CN106040148B - Chemical reaction equipment - Google Patents
Chemical reaction equipment Download PDFInfo
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- CN106040148B CN106040148B CN201610513558.9A CN201610513558A CN106040148B CN 106040148 B CN106040148 B CN 106040148B CN 201610513558 A CN201610513558 A CN 201610513558A CN 106040148 B CN106040148 B CN 106040148B
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- tube body
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- vertical cylinder
- chemical reaction
- charging
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J19/18—Stationary reactors having moving elements inside
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J19/02—Apparatus characterised by being constructed of material selected for its chemically-resistant properties
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J4/00—Feed or outlet devices; Feed or outlet control devices
- B01J4/001—Feed or outlet devices as such, e.g. feeding tubes
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J2219/00761—Details of the reactor
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J2219/02—Apparatus characterised by their chemically-resistant properties
- B01J2219/0204—Apparatus characterised by their chemically-resistant properties comprising coatings on the surfaces in direct contact with the reactive components
- B01J2219/0236—Metal based
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J2219/18—Details relating to the spatial orientation of the reactor
- B01J2219/185—Details relating to the spatial orientation of the reactor vertical
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- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Mixers Of The Rotary Stirring Type (AREA)
- Physical Or Chemical Processes And Apparatus (AREA)
Abstract
A kind of chemical reaction equipment, including vertical cylinder, agitating device, feeding device and material dispersing device.The both ends of vertical cylinder are respectively arranged with upper cover and low head.Agitating device includes support base, driving motor, power output shaft and agitating paddle.Feeding device includes material leakage tube body, conveying tube body, the charging pump housing, charging tube body and multiple components that feed intake.Material dispersing device is placed in inside vertical cylinder, and material dispersing device includes connector drum and dispersion framework.Above-mentioned chemical reaction equipment is by being arranged vertical cylinder, agitating device and feeding device, and control addition opportunity, the effect of continous way feeding operation can be realized to multiple component input materials that feed intake of feeding device again, and feeding operation is more simple and convenient and charging efficiency is higher.
Description
Technical field
The present invention relates to chemical production equipment fields, more particularly to a kind of chemical reaction equipment.
Background technology
Currently, in material production field, it usually needs use consersion unit, e.g., need using as vertical response equipment,
The container that vertical cylinder consersion unit or vertical vertical cylinder consersion unit are carried when being chemically reacted as material, it is wide
It is general to be applied to the industries such as oil, chemical industry, rubber, pesticide, dyestuff, medicine and food.
In some special occasions, generally the region that feeds intake of consersion unit is arranged on floor or platform, that is, reaction is set
Standby feeding port is normally at the top of consersion unit or at the position at top, when needs add liquid object to consersion unit
It when material, needs that material is transported on floor or platform in advance, causes feeding operation more complex, charging is less efficient.
In addition, mechanical strength of the existing consersion unit in order to ensure itself, will not generally be arranged excessive feeding port, just
This leads to existing consersion unit, it is more difficult to the operation for realizing continous way charging, i.e., in the same time relatively difficult to achieve or interval time
In shorter, the operation of various materials is added.
Invention content
Based on this, it is necessary to provide that a kind of feeding operation is more simple and convenient, charging efficiency is higher and being capable of the company of realization
The chemical reaction equipment of continuous formula feeding operation.
A kind of chemical reaction equipment, including:
The both ends of vertical cylinder, the vertical cylinder are respectively arranged with upper cover and low head;
Agitating device, the agitating device include support base, driving motor, power output shaft and agitating paddle, the support
Seat is fixedly mounted on the upper cover, the rotation axis connection of the first end of the power output shaft and the driving motor, institute
The second end for stating power output shaft stretches to inside the vertical cylinder, the second end of the power output shaft and the agitating paddle
Connection, the driving motor is for driving the agitating paddle to rotate;
Feeding device, the feeding device include material leakage tube body, conveying tube body, the charging pump housing, charging tube body and multiple throwings
Expect that component, the first end of the material leakage tube body are connected to the upper cover, second end and the conveying pipeline of the material leakage tube body
The first end of body is connected to, and the second end of the conveying tube body is connected to the discharge end of the charging pump housing, the charging pump housing
Feed end is connected to the charging tube body, and multiple components that feed intake are arranged at intervals at successively on the charging tube body, and multiple
The component that feeds intake is connected to the charging tube body, and the component that feeds intake includes feed intake tube body, cast hopper and the valve that feeds intake, institute
The first end for stating the tube body that feeds intake is connected to the charging tube body, and the second end of the tube body that feeds intake is connected to the cast hopper, institute
It states cast hopper and offers feeding port, the valve that feeds intake is set to described feed intake on tube body;And
Material dispersing device, the material dispersing device are placed in inside the vertical cylinder, the material dispersing device
It is connected to the first end of the material leakage tube body including connector drum and dispersion framework, the first end of the connector drum, described point
Dissipating framework has hollow structure, and interior to form distribution cavity, the second end of the connector drum is connect with the dispersion framework, and
And the second end of the connector drum is connected to the distribution cavity, the described dispersion one end of framework far from the connector drum is opened
Equipped with several dispersion holes being connected to the distribution cavity, several dispersion holes are arranged towards the direction of the low head.
The dispersion framework has hollow columnar structured in one of the embodiments,.
Several dispersion holes are with the central axis circular array point of the dispersion framework in one of the embodiments,
Cloth.
The dispersion hole has the cross-sectional structure of regular polygon in one of the embodiments,.
The dispersion hole has the cross-sectional structure of regular hexagon structure in one of the embodiments,.
