CN106040147A - Novel synthesis equipment - Google Patents

Novel synthesis equipment Download PDF

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Publication number
CN106040147A
CN106040147A CN201610511708.2A CN201610511708A CN106040147A CN 106040147 A CN106040147 A CN 106040147A CN 201610511708 A CN201610511708 A CN 201610511708A CN 106040147 A CN106040147 A CN 106040147A
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China
Prior art keywords
filter
filter screen
parts
rack
novel synthesis
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Granted
Application number
CN201610511708.2A
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Chinese (zh)
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CN106040147B (en
Inventor
吴玲玲
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Wuzhou Zehe High Molecular Material Co ltd
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Huizhou Gregory Technology Co Ltd
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Priority to CN201610511708.2A priority Critical patent/CN106040147B/en
Publication of CN106040147A publication Critical patent/CN106040147A/en
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Publication of CN106040147B publication Critical patent/CN106040147B/en
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    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J19/00Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J19/18Stationary reactors having moving elements inside
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01DSEPARATION
    • B01D29/00Filters with filtering elements stationary during filtration, e.g. pressure or suction filters, not covered by groups B01D24/00 - B01D27/00; Filtering elements therefor
    • B01D29/01Filters with filtering elements stationary during filtration, e.g. pressure or suction filters, not covered by groups B01D24/00 - B01D27/00; Filtering elements therefor with flat filtering elements
    • B01D29/05Filters with filtering elements stationary during filtration, e.g. pressure or suction filters, not covered by groups B01D24/00 - B01D27/00; Filtering elements therefor with flat filtering elements supported
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01DSEPARATION
    • B01D29/00Filters with filtering elements stationary during filtration, e.g. pressure or suction filters, not covered by groups B01D24/00 - B01D27/00; Filtering elements therefor
    • B01D29/50Filters with filtering elements stationary during filtration, e.g. pressure or suction filters, not covered by groups B01D24/00 - B01D27/00; Filtering elements therefor with multiple filtering elements, characterised by their mutual disposition
    • B01D29/56Filters with filtering elements stationary during filtration, e.g. pressure or suction filters, not covered by groups B01D24/00 - B01D27/00; Filtering elements therefor with multiple filtering elements, characterised by their mutual disposition in series connection
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J19/00Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J19/0053Details of the reactor
    • B01J19/006Baffles
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J19/00Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J19/02Apparatus characterised by being constructed of material selected for its chemically-resistant properties
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00761Details of the reactor
    • B01J2219/00763Baffles
    • B01J2219/00765Baffles attached to the reactor wall
    • B01J2219/00768Baffles attached to the reactor wall vertical
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/02Apparatus characterised by their chemically-resistant properties
    • B01J2219/0204Apparatus characterised by their chemically-resistant properties comprising coatings on the surfaces in direct contact with the reactive components
    • B01J2219/0236Metal based
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/18Details relating to the spatial orientation of the reactor
    • B01J2219/185Details relating to the spatial orientation of the reactor vertical

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  • Chemical & Material Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Organic Chemistry (AREA)
  • Physical Or Chemical Processes And Apparatus (AREA)
  • Mixers Of The Rotary Stirring Type (AREA)

Abstract

The invention relates to novel synthesis equipment. The novel synthesis equipment comprises a kettle body, a stirring and mixing device, a material filtering device and a filtration supporting device. An upper head and a lower head are respectively arranged at the two ends of the kettle body. The stirring and mixing device comprises a mounting rack, a driving motor, a driving shaft and a stirring paddle. The material filtering device comprises a material pumping pipe body, a filtration box body, a filter screen assembly, a filter pump body, a return pipe body and a valve. The filtration supporting device comprises a first supporting net rack and a second supporting net rack. The novel synthesis equipment is provided with the kettle body, the stirring and mixing device and the material filtering device, and the material filtering device can carry out circulating filtration and impurity removal operations on materials, so that the impurity removal operation is relatively simple and convenient, and the production efficiency is also relatively high.

Description

Novel synthesis device
Technical field
The present invention relates to chemical industry synthesis device technical field, particularly relate to a kind of novel synthesis device.
Background technology
At present, in material production field, after especially various materials mixing reacts, obtain the situation of final products In, it usually needs use chemical industry synthesis device, for material is stirred mixing, and make it successfully react, be used for Synthesis obtains the final products of higher quality.
Wherein, due to material before the reaction or reaction after, more or less there are some impurity, traditional goes removal of impurity mode For first being taken out from chemical industry synthesis device by the product obtained after reaction, then use the defecator of outside that product was carried out Filter.
But, above-mentioned go deimpurity mode still exist operation more complicated loaded down with trivial details problem, cause production efficiency relatively low.
Summary of the invention
Based on this, it is necessary to provide a kind of and go deimpurity operation more simple and convenient and novel conjunction that production efficiency is higher Forming apparatus.
