CN205948882U - Chemical reaction equipment - Google Patents
Chemical reaction equipment Download PDFInfo
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- CN205948882U CN205948882U CN201620686774.9U CN201620686774U CN205948882U CN 205948882 U CN205948882 U CN 205948882U CN 201620686774 U CN201620686774 U CN 201620686774U CN 205948882 U CN205948882 U CN 205948882U
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Abstract
The utility model provides a chemical reaction equipment, includes vertical barrel body, agitating unit, feeding device and material dispersion devices. Vertical barrel body's both ends are provided with upper cover and low head respectively. Agitating unit includes supporting seat, driving motor, power output shaft and stirring rake. Feeding device includes the material leaking tube body, the conveying pipeline body, the reinforced pump body, reinforced body and a plurality of material subassembly of throwing. Material dispersion devices holding is inside vertical barrel body, and material dispersion devices includes connection tube and dispersion framework. Above -mentioned highly efficient reaction device is through setting up vertical barrel body, agitating unit and feeding device to control joining opportunity well, a plurality of material subassemblies of throwing to feeding device drop into the effects that continuous type feeding operation can be realized to the material again, and feeding operation is simple convenient and feeding efficiency is higher.
Description
Technical field
This utility model is related to chemical production equipment field, more particularly to a kind of chemical reaction equipment.
Background technology
At present, in material production field, it usually needs adopt consersion unit, e.g., need using as vertical response equipment,
The container being carried when vertical cylinder consersion unit or vertical vertical cylinder consersion unit are as material generation chemical reaction, it is wide
General it is applied to the industries such as oil, chemical industry, rubber, pesticide, dyestuff, medicine and food.
In some special occasions, typically the region that feeds intake of consersion unit is arranged on floor or platform, i.e. reaction sets
Standby dog-house is normally at the top of consersion unit or at the position at top, when needs add liquid object to consersion unit
During material, need in advance material to be transported on floor or platform, lead to feeding operation more complicated, charging is less efficient.
Additionally, existing consersion unit, in order to ensure the mechanical strength of itself, typically will not arrange excessive dog-house, just
This leads to existing consersion unit it is more difficult to realize the operation of continuous way charging, that is, in the same time relatively difficult to achieve or interval time
Shorter interior, add the operation of various materials.
Utility model content
Based on this it is necessary to provide that a kind of feeding operation is more simple and convenient, efficiency is higher and the company of being capable of for charging
The chemical reaction equipment of continuous formula feeding operation.
A kind of chemical reaction equipment, including:
Vertical cylinder, the two ends of described vertical cylinder are respectively arranged with upper cover and low head;
Agitating device, described agitating device includes support base, motor, power output shaft and stirring paddle, described support
Seat is fixedly mounted on described upper cover, and the first end of described power output shaft is connected with the rotary shaft of described motor, institute
The second end stating power output shaft stretches to inside described vertical cylinder, the second end of described power output shaft and described stirring paddle
Connect, described motor is used for driving described stirring paddle to rotate;
Feeding device, described feeding device includes material leakage body, conveying body, the charging pump housing, charging body and multiple throwing
Material assembly, the first end of described material leakage body connects with described upper cover, the second end of described material leakage body and described conveying pipeline
The first end connection of body, the second end of described conveying body is connected with the discharge end of the described charging pump housing, the described charging pump housing
Feed end is connected with described charging body, and multiple described assemblies that feed intake are arranged at intervals on described charging body successively, and multiple
The described assembly that feeds intake all is connected with described charging body, and the described assembly that feeds intake includes feed intake body, cast hopper and the valve that feeds intake, institute
The first end stating the body that feeds intake is connected with described charging body, and the second end of the described body that feeds intake is connected with described cast hopper, institute
State cast hopper and offer dog-house, the described valve that feeds intake be arranged at described in feed intake on body;And
Material dispersing device, described material dispersing device is placed in inside described vertical cylinder, described material dispersing device
Including connector drum and dispersion framework, the first end of described connector drum is connected with the first end of described material leakage body, described point
Scattered framework has hollow structure, forms distribution cavity in it, and the second end of described connector drum is connected with described dispersion framework, and
And the second end of described connector drum is connected with described distribution cavity, described dispersion framework is opened away from one end of described connector drum
It is provided with the dispersion hole that some and described distribution cavity connects, some described dispersion hole are all towards the direction setting of described low head.
Wherein in an embodiment, described dispersion framework has the columnar structured of hollow.
Wherein in an embodiment, some described dispersion hole are divided with the central axis circular array of described dispersion framework
Cloth.
Wherein in an embodiment, described dispersion hole has the cross-sectional structure of regular polygon.
Wherein in an embodiment, described dispersion hole has the cross-sectional structure of regular hexagon structure.
Wherein in an embodiment, the first end of described connector drum is spirally connected with the first end of described material leakage body.
Wherein in an embodiment, described connector drum has rounded cylindrical structure.
Above-mentioned highly effective reaction device passes through to arrange vertical cylinder, agitating device and feeding device, and when controlling addition
Machine, then put into, to multiple assemblies that feed intake of feeding device, the effect that material can realize continuous way feeding operation, and feeding operation
More simple and convenient and charging efficiency is higher.