The first end of the connector drum and the first end of the material leakage tube body are spirally connected in one of the embodiments,.
The connector drum has rounded cylindrical structure in one of the embodiments,.
Above-mentioned chemical reaction equipment is by being arranged vertical cylinder, agitating device and feeding device, and when controlling addition
Machine, then put into the effect that continous way feeding operation can be realized in materials, and feeding operation to multiple components that feed intake of feeding device
More simple and convenient and charging efficiency is higher.
Description of the drawings
Fig. 1 is the structural schematic diagram of the chemical reaction equipment of an embodiment of the present invention;
Fig. 2 is enlarged drawings of the Fig. 1 at A;
Fig. 3 is the partial structural diagram of the chemical reaction equipment of another embodiment of the present invention;
Fig. 4 is the partial structural diagram of the chemical reaction equipment of another embodiment of the present invention;
Fig. 5 is the partial structural diagram of the chemical reaction equipment of another embodiment of the present invention;
Fig. 6 is the partial structural diagram of the chemical reaction equipment of another embodiment of the present invention;
Fig. 7 is the partial structural diagram of the chemical reaction equipment of another embodiment of the present invention;
Fig. 8 is the partial structural diagram of the chemical reaction equipment of another embodiment of the present invention.
Specific implementation mode
To facilitate the understanding of the present invention, below with reference to relevant drawings to invention is more fully described.In attached drawing
Give the better embodiment of the present invention.But the present invention can realize in many different forms, however it is not limited to herein
Described embodiment.On the contrary, the purpose of providing these embodiments is that making to understand more the disclosure
Add thorough and comprehensive.
It should be noted that when element is referred to as " being fixed on " another element, it can be directly on another element
Or there may also be elements placed in the middle.When an element is considered as " connection " another element, it can be directly connected to
To another element or it may be simultaneously present centering elements.Term as used herein " vertical ", " horizontal ", " left side ",
" right side " and similar statement for illustrative purposes only, are not offered as being unique embodiment.
Unless otherwise defined, all of technologies and scientific terms used here by the article and belong to the technical field of the present invention
The normally understood meaning of technical staff is identical.Used term is intended merely to description tool in the description of the invention herein
The purpose of the embodiment of body, it is not intended that in the limitation present invention.Term " and or " used herein includes one or more
Any and all combinations of relevant Listed Items.
For example, a kind of chemical reaction equipment, including:The both ends of vertical cylinder, the vertical cylinder are respectively arranged with envelope
Head and low head;Agitating device, the agitating device include support base, driving motor, power output shaft and agitating paddle, the branch
Support seat is fixedly mounted on the upper cover, the rotation axis connection of the first end of the power output shaft and the driving motor,
The second end of the power output shaft stretches to inside the vertical cylinder, the second end of the power output shaft and the stirring
Paddle connects, and the driving motor is for driving the agitating paddle to rotate;Feeding device, the feeding device include material leakage tube body,
Conveying tube body, the charging pump housing, charging tube body and multiple components that feed intake, first end and the upper cover of the material leakage tube body connect
Logical, the second end of the material leakage tube body is connected to the first end of the conveying tube body, the second end of the conveying tube body with it is described
The feed end of the discharge end connection of the charging pump housing, the charging pump housing is connected to the charging tube body, multiple components that feed intake
It is arranged at intervals at successively on the charging tube body, and multiple components that feed intake are connected to the charging tube body, it is described to feed intake
Component includes feed intake tube body, cast hopper and the valve that feeds intake, and the first end of the tube body that feeds intake is connected to the charging tube body, described
The second end of tube body of feeding intake is connected to the cast hopper, and the cast hopper offers feeding port, and the valve that feeds intake is set to institute
It states and feeds intake on tube body;And material dispersing device, the material dispersing device are placed in inside the vertical cylinder, the material point
In bulk set is connected to including connector drum and dispersion framework, the first end of the connector drum with the first end of the material leakage tube body,
The dispersion framework has hollow structure, interior to form distribution cavity, the second end of the connector drum and the dispersion framework
Connection, and the second end of the connector drum is connected to the distribution cavity, and the dispersion framework is far from the connector drum
One end offer several dispersion holes being connected to the distribution cavity, several dispersion holes are towards the side of the low head
To setting.
In order to which further above-mentioned chemical reaction equipment is explained, for example, the chemical reaction of another embodiment
Equipment is as follows:
Referring to Fig. 1, chemical reaction equipment chemical reaction equipment 10 includes vertical cylinder 100, agitating device 200 and charging
Device 300, agitating device 200 and feeding device 300 may be contained in vertical cylinder 100.
Referring to Fig. 1, the both ends of vertical cylinder 100 are respectively arranged with upper cover 110 and low head 120, vertical cylinder 100
For the accommodating material being added, and it is mixed and reacts to material and occasion is provided.For example, upper cover 110 and low head
Vertical cylinder 100 is formed after 120 connections.For another example, the vertical cylinder is an integral molding structure.For another example, in the vertical cylinder
Be installed on outside support during, the upper cover is located at the top of outside support, and the low head is located at outside support
Lower part.