A kind of novel synthesis device, including:
Kettle, the two ends of described kettle are respectively arranged with upper cover and low head;
Mixing stirring device, described mixing stirring device includes installation frame, drives motor, drive shaft and stirring paddle, institute Stating installation frame to be fixedly mounted on described upper cover, described driving motor is arranged on described installation frame, described drive shaft The first end be connected with the rotary shaft of described driving motor, the second end of described drive shaft is connected with described stirring paddle, and described Stirring paddle is positioned at inside described low head;
Material filter, described material filter includes material-pumping tube body, filter box, screen modules, filter pump Body, backflow body and valve, the first end of described material-pumping tube body connects with the bottom of described low head, described filter box hollow Arranging, form filter cavity in it, the second end of described material-pumping tube body is connected with the first end of described filter box, and described in take out Second end of material body connects with described filter cavity, and described screen modules includes the first filter screen, the second filter screen and the 3rd filter Net, described first filter screen, described second filter screen and described 3rd filter screen be arranged at intervals in described filter cavity successively, and described The edge of the edge of one filter screen, the edge of described second filter screen and described 3rd filter screen is all with the medial wall of described filter box even Connecing, described first filter screen is arranged towards the direction of the second end of described material-pumping tube body, and the feed end of the described filtration pump housing is with described Second end of filter box connects, and described filtration pump housing feed end connects with described filter cavity, going out of the described filtration pump housing Material end connects with the first end of described backflow body, and the second end of described backflow body connects with described upper cover, described valve It is arranged on described backflow body;And
Filter support means, described filtration support means include the first support rack and second support rack, described first The edge supporting rack is connected with the medial wall of described filter box, and described first supports rack is positioned at described first filter screen and institute Stating between the second filter screen, described first supports rack offers the first mesh, and described second supports the edge of rack and described mistake The medial wall of filter box body connects, and described second supports rack between described second filter screen and described 3rd filter screen, and described the Two support rack offers the second mesh.
Wherein in an embodiment, the mesh of described first filter screen, the mesh of described second filter screen and described 3rd filter The filter opening size of net is sequentially reduced.
Wherein in an embodiment, described first filter screen, described first support rack, described second filter screen, described the Two support racks and described 3rd filter screen be arranged in parallel.
Wherein in an embodiment, the identical setting of size of the size of described first mesh and described second mesh.
Wherein in an embodiment, described first mesh and described second mesh are rhombus cavernous structure.
Wherein in an embodiment, between described first support rack and described first filter screen and described second filter screen all It is provided with interval.
Wherein in an embodiment, between described second support rack and described second filter screen and described 3rd filter screen all It is provided with interval.
Above-mentioned novel synthesis device is by arranging kettle, mixing stirring device and material filter, and material filtering Device can be circulated filtration and go the removal of impurity to operate material, goes deimpurity operation more simple and convenient, and production efficiency is the most relatively High.
Accompanying drawing explanation
Fig. 1 is the structural representation of the novel synthesis device of an embodiment of the present invention;
Fig. 2 is Fig. 1 enlarged drawing at A;
Fig. 3 is the partial structurtes schematic diagram of the novel synthesis device of another embodiment of the present invention;
Fig. 4 is the partial structurtes schematic diagram of the novel synthesis device of another embodiment of the present invention;
Fig. 5 is the partial structurtes schematic diagram of the novel synthesis device of another embodiment of the present invention;
Fig. 6 is the partial structurtes schematic diagram of the novel synthesis device of another embodiment of the present invention;
Fig. 7 is the partial structurtes schematic diagram of the novel synthesis device of another embodiment of the present invention;
Fig. 8 is the partial structurtes schematic diagram of the novel synthesis device of another embodiment of the present invention;
Fig. 9 is the partial structurtes schematic diagram of the novel synthesis device of another embodiment of the present invention.
Detailed description of the invention
For the ease of understanding the present invention, below with reference to relevant drawings, the present invention is described more fully.In accompanying drawing Give the better embodiment of the present invention.But, the present invention can realize in many different forms, however it is not limited to herein Described embodiment.On the contrary, providing the purpose of these embodiments is to make to understand the disclosure more Add thorough comprehensive.
It should be noted that when element is referred to as " being fixed on " or " being arranged at " another element, and it can be directly separately On one element or element placed in the middle can also be there is.When an element is considered as " connection " another element, and it is permissible It is directly to another element or may be simultaneously present centering elements.Term as used herein " vertical ", " level ", "left", "right" and similar statement for illustrative purposes only, being not offered as is unique embodiment.
Unless otherwise defined, all of technology used herein and scientific terminology and the technical field belonging to the present invention The implication that technical staff is generally understood that is identical.The term used the most in the description of the invention is intended merely to describe tool The purpose of the embodiment of body, it is not intended that in limiting the present invention.Term as used herein " and/or " include one or more Arbitrary and all of combination of relevant Listed Items.
Such as, a kind of novel synthesis device, including: kettle, the two ends of described kettle are respectively arranged with upper cover and lower envelope Head;Mixing stirring device, described mixing stirring device includes installation frame, drives motor, drive shaft and stirring paddle, described installation Frame is fixedly mounted on described upper cover, and described driving motor is arranged on described installation frame, the first of described drive shaft End is connected with the rotary shaft of described driving motor, and the second end of described drive shaft is connected with described stirring paddle, and described stirring paddle It is positioned at inside described low head;Material filter, described material filter includes material-pumping tube body, filter box, drainage screen Assembly, the filtration pump housing, backflow body and valve, the first end of described material-pumping tube body connects with the bottom of described low head, described Filter box hollow is arranged, and forms filter cavity, the second end of described material-pumping tube body and the first end of described filter box in it Connect, and the second end of described material-pumping tube body connect with described filter cavity, described screen modules include the first filter screen, second Filter screen and the 3rd filter screen, described first filter screen, described second filter screen and described 3rd filter screen are arranged at intervals at described filtration successively In cavity, the edge of the edge of described first filter screen, the edge of described second filter screen and described 3rd filter screen all with described filtration The medial wall of casing connects, and described first filter screen is arranged towards the direction of the second end of described material-pumping tube body, the described filtration pump housing Feed end be connected with the second end of described filter box, and described filtration pump housing feed end connects with described filter cavity, institute The discharge end stating the filtration pump housing connects with the first end of described backflow body, the second end of described backflow body and described upper cover Connection, described valve is arranged on described backflow body;And filtration support means, described filtration support means includes the first support Rack and second supports rack, and the described first edge supporting rack is connected with the medial wall of described filter box, and described first Support rack is between described first filter screen and described second filter screen, and described first supports rack offers the first mesh, institute The medial wall at the edge and described filter box of stating the second support rack is connected, and described second supports rack is positioned at described second filter Between net and described 3rd filter screen, described second supports rack offers the second mesh.
