CN105964209B - Efficiently synthesize equipment - Google Patents

Efficiently synthesize equipment Download PDF

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Publication number
CN105964209B
CN105964209B CN201610514340.5A CN201610514340A CN105964209B CN 105964209 B CN105964209 B CN 105964209B CN 201610514340 A CN201610514340 A CN 201610514340A CN 105964209 B CN105964209 B CN 105964209B
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Prior art keywords
strainer
parts
filter
installation
plate body
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CN201610514340.5A
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CN105964209A (en
Inventor
吴玲玲
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Nantong Mengding New Materials Co ltd
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Tao Lemin
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Priority to CN201810553024.8A priority Critical patent/CN108837783A/en
Priority to CN201610514340.5A priority patent/CN105964209B/en
Priority to CN201810553773.0A priority patent/CN108479672A/en
Publication of CN105964209A publication Critical patent/CN105964209A/en
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    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J19/18—Stationary reactors having moving elements inside
    • B01J19/1868—Stationary reactors having moving elements inside resulting in a loop-type movement
    • B01J19/1881—Stationary reactors having moving elements inside resulting in a loop-type movement externally, i.e. the mixture leaving the vessel and subsequently re-entering it
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01F—MIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
    • B01F27/00—Mixers with rotary stirring devices in fixed receptacles; Kneaders
    • B01F27/05—Stirrers
    • B01F27/11—Stirrers characterised by the configuration of the stirrers
    • B01F27/112—Stirrers characterised by the configuration of the stirrers with arms, paddles, vanes or blades
    • B01F27/1122—Stirrers characterised by the configuration of the stirrers with arms, paddles, vanes or blades anchor-shaped
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01F—MIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
    • B01F27/00—Mixers with rotary stirring devices in fixed receptacles; Kneaders
    • B01F27/80—Mixers with rotary stirring devices in fixed receptacles; Kneaders with stirrers rotating about a substantially vertical axis
    • B01F27/90—Mixers with rotary stirring devices in fixed receptacles; Kneaders with stirrers rotating about a substantially vertical axis with paddles or arms 
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01F—MIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
    • B01F27/00—Mixers with rotary stirring devices in fixed receptacles; Kneaders
    • B01F27/80—Mixers with rotary stirring devices in fixed receptacles; Kneaders with stirrers rotating about a substantially vertical axis
    • B01F27/91—Mixers with rotary stirring devices in fixed receptacles; Kneaders with stirrers rotating about a substantially vertical axis with propellers
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01F—MIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
    • B01F33/00—Other mixers; Mixing plants; Combinations of mixers
    • B01F33/80—Mixing plants; Combinations of mixers
    • B01F33/82—Combinations of dissimilar mixers
    • B01F33/822—Combinations of dissimilar mixers with moving and non-moving stirring devices in the same receptacle
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01F—MIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
    • B01F35/00—Accessories for mixers; Auxiliary operations or auxiliary devices; Parts or details of general application
    • B01F35/181—Preventing generation of dust or dirt; Sieves; Filters
    • B01F35/187—Preventing generation of dust or dirt; Sieves; Filters using filters in mixers, e.g. during venting
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J19/0053—Details of the reactor
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J19/0053—Details of the reactor
    • B01J19/006—Baffles
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
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    • B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J19/0053—Details of the reactor
    • B01J19/0066—Stirrers
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