Referring to Fig. 1, agitating device 200 includes support base 210, driving motor 220, power output shaft 230 and agitating paddle
240, support base 210 is fixedly mounted on the upper cover 110 of vertical cylinder 100, first end and the driving electricity of power output shaft 230
The second end of the rotation axis connection of machine 220, power output shaft 230 stretches to inside vertical cylinder 100, e.g., power output shaft 230
Second end stretch to inside the low head 120 of vertical cylinder 100, the second end of power output shaft 230 connects with agitating paddle 240
It connects, e.g., agitating paddle 240 is located inside the low head 120 of vertical cylinder 100, and driving motor 220 is for driving power output shaft
230 rotations, and then drive and rotated with 230 fixed agitating paddle 240 of power output shaft.When needing the object in vertical cylinder 100
When material is stirred hybrid manipulation, control driving motor 220 drives power output shaft 230 to rotate, and then drives 240 turns of agitating paddle
It is dynamic, it is acted on using the flow-disturbing of agitating paddle 240, can play the role of preferably being stirred, and then can be in vertical cylinder 100
Material be stirred hybrid manipulation.
Also referring to Fig. 1 and Fig. 2, feeding device 300 includes material leakage tube body 310, conveying tube body 320, the charging pump housing
330, feed tube body 340 and multiple components 350 that feed intake, upper cover 110, material leakage tube body 310, conveying tube body 320, the charging pump housing
330, feed tube body 340 and the component 350 that feeds intake is sequentially connected, for another example, upper cover 110, material leakage tube body 310, conveying tube body 320,
The charging pump housing 330, charging tube body 340 and the component 350 that feeds intake are sequentially communicated.
Referring to Fig. 1, the first end of material leakage tube body 310 is connected to upper cover 110, the second end of material leakage tube body 310 with it is defeated
The first end of expects pipe body 320 is connected to, and the second end of conveying tube body 320 is connected to the discharge end of the charging pump housing 330, and feed the pump housing
330 feed end is connected to charging tube body 340, and multiple components 350 that feed intake are arranged at intervals at successively on charging tube body 340, and more
A component 350 that feeds intake is connected to charging tube body 340, only need to be to the group that feeds intake when needing that material is added into vertical cylinder 100
Part 350 puts into material and entire feeding operation can be completed, and feeding operation is more simple and convenient and charging efficiency is higher, without volume
These regions that feed intake such as outer setting floor or platform realize the effect for exempting from high-order charging, that is to say, that when to the component that feeds intake
When 350 input material, based on the draft of the charging pump housing 330, the material for the component 350 that feeds intake, which is added, can enter to charging tube body 340
Interior, later, material is entered to by the pump housing 330 that feeds in conveying tube body 320 again, and then, material is entered by conveying tube body 320 again
To material leakage tube body 310, finally, material is entered to by material leakage tube body 310 in the upper cover 110 of vertical cylinder 100 again, Jin Erjin
Enter to entire vertical cylinder 100, at this point, complete entire feeding operation, i.e., it only need to be to the input of component 350 or the addition material of feeding intake
Entire feeding operation can be completed, feeding operation is simple and convenient and charging efficiency is higher.Further, since material leakage tube body 310, conveying
The component 350 that feeds intake, can be arranged far from the region of vertical cylinder 100 by the presence of tube body 320 and charging tube body 340, for example,
Due to the presence of material leakage tube body 310, conveying tube body 320 and the tube body 340 that feeds, the component 350 that can will feed intake setting is convenient for
On the ground of dosing operation or it is arranged in weighing area, in this way, may be implemented to exempt from the high-order effect to feed intake and exempt from feeding platform.
Referring to Fig. 2, the component 350 that feeds intake includes feed intake tube body 351, cast hopper 352 and the valve 353 that feeds intake, feed intake tube body
351 first end is connected to charging tube body 340, and the second end for the tube body 351 that feeds intake is connected to cast hopper 352, and cast hopper 352 opens up
There is feeding port 354, the valve 353 that feeds intake, which is set to, to feed intake on tube body 351.For example, feeding intake described in the feeding device setting three
Component in this way, three kinds of materials can be added simultaneously, and then realizes the effect of continous way feeding operation, certainly, the component that feeds intake
Number be not limited to three, for example, it is also possible to be adjusted according to actual conditions, e.g., each component one that feeds intake is a pair of
Answer a kind of material for participating in reaction.
When need in same time or interval time it is shorter in, to vertical cylinder 100 inside when various materials are added, this
When, the type of material is added simultaneously as needed, it is corresponding to open a certain number of valves 353 that feed intake, then, to multiple cast hoppers
352 feeding port 354 corresponds to input various materials, the charging pump housing 330 is opened, based on the swabbing action of the charging pump housing 330, material
It is vertical along the cast hopper 352- tube body 351- charging tube body 340- charging pump housing 330- conveying tube body 320- material leakage tube bodies 310- that feed intake
The charging path of formula cylinder 100 enters in vertical cylinder 100, at this point, completing entire feeding operation.
When needing that a kind of material is added to the inside of vertical cylinder 100, at this point, opening the feeding port of a cast hopper 352
354 and it is corresponding put into the material, and close remaining valve 353 that feeds intake, material adds along the cast hopper 352- tube body 351- that feed intake
The charging path of expects pipe body 340- charging pump housing 330- conveying tube body 320- material leakage tube body 310- vertical cylinders 100 enters to vertical
In cylinder 100, at this point, completing entire feeding operation.
Above-mentioned chemical reaction equipment 10 is controlled by the way that vertical cylinder 100, agitating device 200 and feeding device 300 is arranged
Addition opportunity is made, then puts into material to multiple components 350 that feed intake of feeding device 300 and continous way feeding operation can be realized
Effect, and feeding operation is more simple and convenient and charging efficiency is higher.
