CN206046013U - Synthesis device - Google Patents

Abstract

A kind of synthesis device, including kettle, mixing stirring device, material filter and activity provision for disengagement.The two ends of kettle are respectively arranged with upper cover and low head.Mixing stirring device includes installation frame, motor, drive shaft and stirring paddle.Material filter includes material-pumping tube body, filter box, screen modules, the filtration pump housing, backflow body and valve.Activity provision for disengagement includes that locking plate body, securing member first installs plate body and the second installation plate body.Above-mentioned synthesis device can be circulated filtration and go the removal of impurity to operate by arranging kettle, mixing stirring device and material filter, and material filter to material, go that deimpurity operation is more simple and convenient, and production efficiency is also higher.

Description

Synthesis device

Technical field

This utility model is related to chemical industry synthesis equipment technical field, more particularly to a kind of synthesis device.

Background technology

At present, in material production field, after especially various materials mixing reacts, obtain the situation of final products In, it usually needs using chemical industry synthesis equipment, for mixing is stirred to material, and make which successfully react, be used for Synthesis obtains the final products of higher quality.

Wherein, as material is before the reaction or after reaction, more or less there are some impurity, traditional goes removal of impurity mode First to take out the product obtained after reaction from chemical industry synthesis equipment, then the defecator using outside was carried out to product Filter.

However, above-mentioned go deimpurity mode still to there is a problem of that operation is more complicated loaded down with trivial details, cause production efficiency relatively low. Also there is the more difficult cleaning of screen modules or replacement operation in existing chemical industry synthesis equipment.

Utility model content

Based on this, it is necessary to provide one kind and go the more simple and convenient and production efficiency of deimpurity operation higher, Yi Jineng It is enough preferably dismantle the screen modules, and then preferably the screen modules can be cleaned or replacement operation Synthesis device.

A kind of synthesis device, including：

Kettle, the two ends of the kettle are respectively arranged with upper cover and low head；

Mixing stirring device, the mixing stirring device include installation frame, motor, drive shaft and stirring paddle, institute State installation frame to be fixedly mounted on the upper cover, the motor is arranged on the installation frame, the drive shaft First end be connected with the rotary shaft of the motor, the second end of the drive shaft is connected with the stirring paddle, and described Stirring paddle is located inside the low head；

Material filter, the material filter include material-pumping tube body, filter box, screen modules, filter pump Body, backflow body and valve, the first end of the material-pumping tube body are connected with the bottom of the low head, and the filter box is hollow Arrange, filter cavity is formed in which, the second end of the material-pumping tube body is connected with the first end of the filter box, and described take out Second end of expects pipe body is connected with the filter cavity, and the screen modules include the first filter screen, the second filter screen and the 3rd filter Net, first filter screen, second filter screen and the 3rd filter screen are arranged at intervals in the filter cavity successively, and described The edge at the edge of one filter screen, the edge of second filter screen and the 3rd filter screen is connected with the medial wall of the filter box Connect, first filter screen towards the second end of the material-pumping tube body direction arrange, it is described filter the pump housing feed end with it is described Second end of filter box connects, and the filtration pump housing feed end is connected with the filter cavity, described to filter going out for the pump housing Material end is connected with the first end of the backflow body, and the second end of the backflow body is connected with the upper cover, the valve It is arranged on the backflow body；And

Activity provision for disengagement, the activity provision for disengagement include that locking plate body, securing member first installs plate body and the second peace Dress plate body, the filter box offer dismounting window, and the locking plate body is at least partly embedded in the dismounting window, And close the dismounting window, and the securing member wears the side wall of the locking plate body and the filter box successively, and described the One first side and the latch for installing plate body is shown consideration for and is closed, and described first installs the second side of plate body respectively with described the The one side connection of one side of one filter screen, a side of second filter screen and the 3rd filter screen, second installing plate The first side of body is another with another side of the first filter screen, another side of second filter screen and the 3rd filter screen respectively One side connects, and the second side for installing plate body is supported with the medial wall of the filter box；

Wherein, the locking plate body be provided with position sealing ring with the setting for window of dismounting, the securing member tool There are threaded portion and head, the first end of the threaded portion wears the side wall of the locking plate body and the filter box, institute successively State head to be connected with the second end of the threaded portion, the head has the cross section of regular hexagon structure, the locking plate body Portion is set in setting, and the portion of setting is embedded in the dismounting window, and described first installs plate body installs plate body with described second It is arranged in parallel, first filter screen, second filter screen and the 3rd filter screen are vertically arranged with the described first installation plate body.

Above-mentioned synthesis device is by arranging kettle, mixing stirring device and material filter, and material filter Filtration can be circulated to material goes the removal of impurity to operate, go it is deimpurity operation it is more simple and convenient, production efficiency is also higher.It is logical The activity provision for disengagement is crossed, the screen modules can be preferably dismantled, and then can preferably to the drainage screen group Part is cleaned or replacement operation.