Brief description
Fig. 1 is the structural representation of the chemical reaction equipment of this utility model one embodiment;
Fig. 2 is enlarged drawing at A for the Fig. 1;
Fig. 3 is the partial structural diagram of the chemical reaction equipment of another embodiment of this utility model;
Fig. 4 is the partial structural diagram of the chemical reaction equipment of another embodiment of this utility model;
Fig. 5 is the partial structural diagram of the chemical reaction equipment of another embodiment of this utility model;
Fig. 6 is the partial structural diagram of the chemical reaction equipment of another embodiment of this utility model;
Fig. 7 is the partial structural diagram of the chemical reaction equipment of another embodiment of this utility model;
Fig. 8 is the partial structural diagram of the chemical reaction equipment of another embodiment of this utility model.
Specific embodiment
For the ease of understanding this utility model, below with reference to relevant drawings, this utility model is more fully retouched
State.Better embodiment of the present utility model is given in accompanying drawing.But, this utility model can come in many different forms
Realize however it is not limited to embodiments described herein.On the contrary, providing the purpose of these embodiments to be to make to this practicality newly
It is more thoroughly comprehensive that the disclosure of type understands.
It should be noted that when element is referred to as " being fixed on " another element, it can be directly on another element
Or can also there is element placed in the middle.When an element is considered as " connection " another element, it can be directly connected to
To another element or may be simultaneously present centering elements.Term as used herein " vertical ", " level ", " left ",
For illustrative purposes only, being not offered as is unique embodiment for " right " and similar statement.
Unless otherwise defined, all of technology used herein and scientific terminology are led with belonging to technology of the present utility model
The implication that the technical staff in domain is generally understood that is identical.In term used in the description of the present utility model it is simply herein
The purpose of description specific embodiment is it is not intended that in limiting this utility model.Term as used herein " and/or " bag
Include the arbitrary and all of combination of the Listed Items of one or more correlations.
For example, a kind of chemical reaction equipment, including:Vertical cylinder, the two ends of described vertical cylinder are respectively arranged with envelope
Head and low head;Agitating device, described agitating device includes support base, motor, power output shaft and stirring paddle, described
Support seat is fixedly mounted on described upper cover, and the first end of described power output shaft is connected with the rotary shaft of described motor,
Second end of described power output shaft stretches to inside described vertical cylinder, the second end of described power output shaft and described stirring
Oar connects, and described motor is used for driving described stirring paddle to rotate;Feeding device, described feeding device include material leakage body,
Conveying body, the charging pump housing, charging body and multiple assembly that feeds intake, the first end of described material leakage body is with described upper cover even
Logical, the second end of described material leakage body is connected with the first end of described conveying body, the second end of described conveying body with described
The discharge end connection of the charging pump housing, the feed end of the described charging pump housing is connected with described charging body, multiple described assemblies that feed intake
It is arranged at intervals at successively on described charging body, and multiple described assembly that feeds intake all is connected with the described body that feeds, and described feeds intake
Assembly includes feed intake body, cast hopper and the valve that feeds intake, and the first end of the described body that feeds intake is connected with described charging body, described
Feed intake the second end of body is connected with described cast hopper, and described cast hopper offers dog-house, and the described valve that feeds intake is arranged at institute
State and feed intake on body;And material dispersing device, described material dispersing device is placed in inside described vertical cylinder, and described material divides
In bulk put including connector drum and dispersion framework, the first end of described connector drum connected with the first end of described material leakage body,
Described dispersion framework has hollow structure, forms distribution cavity, the second end of described connector drum and described dispersion framework in it
Connect, and the second end of described connector drum is connected with described distribution cavity, described dispersion framework is away from described connector drum
One end offer the dispersion hole that some and described distribution cavity connects, some described dispersion hole are all towards the side of described low head
To setting.
In order to explain to above-mentioned chemical reaction equipment further, for example, the chemical reaction of another embodiment
Equipment is as follows:
Refer to Fig. 1, highly effective reaction device 10 includes vertical cylinder 100, agitating device 200 and feeding device 300, stirring
Device 200 and feeding device 300 may be contained within vertical cylinder 100.
Refer to Fig. 1, the two ends of vertical cylinder 100 are respectively arranged with upper cover 110 and low head 120, vertical cylinder 100
For the accommodating material adding, and to material mix and blend and the offer occasion that reacts.For example, upper cover 110 and low head
Form vertical cylinder 100 after 120 connections.And for example, described vertical cylinder is formed in one structure.And for example, in described vertical cylinder
Be installed on outside support during, the top of the externally-located support of described upper cover, the externally-located support of described low head
Bottom.
Refer to Fig. 1, agitating device 200 includes support base 210, motor 220, power output shaft 230 and stirring paddle
240, support base 210 is fixedly mounted on the upper cover 110 of vertical cylinder 100, and the first end of power output shaft 230 is electric with driving
The rotary shaft of machine 220 connects, and the second end of power output shaft 230 stretches to inside vertical cylinder 100, e.g., power output shaft 230
The second end stretch to inside the low head 120 of vertical cylinder 100, the second end of power output shaft 230 and stirring paddle 240 are even
Connect, e.g., stirring paddle 240 is located inside the low head 120 of vertical cylinder 100, and motor 220 is used for driving power output shaft
230 rotations, and then drive the stirring paddle 240 fixing with power output shaft 230 to rotate.Thing in the vertical cylinder 100 of needs
When material is stirred married operation, controls motor 220 to drive power output shaft 230 to rotate, and then drive 240 turns of stirring paddle
Dynamic, using the flow-disturbing effect of stirring paddle 240, preferable stirring immixture can be played, and then can be with vertical cylinder 100
Material be stirred married operation.