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    • B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J19/02—Apparatus characterised by being constructed of material selected for its chemically-resistant properties
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J19/18—Stationary reactors having moving elements inside
    • B01J19/20—Stationary reactors having moving elements inside in the form of helices, e.g. screw reactors
    • C—CHEMISTRY; METALLURGY
    • C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
    • C22C—ALLOYS
    • C22C27/00—Alloys based on rhenium or a refractory metal not mentioned in groups C22C14/00 or C22C16/00
    • C22C27/04—Alloys based on tungsten or molybdenum
    • C—CHEMISTRY; METALLURGY
    • C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
    • C22C—ALLOYS
    • C22C30/00—Alloys containing less than 50% by weight of each constituent
    • C22C30/02—Alloys containing less than 50% by weight of each constituent containing copper
    • C—CHEMISTRY; METALLURGY
    • C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
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    • C22C30/00—Alloys containing less than 50% by weight of each constituent
    • C22C30/04—Alloys containing less than 50% by weight of each constituent containing tin or lead
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    • C22C38/00—Ferrous alloys, e.g. steel alloys
    • C22C38/002—Ferrous alloys, e.g. steel alloys containing In, Mg, or other elements not provided for in one single group C22C38/001 - C22C38/60
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    • C22C38/00—Ferrous alloys, e.g. steel alloys
    • C22C38/005—Ferrous alloys, e.g. steel alloys containing rare earths, i.e. Sc, Y, Lanthanides
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    • C22C38/02—Ferrous alloys, e.g. steel alloys containing silicon
    • C—CHEMISTRY; METALLURGY
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    • C22C38/04—Ferrous alloys, e.g. steel alloys containing manganese
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    • C22C—ALLOYS
    • C22C38/00—Ferrous alloys, e.g. steel alloys
    • C22C38/06—Ferrous alloys, e.g. steel alloys containing aluminium
    • C—CHEMISTRY; METALLURGY
    • C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
    • C22C—ALLOYS
    • C22C38/00—Ferrous alloys, e.g. steel alloys
    • C22C38/18—Ferrous alloys, e.g. steel alloys containing chromium
    • C22C38/40—Ferrous alloys, e.g. steel alloys containing chromium with nickel
    • C22C38/44—Ferrous alloys, e.g. steel alloys containing chromium with nickel with molybdenum or tungsten
    • C—CHEMISTRY; METALLURGY
    • C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
    • C22C—ALLOYS
    • C22C38/00—Ferrous alloys, e.g. steel alloys
    • C22C38/18—Ferrous alloys, e.g. steel alloys containing chromium
    • C22C38/40—Ferrous alloys, e.g. steel alloys containing chromium with nickel
    • C22C38/46—Ferrous alloys, e.g. steel alloys containing chromium with nickel with vanadium
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    • C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
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    • C22C38/00—Ferrous alloys, e.g. steel alloys
    • C22C38/18—Ferrous alloys, e.g. steel alloys containing chromium
    • C22C38/40—Ferrous alloys, e.g. steel alloys containing chromium with nickel
    • C22C38/48—Ferrous alloys, e.g. steel alloys containing chromium with nickel with niobium or tantalum
    • C—CHEMISTRY; METALLURGY
    • C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
    • C22C—ALLOYS
    • C22C38/00—Ferrous alloys, e.g. steel alloys
    • C22C38/18—Ferrous alloys, e.g. steel alloys containing chromium
    • C22C38/40—Ferrous alloys, e.g. steel alloys containing chromium with nickel
    • C22C38/50—Ferrous alloys, e.g. steel alloys containing chromium with nickel with titanium or zirconium
    • C—CHEMISTRY; METALLURGY
    • C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
    • C22C—ALLOYS
    • C22C38/00—Ferrous alloys, e.g. steel alloys
    • C22C38/18—Ferrous alloys, e.g. steel alloys containing chromium
    • C22C38/40—Ferrous alloys, e.g. steel alloys containing chromium with nickel
    • C22C38/52—Ferrous alloys, e.g. steel alloys containing chromium with nickel with cobalt
    • C—CHEMISTRY; METALLURGY
    • C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
    • C22C—ALLOYS
    • C22C38/00—Ferrous alloys, e.g. steel alloys