In order to preferably close the cast hopper, extraneous amount is evaporated into reduce the material in the cast hopper, for example,
Referring to Fig. 3, the chemical reaction equipment further includes locking device 400, locking device 400 includes rotary shaft 410 and closing door
420, the rotary shaft is rotatably dispose at the marginal position of the feeding port of cast hopper 352, the closing door and the rotation
Shaft is fixedly connected, and for the closing door for closing the feeding port, the edge of the closing door is provided with sealing ring, described close
Seal and the edge of the feeding port support;For another example, the feeding port has the cross section of circular configuration;For another example, the closing
Door has circular pan-like structure;For another example, the sealing ring has circular annular form structure;For another example, the closing door is far from the rotation
It is provided with clump weight at the position of shaft;For another example, the side of the sealing ring towards the feeding port offers seal groove, described
The edge of feeding port is inside the seal groove;For another example, the seal groove has loop configuration, in this way, utilizing closing dress
The cast hopper can preferably be closed by setting 400 closing door 420, and the external world is evaporated into reduce the material in the cast hopper
Amount.
In order to preferably put into material into the cast hopper, for example, referring to Fig. 4, the chemical reaction equipment also wraps
Material injection device 500 is included, the material injection device 500 includes that sealing plate 510, first injects the injection of tube body 520 and second
Tube body 530, the sealing plate cover on the feeding port of cast hopper 352, and for closing the feeding port, and described the
The first end of one injection tube body is connect with the sealing plate, and the first end of the first injection tube body connects with the cast hopper
Logical, the second end of the first injection tube body is flexibly connected with the first end of the second injection tube body, second injection pipe
The second end of body is used to be connected to external material injection device, e.g., is connected to external charging bucket, the charging bucket is equipped with
Material;For another example, the lateral wall of the second end of the first injection tube body offers external screw thread, and described second injects the second of tube body
The madial wall at end offers internal thread, the internal thread and the external thread bolt connection;For another example, the second of the first injection tube body
The junction for the first end that tube body is injected in end with described second is provided with hoop component;For another example, the hoop component includes clip
Ontology and connecting screw, the second end that the clip ontology is set to the first injection tube body inject tube body with described second
The junction of first end, the both ends of the both ends of the connecting screw respectively with the clip ontology are spirally connected;For another example, the clip sheet
Body has arcuate structure;For another example, be provided with reinforcing rib on the clip ontology, the reinforcing rib by the clip ontology one end
Extend to the other end of the clip ontology;For another example, the reinforcing rib has semicircular structure cross section, in this way, only needing will be outer
The material injection device in portion is connected to the second end of the second injection tube body and dosing operation can be completed, so as to preferably
Material is put into the cast hopper.
It is appreciated that when excessive material is added to the cast hopper, it is possible to cause the cast hopper that flash occurs
The problem of, in order to make the cast hopper preferably to material into row buffering, to reduce flash the problem of occurs, for example, please referring to
Fig. 5, the chemical reaction equipment further include material buffer device 600, the material buffer device 600 include buffering bucket 610 and
Cover board 620, the buffering bucket 610 have the structure of the shaped hollow round table of both ends open, the bottom opening of the buffering bucket 610 solid
Surely it is placed on the cast hopper 352 and at the position of the neighbouring tube body that feeds intake, the cover board has loop configuration, the lid
It is connect at the outer ledge of plate and the open-topped marginal position of the buffering bucket, the inside edge of the cover board and the throwing
The lateral wall of hopper connects, and the side wall of the cast hopper offers cushion hole, the cushion hole respectively with the cast hopper and institute
Buffering bucket connection is stated, material can be flowed by the cushion hole between the buffering bucket and the cast hopper, slow to play
The effect of punching;For another example, the side wall of the cast hopper offers several cushion holes, and the cushion hole is in the cast hopper
Mandrel line radially distributes;For another example, equal between cushion hole described in each adjacent two;For another example, the buffering hole location
It is provided with filter screen;For another example, the cast hopper has cirque structure cross section;For another example, the inside edge of the cover board and institute
It states and is provided with sealing strip at the link position of the lateral wall of buffering bucket;For another example, the sealing strip has loop configuration, in this way, sharp
The cast hopper can be made preferably to material into row buffering with material buffer device 600, to reduce flash the problem of occurs.
In order to preferably carry the logistics flowed out out of described material leakage tube body, and then reduces material and fall to the vertical cylinder
The problem of material sputtering generated in vivo, for example, referring to Fig. 6, the chemical reaction equipment further includes material bogey
700, the material bogey 700 includes loading plate 710 and connecting plate 720, the inside of the loading plate and the upper cover
Wall connects, and the loading plate is arranged towards the material leakage tube body, the extending direction of the loading plate and the vertical cylinder
Acute angle is formed between central axis, the first end of the connecting plate is connect with the madial wall of the upper cover, the connecting plate
Second end is connect with the loading plate, and the side of the loading plate 710 towards the material leakage tube body 310 is provided with flow-disturbing protrusion
711;For another example, the loading plate is provided with several flow-disturbing protrusions;For another example, several flow-disturbing protrusion rectangular arrays are distributed in institute
It states in carrying;For another example, the flow-disturbing protrusion has hemispherical structure;For another example, the loading plate is to close to the low head
It is gradually obliquely installed at position;For another example, the connecting plate has the cross section of trapezium structure;For another example, the loading plate is towards institute
The side for stating material leakage tube body is further opened with liquid leakage tank, in this way, the loading plate 710 by material bogey 700 holds material
Load and buffering effect, it is possible to reduce material falls to the flow velocity inside the vertical cylinder, and can also play the effect of dispersed material
Fruit, and then the logistics flowed out out of described material leakage tube body can be preferably carried, fall to the vertical cylinder to reduce material
The problem of material sputtering of interior generation.