In order to further above-mentioned novel synthesis device be explained, such as, the novel synthesis of another embodiment Equipment is as follows:
Referring to Fig. 1, novel synthesis device 10 includes kettle 100, mixing stirring device 200 and material filter 300, Mixing stirring device 200 and material filter 300 may be contained within kettle 100.
Referring to Fig. 1, the two ends of kettle 100 are respectively arranged with upper cover 110 and low head 120, and kettle 100 is used for housing The material added, and material mix and blend and the offer occasion that reacts are provided.Such as, after upper cover 110 is connected with low head 120 Form kettle 100.And for example, described kettle is formed in one structure.And for example, in the process being installed on outside support of described kettle In, the top of the externally-located support of described upper cover, the bottom of the externally-located support of described low head.
Such as, it is hemispherical columnar structured that described kettle has two ends, and certainly, described kettle can also be according to reality Situation selects, and such as, using two ends is the columnar structured of plane.
Referring to Fig. 1, mixing stirring device 200 includes installation frame 210, drives motor 220, drive shaft 230 and stirring Oar 240, installation frame 210 is fixedly mounted on the upper cover 110 of kettle 100, drives motor 220 to be arranged at installation frame 210 On, the first end of drive shaft 230 is connected with the rotary shaft driving motor 220, and the second end of drive shaft 230 stretches to kettle 100 Inside, e.g., the low head 120 that the second end of drive shaft 230 stretches to kettle 100 is internal, the second end of drive shaft 230 and stirring Oar 240 connects, and e.g., the low head 120 that stirring paddle 240 is positioned at kettle 100 is internal.
Such as, described stirring paddle is anchor formula stirring paddle or propeller, certainly, can also select according to actual needs Use other kinds of stirring paddle.
Refer to Fig. 1, drive motor 220 to be used for driving drive shaft 230 to rotate, and then drive fixing with drive shaft 230 Stirring paddle 240 rotates.When needing the material in kettle 100 is stirred married operation, control to drive motor 220 to drive and drive Moving axis 230 rotates, and then drives stirring paddle 240 to rotate, and utilizes the flow-disturbing effect of stirring paddle 240, can play preferably stirring Immixture, and then the material in kettle 100 can be stirred married operation.
Seeing also Fig. 1 and Fig. 2, material filter 300 includes material-pumping tube body 310, filter box 320, drainage screen Assembly 330, the filtration pump housing 340, backflow body 350 and valve 360, low head 120, material-pumping tube body 310, filter box 320, mistake Filter pump body 340, backflow body 350 and upper cover 110 are sequentially communicated, and it is internal that screen modules 330 is placed in filter box 320, Valve 360 is arranged on backflow body 350.
Seeing also Fig. 1 and Fig. 2, the first end of material-pumping tube body 310 connects with the bottom of low head 120, so, works as still Material in body 100 is when reacting, and material can flow into material-pumping tube body 310 in low head 120, and then after carrying out Continuous filter operation.
Referring to Fig. 2, filter box 320 hollow is arranged, and forms filter cavity 321, material-pumping tube body in filter box 320 Second end of 310 is connected with the first end of filter box 320, and the second end of material-pumping tube body 310 connects with filter cavity 321, So, it is internal that the material to be filtered flowed in material-pumping tube body 310 just can flow into filter cavity 321, and at filter cavity Filter operation is completed in 321.
Referring to Fig. 2, screen modules 330 includes the first filter screen the 331, second filter screen 332 and the 3rd filter screen 333, first Filter screen the 331, second filter screen 332 and the 3rd filter screen 333 are arranged at intervals in filter cavity 321 successively, the edge of the first filter screen 331, all medial walls with filter box 320, the edge of the edge 332 of the second filter screen and the 3rd filter screen 333 are connected, so, from taking out The material flowed out in material body 310 is successively through the first filter screen the 331, second filter screen 332 and the 3rd filter screen 333, so that material Complete filter operation, it is possible to preferably remove the impurity in material, operate more convenient simply.Such as, the first filter screen 331, second Filter screen 332 and the 3rd filter screen 333 are spaced setting successively, so that leave gap between filter screen, in such manner, it is possible to better profit from Described gap accommodates the impurity being filtered out, and and for example, clears up, at interval of Preset Time, the impurity being filtered out, to reduce filter screen Or the problem of casing blocking occurs.
In order to preferably improve the filter effect of described screen modules, such as, described first filter screen, described second filter screen And the filter opening aperture of described 3rd filter screen is sequentially reduced, so, take three layers of effect progressively filtered, it is possible to for different-grain diameter Impurity, to optimize filtration path, and then can preferably improve the filter effect of described screen modules.
Seeing also Fig. 1 and Fig. 2, the feed end filtering the pump housing 340 is connected with the second end of filter box 320, and mistake Filter pump body 340 feed end connects with filter cavity 321, and the first end of the discharge end and backflow body 350 that filter the pump housing 340 connects Logical, the second end of backflow body 350 connects with upper cover 110.So, based on the filtration pump housing 340 when normally working, generation Suction, material can be filtered the pump housing 340 and is pumped to material-pumping tube body 310 from low head 120, then be taken out by material-pumping tube body 310 It is drawn in filter box 320, and first filter screen the 331, second filter screen 332 and that material is in described filter box 320 During three filter screens 333, complete filter operation, i.e. complete deimpurity operation, after material completes filter operation, then, pass through The described filtration pump housing 340 by the material after filtering, under the effect filtering the pump housing 340, is pulled in backflow body 350, Finally, then be back in upper cover 110, i.e. be back to kettle 100 internal, now, material completes a filter operation, certainly, In order to improve the removal effect of impurity further, according to practical situation, it is also possible to perform circulating filtration operation.