See also Fig. 1 and Fig. 2, feeding device 300 includes material leakage body 310, conveying body 320, the charging pump housing
330th, charging body 340 and multiple assembly 350 that feeds intake, upper cover 110, material leakage body 310, conveying body 320, the charging pump housing
330th, charging body 340 and the assembly 350 that feeds intake be sequentially connected, and for example, upper cover 110, material leakage body 310, conveying body 320,
The charging pump housing 330, charging body 340 and the assembly 350 that feeds intake are sequentially communicated.
Refer to Fig. 1, the first end of material leakage body 310 is connected with upper cover 110, the second end of material leakage body 310 with defeated
The first end connection of expects pipe body 320, the second end of conveying body 320 is connected with the discharge end of the charging pump housing 330, and feed the pump housing
330 feed end is connected with charging body 340, and multiple assemblies 350 that feed intake are arranged at intervals on charging body 340 successively, and many
The individual assembly 350 that feeds intake all is connected with charging body 340, when needing to add material in vertical cylinder 100, only need to be to the group that feeds intake
Part 350 puts into material and can complete whole feeding operation, and feeding operation is more simple and convenient and the efficiency that feeds is higher, and without volume
These regions that feed intake of outer setting floor or platform etc. are it is achieved that exempt from the effect of high-order charging that is to say, that working as to the assembly that feeds intake
During 350 input material, based on the draft of the charging pump housing 330, add the material of the assembly 350 that feeds intake can enter to charging body 340
Interior, afterwards, material passes through the charging pump housing 330 again and enters in conveying body 320, and then, material is entered by conveying body 320 again
To material leakage body 310, finally, material enters in the upper cover 110 of vertical cylinder 100 by material leakage body 310 again, Jin Erjin
Enter to whole vertical cylinder 100, now, complete whole feeding operation, only need to put into the assembly 350 that feeds intake or add material
Whole feeding operation can be completed, feeding operation is simple and convenient and the efficiency that feeds is higher.Further, since material leakage body 310, conveying
The assembly 350 that feeds intake can be arranged far from the region of vertical cylinder 100 by body 320 and the presence of charging body 340, for example,
Due to the presence of material leakage body 310, conveying body 320 and charging body 340, assembly 350 setting that feeds intake can be convenient for
On the ground of dosing operation or be arranged in weighing area, so, it is possible to achieve exempt from the effect that a high position feeds intake and exempts from feeding platform.
Refer to Fig. 2, the assembly 350 that feeds intake includes feed intake body 351, cast hopper 352 and the valve 353 that feeds intake, and feed intake body
351 first end is connected with charging body 340, and the second end of the body 351 that feeds intake is connected with cast hopper 352, and cast hopper 352 opens up
There is dog-house 354, the valve 353 that feeds intake is arranged at and feeds intake on body 351.For example, described feeding device arrange three described in feed intake
Assembly, as such, it is possible to be simultaneously introduced three kinds of materials, and then realizes the effect of continuous way feeding operation, certainly, the described assembly that feeds intake
Number be not limited to three, for example, it is also possible to be adjusted according to practical situation, e.g., each described a pair of assembly 1 of feeding intake
Should a kind of material participating in reaction.
When need the same time in or interval time shorter interior, to the inside of vertical cylinder 100 add various materials when, this
When, it is simultaneously introduced the species of material as needed, a number of valve 353 that feeds intake of corresponding unlatching, then, to multiple cast hoppers
352 dog-house 354 is corresponding to put into various materials, opens the charging pump housing 330, based on the swabbing action of the charging pump housing 330, material
Along cast hopper 352- feed intake body 351- charging body 340- charging pump housing 330- conveying body 320- material leakage body 310- stand
The charging path of formula cylinder 100 enters in vertical cylinder 100, now, completes whole feeding operation.
When needing to add a kind of material inside to vertical cylinder 100, now, open the dog-house of a cast hopper 352
354 and corresponding put into this material, and close remaining valve 353 that feeds intake, material adds along the cast hopper 352- body 351- that feeds intake
The charging path of expects pipe body 340- charging pump housing 330- conveying body 320- material leakage body 310- vertical cylinder 100 enters to vertical
In cylinder 100, now, complete whole feeding operation.
Above-mentioned highly effective reaction device 10 passes through to arrange vertical cylinder 100, agitating device 200 and feeding device 300, and controls
Make addition opportunity, then put into material to multiple assemblies 350 that feed intake of feeding device 300 and can realize continuous way feeding operation
Effect, and feeding operation is more simple and convenient and charging efficiency is higher.