In order to make the material flowed out out of described material leakage tube body carry out better dispersing operation, it is conducive to entire reaction process
In, the mixed effect of each material, for example, referring to Fig. 7, the chemical reaction equipment further includes material dispersing device 800, it is described
Material dispersing device 800 is placed in inside the vertical cylinder 10, the material dispersing device 800 include connector drum 810 and
Disperse framework 820, the first end of the connector drum is connected to the first end of the material leakage tube body, during the dispersion framework has
Hollow structure, interior to form distribution cavity, the second end of the connector drum is connect with the dispersion framework, and the connecting cylinder
The second end of body is connected to the distribution cavity, and the described dispersion one end of framework 820 far from the connector drum offers several
The dispersion hole 821 of the distribution cavity connection, the dispersion hole are arranged towards the low head 120, and e.g., material is by each described point
Hole 821 is dissipated to fall to inside the vertical cylinder;For another example, the dispersion framework has hollow columnar structured;For another example, several
The dispersion hole is distributed with the central axis circular array of the dispersion framework;For another example, the dispersion hole has regular polygon
Cross-sectional structure;For another example, the dispersion hole has the cross-sectional structure of regular hexagon structure;For another example, the connector drum
First end and the first end of the material leakage tube body are spirally connected;For another example, the connector drum has rounded cylindrical structure, in this way, utilizing
The material dispersing device can make the material flowed out out of described material leakage tube body carry out better dispersing operation, be conducive to entire anti-
During answering, the mixed effect of each material.
It should be pointed out that each material for being stirred hybrid manipulation inside the vertical cylinder carries out combination reaction
When, and most of combination reaction is all exothermic reaction, when the yield of rate and the product generation of reaction is also required to dependent reaction
The heat of releasing, for improving reaction rate and yield.In addition, in whipping process, the agitating device can do work to material,
That is material shows as outwardly releasing heat during being mutually mixed agitation, especially the stronger material of toughness, puts
Thermal phenomenon becomes apparent from, therefore, based on the above situation, for the combination reaction of some dependence higher temperatures, such as certainly dependent on reaction
The combination reaction of body heat release and stirring heat production, and additional heating device is not needed for the reaction that it is heated, especially need
Ensure the heat-insulating property of the vertical cylinder.Further, in order to be directed to some acid materials, therefore, to assure that the vertical cylinder
The madial wall of the madial wall of body, i.e., the vertical cylinder directly contacted with acid material has higher acid etch resistance energy, uses
The service life of vertical cylinder described in Yu Yansheng and being normally carried out for reaction.Further, the lateral wall of the vertical cylinder by
In often being contacted with corrosive materials, e.g., the corrosive materials of the forms such as gaseous state or liquid contact, it is therefore desirable to have preferable
Corrosion resistance, for preferably protecting the vertical cylinder.
In order to improve acid etch resistance energy, heat-insulating property and the corrosion resistance of the vertical cylinder, for example, referring to Fig. 8,
The vertical cylinder, e.g., the side wall of the vertical cylinder include the resistance to acid attack layer 130 being cascading, insulating layer 140, branch
Support layer 150, weight coating 160 and protective layer 170, the resistance to acid attack layer are located at the madial wall of the vertical cylinder, and described resistance to
Directly and material, e.g., acid material contact, the protective layer is located at the lateral wall of the vertical cylinder, i.e., the described guarantor to acid etching layer
Sheath is directly naked to be exposed on the external.
For example, the resistance to acid attack layer of an embodiment includes each component of following mass parts:75 parts~88 parts of iron, titanium 30
Part~34 parts, 20 parts~25 parts of chromium, 2.5~3.4 parts of antimony, 2.3~3.4 parts of copper part, 1.5 parts~2.7 parts of zinc, aluminium 0.9~1.4
Part, 0.15 part~0.27 part of carbon, 0.25 part~0.46 part of silicon, 0.12 part~0.18 part of boron, 0.04 part~0.09 part of cobalt, phosphorus
0.001 part~0.03 part, 0.001 part~0.03 part of sulphur, 0.02 part~0.03 part of strontium, 0.03 part~0.04 part of bismuth, 0.01 part of scandium
~0.02 part and 0.001 part~0.002 part of gadolinium.
Basis basis member using 75 parts~88 parts of iron, 20 parts~25 parts of 30 parts~34 parts of titanium and chromium as resistance to acid attack layer
Element, so as to enable the resistance to acid attack layer to have certain acid etch resistance, in addition, by adding 2.5~3.4 parts of antimony, copper
2.3 parts~3.4 parts, 1.5 parts~2.7 parts of zinc, 0.9~1.4 part of aluminium, 0.04 part~0.09 part of cobalt, 0.02 part~0.03 part of strontium, bismuth
0.001 part~0.002 part of 0.03 part~0.04 part, 0.01 part~0.02 part of scandium and gadolinium are compounded, additionally it is possible to be advanced optimized
The properties of the resistance to acid attack layer can especially advanced optimize the acid etch resistance energy of the resistance to acid attack layer, so as to
Better against the acid etching of material, service life for further increasing the vertical cylinder and ensure reaction it is normal into
Row.