    • C22C38/18—Ferrous alloys, e.g. steel alloys containing chromium
    • C22C38/40—Ferrous alloys, e.g. steel alloys containing chromium with nickel
    • C22C38/54—Ferrous alloys, e.g. steel alloys containing chromium with nickel with boron
    • C—CHEMISTRY; METALLURGY
    • C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
    • C22C—ALLOYS
    • C22C38/00—Ferrous alloys, e.g. steel alloys
    • C22C38/18—Ferrous alloys, e.g. steel alloys containing chromium
    • C22C38/40—Ferrous alloys, e.g. steel alloys containing chromium with nickel
    • C22C38/58—Ferrous alloys, e.g. steel alloys containing chromium with nickel with more than 1.5% by weight of manganese
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00049—Controlling or regulating processes
    • B01J2219/00051—Controlling the temperature
    • B01J2219/0015—Controlling the temperature by thermal insulation means
    • B01J2219/00155—Controlling the temperature by thermal insulation means using insulating materials or refractories
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
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    • B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00761—Details of the reactor
    • B01J2219/00763—Baffles
    • B01J2219/00765—Baffles attached to the reactor wall
    • B01J2219/00768—Baffles attached to the reactor wall vertical
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00761—Details of the reactor
    • B01J2219/00763—Baffles
    • B01J2219/00765—Baffles attached to the reactor wall
    • B01J2219/00777—Baffles attached to the reactor wall horizontal
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/02—Apparatus characterised by their chemically-resistant properties
    • B01J2219/0204—Apparatus characterised by their chemically-resistant properties comprising coatings on the surfaces in direct contact with the reactive components
    • B01J2219/0236—Metal based

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  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Engineering & Computer Science (AREA)
  • Materials Engineering (AREA)
  • Mechanical Engineering (AREA)
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  • Chemical Kinetics & Catalysis (AREA)
  • Physical Or Chemical Processes And Apparatus (AREA)
  • Mixers Of The Rotary Stirring Type (AREA)

Abstract

One kind efficiently synthesizes equipment, including autoclave body, mixing stirring device, material filter and baffle means.The both ends of autoclave body are respectively arranged with upper cover and low head.Mixing stirring device includes installation frame, driving motor, drive shaft and agitating paddle.Material filter includes material-pumping tube body, filter box, screen modules, the filtering pump housing, reflux tube body and valve.Baffle means include the installation body of rod, baffling montant and several baffling cross bars.The above-mentioned equipment that efficiently synthesizes is by setting autoclave body, mixing stirring device and material filter, and material filter can carry out material circulating filtration removal impurity operation, goes that deimpurity operation is more simple and convenient, and production efficiency is also higher.

Description

Efficiently synthesize equipment
Technical field
The present invention relates to chemical industry synthesis equipment technical fields, and equipment is efficiently synthesized more particularly to one kind.
Background technology
At present, in material production field, after especially various materials mixing reacts, the situation of final products is obtained In, it usually needs using chemical industry synthesis equipment, for being stirred mixing to material, and it is made successfully to react, be used for Synthesis obtains the final products of higher quality.
Wherein, due to material before the reaction or after reaction, more or less there are some impurity, traditional removal impurity modes First the product obtained after reaction to be taken out from chemical industry synthesis equipment, then the filter device outside carried out product Filter.
However, above-mentioned go deimpurity mode to still remain the problem of operation is more complicated cumbersome, cause production efficiency relatively low.
Invention content
Based on this, it is necessary to provide a kind of efficient conjunction for going deimpurity operation more simple and convenient and higher production efficiency Forming apparatus.