In order to preferably close described cast hopper, to reduce the amount that the material in described cast hopper evaporates into the external world, for example,
Refer to Fig. 3, described highly effective reaction device also includes locking device 400, locking device 400 includes rotary shaft 410 and closing door
420, described rotary shaft rotates and is arranged at the marginal position of described dog-house of cast hopper 352, described closing door and described rotation
Rotating shaft is fixedly connected, and described closing door is used for closing described dog-house, and the edge of described closing door is provided with sealing ring, described close
Seal is supported with the edge of described dog-house;And for example, described dog-house has the cross section of circular configuration;And for example, described closing
Door has circular pan-like structure;And for example, described sealing ring has circular annular form structure;And for example, described closing door is away from described rotation
It is provided with balancing weight at the position of rotating shaft;And for example, described sealing ring offers seal groove towards the side of described dog-house, described
The edge of dog-house is embedded inside described seal groove;And for example, described seal groove has loop configuration, so, using closing dress
The closing door 420 putting 400 can preferably close described cast hopper, evaporates into the external world to reduce the material in described cast hopper
Amount.
In order to put into material preferably into described cast hopper, for example, refer to Fig. 4, described highly effective reaction device also wraps
Include material injection device 500, described material injection device 500 includes sealing plate 510, first injection body 520 and the second injection
Body 530, described sealing plate covers on the described dog-house of cast hopper 352, and is used for closing described dog-house, and described
The first end of one injection body is connected with described sealing plate, and the first end of described first injection body is with described cast hopper even
Logical, the second end of described first injection body is flexibly connected with the first end of the described second injection body, described second ascending pipe
Second end of body is used for connecting with outside material injection device, e.g., connects with outside charging bucket, described charging bucket is equipped with
Material;And for example, the lateral wall at the second end of described first injection body offers external screw thread, and described second injects the second of body
The medial wall at end offers female thread, described female thread and described external thread bolt connection;And for example, the second of described first injection body
End is provided with hoop component with the junction of the first end of described second injection body;And for example, described hoop component includes clip
Body and connecting screw rod, described clip body is arranged at the second end of described first injection body and described second injection body
The junction of first end, the two ends of described connecting screw rod are spirally connected with the two ends of described clip body respectively;And for example, described clip basis
Body has arcuate structure;And for example, described clip body is provided with reinforcement, described reinforcement is by one end of described clip body
Extend to the other end of described clip body;And for example, described reinforcement has semicircular structure cross section, so, only need to outward
The material injection device in portion is connected with the second end of the described second injection body and can complete dosing operation such that it is able to preferably
Material is put into into described cast hopper.
It is appreciated that when adding excessive material to described cast hopper it is possible to cause described cast hopper that flash occurs
Problem, in order that described cast hopper preferably enters row buffering to material, with reduce flash problem occur, for example, refer to
Fig. 5, described highly effective reaction device also includes material buffer device 600, described material buffer device 600 include buffering bucket 610 and
Cover plate 620, described buffering bucket 610 has the structure of the shaped hollow round table of both ends open, and the bottom opening of described buffering bucket 610 is solid
Surely it is placed on described cast hopper 352 and at the position of the neighbouring described body that feeds intake, described cover plate has loop configuration, described lid
The outer ledge of plate is connected with the open-topped marginal position of described buffering bucket, the inside edge of described cover plate and described throwing
The lateral wall of hopper connects, and the side wall of described cast hopper offers cushion hole, described cushion hole respectively with described cast hopper and institute
State buffering bucket connection, material can be flowed between described buffering bucket and described cast hopper by described cushion hole, slow to play
The effect of punching;And for example, the side wall of described cast hopper offers some described cushion holes, and described cushion hole is with described cast hopper
Heart axis radially distributes;And for example, often equal between two neighboring described cushion hole;And for example, described buffering hole location
It is provided with drainage screen;And for example, described cast hopper has cirque structure cross section;And for example, the inside edge of described cover plate and institute
It is provided with sealing strip at the link position of the lateral wall stating buffering bucket;And for example, described sealing strip has loop configuration, so, profit
Described cast hopper can be made preferably to enter row buffering to material with material buffer device 600, be occurred with the problem reducing flash.
In order to preferably carry the logistics flowing out in described material leakage body, and then minimizing material falls to described vertical cylinder
The problem of the internal material sputtering producing, for example, refers to Fig. 6, described highly effective reaction device also includes material bogey
700, described material bogey 700 includes loading plate 710 and connecting plate 720, the inner side of described loading plate and described upper cover
Wall connects, and described loading plate arrange towards described material leakage body, the bearing of trend of described loading plate and described vertical cylinder
Form acute angle, the first end of described connecting plate is connected with the medial wall of described upper cover, described connecting plate between central axis
Second end is connected with described loading plate, and described loading plate 710 is provided with flow-disturbing projection towards the side of described material leakage body 310
711;And for example, described loading plate is provided with some flow-disturbings projections;And for example, some described flow-disturbing projection rectangular array are distributed in institute
State in carrying;And for example, described flow-disturbing projection has hemispherical structure;And for example, described loading plate is near described low head
Gradually it is obliquely installed at position;And for example, described connecting plate has the cross section of trapezium structure;And for example, described loading plate is towards institute
The side stating material leakage body is further opened with liquid leakage tank, so, by the loading plate 710 of material bogey 700, material is held
Carry and buffering effect, it is possible to reduce material drops to the flow velocity within described vertical cylinder, and can also play the effect of dispersed material
Really, so can preferably carry in described material leakage body flow out logistics, fall to described vertical cylinder to reduce material
The problem of the material sputtering of interior generation.