For another example, the resistance to acid attack layer of another embodiment includes each component of following mass parts:75 parts~80 parts of iron, titanium
33 parts~34 parts, 24 parts~25 parts of chromium, 2.7~3.4 parts of antimony, 2.7 parts~3.4 parts of copper, 1.8 parts~2.5 parts of zinc, aluminium 1.1~1.4
Part, 0.18 part~0.27 part of carbon, 0.27 part~0.46 part of silicon, 0.13 part~0.18 part of boron, 0.04 part~0.09 part of cobalt, phosphorus
0.001 part~0.03 part, 0.001 part~0.03 part of sulphur, 0.02 part~0.03 part of strontium, 0.03 part~0.04 part of bismuth, 0.01 part of scandium
~0.02 part and 0.001 part~0.002 part of gadolinium.
For another example, the resistance to acid attack layer of another embodiment includes each component of following mass parts:77 parts of iron, 33 parts of titanium,
25 parts of chromium, 3.4 parts of antimony, 2.7 parts of copper, 1.9 parts of zinc, 1.3 parts of aluminium, 0.27 part of carbon, 0.46 part of silicon, 0.18 part of boron, 0.04 part of cobalt, phosphorus
0.03 part, 0.001 part of sulphur, 0.03 part of strontium, 0.04 part of bismuth, 0.01 part and 0.002 part of scandium.
For example, the insulating layer of an embodiment includes each component of following mass parts:It is 15 parts~22 parts of land plaster, white
8~20 parts of cotton, 8 parts~15 parts of rock wool, 7 parts~9 parts of glass fibre, 10 parts~20 parts of Lauxite, 3.5 parts of polyacrylamide~
4.5 parts, 1 part~3 parts of basalt fibre, 3~5 parts of rubber foam, 1 part~2 parts of magnesium hydroxide, aminopropyl triethoxysilane 1
Part~2 parts, 1 part~2 parts of aluminium oxide, 1 part~2 parts of 3,5- di-tert-butyl-4-hydroxybenzoic acids methyl esters, 3~4 parts of polypropylene fiber,
0.2~0.8 part of 1 part~2 parts of polysulfide rubber and lauryl sodium sulfate.
It can make the insulating layer that there is good heat-insulating property using each component of mass parts as above, when the vertical cylinder
When exothermic reaction occurs for the material in internal portion, and after transferring heat to the resistance to acid attack layer, had based on the insulating layer good
Good heat-insulated and heat-insulating property, can limit heat and be further transmitted through the vertical cylinder, and then heat is avoided to be transferred directly to
In external environment, it is ensured that the material inside the vertical cylinder is reacted at a suitable temperature, for improving reaction speed
The yield of rate and product.
For another example, the insulating layer of another embodiment includes each component of following mass parts:17 parts~21 parts of land plaster,
White 17~20 parts of cotton, 10 parts~15 parts of rock wool, 7 parts~9 parts of glass fibre, 10 parts~20 parts of Lauxite, polyacrylamide 3.5
Part~4.5 parts, 1 part~2.5 parts of basalt fibre, 3.5~5 parts of rubber foam, 1.5 parts~2 parts of magnesium hydroxide, three second of aminopropyl
1.5 parts~2 parts of oxysilane, 1 part~2 parts of aluminium oxide, 1 part~1.4 parts of 3,5- di-tert-butyl-4-hydroxybenzoic acids methyl esters, third
0.2~0.5 part of 3.3~4 parts of synthetic fibre fiber, 1 part~2 parts of polysulfide rubber and lauryl sodium sulfate.
For another example, the insulating layer of another embodiment includes each component of following mass parts:19 parts of land plaster, white cotton 17
~20 parts, 15 parts of rock wool, 9 parts of glass fibre, 20 parts of Lauxite, 3.8 parts of polyacrylamide, 2.1 parts of basalt fibre, rubber
4.6 parts of foam, 1.7 parts of magnesium hydroxide, 2 parts of aminopropyl triethoxysilane, 1.8 parts of aluminium oxide, 3,5- di-t-butyl -4- hydroxyls
0.4 part of 1.4 parts of methyl benzoate, 4 parts of polypropylene fiber, 1.9 parts of polysulfide rubber and lauryl sodium sulfate.
For example, the supporting layer of an embodiment includes each component of following mass parts:95 parts~98 parts of iron, manganese 0.4
Part~0.95 part, 0.1 part~0.5 part of molybdenum, 0.01 part~0.05 part of titanium, 0.02 part~0.1 part of aluminium, 0.06 part~0.25 part of carbon,
0.1 part~0.3 part of silicon, 0.05 part~0.1 part of phosphorus, 0.001 part~0.01 part of boron, 0.05 part~0.5 part of hafnium, 0.05 part of scandium~
0.3 part, 0.05 part~0.3 part of chromium, 0.01 part~0.05 part of nickel, 0.01 part~0.05 part of cerium, 0.01 part~0.05 part of thorium and zirconium
0.01 part~0.05 part.
It is appreciated that in order to make the vertical cylinder have preferable heat-insulating property, need to introduce the insulating layer, and institute
The mechanical strength for stating insulating layer is poor, in order to reinforce the integrally-built mechanical strength of the vertical cylinder, needs to introduce the branch
Layer is supportted, it is made to be in direct contact with the insulating layer, for improving the integrally-built mechanical strength of the vertical cylinder, to reach peace
The purpose produced entirely.Based on the above situation, this just necessarily requires the supporting layer to have higher mechanical strength and anti-deformation behavior
Can, by using each component of mass parts as above, the especially described supporting layer contain 0.05 part~0.5 part of hafnium, 0.05 part of scandium~
0.3 part, 0.05 part~0.3 part of chromium, 0.01 part~0.05 part of nickel, 0.01 part~0.05 part of cerium, 0.01 part~0.05 part of thorium and zirconium
0.01 part~0.05 part, the mechanical strength of traditional ferroalloy can be improved, keep its mechanical strength and anti-deformation nature more excellent,
It disclosure satisfy that requirement.