One kind efficiently synthesizes equipment, including：
Autoclave body, the both ends of the autoclave body are respectively arranged with upper cover and low head；
Mixing stirring device, the mixing stirring device include installation frame, driving motor, drive shaft and agitating paddle, institute It states installation frame to be fixedly mounted on the upper cover, the driving motor is set on the installation frame, the drive shaft First end and the driving motor rotation axis connection, the second end of the drive shaft connect, and described with the agitating paddle Agitating paddle is located inside the low head；
Material filter, the material filter include material-pumping tube body, filter box, screen modules, filter pump Body, reflux tube body and valve, the first end of the material-pumping tube body are connected with the bottom of the low head, and the filter box is hollow Setting, interior to form filter cavity, the second end of the material-pumping tube body is connect with the first end of the filter box, and the pumping The second end of expects pipe body is connected with the filter cavity, and the screen modules include the first strainer, the second strainer and third filter Net, first strainer, second strainer and the third strainer are arranged at intervals at successively in the filter cavity, and described The edge at the edge of one strainer, the edge of second strainer and the third strainer connects with the madial wall of the filter box Connect, first strainer towards the second end of the material-pumping tube body direction set, it is described filtering the pump housing feed end with it is described The second end connection of filter box, and the filtering pump housing feed end is connected with the filter cavity, the filtering pump housing goes out Material end is connected with the first end of the reflux tube body, and the second end of the reflux tube body is connected with the upper cover, the valve It is set on the reflux tube body；And
Baffle means, the baffle means include the installation body of rod, baffling montant and several baffling cross bars, the installation body of rod First end connect with the madial wall of the low head, the baffling montant with it is described installation the body of rod second end connect, it is several The baffling cross bar is arranged at intervals at successively on the baffling montant, and several baffling cross bars are arranged in parallel.
The first end of the installation body of rod is provided with the binding face of arc-shaped curved surface structure, institute in one of the embodiments, The madial wall that binding face is stated with the low head is bonded.
The installation body of rod is provided with reinforcing rib in one of the embodiments,.
The reinforcing rib is from the first end of the installation body of rod to the of the installation body of rod in one of the embodiments, Two ends are extended.
The baffling montant is arranged in parallel with the drive shaft in one of the embodiments,.
The baffling montant has hollow structure in one of the embodiments,.
The end of the baffling cross bar has hemispherical structure in one of the embodiments,.
The above-mentioned equipment that efficiently synthesizes is by setting autoclave body, mixing stirring device and material filter, and material filtering Device can to material carry out circulating filtration removal impurity operation, go it is deimpurity operation it is more simple and convenient, production efficiency also compared with It is high.
Description of the drawings
Fig. 1 is the structure diagram for efficiently synthesizing equipment of an embodiment of the present invention；
Fig. 2 is enlarged drawings of the Fig. 1 at A；
Fig. 3 is the partial structural diagram for efficiently synthesizing equipment of another embodiment of the present invention；
Fig. 4 is the partial structural diagram for efficiently synthesizing equipment of another embodiment of the present invention；
Fig. 5 is the partial structural diagram for efficiently synthesizing equipment of another embodiment of the present invention；
Fig. 6 is the partial structural diagram for efficiently synthesizing equipment of another embodiment of the present invention；
Fig. 7 is the partial structural diagram for efficiently synthesizing equipment of another embodiment of the present invention；
Fig. 8 is the partial structural diagram for efficiently synthesizing equipment of another embodiment of the present invention；
Fig. 9 is the partial structural diagram for efficiently synthesizing equipment of another embodiment of the present invention.
Specific embodiment
For the ease of understanding the present invention, the present invention is described more fully below with reference to relevant drawings.In attached drawing Give the better embodiment of the present invention.But the present invention can realize in many different forms, however it is not limited to herein Described embodiment.On the contrary, the purpose of providing these embodiments is that make to understand more the disclosure Add thorough and comprehensive.
It should be noted that when element is referred to as " being fixed on " or " being set to " another element, it can be directly another On one element or there may also be elements placed in the middle.When an element is considered as " connection " another element, it can be with It is directly to another element or may be simultaneously present centering elements.Term as used herein " vertically ", " level ", "left", "right" and similar statement for illustrative purposes only, it is unique embodiment to be not offered as.