In order that the material flowing out in described material leakage body carries out preferably scatter operation, beneficial to whole course of reaction
In, the mixed effect of each material, for example, refer to Fig. 7, described highly effective reaction device also includes material dispersing device 800, described
Material dispersing device 800 is placed in inside described vertical cylinder 10, described material dispersing device 800 include connector drum 810 and
Dispersion framework 820, the first end of described connector drum is connected with the first end of described material leakage body, during described dispersion framework has
Hollow structure, forms distribution cavity, the second end of described connector drum is connected with described dispersion framework, and described connecting cylinder in it
Second end of body is connected with described distribution cavity, described dispersion framework 820 away from described connector drum one end offer some
The dispersion hole 821 of described distribution cavity connection, described dispersion hole is arranged towards described low head 120, and e.g., material is by each described point
Scattered hole 821 falls to inside described vertical cylinder;And for example, described dispersion framework has the columnar structured of hollow;And for example, some
Described dispersion hole is with the central axis circular array distribution of described dispersion framework;And for example, described dispersion hole has regular polygon
Cross-sectional structure;And for example, described dispersion hole has the cross-sectional structure of regular hexagon structure;And for example, described connector drum
First end is spirally connected with the first end of described material leakage body;And for example, described connector drum has rounded cylindrical structure, so, utilizes
Described material dispersing device can make the material flowing out in described material leakage body carry out preferably scatter operation, beneficial to entirely anti-
During answering, the mixed effect of each material.
It is pointed out that each material being stirred married operation inside described vertical cylinder carries out combination reaction
When, and most combination reaction is all exothermic reaction, when the yield of the speed of reaction and product generation is also required to dependent reaction
Liberated heat, for improving reaction rate and yield.Additionally, in whipping process, described agitating device can do work to material,
I.e. material, during being mutually mixed agitation, shows as outwardly releasing heat, the especially stronger material of toughness, it is put
Thermal phenomenon becomes apparent from, and therefore, based on above-mentioned situation, relies on the combination reaction of higher temperature for some, such as depends on reaction certainly
Body heat release and the combination reaction of stirring heat production, and do not need extra heater for the reaction that it is heated, especially need
Guarantee the heat-insulating property of described vertical cylinder.Further, in order to for some acid materials therefore, to assure that described vertical cylinder
The medial wall of body, the medial wall of the described vertical cylinder directly contacting with acid material possesses higher resistance to acid attack performance, uses
The service life of vertical cylinder described in Yu Yansheng is normally carried out with reaction.Further, the lateral wall of described vertical cylinder by
In often contacting with corrosive materials, e.g., the corrosive materials contact of the form such as gaseous state or liquid is it is therefore desirable to possess preferably
Decay resistance, for preferably protecting described vertical cylinder.
In order to improve resistance to acid attack performance, heat-insulating property and the decay resistance of described vertical cylinder, for example, refer to Fig. 8,
Described vertical cylinder, e.g., resistance to acid attack layer 130 that the side wall of described vertical cylinder includes being cascading, heat-insulation layer 140,
Support layer 150, weight coating 160 and protective layer 170, described resistance to acid attack layer is located at the medial wall of described vertical cylinder, and described resistance to
Acid etching layer directly and material, e.g., acid material contact, described protective layer is located at the lateral wall of described vertical cylinder, i.e. described guarantor
Sheath is directly naked to be exposed on the external.
For example, the described resistance to acid attack layer of an embodiment includes each component of following mass parts:75 parts~88 parts of ferrum, titanium 30
Part~34 parts, 20 parts~25 parts of chromium, 2.5~3.4 parts of antimony, 2.3~3.4 parts of copper part, 1.5 parts~2.7 parts of zinc, aluminum 0.9~1.4
Part, 0.15 part~0.27 part of carbon, 0.25 part~0.46 part of silicon, 0.12 part~0.18 part of boron, 0.04 part~0.09 part of cobalt, phosphorus
0.001 part~0.03 part, 0.001 part~0.03 part of sulfur, 0.02 part~0.03 part of strontium, 0.03 part~0.04 part of bismuth, 0.01 part of scandium
~0.02 part and 0.001 part~0.002 part of gadolinium.
Using 75 parts~88 parts of ferrum, 30 parts~34 parts of titanium and 20 parts~25 parts basis basis units as resistance to acid attack layer of chromium
Element such that it is able to make described resistance to acid attack layer possess certain resistance to acid attack performance, additionally, by adding 2.5~3.4 parts of antimony, copper
2.3 parts~3.4 parts, 1.5 parts~2.7 parts of zinc, 0.9~1.4 part of aluminum, 0.04 part~0.09 part of cobalt, 0.02 part~0.03 part of strontium, bismuth
0.03 part~0.04 part, 0.01 part~0.02 part of scandium and 0.001 part~0.002 part of gadolinium carry out compounding additionally it is possible to optimize further
The properties of described resistance to acid attack layer, especially can optimize the resistance to acid attack performance of described resistance to acid attack layer further such that it is able to
Better against the acid etching of material, for improving the service life of described vertical cylinder further and guaranteeing that reacts normally enters
OK.