Description of the drawings

Structural representations of the Fig. 1 for the synthesis device of one embodiment of this utility model；

Fig. 2 is enlarged drawings of the Fig. 1 at A；

Partial structural diagrams of the Fig. 3 for the synthesis device of another embodiment of this utility model；

Partial structural diagrams of the Fig. 4 for the synthesis device of another embodiment of this utility model；

Partial structural diagrams of the Fig. 5 for the synthesis device of another embodiment of this utility model；

Partial structural diagrams of the Fig. 6 for the synthesis device of another embodiment of this utility model；

Partial structural diagrams of the Fig. 7 for the synthesis device of another embodiment of this utility model；

Partial structural diagrams of the Fig. 8 for the synthesis device of another embodiment of this utility model；

Partial structural diagrams of the Fig. 9 for the synthesis device of another embodiment of this utility model.

Specific embodiment

For the ease of understanding this utility model, this utility model is more fully retouched below with reference to relevant drawings State.Better embodiment of the present utility model is given in accompanying drawing.But, this utility model can come in many different forms Realize, however it is not limited to embodiments described herein.On the contrary, the purpose for providing these embodiments is to make to this practicality newly It is more thorough comprehensive that the disclosure of type understands.

It should be noted that when element is referred to as " being fixed on " or " being arranged at " another element, it can be directly another On one element or can also there is element placed in the middle.When an element is considered as " connection " another element, it can be with It is directly to another element or may be simultaneously present centering elements.Term as used herein " vertical ", " level ", "left", "right" and similar statement for illustrative purposes only, it is unique embodiment to be not offered as.

Unless otherwise defined, all of technology used herein and scientific terminology are led with technology of the present utility model is belonged to The implication that the technical staff in domain is generally understood that is identical.In term used in the description of the present utility model it is simply herein The purpose of description specific embodiment, it is not intended that in limiting this utility model.Term as used herein " and/or " bag Include the arbitrary and all of combination of one or more related Listed Items.

For example, a kind of synthesis device, including：Kettle, the two ends of the kettle are respectively arranged with upper cover and low head；Stir Mixing arrangement is mixed, the mixing stirring device includes installation frame, motor, drive shaft and stirring paddle, the installation frame Be fixedly mounted on the upper cover, the motor is arranged on the installation frame, the first end of the drive shaft with The rotary shaft connection of the motor, the second end of the drive shaft is connected with the stirring paddle, and the stirring paddle is located at Inside the low head；Material filter, the material filter include material-pumping tube body, filter box, screen modules, The pump housing, backflow body and valve are filtered, the first end of the material-pumping tube body is connected with the bottom of the low head, the Rose Box The hollow setting of body, forms filter cavity in which, the second end of the material-pumping tube body is connected with the first end of the filter box, and Second end of the material-pumping tube body is connected with the filter cavity, the screen modules include the first filter screen, the second filter screen and 3rd filter screen, first filter screen, second filter screen and the 3rd filter screen are arranged at intervals in the filter cavity successively, The edge at the edge of first filter screen, the edge of second filter screen and the 3rd filter screen with the filter box in Side wall connection, first filter screen are arranged towards the direction at the second end of the material-pumping tube body, the feed end for filtering the pump housing It is connected with the second end of the filter box, and the filtration pump housing feed end is connected with the filter cavity, the filter pump The discharge end of body is connected with the first end of the backflow body, and the second end of the backflow body is connected with the upper cover, institute State valve to be arranged on the backflow body；And activity provision for disengagement, the activity provision for disengagement include lock plate body, securing member First installs plate body and second installs plate body, and the filter box offers dismounting window, the locking plate body it is at least part of It is embedded in the dismounting window, and closes the dismounting window, the securing member wears the locking plate body and described successively The side wall of filter box, the described first first side for installing plate body are shown consideration for the latch and are closed, and described first installs plate body A second side side, a side of second filter screen and the 3rd filter screen respectively with first filter screen side Side connect, it is described second install plate body first side respectively with another side of the first filter screen, second filter screen it is another Side and another side connection of the 3rd filter screen, the second side of the installation plate body and the medial wall of the filter box Support.

In order to further explain to above-mentioned synthesis device, for example, the synthesis device of another embodiment is as follows：

Fig. 1 is referred to, synthesis device 10 includes kettle 100, mixing stirring device 200 and material filter 300, stirred Mixing arrangement 200 and material filter 300 are may be contained within kettle 100.

Fig. 1 is referred to, the two ends of kettle 100 are respectively arranged with upper cover 110 and low head 120, and kettle 100 is used to house The material of addition, and mix to material and the offer occasion that reacts.For example, after upper cover 110 is connected with low head 120 Form kettle 100.And for example, the kettle is formed in one structure.And for example, in the process for being installed on outside support of the kettle In, the top of the externally-located support of the upper cover, the bottom of the externally-located support of the low head.

For example, it is hemispherical columnar structured that the kettle has two ends, and certainly, the kettle can be with according to reality Situation is selected, and for example, adopts two ends for the columnar structured of plane.

Fig. 1 is referred to, mixing stirring device 200 includes installation frame 210, motor 220, drive shaft 230 and stirring Oar 240, installation frame 210 are fixedly mounted on the upper cover 110 of kettle 100, and motor 220 is arranged at installation frame 210 On, the first end of drive shaft 230 is connected with the rotary shaft of motor 220, and the second end of drive shaft 230 stretches to kettle 100 Inside, e.g., the second end of drive shaft 230 is stretched to inside the low head 120 of kettle 100, the second end and the stirring of drive shaft 230 Oar 240 connects, and e.g., stirring paddle 240 is located inside the low head 120 of kettle 100.

