 8 weight portions of 10 weight portions are slowly added in the deionized water of 40 weight portions successively
25% ammonia, room temperature is sufficiently stirred for 50-60 minutes；
(2) isomerous tridecanol polyoxyethylene ether 1302, the isomery 13 of 3 weight portions of 3 weight portions are slowly added into again successively
Polyoxyethylenated alcohol 1306, the isomerous tridecanol polyoxyethylene ether 1307 of 6 weight portions, the isomerous tridecanol polyoxy second of 5 weight portions
Alkene ether 1308, the isomerous tridecanol polyoxyethylene ether 1309 of 9 weight portions, the surfactant 1227 of 7 weight portions, 2 weight portions
The solubilizing agent S of empgen BB BS-12 and 2 weight portions, is sufficiently stirred for 15-20 minutes；
(3) 50 DEG C are slowly ramped to and 95% industrial alcohol of 5 weight portions after continuing to stir 80-90 minutes, is slowly added to,
Continue stirring 15-20 minutes；
(4) add the defoamer of 0.1-0.2 weight portions according to the foam situation that solution is produced as one sees fit, continue 20 points of stirring
Clock, obtains final product the textile highly effective oil remover.
Embodiment two
Textile highly effective oil remover of the present invention, is specifically prepared from by the raw material of following weight portion：The isomery ten of 3 weight portions
Three polyoxyethylenated alcohol 1302, the isomerous tridecanol polyoxyethylene ether 1306 of 3.5 weight portions, the isomerous tridecanol of 5 weight portions gather
Oxygen vinyl Ether 1307, the isomerous tridecanol polyoxyethylene ether 1308 of 6 weight portions, the isomerous tridecanol polyoxyethylene ether of 8 weight portions
1309th, the surfactant 1227 of 7.5 weight portions, the empgen BB BS-12 of 2.5 weight portions, the 12 of 11 weight portions
Alkyl sulfonic acid, the solubilizing agent S of 2.5 weight portions, 25% ammonia of 9 weight portions, the defoamer of 0.1-0.2 weight portions, 5.5 weight portions
95% industrial alcohol and 36.5 weight portions deionized water.
The preparation method of the textile highly effective oil remover in the present embodiment, is realized according to the following steps：
(1) dodecyl sodium sulfonate and 9 weight of 11 weight portions are slowly added in the deionized water of 36.5 weight portions successively
25% ammonia of part, room temperature are sufficiently stirred for 50-60 minutes；
(2) isomerous tridecanol polyoxyethylene ether 1302, the isomery ten of 3.5 weight portions of 3 weight portions are slowly added into again successively
Three polyoxyethylenated alcohol 1306, the isomerous tridecanol polyoxyethylene ether 1307 of 5 weight portions, the isomerous tridecanol polyoxy of 6 weight portions
Vinyl Ether 1308, the isomerous tridecanol polyoxyethylene ether 1309 of 8 weight portions, the surfactant 1227 of 7.5 weight portions, 2.5 weights
The solubilizing agent S of the empgen BB BS-12 and 2.5 weight portions of amount part, is sufficiently stirred for 15-20 minutes；
(3) 50 DEG C are slowly ramped to and 95% industrial wine of 5.5 weight portions after continuing to stir 80-90 minutes, is slowly added to
Essence, continues stirring 15-20 minutes；
(4) add the defoamer of 0.1-0.2 weight portions according to the foam situation that solution is produced as one sees fit, continue 20 points of stirring
Clock, obtains final product the textile highly effective oil remover.
Embodiment three
Textile highly effective oil remover of the present invention, is specifically prepared from by the raw material of following weight portion：The isomery ten of 2 weight portions
Three polyoxyethylenated alcohol 1302, the isomerous tridecanol polyoxyethylene ether 1306 of 4 weight portions, the isomerous tridecanol polyoxy of 4 weight portions
Vinyl Ether 1307, the isomerous tridecanol polyoxyethylene ether 1308 of 7 weight portions, the isomerous tridecanol polyoxyethylene ether of 7 weight portions
1309th, the surfactant 1227 of 8 weight portions, the empgen BB BS-12 of 3 weight portions, the dodecyl of 12 weight portions
Sulfonic acid, the solubilizing agent S of 3 weight portions, 25% ammonia of 10 weight portions, the defoamer of 0.1-0.2 weight portions, the 95% of 6 weight portions
The deionized water of industrial alcohol and 35 weight portions.
The preparation method of the textile highly effective oil remover in the present embodiment, is realized according to the following steps：
(1) dodecyl sodium sulfonate and 10 weight portions of 12 weight portions are slowly added in the deionized water of 35 weight portions successively
25% ammonia, room temperature is sufficiently stirred for 50-60 minutes；
(2) isomerous tridecanol polyoxyethylene ether 1302, the isomery 13 of 4 weight portions of 2 weight portions are slowly added into again successively
Polyoxyethylenated alcohol 1306, the isomerous tridecanol polyoxyethylene ether 1307 of 4 weight portions, the isomerous tridecanol polyoxy second of 7 weight portions
Alkene ether 1308, the isomerous tridecanol polyoxyethylene ether 1309 of 7 weight portions, the surfactant 1227 of 8 weight portions, 3 weight portions
The solubilizing agent S of empgen BB BS-12 and 3 weight portions, is sufficiently stirred for 15-20 minutes；
(3) 50 DEG C are slowly ramped to and 95% industrial alcohol of 6 weight portions after continuing to stir 80-90 minutes, is slowly added to,
Continue stirring 15-20 minutes；
(4) add the defoamer of 0.1-0.2 weight portions according to the foam situation that solution is produced as one sees fit, continue 20 points of stirring
Clock, obtains final product the textile highly effective oil remover.