Such as, the first filter screen 331 is arranged towards the direction of the second end of material-pumping tube body 310, and the 3rd filter screen 333 is towards backflow Body 350 is arranged.
Referring to Fig. 2, valve 360 is arranged on backflow body 350, when needs carry out filter operation, opens valve 360, now, material carries out filter operation at material filter 300 internal circulation flow, after completing filter operation, closes valve closing Door 360, now, material stops flowing in material filter 300.
Above-mentioned novel synthesis device 10 by arranging kettle 100, mixing stirring device 200 and material filter 300, and And material filter 300 can be circulated filtration and go the removal of impurity to operate material, go deimpurity operation more simple and convenient, Production efficiency is the highest.
In order to reduce the problem to screen modules impact because of the excessive generation of material pressure, preferably to protect drainage screen Assembly and the dispersion effect of strength imparting material, such as, see also Fig. 3 and Fig. 4, and described novel synthesis device also includes pressure Buffer unit 400, described pressure buffer device 400 is positioned at the first filter screen of described material-pumping tube body 310 and screen modules 330 Between 331, described pressure buffer device 400 includes that some buffering plate bodys 410, some described buffering plate bodys are arranged at intervals at successively In described filter cavity, and all medial walls with described filter box, the edge of some described buffering plate bodys are connected, described buffering Plate body 410 offers flowing hole 411;And for example, described buffering plate body offers some flowing holes;And for example, some described flowing holes Rectangular array is distributed on described buffering plate body;And for example, the described flowing hole of adjacent two described buffering plate bodys shifts to install; And for example, described flowing hole has the cross section of regular polygon structure;And for example, to have regular hexagon structure transversal for described flowing hole Face;And for example, described buffering plate body has cuboid shape structure, so, when material is through pressure buffer device 400, it is possible to subtract Few because of the problem to screen modules impact of the excessive generation of material pressure, preferably to protect screen modules and stiffener The dispersion effect of material.
In order to preferably dismantle described screen modules, so can preferably described screen modules be carried out or Replacement operation, such as, sees also 5, and described novel synthesis device also includes activity provision for disengagement 500, described movable dismounting Device 500 includes locking plate body 510, securing member 520 first is installed plate body 530 and second and installed plate body 540, described filter box 320 offer dismounting window 322, being at least partly embedded in described dismounting window of described locking plate body, and tear open described in closing Unloading window, described securing member wears described locking plate body and the sidewall of described filter box successively, and described first installs plate body First side and described latch are shown consideration for and are closed, described first install the second side of plate body respectively with the side of described first filter screen One side of limit, a side of described second filter screen and described 3rd filter screen connects, and described second installs the first side of plate body Another side with another side of the first filter screen, another side of described second filter screen and described 3rd filter screen is connected respectively, Second side of described installation plate body supports with the medial wall of described filter box.Described locking plate body and described dismounting window Set position and be provided with sealing ring;And for example, described securing member has threaded portion and head, and the first end of described threaded portion is successively Wearing described locking plate body and the sidewall of described filter box, described head is connected with the second end of described threaded portion;And for example, institute State head and there is the cross section of regular hexagon structure;And for example, described locking plate body arrange set portion, described in the portion of setting be embedded at institute State in dismounting window;And for example, described first installation plate body be arranged in parallel with described second installation plate body;And for example, described first filter Net, described second filter screen and described 3rd filter screen are installed plate body with described first and are vertically arranged, so, by described movable dismounting Device 500, it is possible to preferably dismantle described screen modules, so can preferably described screen modules be carried out or Replacement operation.
In order to preferably support described screen modules, for preferably protecting described screen modules, such as, refer to Fig. 6, described novel synthesis device also includes filtering support means 600, and described filtration support means 600 includes the first support rack 610 and second support rack 620, and the described first edge supporting rack is connected with the medial wall of described filter box, and described the One support rack is between described first filter screen and described second filter screen, and described first supports rack offers the first mesh, Described second edge supporting rack is connected with the medial wall of described filter box, and described second supports rack is positioned at described second Between filter screen and described 3rd filter screen, described second supports rack offers the second mesh.The mesh of described first filter screen, described The mesh of the second filter screen and the filter opening size of described 3rd filter screen are sequentially reduced;And for example, described first filter screen, described first support Rack, described second filter screen, described second support rack and described 3rd filter screen be arranged in parallel;And for example, described first mesh The identical setting of size of size and described second mesh;And for example, to be rhombus poroid for described first mesh and described second mesh Structure;And for example, it is provided with interval between described first support rack and described first filter screen and described second filter screen;And for example, Described second supports and is provided with interval between rack and described second filter screen and described 3rd filter screen, so, by arranging the One supports rack 610 and second supports rack 620, it is possible to preferably support described screen modules, for preferably protecting institute State screen modules.