For example, the stirring paddle is anchor formula stirring paddle or propeller, certainly, can also be selected according to actual needs Use other kinds of stirring paddle.

Fig. 1 is referred to, motor 220 is used to drive drive shaft 230 to rotate, and then driven and the fixation of drive shaft 230 Stirring paddle 240 is rotated.When needing to be stirred married operation to the material in kettle 100, control motor 220 drives and drives Moving axis 230 is rotated, and then drives stirring paddle 240 to rotate, and is acted on using the flow-disturbing of stirring paddle 240, can play preferably stirring Immixture, and then married operation can be stirred to the material in kettle 100.

Fig. 1 and Fig. 2 is seen also, material filter 300 includes material-pumping tube body 310, filter box 320, drainage screen Component 330, the filtration pump housing 340, backflow body 350 and valve 360, low head 120, material-pumping tube body 310, filter box 320, mistake Filter pump body 340, backflow body 350 and upper cover 110 are sequentially communicated, and screen modules 330 are placed in inside filter box 320, Valve 360 is arranged on backflow body 350.

Fig. 1 and Fig. 2 is seen also, the first end of material-pumping tube body 310 is connected with the bottom of low head 120, so, works as kettle When being reacted, material can be flowed in material-pumping tube body 310, and then after carrying out from low head 120 material in body 100 Continuous filter operation.

Fig. 2 is referred to, 320 hollow setting of filter box forms filter cavity 321, material-pumping tube body in filter box 320 310 the second end is connected with the first end of filter box 320, and the second end of material-pumping tube body 310 is connected with filter cavity 321, So, the material to be filtered for flowing into from material-pumping tube body 310 can be just flowed into inside filter cavity 321, and in filter cavity Filter operation is completed in 321.

Refer to Fig. 2, screen modules 330 include the first filter screen 331, the second filter screen 332 and the 3rd filter screen 333, first Filter screen 331, the second filter screen 332 and the 3rd filter screen 333 are arranged at intervals in filter cavity 321 successively, the edge of the first filter screen 331st, the edge at the edge 332 and the 3rd filter screen 333 of the second filter screen is connected with the medial wall of filter box 320, so, from taking out The material flowed out in expects pipe body 310 passes through the first filter screen 331, the second filter screen 332 and the 3rd filter screen 333 successively, so that material Filter operation is completed, the impurity in material can be preferably removed, is operated more convenient simple.For example, the first filter screen 331, second Filter screen 332 and the 3rd filter screen 333 interval setting successively, so that gap between filter screen, is left, in such manner, it is possible to better profit from The gap accommodates the impurity being filtered out, and and for example, the impurity being filtered out is cleared up at interval of Preset Time, to reduce filter screen Or the problem of casing blocking occurs.

In order to preferably improve the filter effect of the screen modules, for example, first filter screen, second filter screen And the filter opening aperture of the 3rd filter screen is sequentially reduced, so, three layers of effect for progressively filtering are taken, different-grain diameter can be directed to Impurity, to optimize filtration path, and then can preferably improve the filter effect of the screen modules.

Fig. 1 and Fig. 2 is seen also, the feed end for filtering the pump housing 340 is connected with the second end of filter box 320, and mistake 340 feed end of filter pump body is connected with filter cavity 321, and the discharge end and the first end of backflow body 350 for filtering the pump housing 340 connects Logical, the second end of the body 350 that flows back is connected with upper cover 110.Thus, based on the filtration pump housing 340 in normal work, generation Suction, material can be filtered the pump housing 340 and is pumped in material-pumping tube body 310 from low head 120, then be taken out by material-pumping tube body 310 It is drawn in filter box 320, and first filter screen 331 of the material in the filter box 320, the second filter screen 332 and During three filter screens 333, filter operation is completed, that is, complete deimpurity operation, after material completes filter operation, then, passed through It is described to filter the pump housing 340 material after being filtered, in the presence of the pump housing 340 is filtered, it is pulled in backflow body 350, Finally, then it is back in upper cover 110, i.e. be back to inside kettle 100, now, material completes a filter operation, certainly, In order to further improve the removal effect of impurity, according to practical situation, circulating filtration operation is can also carry out.

For example, the first filter screen 331 is arranged towards the direction at the second end of material-pumping tube body 310, and the 3rd filter screen 333 is towards backflow Body 350 is arranged.

Fig. 2 is referred to, valve 360 is arranged on backflow body 350, when needing to carry out filter operation, opens valve 360, now, material carries out filter operation, after filter operation is completed, shutoff valve in 300 internal circulation flow of material filter Door 360, now, material stops flowing in material filter 300.

Above-mentioned synthesis device 10 is by arranging kettle 100, mixing stirring device 200 and material filter 300, and thing Material defecator 300 can be circulated filtration and go the removal of impurity to operate to material, go deimpurity operation more simple and convenient, production Efficiency is also higher.