For another example, the supporting layer of another embodiment includes each component of following mass parts:97 parts~98 parts of iron, manganese
0.55 part~0.95 part, 0.35 part~0.5 part of molybdenum, 0.01 part~0.05 part of titanium, 0.02 part~0.1 part of aluminium, 0.17 part of carbon~
0.25 part, 0.1 part~0.25 part of silicon, 0.05 part~0.1 part of phosphorus, 0.008 part~0.01 part of boron, 0.1 part~0.5 part of hafnium, scandium 0.1
Part~0.3 part, 0.1 part~0.3 part of chromium, 0.02 part~0.05 part of nickel, 0.02 part~0.05 part of cerium, 0.02 part~0.05 part of thorium and
0.02 part~0.05 part of zirconium.
For another example, the supporting layer of another embodiment includes each component of following mass parts:97 parts of iron, 0.75 part of manganese,
0.5 part of molybdenum, 0.05 part of titanium, 0.02 part of aluminium, 0.17 part of carbon, 0.25 part of silicon, 0.1 part of phosphorus, 0.008 part of boron, 0.5 part of hafnium, scandium 0.2
Part, 0.2 part of chromium, 0.05 part of nickel, 0.05 part of cerium, 0.05 part and 0.05 part of thorium.
For example, the weight coating of an embodiment includes each component of following mass parts:85 parts~95 parts of tungsten, 30 parts of nickel
0.5 part~5 parts of~60 parts, 15 parts~40 parts of iron, 1.5 parts~10 parts of chromium, 1.5 parts~10 parts of lead, 1 part~6 parts of copper and molybdenum.
It is appreciated that in produce reaction process, need that intensity is higher stirs to the material progress in the vertical cylinder
Operation is mixed, and since thickness is larger and the presence of the insulating layer of lighter weight, in order to avoid the entirety of the vertical cylinder
The quality of structure kicks the beam, and then reduces influence of the external impacts to the vertical cylinder, you can is sent out with reducing the vertical cylinder
Raw concussion or displacement problem.The weight coating can be made to have excellent counterweight performance, energy using each component of mass parts as above
It is enough effectively to increase the integrally-built weight of the vertical cylinder, keep it identical as the weight of traditional vertical cylinder or is adapted to,
So as to improve the security performance in production process.
For another example, the weight coating of another embodiment includes each component of following mass parts:90 parts~95 parts of tungsten, nickel 30
0.5 part of part~45 parts, 27 parts~40 parts of iron, 1.5 parts~2.3 parts of chromium, 1.5 parts~3.3 parts of lead, 1 part~5.5 parts of copper and molybdenum~
4.9 part.
For another example, the weight coating of another embodiment includes each component of following mass parts:92 parts of tungsten, 38 parts of nickel, iron
3.8 parts of 29 parts, 2.1 parts of chromium, 2.1 parts of lead, 3.5 parts of copper and molybdenum.
For example, the protective layer of an embodiment includes each component of following mass parts:65 parts~80 parts of iron, lithium 16~
18 parts, 18 parts~25 parts of nickel, 3.5 parts~4 parts of molybdenum, 2 parts~5 parts of chromium, 1 part~5 parts of cobalt, 1 part~5 parts of vanadium, 1 part~2 parts of manganese, iridium
0.8 part~2.5 parts, 0.5 part~2.5 parts of niobium, 0.3 part~2.5 parts of scandium, 0.2 part~2.5 parts of strontium, 0.2 part~2.5 parts of caesium, tungsten
0.2 part~2.5 parts and 0.2 part~2.5 parts of titanium.
It is appreciated that the lateral wall of the vertical cylinder is with corrosive materials due to often contacting, and e.g., gaseous state or liquid etc.
The corrosive materials of form contact, it is therefore desirable to have preferable corrosion resistance, for preferably protecting the vertical cylinder.
By each component of mass parts as above, the protective layer can be made to have good Corrosion Protection, and then preferably protect institute
Vertical cylinder is stated, the service life for extending the vertical cylinder.
For another example, the protective layer of another embodiment includes each component of following mass parts:65 parts~70 parts of iron, lithium 16
Part~16.5 parts, 18~21 parts of nickel, 3.5 parts~3.9 parts of molybdenum, 2 parts~4.4 parts of chromium, 1 part~3.9 parts of cobalt, 1 part~4.5 parts of vanadium,
1 part~1.7 parts of manganese, 0.8 part~2.3 parts of iridium, 0.5 part~2.2 parts of niobium, 0.3 part~2.3 parts of scandium, 0.2 part~2.3 parts of strontium, caesium
0.2 part~1.9 parts of 0.2 part~2.4 parts, 0.2 part~2.1 parts of tungsten and titanium.
For another example, the protective layer of another embodiment includes each component of following mass parts:65 parts of iron, 16.5 parts of lithium,
21 parts of nickel, 3.5 parts of molybdenum, 3.5 parts of chromium, 2.8 parts of cobalt, 3.7 parts of vanadium, 1.5 parts of manganese, 2.3 parts of iridium, 2.2 parts of niobium, 2.3 parts of scandium, strontium 2.3
Part, 2.4 parts of caesium, 0.2 part of tungsten and 0.2 part of titanium.