In order to minimizing vortex phenomenon, and flow-disturbing degree when can improve stirring operation, such as, refer to Fig. 7, Described novel synthesis device also includes that baffle means 700, described baffle means 700 include installing the body of rod 710, baffling montant 720 And some baffling cross bars 730, the first end of the described installation body of rod 710 is connected with the medial wall of described low head 120, described baffling Montant is connected with the second end of the described installation body of rod, and some described baffling cross bars are arranged at intervals on described baffling montant successively, And some described baffling cross bars be arranged in parallel.First end of the described installation body of rod is provided with the binding face of arc-shaped curved surface structure, institute State the medial wall laminating of binding face and described low head;And for example, the described installation body of rod is provided with reinforcement;And for example, described reinforcement Muscle is extended to the second end of the described installation body of rod by the first end of the described installation body of rod;And for example, described baffling montant and institute State drive shaft to be arranged in parallel;And for example, described baffling montant has hollow structure;And for example, the end of described baffling cross bar has half Spherical structure, so, by arranging baffle means 700, it is possible to reduces vortex phenomenon, and when can improve stirring operation Flow-disturbing degree.
In order to reduce described drive shaft rotate time, the concussion problem of generation, such as, refer to Fig. 8, described novel synthesis Equipment also includes stirring stopping means 800, and described stirring stopping means 800 includes spacing body 810 and spacing connecting rod 820, Described spacing body 810 is placed on outside the second end of described drive shaft 230, and described spacing body 810 is positioned at described stirring paddle 240 and described low head 120 bottom between, between medial wall and the lateral wall of described drive shaft of described spacing body arrange Interval, the first end of the described spacing body of rod is had to be connected with described spacing body, the second end of the described spacing body of rod and described lower envelope The bottom of head connects, and the bearing of trend of the bearing of trend of the described spacing body of rod and described drive shaft forms angle;And for example, described Stirring paddle is propeller;And for example, described spacing body has rounded cylindrical structure;And for example, the center of described spacing body Axis and the central axes of described drive shaft;And for example, described stirring stopping means arranges some described spacing connecting rods, if Dry described spacing connecting rod radially puts distribution with the center of described drive shaft;And for example, described stirring stopping means arranges two Individual described spacing connecting rod, forms angle between two described spacing connecting rods;And for example, the number of degrees of described angle be 60 degree~ 120 degree, so, by arrange stirring stopping means 800, it is possible to reduce described drive shaft rotate time, the concussion problem of generation.
When it is pointed out that being stirred each material of married operation inside described kettle carries out combination reaction, and Most combination reaction is all exothermic reaction, and the productivity that the speed of reaction and product generate is also required to releasing during dependent reaction Heat, is used for improving reaction rate and productivity.Additionally, in whipping process, material can be done work, i.e. by described mixing stirring device Material, during being mutually mixed agitation, shows as outwardly releasing the material that heat, especially toughness are stronger, its heat release Phenomenon becomes apparent from, and therefore, based on above-mentioned situation, relies on the combination reaction of higher temperature for some, as depended on reaction self Heat release and the combination reaction of stirring heat production, and need not extra heater for the reaction that it heats, it is especially desirable to Guarantee the heat-insulating property of described kettle.Further, in order to for some acid materials, therefore, to assure that the inner side of described kettle Wall, the medial wall of the described kettle i.e. directly contacted with acid material possesses higher resistance to acid attack performance, is used for prolonging raw described still The service life of body and being normally carried out of reaction.Further, the lateral wall of described kettle is owing to often connecing with corrosive materials Touching, e.g., the corrosive materials contact of the form such as gaseous state or liquid, it is therefore desirable to possess preferable decay resistance, for more preferably Described kettle is protected on ground.
In order to improve resistance to acid attack performance, heat-insulating property and the decay resistance of described kettle, such as, refer to Fig. 8, described Kettle, e.g., resistance to acid attack layer 130 that the sidewall of described kettle includes being cascading, heat-insulation layer 140, supporting layer 150, counterweight Layer 160 and protective layer 170, described resistance to acid attack layer is positioned at the medial wall of described kettle, and described resistance to acid attack layer is direct and material, As, acid material contact, described protective layer is positioned at the lateral wall of described kettle, and the most described protective layer is the most naked to be exposed on the external.
Such as, the described resistance to acid attack layer of an embodiment includes each component of following mass parts: ferrum 75 parts~88 parts, titanium 30 Part~34 parts, chromium 20 parts~25 parts, antimony 2.5~3.4 parts, copper part 2.3~3.4 parts, 1.5 parts~2.7 parts of zinc, aluminum 0.9~1.4 Part, 0.15 part~0.27 part of carbon, silicon 0.25 part~0.46 part, boron 0.12 part~0.18 part, cobalt 0.04 part~0.09 part, phosphorus 0.001 part~0.03 part, sulfur 0.001 part~0.03 part, 0.02 part~0.03 part of strontium, bismuth 0.03 part~0.04 part, scandium 0.01 part ~0.02 part and gadolinium 0.001 part~0.002 part.Wherein, scandium is scandium or contains scadium compound, wherein, is contained within scandium containing scadium compound Element;Gadolinium is gadolinium or contains gadolinium compound, wherein, is contained within gadolinium element containing gadolinium compound;Bismuth is bismuth or bismuth-containing compound, wherein, Bismuth gadolinium compound is contained within bismuth element;Strontium is strontium or contains strontium compound, and wherein, strontium gadolinium compound is contained within strontium element.
Use ferrum 75 parts~88 parts, titanium 30 parts~34 parts and 20 parts~25 parts infrastructure elements as resistance to acid attack layer of chromium, from And described resistance to acid attack layer can be made to possess certain resistance to acid attack performance, additionally, by adding antimony 2.5~3.4 parts, copper 2.3 parts ~3.4 parts, 1.5 parts~2.7 parts of zinc, aluminum 0.9~1.4 parts, cobalt 0.04 part~0.09 part, 0.02 part~0.03 part of strontium, bismuth 0.03 Part~0.04 part, scandium 0.01 part~0.02 part and gadolinium 0.001 part~0.002 part compound, additionally it is possible to optimize described further The properties of resistance to acid attack layer, especially can optimize the resistance to acid attack performance of described resistance to acid attack layer further such that it is able to more preferably The acid etching of ground opposing material, for improving the service life of described kettle further and guaranteeing being normally carried out of reaction.