In order to reduce the problem to screen modules impact because of the excessive generation of material pressure, preferably to protect drainage screen The dispersion effect of component and strength imparting material, for example, sees also Fig. 3 and Fig. 4, and the synthesis device also includes pressure buffer Device 400, the pressure buffer device 400 be located at the material-pumping tube body 310 and screen modules 330 the first filter screen 331 it Between, the pressure buffer device 400 includes some buffering plate bodys 410, and some buffering plate bodys are arranged at intervals at described successively In filter cavity, and the edge of some buffering plate bodys is connected with the medial wall of the filter box, the buffering plate body 410 offer flowing hole 411；And for example, the buffering plate body offers some flowing holes；And for example, some flowing holes are in square Shape array distribution is on the buffering plate body；And for example, the flowing hole of the two neighboring buffering plate body is shifted to install；Again Such as, the flowing hole has the cross section of regular polygon structure；And for example, the flowing hole has regular hexagon feature cross-section； And for example, it is described buffering plate body there is cuboid shape structure, so, when material is through pressure buffer device 400, can reduce because The problem to screen modules impact of the excessive generation of material pressure, preferably to protect screen modules and strength imparting material Dispersion effect.

In order to preferably dismantle the screen modules, so preferably the screen modules can be cleaned or Replacement operation, for example, sees also 5, and the synthesis device also includes activity provision for disengagement 500, the activity provision for disengagement 500 include that locking plate body 510, securing member 520 first installs plate body 530 and the second installation plate body 540, the filter box 320 Offer dismounting window 322, the locking plate body is at least partly embedded in the dismounting window, and closes the dismounting window Mouthful, the securing member wears the side wall of the locking plate body and the filter box successively, and described first installs the first of plate body Side and the latch are shown consideration for and are closed, described first install the second side of a plate body side respectively with first filter screen, The one side connection of one side of second filter screen and the 3rd filter screen, described second installs the first side difference of plate body It is connected with another side of another side of the first filter screen, another side of second filter screen and the 3rd filter screen, it is described The second side for installing plate body is supported with the medial wall of the filter box.The locking plate body is set with the dismounting window Sealing ring is provided with position；And for example, the first end that the securing member has threaded portion and head, the threaded portion is worn successively The side wall of the locking plate body and the filter box, the head are connected with the second end of the threaded portion；And for example, the head Portion has the cross section of regular hexagon structure；And for example, the locking plate body arranges the portion that sets, and the portion of setting is embedded at described tearing open Unload in window；And for example, the first installation plate body is be arranged in parallel with the described second installation plate body；And for example, first filter screen, institute State the second filter screen and the 3rd filter screen to be vertically arranged with the described first installation plate body, so, by the activity provision for disengagement 500, the screen modules can be preferably dismantled, and then preferably the screen modules can be cleaned or be changed Operation.

In order to preferably support the screen modules, for preferably protecting the screen modules, for example, refer to Fig. 6, the synthesis device also include filtering support meanss 600, and the filtration support meanss 600 include the first support rack 610 And second support rack 620, it is described first support rack edge be connected with the medial wall of the filter box, described first Support rack is located between first filter screen and second filter screen, and the first support rack offers the first mesh, described The edge of the second support rack is connected with the medial wall of the filter box, and described second supports rack to be located at second filter screen And between the 3rd filter screen, the second support rack offers the second mesh.The mesh of first filter screen, described second The filter opening size of the mesh of filter screen and the 3rd filter screen is sequentially reduced；And for example, first filter screen, first supporting network Frame, second filter screen, the second support rack and the 3rd filter screen be arranged in parallel；And for example, first mesh is big Little setting identical with the size of second mesh；And for example, first mesh and second mesh are the poroid knot of rhombus Structure；And for example, interval is provided between the first support rack and first filter screen and second filter screen；And for example, institute State and interval is provided between the second support rack and second filter screen and the 3rd filter screen, so, by arranging first Support rack 610 and second to support rack 620, can preferably support the screen modules, for preferably protecting described Screen modules.

In order to reduce vortex phenomenon, and flow-disturbing degree when can improve stirring operation, for example, Fig. 7 is referred to, The synthesis device also include baffle means 700, if the baffle means 700 include install the body of rod 710, baffling montant 720 and Dry baffling cross bar 730, the first end for installing the body of rod 710 are connected with the medial wall of the low head 120, the baffling montant It is connected with second end for installing the body of rod, some baffling cross bars are arranged at intervals on the baffling montant successively, and if Do the baffling cross bar to be arranged in parallel.The first end for installing the body of rod is provided with the binding face of arc-shaped curved surface structure, the patch Fit with the medial wall of the low head in conjunction face；And for example, the installation body of rod is provided with reinforcement；And for example, the reinforcement by The first end for installing the body of rod is extended to second end for installing the body of rod；And for example, the baffling montant and the drive Moving axis be arranged in parallel；And for example, the baffling montant has hollow structure；And for example, the end of the baffling cross bar has hemispherical Structure, flow-disturbing when so, by arranging baffle means 700, vortex phenomenon can be reduced, and can improve stirring operation Degree.