Unless otherwise defined, all of technologies and scientific terms used here by the article is with belonging to technical field of the invention The normally understood meaning of technical staff is identical.Term used in the description of the invention herein is intended merely to description tool The purpose of the embodiment of body, it is not intended that in the limitation present invention.Term as used herein " and/or " including one or more The arbitrary and all combination of relevant Listed Items.
For example, one kind efficiently synthesizes equipment, including：Autoclave body, the both ends of the autoclave body are respectively arranged with upper cover and lower envelope Head；Mixing stirring device, the mixing stirring device include installation frame, driving motor, drive shaft and agitating paddle, the installation Rack is fixedly mounted on the upper cover, and the driving motor is set on the installation frame, and the first of the drive shaft End and the rotation axis connection of the driving motor, the second end of the drive shaft is connect with the agitating paddle, and the agitating paddle Inside the low head；Material filter, the material filter include material-pumping tube body, filter box, filter screen Component, the filtering pump housing, reflux tube body and valve, the first end of the material-pumping tube body is connected with the bottom of the low head, described The hollow setting of filter box, it is interior to form filter cavity, the second end of the material-pumping tube body and the first end of the filter box Connection, and the second end of the material-pumping tube body is connected with the filter cavity, the screen modules include the first strainer, second Strainer and third strainer, first strainer, second strainer and the third strainer are arranged at intervals at the filtering successively In cavity, the edge at the edge of first strainer, the edge of second strainer and the third strainer with the filtering The madial wall connection of babinet, first strainer are set towards the direction of the second end of the material-pumping tube body, the filtering pump housing Feed end connect with the second end of the filter box, and it is described filtering pump housing feed end connected with the filter cavity, institute The discharge end for stating the filtering pump housing is connected with the first end of the reflux tube body, the second end of the reflux tube body and the upper cover Connection, the valve are set on the reflux tube body；And baffle means, the baffle means include the installation body of rod, baffling erects Bar and several baffling cross bars, it is described installation the body of rod first end connect with the madial wall of the low head, the baffling montant and The second end connection of the installation body of rod, several baffling cross bars are arranged at intervals on the baffling montant, and several successively The baffling cross bar is arranged in parallel.
In order to which further the above-mentioned equipment that efficiently synthesizes is explained, for example, another embodiment efficiently synthesizes Equipment is as follows：
Referring to Fig. 1, efficiently synthesizing equipment 10 includes autoclave body 100, mixing stirring device 200 and material filter 300, Mixing stirring device 200 and material filter 300 may be contained on autoclave body 100.
Referring to Fig. 1, the both ends of autoclave body 100 are respectively arranged with upper cover 110 and low head 120, autoclave body 100 is used to house The material of addition, and be mixed and react to material and occasion is provided.For example, after upper cover 110 is connect with low head 120 Form autoclave body 100.For another example, the autoclave body is an integral molding structure.For another example, in the process for being installed on outside support of the autoclave body In, the upper cover is located at the top of outside support, and the low head is located at the lower part of outside support.
For example, the autoclave body has both ends to be hemispherical columnar structured, certainly, the autoclave body can also be according to reality Situation is selected, for example, using both ends as the columnar structured of plane.
Referring to Fig. 1, mixing stirring device 200 includes installation frame 210, driving motor 220, drive shaft 230 and stirring Paddle 240, installation frame 210 are fixedly mounted on the upper cover 110 of autoclave body 100, and driving motor 220 is set to installation frame 210 On, the first end of drive shaft 230 and the rotation axis connection of driving motor 220, the second end of drive shaft 230 stretch to autoclave body 100 Inside, e.g., the second end of drive shaft 230 are stretched to inside the low head 120 of autoclave body 100, the second end of drive shaft 230 and stirring Paddle 240 connects, and e.g., agitating paddle 240 is located inside the low head 120 of autoclave body 100.
For example, the agitating paddle is anchor formula agitating paddle or propeller, certainly, can also be selected according to actual needs With other kinds of agitating paddle.