And for example, the described resistance to acid attack layer of another embodiment includes each component of following mass parts:75 parts~80 parts of ferrum, titanium
33 parts~34 parts, 24 parts~25 parts of chromium, 2.7~3.4 parts of antimony, 2.7 parts~3.4 parts of copper, 1.8 parts~2.5 parts of zinc, aluminum 1.1~1.4
Part, 0.18 part~0.27 part of carbon, 0.27 part~0.46 part of silicon, 0.13 part~0.18 part of boron, 0.04 part~0.09 part of cobalt, phosphorus
0.001 part~0.03 part, 0.001 part~0.03 part of sulfur, 0.02 part~0.03 part of strontium, 0.03 part~0.04 part of bismuth, 0.01 part of scandium
~0.02 part and 0.001 part~0.002 part of gadolinium.
And for example, the described resistance to acid attack layer of another embodiment includes each component of following mass parts:77 parts of ferrum, 33 parts of titanium,
25 parts of chromium, 3.4 parts of antimony, 2.7 parts of copper, 1.9 parts of zinc, 1.3 parts of aluminum, 0.27 part of carbon, 0.46 part of silicon, 0.18 part of boron, 0.04 part of cobalt, phosphorus
0.03 part, 0.001 part of sulfur, 0.03 part of strontium, 0.04 part of bismuth, 0.01 part and 0.002 part of scandium.
For example, the described heat-insulation layer of an embodiment includes each component of following mass parts:15 parts~22 parts of Gypsum Fibrosum powder, white
8~20 parts of cotton, 8 parts~15 parts of rock wool, 7 parts~9 parts of glass fibre, 10 parts~20 parts of Lauxite, 3.5 parts of polyacrylamide~
4.5 parts, 1 part~3 parts of basalt fibre, 3~5 parts of rubber foam, 1 part~2 parts of magnesium hydroxide, aminopropyl triethoxysilane 1
Part~2 parts, 1 part~2 parts of aluminium oxide, 1 part~2 parts of 3,5- di-tert-butyl-4-hydroxybenzoic acid methyl ester, 3~4 parts of polypropylene fiber,
1 part~2 parts of thiorubber. and 0.2~0.8 part of sodium lauryl sulphate.
Described heat-insulation layer can be made to have good heat-insulating property using each component of as above mass parts, when described vertical cylinder
When the material in internal portion occurs exothermic reaction, and after transferring heat to described resistance to acid attack layer, had good based on described heat-insulation layer
Good heat-insulated and heat-insulating property, can limit heat and be further transmitted through described vertical cylinder, and then avoid heat to be transferred directly to
It is ensured that the material within described vertical cylinder is reacted at a suitable temperature in external environment, for improving reaction speed
Rate and the yield of product.
And for example, the described heat-insulation layer of another embodiment includes each component of following mass parts:17 parts~21 parts of Gypsum Fibrosum powder,
White 17~20 parts of cotton, 10 parts~15 parts of rock wool, 7 parts~9 parts of glass fibre, 10 parts~20 parts of Lauxite, polyacrylamide 3.5
Part~4.5 parts, 1 part~2.5 parts of basalt fibre, 3.5~5 parts of rubber foam, 1.5 parts~2 parts of magnesium hydroxide, aminopropyl three second
1.5 parts~2 parts of TMOS, 1 part~2 parts of aluminium oxide, 1 part~1.4 parts of 3,5- di-tert-butyl-4-hydroxybenzoic acid methyl ester, third
3.3~4 parts of synthetic fibre fiber, 1 part~2 parts of thiorubber. and 0.2~0.5 part of sodium lauryl sulphate.
And for example, the described heat-insulation layer of another embodiment includes each component of following mass parts:19 parts of Gypsum Fibrosum powder, white cotton 17
~20 parts, 15 parts of rock wool, 9 parts of glass fibre, 20 parts of Lauxite, 3.8 parts of polyacrylamide, 2.1 parts of basalt fibre, rubber
4.6 parts of foam, 1.7 parts of magnesium hydroxide, 2 parts of aminopropyl triethoxysilane, 1.8 parts of aluminium oxide, 3,5- di-t-butyl -4- hydroxyl
1.4 parts of essence of Niobe, 4 parts of polypropylene fiber, 1.9 parts of thiorubber. and 0.4 part of sodium lauryl sulphate.
For example, the described supporting layer of an embodiment includes each component of following mass parts:95 parts~98 parts of ferrum, manganese 0.4
Part~0.95 part, 0.1 part~0.5 part of molybdenum, 0.01 part~0.05 part of titanium, 0.02 part~0.1 part of aluminum, 0.06 part~0.25 part of carbon,
0.1 part~0.3 part of silicon, 0.05 part~0.1 part of phosphorus, 0.001 part~0.01 part of boron, 0.05 part~0.5 part of hafnium, 0.05 part of scandium~
0.3 part, 0.05 part~0.3 part of chromium, 0.01 part~0.05 part of nickel, 0.01 part~0.05 part of cerium, 0.01 part~0.05 part of thorium and zirconium
0.01 part~0.05 part.