In order to reduce the drive shaft when rotating, the concussion problem of generation for example, refers to Fig. 8, the synthesis device Also include stirring stopping means 800, the stirring stopping means 800 include spacing body 810 and spacing connecting rod 820, described Spacing body 810 is placed on outside the second end of the drive shaft 230, and the spacing body 810 be located at the stirring paddle 240 and Between the bottom of the low head 120, between being provided between the medial wall of the spacing body and the lateral wall of the drive shaft Every the first end of the spacing body of rod is connected with the spacing body, the second end and the low head of the spacing body of rod Bottom connects, and the bearing of trend of the spacing body of rod forms angle with the bearing of trend of the drive shaft；And for example, the stirring Oar is propeller；And for example, the spacing body has rounded cylindrical structure；And for example, the central axis of the spacing body With the central axes of the drive shaft；And for example, the stirring stopping means arrange some spacing connecting rods, Ruo Gansuo State spacing connecting rod distribution is put so that the center of the drive shaft is radial；And for example, the stirring stopping means arrange two institutes Spacing connecting rod is stated, between two spacing connecting rods, angle is formed；And for example, the number of degrees of the angle are 60 degree～120 degree, So, by arrange stirring stopping means 800, can reduce the drive shaft rotate when, the concussion problem of generation.

It is pointed out that when each material that married operation is stirred inside the kettle carries out combination reaction, and Most combination reaction is all that the yield of exothermic reaction, the speed of reaction and product generation is also required to what is released during dependent reaction Heat, for improving reaction rate and yield.Additionally, in whipping process, the mixing stirring device can do work to material, i.e., Material during agitation is mutually mixed shows as outwardly releasing heat, especially the stronger material of toughness, its heat release Phenomenon becomes apparent from, therefore, based on above-mentioned situation, for the combination reaction of some dependence higher temperatures, such as depend on reaction itself Heat release and the combination reaction of stirring heat production, and do not need extra heater for the reaction heated by which, it is especially desirable to Guarantee the heat-insulating property of the kettle.Further, in order to be directed to some acid materials, therefore, to assure that the inner side of the kettle Wall, i.e., the medial wall of the kettle for directly contacting with acid material possess higher acid etch resistance energy, for prolonging the life kettle The service life of body and being normally carried out for reaction.Further, the lateral wall of the kettle is often connect with corrosive materials due to Jing Touch, e.g., the corrosive materials contact of the form such as gaseous state or liquid, it is therefore desirable to possess preferable decay resistance, for more preferable The ground protection kettle.

In order to improve acid etch resistance energy, heat-insulating property and the decay resistance of the kettle, for example, Fig. 8 is referred to, it is described Kettle, e.g., resistance to acid attack layer 130 that the side wall of the kettle includes being cascading, heat-insulation layer 140, supporting layer 150, counterweight Layer 160 and protective layer 170, the resistance to acid attack layer are located at the medial wall of the kettle, and the resistance to acid attack layer is directly and material, Such as, acid material contact, the protective layer are located at the lateral wall of the kettle, i.e., described protective layer is directly naked to be exposed on the external.

For example, the resistance to acid attack layer of an embodiment includes each component of following mass parts：75 parts～88 parts of ferrum, titanium 30 Part～34 parts, 20 parts～25 parts of chromium, 2.5～3.4 parts of antimony, 2.3～3.4 parts of copper part, 1.5 parts～2.7 parts of zinc, aluminum 0.9～1.4 Part, 0.15 part～0.27 part of carbon, 0.25 part～0.46 part of silicon, 0.12 part～0.18 part of boron, 0.04 part～0.09 part of cobalt, phosphorus 0.001 part～0.03 part, 0.001 part～0.03 part of sulfur, 0.02 part～0.03 part of strontium, 0.03 part～0.04 part of bismuth, 0.01 part of scandium ～0.02 part and 0.001 part～0.002 part of gadolinium.Wherein, scandium is for scandium or contains scadium compound, wherein, scandium is contained within containing scadium compound Element；Gadolinium is for gadolinium or contains gadolinium compound, wherein, gadolinium element is contained within containing gadolinium compound；Bismuth is bismuth or bismuth-containing compound, wherein, Bismuth gadolinium compound is contained within bismuth element；Strontium is for strontium or contains strontium compound, wherein, strontium gadolinium compound is contained within strontium element.

Using 75 parts～88 parts of ferrum, 20 parts～25 parts infrastructure elements as resistance to acid attack layer of 30 parts～34 parts of titanium and chromium, from And the resistance to acid attack layer can be enable to possess certain acid etch resistance, additionally, by adding 2.5～3.4 parts of antimony, 2.3 parts of copper ～3.4 parts, 1.5 parts～2.7 parts of zinc, 0.9～1.4 part of aluminum, 0.04 part～0.09 part of cobalt, 0.02 part～0.03 part of strontium, bismuth 0.03 0.001 part～0.002 part of part～0.04 part, 0.01 part～0.02 part of scandium and gadolinium are compounded, additionally it is possible to further optimized described The properties of resistance to acid attack layer, especially can further optimize the acid etch resistance energy of the resistance to acid attack layer such that it is able to more preferably The acid etching of ground opposing material, for further improving the service life of the kettle and guaranteeing that what is reacted is normally carried out.

And for example, the resistance to acid attack layer of another embodiment includes each component of following mass parts：75 parts～80 parts of ferrum, titanium 33 parts～34 parts, 24 parts～25 parts of chromium, 2.7～3.4 parts of antimony, 2.7 parts～3.4 parts of copper, 1.8 parts～2.5 parts of zinc, aluminum 1.1～1.4 Part, 0.18 part～0.27 part of carbon, 0.27 part～0.46 part of silicon, 0.13 part～0.18 part of boron, 0.04 part～0.09 part of cobalt, phosphorus 0.001 part～0.03 part, 0.001 part～0.03 part of sulfur, 0.02 part～0.03 part of strontium, 0.03 part～0.04 part of bismuth, 0.01 part of scandium ～0.02 part and 0.001 part～0.002 part of gadolinium.