And for example, the described resistance to acid attack layer of another embodiment includes each component of following mass parts: ferrum 75 parts~80 parts, titanium 33 parts~34 parts, chromium 24 parts~25 parts, antimony 2.7~3.4 parts, copper 2.7 parts~3.4 parts, 1.8 parts~2.5 parts of zinc, aluminum 1.1~1.4 Part, 0.18 part~0.27 part of carbon, silicon 0.27 part~0.46 part, boron 0.13 part~0.18 part, cobalt 0.04 part~0.09 part, phosphorus 0.001 part~0.03 part, sulfur 0.001 part~0.03 part, 0.02 part~0.03 part of strontium, bismuth 0.03 part~0.04 part, scandium 0.01 part ~0.02 part and gadolinium 0.001 part~0.002 part.
And for example, the described resistance to acid attack layer of another embodiment includes each component of following mass parts: ferrum 77 parts, titanium 33 parts, Chromium 25 parts, 3.4 parts of antimony, copper 2.7 parts, 1.9 parts of zinc, 1.3 parts of aluminum, 0.27 part of carbon, silicon 0.46 part, boron 0.18 part, cobalt 0.04 part, phosphorus 0.03 part, sulfur 0.001 part, 0.03 part of strontium, bismuth 0.04 part, scandium 0.01 part and gadolinium 0.002 part.
Such as, the described heat-insulation layer of an embodiment includes each component of following mass parts: Gypsum Fibrosum powder 15 parts~22 parts, white Cotton 8~20 parts, rock wool 8 parts~15 parts, glass fibre 7 parts~9 parts, Lauxite 10 parts~20 parts, polyacrylamide 3.5 parts~ 4.5 parts, basalt fibre 1 part~3 parts, rubber foam 3~5 parts, 1 part~2 parts of magnesium hydroxide, aminopropyl triethoxysilane 1 Part~2 parts, aluminium oxide 1 part~2 parts, 3,5-di-tert-butyl-4-hydroxybenzoic acid methyl ester 1 part~2 parts, polypropylene fiber 3~4 parts, Thiorubber. 1 part~2 parts and sodium lauryl sulphate 0.2~0.8 part.
The each component using as above mass parts can make described heat-insulation layer have good heat-insulating property, when in described kettle During the material generation exothermic reaction in portion, and after transferring heat to described resistance to acid attack layer, have good based on described heat-insulation layer Heat insulation and heat-insulating property, can limit heat and be further transmitted through described kettle, and then avoid heat to be transferred directly to external environment In, it is ensured that the material within described kettle reacts at a suitable temperature, for improving the product of reaction rate and product Rate.
And for example, the described heat-insulation layer of another embodiment includes each component of following mass parts: Gypsum Fibrosum powder 17 parts~21 parts, White cotton 17~20 parts, rock wool 10 parts~15 parts, glass fibre 7 parts~9 parts, Lauxite 10 parts~20 parts, polyacrylamide 3.5 Part~4.5 parts, basalt fibre 1 part~2.5 parts, rubber foam 3.5~5 parts, 1.5 parts~2 parts of magnesium hydroxide, aminopropyl three second TMOS 1.5 parts~2 parts, aluminium oxide 1 part~2 parts, 3,5-di-tert-butyl-4-hydroxybenzoic acid methyl ester 1 part~1.4 parts, third Synthetic fibre fiber 3.3~4 parts, thiorubber. 1 part~2 parts and sodium lauryl sulphate 0.2~0.5 part.
And for example, the described heat-insulation layer of another embodiment includes each component of following mass parts: Gypsum Fibrosum powder 19 parts, white cotton 17 ~20 parts, rock wool 15 parts, glass fibre 9 parts, Lauxite 20 parts, polyacrylamide 3.8 parts, basalt fibre 2.1 parts, rubber Foam 4.6 parts, 1.7 parts of magnesium hydroxide, aminopropyl triethoxysilane 2 parts, aluminium oxide 1.8 parts, 3,5-di-t-butyl-4-hydroxyl Essence of Niobe 1.4 parts, polypropylene fiber 4 parts, thiorubber. 1.9 parts and sodium lauryl sulphate 0.4 part.
Such as, the described supporting layer of an embodiment includes each component of following mass parts: ferrum 95 parts~98 parts, manganese 0.4 Part~0.95 part, molybdenum 0.1 part~0.5 part, titanium 0.01 part~0.05 part, 0.02 part~0.1 part of aluminum, 0.06 part~0.25 part of carbon, Silicon 0.1 part~0.3 part, 0.05 part~0.1 part of phosphorus, boron 0.001 part~0.01 part, hafnium 0.05 part~0.5 part, scandium 0.05 part~ 0.3 part, chromium 0.05 part~0.3 part, 0.01 part~0.05 part of nickel, cerium 0.01 part~0.05 part, thorium 0.01 part~0.05 part and zirconium 0.01 part~0.05 part.Wherein, hafnium is hafnium or contains hafnium compound, wherein, is contained within hafnium element containing hafnium compound;Scandium is scandium or contains Scadium compound, wherein, is contained within scandium element containing scadium compound;Thorium is thorium or contains thorium compound, and wherein, cerium-containing compound is contained within Ce elements;Cerium is cerium or cerium-containing compound, and wherein, cerium-containing compound is contained within Ce elements.