In order to advanced optimize the vertical cylinder, e.g., the structure of the side wall of the vertical cylinder, for example, described acidproof
The thickness ratio for losing layer, the insulating layer, the supporting layer, the weight coating and the protective layer is (1~1.5):(15~20):
(5~5.5):(8~9.8):(0.5~1.2);For another example, the thickness of the weight coating and protective layer ratio is 1:15:5:9.5:
1.1。
It is combined with each other it should be noted that the other embodiment of the present invention further includes technical characteristic in the various embodiments described above
The chemical reaction equipment that can be formed, and can implemented.
It is combined with each other it should be noted that the other embodiment of the present invention further includes technical characteristic in the various embodiments described above
The chemical reaction equipment that can be formed, and can implemented.
Each technical characteristic of embodiment described above can be combined arbitrarily, to keep description succinct, not to above-mentioned reality
It applies all possible combination of each technical characteristic in example to be all described, as long as however, the combination of these technical characteristics is not deposited
In contradiction, it is all considered to be the range of this specification record.
Only several embodiments of the present invention are expressed for embodiment described above, the description thereof is more specific and detailed, but
It cannot be construed as a limitation to the scope of the present invention.It should be pointed out that for the ordinary skill people of this field
For member, without departing from the inventive concept of the premise, various modifications and improvements can be made, these belong to the present invention's
Protection domain.Therefore, the protection domain of patent of the present invention should be determined by the appended claims.
Claims (7)
1. a kind of chemical reaction equipment, which is characterized in that including:
The both ends of vertical cylinder, the vertical cylinder are respectively arranged with upper cover and low head;
Agitating device, the agitating device include support base, driving motor, power output shaft and agitating paddle, and the support base is solid
Dingan County is on the upper cover, the rotation axis connection of the first end of the power output shaft and the driving motor, described dynamic
The second end of power output shaft stretches to inside the vertical cylinder, and the second end of the power output shaft connects with the agitating paddle
It connects, the driving motor is for driving the agitating paddle to rotate;
Feeding device, the feeding device include material leakage tube body, conveying tube body, the charging pump housing, charging tube body and multiple groups that feed intake
The first end of part, the material leakage tube body is connected to the upper cover, the second end of the material leakage tube body and the conveying tube body
First end is connected to, and the second end of the conveying tube body is connected to the discharge end of the charging pump housing, the charging of the charging pump housing
End is connected to the charging tube body, and multiple components that feed intake are arranged at intervals at successively on the charging tube body, and multiple described
The component that feeds intake is connected to the charging tube body, and the component that feeds intake includes feed intake tube body, cast hopper and the valve that feeds intake, the throwing
The first end of expects pipe body is connected to the charging tube body, and the second end of the tube body that feeds intake is connected to the cast hopper, the throwing
Hopper offers feeding port, and the valve that feeds intake is set to described feed intake on tube body;And
Material dispersing device, the material dispersing device are placed in inside the vertical cylinder, and the material dispersing device includes
Connector drum and dispersion framework, the first end of the connector drum are connected to the first end of the material leakage tube body, the dispersion frame
Body has hollow structure, and interior to form distribution cavity, the second end of the connector drum is connect with the dispersion framework, and institute
The second end for stating connector drum is connected to the distribution cavity, and the described dispersion one end of framework far from the connector drum offers
Several dispersion holes being connected to the distribution cavity, several dispersion holes are arranged towards the direction of the low head;
Wherein, the chemical reaction equipment further includes material bogey, and the material bogey includes loading plate and connection
Plate, the loading plate are connect with the madial wall of the upper cover, and the loading plate is arranged towards the material leakage tube body, described to hold
Form acute angle between the extending direction of support plate and the central axis of the vertical cylinder, the first end of the connecting plate with it is described on
The madial wall of end socket connects, and the second end of the connecting plate is connect with the loading plate, and the loading plate is towards the material leakage pipe
The side of body is provided with flow-disturbing protrusion;The loading plate is provided with several flow-disturbing protrusions;The rectangular battle array of several flow-disturbing protrusions
Column distribution is in the carrying;The flow-disturbing protrusion has hemispherical structure;The loading plate is to close to the low head
It is gradually obliquely installed at position;The connecting plate has the cross section of trapezium structure;The loading plate is towards the material leakage tube body
Side be further opened with liquid leakage tank.
2. chemical reaction equipment according to claim 1, which is characterized in that the dispersion framework has hollow cylindrical shape
Structure.
3. chemical reaction equipment according to claim 2, which is characterized in that several dispersion holes are with the dispersion framework
Central axis circular array distribution.
4. chemical reaction equipment according to claim 3, which is characterized in that the dispersion hole has the transversal of regular polygon
Face structure.
5. chemical reaction equipment according to claim 4, which is characterized in that the dispersion hole has regular hexagon structure
Cross-sectional structure.
6. chemical reaction equipment according to claim 1, which is characterized in that the first end of the connector drum and the leakage
The first end of expects pipe body is spirally connected.
7. chemical reaction equipment according to claim 1, which is characterized in that the connector drum has rounded cylindrical knot
Structure.
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CN204768663U (en) * | 2015-05-29 | 2015-11-18 | 惠州市建科实业有限公司 | Agitated reactor |
CN205948882U (en) * | 2016-06-30 | 2017-02-15 | 惠州市格雷戈里科技有限公司 | Chemical reaction equipment |
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CN204768663U (en) * | 2015-05-29 | 2015-11-18 | 惠州市建科实业有限公司 | Agitated reactor |
CN205948882U (en) * | 2016-06-30 | 2017-02-15 | 惠州市格雷戈里科技有限公司 | Chemical reaction equipment |
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