And for example, the resistance to acid attack layer of another embodiment includes each component of following mass parts：77 parts of ferrum, 33 parts of titanium, 25 parts of chromium, 3.4 parts of antimony, 2.7 parts of copper, 1.9 parts of zinc, 1.3 parts of aluminum, 0.27 part of carbon, 0.46 part of silicon, 0.18 part of boron, 0.04 part of cobalt, phosphorus 0.002 part of 0.03 part, 0.001 part of sulfur, 0.03 part of strontium, 0.04 part of bismuth, 0.01 part of scandium and gadolinium.

For example, the heat-insulation layer of an embodiment includes each component of following mass parts：It is 15 parts～22 parts of Gypsum Fibrosum powder, white 8～20 parts of cotton, 8 parts～15 parts of rock wool, 7 parts～9 parts of glass fibre, 10 parts～20 parts of Lauxite, 3.5 parts of polyacrylamide～ 4.5 parts, 1 part～3 parts of basalt fibre, 3～5 parts of rubber foam, 1 part～2 parts of magnesium hydroxide, aminopropyl triethoxysilane 1 Part～2 parts, 1 part～2 parts of aluminium oxide, 1 part～2 parts of 3,5- di-tert-butyl-4-hydroxybenzoic acids methyl ester, 3～4 parts of polypropylene fiber, 0.2～0.8 part of 1 part～2 parts of thiorubber. and sodium lauryl sulphate.

Can make the heat-insulation layer that there is good heat-insulating property using each component of as above mass parts, when in the kettle When the material in portion occurs exothermic reaction, and after transferring heat to the resistance to acid attack layer, had based on the heat-insulation layer good Heat-insulated and heat-insulating property, can limit heat and be further transmitted through the kettle, and then avoid heat from being transferred directly to external environment In, it is ensured that the material inside the kettle is reacted at a suitable temperature, for improving the product of reaction rate and product Rate.

And for example, the heat-insulation layer of another embodiment includes each component of following mass parts：17 parts～21 parts of Gypsum Fibrosum powder, White 17～20 parts of cotton, 10 parts～15 parts of rock wool, 7 parts～9 parts of glass fibre, 10 parts～20 parts of Lauxite, polyacrylamide 3.5 Part～4.5 parts, 1 part～2.5 parts of basalt fibre, 3.5～5 parts of rubber foam, 1.5 parts～2 parts of magnesium hydroxide, three second of aminopropyl 1.5 parts～2 parts of TMOS, 1 part～2 parts of aluminium oxide, 1 part～1.4 parts of 3,5- di-tert-butyl-4-hydroxybenzoic acids methyl ester, third 0.2～0.5 part of 3.3～4 parts of synthetic fibre fiber, 1 part～2 parts of thiorubber. and sodium lauryl sulphate.

And for example, the heat-insulation layer of another embodiment includes each component of following mass parts：19 parts of Gypsum Fibrosum powder, white cotton 17 ～20 parts, 15 parts of rock wool, 9 parts of glass fibre, 20 parts of Lauxite, 3.8 parts of polyacrylamide, 2.1 parts of basalt fibre, rubber 4.6 parts of foam, 1.7 parts of magnesium hydroxide, 2 parts of aminopropyl triethoxysilane, 1.8 parts of aluminium oxide, 3,5- di-t-butyl -4- hydroxyls 0.4 part of 1.4 parts of essence of Niobe, 4 parts of polypropylene fiber, 1.9 parts of thiorubber. and sodium lauryl sulphate.

For example, the supporting layer of an embodiment includes each component of following mass parts：95 parts～98 parts of ferrum, manganese 0.4 Part～0.95 part, 0.1 part～0.5 part of molybdenum, 0.01 part～0.05 part of titanium, 0.02 part～0.1 part of aluminum, 0.06 part～0.25 part of carbon, 0.1 part～0.3 part of silicon, 0.05 part～0.1 part of phosphorus, 0.001 part～0.01 part of boron, 0.05 part～0.5 part of hafnium, 0.05 part of scandium～ 0.3 part, 0.05 part～0.3 part of chromium, 0.01 part～0.05 part of nickel, 0.01 part～0.05 part of cerium, 0.01 part～0.05 part of thorium and zirconium 0.01 part～0.05 part.Wherein, hafnium is for hafnium or contains hafnium compound, wherein, hafnium element is contained within containing hafnium compound；Scandium is scandium or contains Scadium compound, wherein, scandium element is contained within containing scadium compound；Thorium is for thorium or contains thorium compound, wherein, cerium-containing compound is contained within Ce elements；Cerium is cerium or cerium-containing compound, wherein, cerium-containing compound is contained within Ce elements.