It is appreciated that in order that described vertical cylinder possesses preferable heat-insulating property, needing to introduce described heat-insulation layer, and institute
The mechanical strength stating heat-insulation layer is poor, in order to strengthen the integrally-built mechanical strength of described vertical cylinder, needs to introduce described
Support layer so as to described heat-insulation layer directly contact, for improving the integrally-built mechanical strength of described vertical cylinder, to reach peace
The full purpose producing.Based on above-mentioned situation, this is necessary for requiring described supporting layer to possess higher mechanical strength and anti-deformation behavior
Can, by each component using as above mass parts, especially described supporting layer contain 0.05 part~0.5 part of hafnium, 0.05 part of scandium~
0.3 part, 0.05 part~0.3 part of chromium, 0.01 part~0.05 part of nickel, 0.01 part~0.05 part of cerium, 0.01 part~0.05 part of thorium and zirconium
0.01 part~0.05 part, the mechanical strength of traditional ferroalloy can be improved so as to mechanical strength and anti-deformation nature are more excellent,
Disclosure satisfy that requirement.
And for example, the described supporting layer of another embodiment includes each component of following mass parts:97 parts~98 parts of ferrum, manganese
0.55 part~0.95 part, 0.35 part~0.5 part of molybdenum, 0.01 part~0.05 part of titanium, 0.02 part~0.1 part of aluminum, 0.17 part of carbon~
0.25 part, 0.1 part~0.25 part of silicon, 0.05 part~0.1 part of phosphorus, 0.008 part~0.01 part of boron, 0.1 part~0.5 part of hafnium, scandium 0.1
Part~0.3 part, 0.1 part~0.3 part of chromium, 0.02 part~0.05 part of nickel, 0.02 part~0.05 part of cerium, 0.02 part~0.05 part of thorium and
0.02 part~0.05 part of zirconium.
And for example, the described supporting layer of another embodiment includes each component of following mass parts:97 parts of ferrum, 0.75 part of manganese,
0.5 part of molybdenum, 0.05 part of titanium, 0.02 part of aluminum, 0.17 part of carbon, 0.25 part of silicon, 0.1 part of phosphorus, 0.008 part of boron, 0.5 part of hafnium, scandium 0.2
Part, 0.2 part of chromium, 0.05 part of nickel, 0.05 part of cerium, 0.05 part and 0.05 part of thorium.
For example, the described weight coating of an embodiment includes each component of following mass parts:85 parts~95 parts of tungsten, 30 parts of nickel
~60 parts, 15 parts~40 parts of ferrum, 1.5 parts~10 parts of chromium, 1.5 parts~10 parts of lead, 1 part~6 parts of copper and 0.5 part~5 parts of molybdenum.
It is appreciated that in producing course of reaction, needing the material in described vertical cylinder is carried out higher the stirring of intensity
Mix operation, and because thickness is larger and the presence of the described heat-insulation layer of lighter weight, in order to avoid the entirety of described vertical cylinder
The quality of structure kicks the beam, and then reduces the impact to described vertical cylinder for the external impacts, you can sent out with reducing described vertical cylinder
Raw concussion or displacement problem.Described weight coating can be made to possess excellent counterweight performance, energy using each component of as above mass parts
Enough effectively increase the integrally-built weight of described vertical cylinder so as to or adaptation identical with the weight of traditional vertical cylinder,
Such that it is able to improve the security performance in production process.
And for example, the described weight coating of another embodiment includes each component of following mass parts:90 parts~95 parts of tungsten, nickel 30
Part~45 parts, 27 parts~40 parts of ferrum, 1.5 parts~2.3 parts of chromium, 1.5 parts~3.3 parts of lead, 1 part~5.5 parts of copper and 0.5 part of molybdenum~
4.9 part.
And for example, the described weight coating of another embodiment includes each component of following mass parts:92 parts of tungsten, 38 parts of nickel, ferrum
29 parts, 2.1 parts of chromium, 2.1 parts of lead, 3.5 parts of copper and 3.8 parts of molybdenum.
For example, the described protective layer of an embodiment includes each component of following mass parts:65 parts~80 parts of ferrum, lithium 16~
18 parts, 18 parts~25 parts of nickel, 3.5 parts~4 parts of molybdenum, 2 parts~5 parts of chromium, 1 part~5 parts of cobalt, 1 part~5 parts of vanadium, 1 part~2 parts of manganese, iridium
0.8 part~2.5 parts, 0.5 part~2.5 parts of niobium, 0.3 part~2.5 parts of scandium, 0.2 part~2.5 parts of strontium, 0.2 part~2.5 parts of caesium, tungsten
0.2 part~2.5 parts and 0.2 part~2.5 parts of titanium.
It is appreciated that the lateral wall of described vertical cylinder is due to often contacting with corrosive materials, e.g., gaseous state or liquid etc.
The corrosive materials of form contact it is therefore desirable to possess preferable decay resistance, for preferably protecting described vertical cylinder.
By each component of as above mass parts, described protective layer can be made to possess good Corrosion Protection, and then preferably protect institute
State vertical cylinder, for extending the service life of described vertical cylinder.
And for example, the described protective layer of another embodiment includes each component of following mass parts:65 parts~70 parts of ferrum, lithium 16
Part~16.5 parts, 18~21 parts of nickel, 3.5 parts~3.9 parts of molybdenum, 2 parts~4.4 parts of chromium, 1 part~3.9 parts of cobalt, 1 part~4.5 parts of vanadium,
1 part~1.7 parts of manganese, 0.8 part~2.3 parts of iridium, 0.5 part~2.2 parts of niobium, 0.3 part~2.3 parts of scandium, 0.2 part~2.3 parts of strontium, caesium
0.2 part~2.4 parts, 0.2 part~2.1 parts of tungsten and 0.2 part~1.9 parts of titanium.