As present weaving mill is using a large amount of non-woven oil preparationes or textile oil preparation inferior, traditional degreaser pair is thus resulted in
Present textile oil removing has that oil removing is not net always.A kind of textile highly effective oil remover of the present invention then solves this
A difficult problem, the indices performance with regard to the textile highly effective oil remover in dyeing course and tradition below by specific experiment technique
Degreaser launches contrast and inquires into.
First, experiment content：
1st, experimental project：
Contrast a kind of textile highly effective oil remover of the invention and traditional degreaser every base values in dyeing course
Performance situation.
2nd, experiment material：Pure polyester knitting thing
3rd, experimental drug：
1., (Rhizoma Arisaematis) highly effective oil remover NX-138 (textile highly effective oil remover i.e. of the present invention)；
2., certain company degreaser 1# (i.e. traditional degreaser)；
3., disperse dyes, high temperature levelling agent PS-15；
4., 98%HAc.
4th, test apparatuses and equipment：Weighing botle, Sartorius electronic balance (precision：0.001 and 0.01 two kinds of precision),
It is German Copower flint dries machine, Germany's Copower infrared high-temperature dyeing machines, auspicious than (Rapid) drying and setting machine, vacuum
Sucking filtration machine, 100ml tool plug graduated cylinders.
5th, test method：
The measure of 5.1 solid contents：Highly effective oil remover NX-1381.00g each five parts and oil removing are weighed accurately using weighing botle
Agent 1#1.00g is each five parts, is respectively placed in flint dry machine, 105 DEG C bake 4 hours after take out weigh, calculate efficient degreasing
Average after the solid content data of agent NX-138 and degreaser 1#, obtain final product the accurate solid content data of the material.
5.2 spumescence：It is each five parts 500ml to be prepared using distilled water accurately by formula as below concentration：
Highly effective oil remover NX-138 1%
Degreaser 1# 1%；
Have the foam data that plug graduated cylinder accurately tests each solution using 100ml, calculate the flat of corresponding five groups of data
Average obtains final product the foam data of highly effective oil remover NX-138 and degreaser 1#.
The measure of 5.3 emulsifying capacities：It is each five parts 250ml to be prepared using distilled water accurately by formula as below concentration：
Highly effective oil remover NX-138 1%
Degreaser 1# 1%；
After being sufficiently stirred in the graduated cylinder of falling 250ml, record aqueous solution is layered to needed for 2.5mm, 3.5mm, 5mm from top to bottom
Time, the time, longer explanation emulsifying capacity was better, and repetition calculates meansigma methodss as two kinds of oil removings of evaluation after measuring five groups of data
The foundation of the emulsifying capacity of agent.
5.4 one-bath deoiling Contrast on effect：Oil removing dyeing is carried out using different degreasers by following technique with self-control oilcloth：
Technique：Bath raio 1:15,130 DEG C × 30min, 2 DEG C/min of heating rate, dyeing wash clean, drying, determine after finishing
Type, on contrast various kinds cloth, oil clot removes situation.
The impact of 5.5 pairs of disperse dyes high temperature dispersibilities：Working solution is prepared by following technical recipe using different degreasers
Each 100ml：
135 DEG C × 45min, 2.5 DEG C/min of heating rate.Take out after being cooled to 80 DEG C after being disposed, taken out using vacuum
Filter sucking filtration, after the filter paper for obtaining is dried naturally, according to residual dye situation on filter paper and using the R1 of degreaser 1# as ginseng
According to thing by following rule grading：Object of reference is 1 grade, is divided into 5 grades, and on filter paper, residual dye is fewer, is graded higher.
2nd, experimental result：
1st, the measure of solid content：
| Reagent name | Solid content (%) |
| Degreaser 1# | 39.1 |
| Highly effective oil remover NX-138 | 40.0 |
2nd, spumescence：
3rd, the measure of emulsifying capacity：
4th, one-bath deoiling Contrast on effect：
| Reagent name | Deoiling effect |
| Degreaser 1# | Cloth cover remaining large area dark color oil clot |
| Highly effective oil remover NX-138 | It is uniform that cloth cover obtains color |
5th, the impact to disperse dyes high temperature dispersibility：
3rd, conclusion：
The present invention this textile highly effective oil remover, either deoiling effect still the dyeing system of disperse dyes is changed
The needs in market have been reached on kind, have been a kind of highly effective oil removers of preferable environment-friendly type.
The product form and style of above-described embodiment the non-limiting present invention, the ordinary skill people of any art
Appropriate change or modification that member is done to which, all should be regarded as the patent category without departing from the present invention.
Claims (1)
1. a kind of textile highly effective oil remover, it is characterised in that：By weight, the composition of each raw material and content are：
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| CN106978727A (en) * | 2017-04-28 | 2017-07-25 | 晋江市南星印染材料有限公司 | A kind of spandex refining degreaser used for textiles containing spandex |
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| CN108570360B (en) * | 2018-04-26 | 2021-12-17 | 浙江汉邦新材料股份有限公司 | Color-preserving brightening oil stain removing agent |
| CN111996803B (en) * | 2020-09-02 | 2022-10-18 | 多恩生物科技有限公司 | Novel environment-friendly low-foam low-temperature degreasing agent and preparation method thereof |
| CN115651773A (en) * | 2022-10-14 | 2023-01-31 | 丽友清洁科技(湖北)有限公司 | Polyester fabric low-temperature degreasing agent and preparation method and preparation device thereof |
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| CN105002022A (en) * | 2015-07-24 | 2015-10-28 | 邦诺（福建）纺织实业有限责任公司 | Low-temperature deoiling scouring agent and preparation method thereof |
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| CN106087407A (en) | 2016-11-09 |
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