It is appreciated that in order that the kettle possesses preferable heat-insulating property, need to introduce the heat-insulation layer, and the guarantor The mechanical strength of warm layer is poor, in order to strengthen the integrally-built mechanical strength of the kettle, needs to introduce the supporting layer so as to With the heat-insulation layer directly contact, for improving the integrally-built mechanical strength of the kettle, to reach the purpose of safety in production. Based on above-mentioned situation, this just necessarily requires the supporting layer to possess higher mechanical strength and anti-deformation nature, by adopting such as The improve quality each component of part, the especially supporting layer contains 0.05 part～0.5 part of hafnium, 0.05 part～0.3 part of scandium, 0.05 part of chromium 0.01 part～0.05 part of～0.3 part, 0.01 part～0.05 part of nickel, 0.01 part～0.05 part of cerium, 0.01 part～0.05 part of thorium and zirconium, The mechanical strength of traditional ferroalloy can be improved so as to which mechanical strength and anti-deformation nature are more excellent, disclosure satisfy that requirement.

And for example, the supporting layer of another embodiment includes each component of following mass parts：97 parts～98 parts of ferrum, manganese 0.55 part～0.95 part, 0.35 part～0.5 part of molybdenum, 0.01 part～0.05 part of titanium, 0.02 part～0.1 part of aluminum, 0.17 part of carbon～ 0.25 part, 0.1 part～0.25 part of silicon, 0.05 part～0.1 part of phosphorus, 0.008 part～0.01 part of boron, 0.1 part～0.5 part of hafnium, scandium 0.1 Part～0.3 part, 0.1 part～0.3 part of chromium, 0.02 part～0.05 part of nickel, 0.02 part～0.05 part of cerium, 0.02 part～0.05 part of thorium and 0.02 part～0.05 part of zirconium.

And for example, the supporting layer of another embodiment includes each component of following mass parts：97 parts of ferrum, 0.75 part of manganese, 0.5 part of molybdenum, 0.05 part of titanium, 0.02 part of aluminum, 0.17 part of carbon, 0.25 part of silicon, 0.1 part of phosphorus, 0.008 part of boron, 0.5 part of hafnium, scandium 0.2 Part, 0.2 part of chromium, 0.05 part of nickel, 0.05 part of cerium, 0.05 part of thorium and 0.05 part of zirconium.

For example, the weight coating of an embodiment includes each component of following mass parts：85 parts～95 parts of tungsten, 30 parts of nickel 0.5 part～5 parts of～60 parts, 15 parts～40 parts of ferrum, 1.5 parts～10 parts of chromium, 1.5 parts～10 parts of lead, 1 part～6 parts of copper and molybdenum.

It is appreciated that in production course of reaction, needs carry out the higher stirring behaviour of intensity to the material in the kettle Make, and as thickness is larger and the presence of the heat-insulation layer of lighter weight, in order to avoid the integrally-built matter of the kettle Amount kicks the beam, and then reduces impact of the external impacts to the kettle, you can concussion or displacement problem occur to reduce the kettle. The weight coating can be made to possess excellent counterweight performance using each component of as above mass parts, can effectively increase the kettle The integrally-built weight of body so as to or adaptation identical with the weight of traditional kettle, such that it is able to improve the peace in production process Full performance.

And for example, the weight coating of another embodiment includes each component of following mass parts：90 parts～95 parts of tungsten, nickel 30 0.5 part of part～45 parts, 27 parts～40 parts of ferrum, 1.5 parts～2.3 parts of chromium, 1.5 parts～3.3 parts of lead, 1 part～5.5 parts of copper and molybdenum～ 4.9 part.

And for example, the weight coating of another embodiment includes each component of following mass parts：92 parts of tungsten, 38 parts of nickel, ferrum 3.8 parts of 29 parts, 2.1 parts of chromium, 2.1 parts of lead, 3.5 parts of copper and molybdenum.

For example, the protective layer of an embodiment includes each component of following mass parts：65 parts～80 parts of ferrum, lithium 16～ 18 parts, 18 parts～25 parts of nickel, 3.5 parts～4 parts of molybdenum, 2 parts～5 parts of chromium, 1 part～5 parts of cobalt, 1 part～5 parts of vanadium, 1 part～2 parts of manganese, iridium 0.8 part～2.5 parts, 0.5 part～2.5 parts of niobium, 0.3 part～2.5 parts of scandium, 0.2 part～2.5 parts of strontium, 0.2 part～2.5 parts of caesium, tungsten 0.2 part～2.5 parts and 0.2 part～2.5 parts of titanium.Wherein, caesium is for caesium or contains cesium compound, wherein, caesium is contained within containing cesium compound Element；Wherein, strontium is for strontium or contains strontium compound, wherein, strontium element is contained within containing strontium compound；Wherein, scandium is scandium or contains scandium Compound, wherein, scandium element is contained within containing scadium compound；Wherein, niobium is for niobium or contains niobium compound, wherein, include containing niobium compound There is niobium element；Wherein, iridium is for iridium or contains iridic compound, wherein, iridium is contained within containing iridic compound.

It is appreciated that the lateral wall of the kettle is often contacted with corrosive materials due to Jing, and e.g., the form such as gaseous state or liquid Corrosive materials contact, it is therefore desirable to possess preferable decay resistance, for preferably protecting the kettle.By as above The each component of mass parts, can make the protective layer possess good Corrosion Protection, and then preferably protect the kettle, use In the service life for extending the kettle.