It is appreciated that to make described kettle possess preferable heat-insulating property, needs to introduce described heat-insulation layer, and described guarantor The mechanical strength of temperature layer is poor, in order to strengthen the integrally-built mechanical strength of described kettle, needs to introduce described supporting layer so that it is Directly contact with described heat-insulation layer, be used for improving the integrally-built mechanical strength of described kettle, to reach the purpose of safety in production. Based on above-mentioned situation, this is necessary for requiring that described supporting layer possesses higher mechanical strength and anti-deformation nature, by using such as Improving quality each component of part, the most described supporting layer contains hafnium 0.05 part~0.5 part, scandium 0.05 part~0.3 part, chromium 0.05 part ~0.3 part, 0.01 part~0.05 part of nickel, cerium 0.01 part~0.05 part, thorium 0.01 part~0.05 part and zirconium 0.01 part~0.05 part, The mechanical strength of conventional iron alloy can be improved so that it is mechanical strength and anti-deformation nature are more excellent, it is possible to meet requirement.
And for example, the described supporting layer of another embodiment includes each component of following mass parts: ferrum 97 parts~98 parts, manganese 0.55 part~0.95 part, molybdenum 0.35 part~0.5 part, titanium 0.01 part~0.05 part, 0.02 part~0.1 part of aluminum, 0.17 part of carbon~ 0.25 part, silicon 0.1 part~0.25 part, 0.05 part~0.1 part of phosphorus, boron 0.008 part~0.01 part, hafnium 0.1 part~0.5 part, scandium 0.1 Part~0.3 part, chromium 0.1 part~0.3 part, 0.02 part~0.05 part of nickel, cerium 0.02 part~0.05 part, thorium 0.02 part~0.05 part and Zirconium 0.02 part~0.05 part.
And for example, the described supporting layer of another embodiment includes each component of following mass parts: ferrum 97 parts, 0.75 part of manganese, Molybdenum 0.5 part, titanium 0.05 part, 0.02 part of aluminum, 0.17 part of carbon, silicon 0.25 part, 0.1 part of phosphorus, boron 0.008 part, hafnium 0.5 part, scandium 0.2 Part, chromium 0.2 part, 0.05 part of nickel, cerium 0.05 part, thorium 0.05 part and zirconium 0.05 part.
Such as, the described weight coating of an embodiment includes each component of following mass parts: 85 parts~95 parts of tungsten, 30 parts of nickel ~60 parts, ferrum 15 parts~40 parts, chromium 1.5 parts~10 parts, 1.5 parts~10 parts of lead, copper 1 part~6 parts and molybdenum 0.5 part~5 parts.
It is appreciated that in producing course of reaction, needs the material in described kettle carries out the stirring behaviour that intensity is higher Make, and the existence of the described heat-insulation layer of and lighter weight relatively big due to thickness, in order to avoid the integrally-built matter of described kettle Amount kicks the beam, and then reduces the external impacts impact on described kettle, i.e. can reduce described kettle and concussion or displacement problem occur. The each component using as above mass parts can make described weight coating possess excellent counterweight performance, it is possible to effectively increases described still The integrally-built weight of body so that it is identical or adaptive with the weight of traditional kettle, such that it is able to the peace improved in production process Full performance.
And for example, the described weight coating of another embodiment includes each component of following mass parts: 90 parts~95 parts of tungsten, nickel 30 Part~45 parts, ferrum 27 parts~40 parts, chromium 1.5 parts~2.3 parts, 1.5 parts~3.3 parts of lead, copper 1 part~5.5 parts and molybdenum 0.5 part~ 4.9 part.
And for example, the described weight coating of another embodiment includes each component of following mass parts: 92 parts of tungsten, 38 parts of nickel, ferrum 29 parts, chromium 2.1 parts, 2.1 parts of lead, copper 3.5 parts and molybdenum 3.8 parts.
Such as, the described protective layer of an embodiment includes each component of following mass parts: ferrum 65 parts~80 parts, lithium 16~ 18 parts, 18 parts~25 parts of nickel, molybdenum 3.5 parts~4 parts, chromium 2 parts~5 parts, cobalt 1 part~5 parts, vanadium 1 part~5 parts, 1 part~2 parts of manganese, iridium 0.8 part~2.5 parts, niobium 0.5 part~2.5 parts, scandium 0.3 part~2.5 parts, 0.2 part~2.5 parts of strontium, caesium 0.2 part~2.5 parts, tungsten 0.2 part~2.5 parts and titanium 0.2 part~2.5 parts.Wherein, caesium is caesium or contains cesium compound, wherein, is contained within caesium containing cesium compound Element;Wherein, strontium is strontium or contains strontium compound, wherein, is contained within strontium element containing strontium compound;Wherein, scandium is scandium or contains scandium Compound, wherein, is contained within scandium element containing scadium compound;Wherein, niobium is niobium or contains niobium compound, wherein, includes containing niobium compound There is niobium element;Wherein, iridium is iridium or contains iridic compound, wherein, is contained within iridium containing iridic compound.
Be appreciated that the lateral wall of described kettle owing to often contacting with corrosive materials, e.g., the form such as gaseous state or liquid Corrosive materials contact, it is therefore desirable to possess preferable decay resistance, for preferably protecting described kettle.By as above Each component of mass parts, can make described protective layer possess good Corrosion Protection, and then preferably protect described kettle, uses The service life extending described kettle.
And for example, the described protective layer of another embodiment includes each component of following mass parts: ferrum 65 parts~70 parts, lithium 16 Part~16.5 parts, nickel 18~21 parts, molybdenum 3.5 parts~3.9 parts, chromium 2 parts~4.4 parts, cobalt 1 part~3.9 parts, vanadium 1 part~4.5 parts, 1 part~1.7 parts of manganese, 0.8 part~2.3 parts of iridium, niobium 0.5 part~2.2 parts, scandium 0.3 part~2.3 parts, 0.2 part~2.3 parts of strontium, caesium 0.2 part~2.4 parts, 0.2 part~2.1 parts of tungsten and titanium 0.2 part~1.9 parts.