And for example, the described protective layer of another embodiment includes each component of following mass parts:65 parts of ferrum, 16.5 parts of lithium,
21 parts of nickel, 3.5 parts of molybdenum, 3.5 parts of chromium, 2.8 parts of cobalt, 3.7 parts of vanadium, 1.5 parts of manganese, 2.3 parts of iridium, 2.2 parts of niobium, 2.3 parts of scandium, strontium 2.3
Part, 2.4 parts of caesium, 0.2 part of tungsten and 0.2 part of titanium.
In order to optimize described vertical cylinder further, e.g., the structure of the side wall of described vertical cylinder, for example, described acidproof
Erosion layer, described heat-insulation layer, the thickness ratio of described supporting layer, described weight coating and described protective layer are (1~1.5):(15~20):
(5~5.5):(8~9.8):(0.5~1.2);And for example, the thickness of described weight coating and described protective layer is than for 1:15:5:9.5:
1.1.
It should be noted that the technical characteristic that other embodiment of the present utility model is also included in the various embodiments described above is mutual
In conjunction with can be formed, and the highly effective reaction device that can implement.
It should be noted that the technical characteristic that other embodiment of the present utility model is also included in the various embodiments described above is mutual
In conjunction with can be formed, and the chemical reaction equipment that can implement.
Each technical characteristic of embodiment described above can arbitrarily be combined, for making description succinct, not to above-mentioned reality
The all possible combination of each technical characteristic applied in example is all described, as long as however, the combination of these technical characteristics is not deposited
In contradiction, all it is considered to be the scope of this specification record.
The above embodiment only have expressed several embodiments of the present utility model, and its description is more concrete and detailed
Carefully, but therefore can not be interpreted as the restriction to this utility model the scope of the claims.It should be pointed out that it is general for this area
For logical technical staff, without departing from the concept of the premise utility, some deformation can also be made and improve, these are all
Belong to protection domain of the present utility model.Therefore, the protection domain of this utility model patent should be defined by claims.
Claims (7)
1. a kind of chemical reaction equipment is it is characterised in that include:
Vertical cylinder, the two ends of described vertical cylinder are respectively arranged with upper cover and low head;
Agitating device, described agitating device includes support base, motor, power output shaft and stirring paddle, and described support base is solid
Dingan County is contained on described upper cover, and the first end of described power output shaft is connected with the rotary shaft of described motor, described dynamic
Second end of power output shaft stretches to inside described vertical cylinder, and the second end of described power output shaft is with described stirring paddle even
Connect, described motor is used for driving described stirring paddle to rotate;
Feeding device, described feeding device includes material leakage body, conveying body, the charging pump housing, charging body and multiple group that feeds intake
Part, the first end of described material leakage body is connected with described upper cover, the second end of described material leakage body and described conveying body
First end connects, and the second end of described conveying body is connected with the discharge end of the described charging pump housing, the charging of the described charging pump housing
End is connected with described charging body, and multiple described assemblies that feed intake are arranged at intervals on described charging body successively, and multiple described
The assembly that feeds intake all is connected with described charging body, and the described assembly that feeds intake includes feed intake body, cast hopper and the valve that feeds intake, described throwing
The first end of expects pipe body is connected with described charging body, and the second end of the described body that feeds intake is connected with described cast hopper, described throwing
Hopper offers dog-house, the described valve that feeds intake be arranged at described in feed intake on body;And
Material dispersing device, described material dispersing device is placed in inside described vertical cylinder, and described material dispersing device includes
Connector drum and dispersion framework, the first end of described connector drum is connected with the first end of described material leakage body, described dispersion frame
Body has hollow structure, forms distribution cavity, the second end of described connector drum is connected with described dispersion framework, and institute in it
The second end stating connector drum is connected with described distribution cavity, and described dispersion framework offers away from one end of described connector drum
The dispersion hole that some and described distribution cavity connects, some described dispersion hole are all towards the direction setting of described low head.
2. chemical reaction equipment according to claim 1 is it is characterised in that described dispersion framework has the cylindrical shape of hollow
Structure.
3. chemical reaction equipment according to claim 2 is it is characterised in that some described dispersion hole are with described dispersion framework
Central axis circular array distribution.
4. chemical reaction equipment according to claim 3 is it is characterised in that described dispersion hole has the transversal of regular polygon
Face structure.
5. chemical reaction equipment according to claim 4 is it is characterised in that described dispersion hole has regular hexagon structure
Cross-sectional structure.
6. chemical reaction equipment according to claim 1 is it is characterised in that the first end of described connector drum and described leakage
The first end of expects pipe body is spirally connected.
7. chemical reaction equipment according to claim 1 is it is characterised in that described connector drum has rounded cylindrical knot
Structure.
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CN106040148A (en) * | 2016-06-30 | 2016-10-26 | 惠州市格雷戈里科技有限公司 | Chemical reaction device |
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CN106040148A (en) * | 2016-06-30 | 2016-10-26 | 惠州市格雷戈里科技有限公司 | Chemical reaction device |
CN106040148B (en) * | 2016-06-30 | 2018-07-20 | 临沂市科翰硅制品有限公司 | Chemical reaction equipment |
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