And for example, the protective layer of another embodiment includes each component of following mass parts：65 parts～70 parts of ferrum, lithium 16 Part～16.5 parts, 18～21 parts of nickel, 3.5 parts～3.9 parts of molybdenum, 2 parts～4.4 parts of chromium, 1 part～3.9 parts of cobalt, 1 part～4.5 parts of vanadium, 1 part～1.7 parts of manganese, 0.8 part～2.3 parts of iridium, 0.5 part～2.2 parts of niobium, 0.3 part～2.3 parts of scandium, 0.2 part～2.3 parts of strontium, caesium 0.2 part～1.9 parts of 0.2 part～2.4 parts, 0.2 part～2.1 parts of tungsten and titanium.

And for example, the protective layer of another embodiment includes each component of following mass parts：65 parts of ferrum, 16.5 parts of lithium, 21 parts of nickel, 3.5 parts of molybdenum, 3.5 parts of chromium, 2.8 parts of cobalt, 3.7 parts of vanadium, 1.5 parts of manganese, 2.3 parts of iridium, 2.2 parts of niobium, 2.3 parts of scandium, strontium 2.3 Part, 2.4 parts of caesium, 0.2 part of tungsten and 0.2 part of titanium.

In order to further optimize the kettle, e.g., the structure of the side wall of the kettle, for example it is, the resistance to acid attack layer, described The thickness ratio of heat-insulation layer, the supporting layer, the weight coating and the protective layer is (1～1.5)：(15～20)：(5～5.5)： (8～9.8)：(0.5～1.2)；And for example, the thickness ratio of the weight coating and the protective layer is 1：15：5：9.5：1.1.

It should be noted that other embodiment of the present utility model also includes that the technical characteristic in the various embodiments described above is mutual With reference to what is can formed, and the synthesis device that can implement.

Each technical characteristic of embodiment described above arbitrarily can be combined, to make description succinct, not to above-mentioned reality Apply all possible combination of each technical characteristic in example to be all described, as long as however, the combination of these technical characteristics is not deposited In contradiction, the scope of this specification record is all considered to be.

The above embodiment only expresses several embodiments of the present utility model, and its description is more concrete and detailed Therefore carefully, but the restriction to this utility model the scope of the claims can not be interpreted as.It should be pointed out that general for this area For logical technical staff, without departing from the concept of the premise utility, some deformations and improvement can also be made, these are all Belong to protection domain of the present utility model.Therefore, the protection domain of this utility model patent should be defined by claims.

Claims (1)

1. a kind of synthesis device, it is characterised in that include：

Kettle, the two ends of the kettle are respectively arranged with upper cover and low head；

Mixing stirring device, the mixing stirring device include installation frame, motor, drive shaft and stirring paddle, the peace Installation frame is fixedly mounted on the upper cover, and the motor is arranged on the installation frame, and the of the drive shaft One end is connected with the rotary shaft of the motor, and the second end of the drive shaft is connected with the stirring paddle, and the stirring Oar is located inside the low head；

Material filter, the material filter include material-pumping tube body, filter box, screen modules, filter the pump housing, return Flow tube body and valve, the first end of the material-pumping tube body are connected with the bottom of the low head, the hollow setting of the filter box, Filter cavity is formed in which, the second end of the material-pumping tube body is connected with the first end of the filter box, and the material-pumping tube Second end of body is connected with the filter cavity, and the screen modules include the first filter screen, the second filter screen and the 3rd filter screen, institute State the first filter screen, second filter screen and the 3rd filter screen to be arranged at intervals in the filter cavity successively, first filter The edge at the edge of net, the edge of second filter screen and the 3rd filter screen is connected with the medial wall of the filter box, Direction setting of first filter screen towards the second end of the material-pumping tube body, the feed end for filtering the pump housing and the filtration Second end of casing connects, and the filtration pump housing feed end is connected with the filter cavity, the discharge end for filtering the pump housing Connect with the first end of the backflow body, the second end of the backflow body is connected with the upper cover, and the valve is arranged On the backflow body；And

Activity provision for disengagement, the activity provision for disengagement include that locking plate body, securing member first installs plate body and the second installing plate Body, the filter box offer dismounting window, and the locking plate body is at least partly embedded in the dismounting window, and seals The dismounting window is closed, the securing member wears the side wall of the locking plate body and the filter box, first peace successively The first side of dress plate body is shown consideration for the latch and is closed, and the described first second side for installing plate body is filtered with described first respectively The one side connection of one side, a side of second filter screen and the 3rd filter screen of net, described second installs plate body First side opposite side respectively with another side of the first filter screen, another side of second filter screen and the 3rd filter screen Side connects, and the second side for installing plate body is supported with the medial wall of the filter box；

Wherein, the locking plate body be provided with position sealing ring with the setting for window of dismounting, and the securing member has spiral shell Stricture of vagina portion and head, the first end of the threaded portion wear the side wall of the locking plate body and the filter box, the head successively Portion is connected with the second end of the threaded portion, and the head has the cross section of regular hexagon structure, and the locking plate body is arranged Portion is set, the portion of setting is embedded in the dismounting window, and it is parallel that the first installation plate body installs plate body with described second Arrange, first filter screen, second filter screen and the 3rd filter screen are vertically arranged with the described first installation plate body.