And for example, the described protective layer of another embodiment includes each component of following mass parts: ferrum 65 parts, lithium 16.5 parts, 21 parts of nickel, molybdenum 3.5 parts, chromium 3.5 parts, cobalt 2.8 parts, vanadium 3.7 parts, 1.5 parts of manganese, 2.3 parts of iridium, niobium 2.2 parts, scandium 2.3 parts, strontium 2.3 Part, caesium 2.4 parts, 0.2 part of tungsten and titanium 0.2 part.
In order to optimize described kettle further, e.g., the structure of the sidewall of described kettle, such as, described resistance to acid attack layer, described The thickness of heat-insulation layer, described supporting layer, described weight coating and described protective layer is than being (1~1.5): (15~20): (5~5.5): (8~9.8): (0.5~1.2);And for example, the thickness of described weight coating and described protective layer is than for 1:15:5:9.5:1.1.
It should be noted that other embodiments of the present invention also include that the technical characteristic in the various embodiments described above be combined with each other Can be formed, and the novel synthesis device that can implement.
Each technical characteristic of embodiment described above can combine arbitrarily, for making description succinct, not to above-mentioned reality The all possible combination of each technical characteristic executed in example is all described, but, as long as the combination of these technical characteristics is not deposited In contradiction, all it is considered to be the scope that this specification is recorded.
The above embodiment only have expressed the several embodiments of the present invention, and it describes more concrete and detailed, but Therefore the restriction to the scope of the claims of the present invention can not be interpreted as.It should be pointed out that, for the ordinary skill people of this area For Yuan, without departing from the inventive concept of the premise, it is also possible to make some deformation and improvement, these broadly fall into the present invention's Protection domain.Therefore, the protection domain of patent of the present invention should be as the criterion with claims.

Claims (7)

1. a novel synthesis device, it is characterised in that including:
Kettle, the two ends of described kettle are respectively arranged with upper cover and low head;
Mixing stirring device, described mixing stirring device includes installation frame, drives motor, drive shaft and stirring paddle, described peace Installation frame is fixedly mounted on described upper cover, and described driving motor is arranged on described installation frame, the of described drive shaft One end is connected with the rotary shaft of described driving motor, and the second end of described drive shaft is connected with described stirring paddle, and described stirring Oar is positioned at inside described low head;
Material filter, described material filter includes material-pumping tube body, filter box, screen modules, the filtration pump housing, returns Flow tube body and valve, the first end of described material-pumping tube body connects with the bottom of described low head, and described filter box hollow is arranged, Forming filter cavity in it, the second end of described material-pumping tube body is connected with the first end of described filter box, and described material-pumping tube Second end of body connects with described filter cavity, and described screen modules includes the first filter screen, the second filter screen and the 3rd filter screen, institute State the first filter screen, described second filter screen and described 3rd filter screen to be arranged at intervals at successively in described filter cavity, described first filter All medial walls with described filter box, the edge of edge, the edge of described second filter screen and described 3rd filter screen of net are connected, Described first filter screen is arranged towards the direction of the second end of described material-pumping tube body, the feed end of the described filtration pump housing and described filtration Second end of casing connects, and described filtration pump housing feed end connects with described filter cavity, the discharge end of the described filtration pump housing Connecting with the first end of described backflow body, the second end of described backflow body connects with described upper cover, and described valve is arranged On described backflow body;And
Filtering support means, described filtration support means includes that the first support rack and second supports rack, and described first supports The edge of rack is connected with the medial wall of described filter box, and described first supports rack is positioned at described first filter screen and described the Between two filter screens, described first supports rack offers the first mesh, and described second supports the edge of rack and described Rose Box The medial wall of body connects, and described second supports rack between described second filter screen and described 3rd filter screen, described second Support rack offers the second mesh.
Novel synthesis device the most according to claim 1, it is characterised in that the mesh of described first filter screen, described second The mesh of filter screen and the filter opening size of described 3rd filter screen are sequentially reduced.
Novel synthesis device the most according to claim 1, it is characterised in that described first filter screen, described first supporting network Frame, described second filter screen, described second support rack and described 3rd filter screen be arranged in parallel.
Novel synthesis device the most according to claim 1, it is characterised in that the size of described first mesh and described second The identical setting of size of mesh.
Novel synthesis device the most according to claim 1, it is characterised in that described first mesh and described second mesh are equal For rhombus cavernous structure.
Novel synthesis device the most according to claim 1, it is characterised in that described first supports rack and described first filter It is provided with interval between net and described second filter screen.
Novel synthesis device the most according to claim 1, it is characterised in that described second supports rack and described second filter It is provided with interval between net and described 3rd filter screen.
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Citations (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN103083973A (en) * 2011-11-05 2013-05-08 海门市大生水处理设备(厂)有限公司 Air-liquid pipeline filter
CN205055928U (en) * 2015-09-15 2016-03-02 山东东源新材料科技有限公司 Produce no vanadium tombarthite base titanium and tungsten powder's stirring mixing apparatus

Patent Citations (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN103083973A (en) * 2011-11-05 2013-05-08 海门市大生水处理设备(厂)有限公司 Air-liquid pipeline filter
CN205055928U (en) * 2015-09-15 2016-03-02 山东东源新材料科技有限公司 Produce no vanadium tombarthite base titanium and tungsten powder's stirring mixing apparatus

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