Referring to Fig. 1, driving motor 220 is used to that drive shaft 230 to be driven to rotate, and then drive fixed with drive shaft 230 Agitating paddle 240 rotates.When needing to be stirred hybrid manipulation to the material in autoclave body 100, control driving motor 220, which drives, to be driven Moving axis 230 rotates, and then agitating paddle 240 is driven to rotate, and is acted on using the flow-disturbing of agitating paddle 240, can play preferable stirring Immixture, and then hybrid manipulation can be stirred to the material in autoclave body 100.
Also referring to Fig. 1 and Fig. 2, material filter 300 includes material-pumping tube body 310, filter box 320, filter screen Component 330, the filtering pump housing 340, reflux tube body 350 and valve 360, low head 120, material-pumping tube body 310, filter box 320, mistake Filter pump body 340, reflux tube body 350 and upper cover 110 are sequentially communicated, and screen modules 330 are placed in inside filter box 320, Valve 360 is set on reflux tube body 350.
Also referring to Fig. 1 and Fig. 2, the first end of material-pumping tube body 310 is connected with the bottom of low head 120, in this way, working as kettle When being reacted, material can flow into material-pumping tube body 310 material in body 100 out of low head 120, and then after progress Continuous filter operation.
Referring to Fig. 2,320 hollow setting of filter box, filter box 320 is interior to form filter cavity 321, material-pumping tube body 310 second end is connect with the first end of filter box 320, and the second end of material-pumping tube body 310 is connected with filter cavity 321, In this way, the material to be filtered flowed into out of material-pumping tube body 310 can be just flowed into inside filter cavity 321, and in filter cavity Filter operation is completed in 321.
Referring to Fig. 2, screen modules 330 include the first strainer 331, the second strainer 332 and third strainer 333, first Strainer 331, the second strainer 332 and third strainer 333 are arranged at intervals at successively in filter cavity 321, the edge of the first strainer 331st, the madial wall of the edge 332 of the second strainer and the edge of third strainer 333 with filter box 320 is connect, in this way, from pumping The material flowed out in expects pipe body 310 is successively through the first strainer 331, the second strainer 332 and third strainer 333, so as to make material Filter operation is completed, can preferably remove the impurity in material, is operated more convenient simple.For example, the first strainer 331, second Strainer 332 and third strainer 333 are arranged at intervals successively, so that there are gap between strainer, in such manner, it is possible to preferably utilize The gap accommodates the impurity being filtered out, and for another example, the impurity being filtered out is cleared up at interval of preset time, to reduce strainer Or babinet the problem of blocking.
In order to preferably improve the filter effect of the screen modules, for example, first strainer, second strainer And the filter opening aperture of the third strainer is sequentially reduced, in this way, taking three layers of effect gradually filtered, can be directed to different-grain diameter Impurity, to optimize filtration path, and then can preferably improve the filter effect of the screen modules.
Also referring to Fig. 1 and Fig. 2, the feed end of the filtering pump housing 340 is connect, and mistake with the second end of filter box 320 340 feed end of filter pump body is connected with filter cavity 321, and the first end for filtering the discharge end and reflux tube body 350 of the pump housing 340 connects Logical, the second end of reflux tube body 350 is connected with upper cover 110.In this way, based on the filtering pump housing 340 in normal work, generation Suction, material can be pumped to from low head 120 in material-pumping tube body 310, then taken out by material-pumping tube body 310 by the filtering pump housing 340 It is drawn in filter box 320, and material is by the first strainer 331, the second strainer 332 and the in the filter box 320 During three strainers 333, filter operation is completed, that is, completes to go deimpurity operation, after material completes filter operation, then, is passed through The filtering pump housing 340 and the material after being filtered under the action of the pump housing 340 filter, are pulled into and flow back in tube body 350, Finally, it then is back in upper cover 110, that is, it is back to inside autoclave body 100, at this point, material completes a filter operation, certainly, In order to further improve the removal effect of impurity, according to actual conditions, circulating filtration operation can also be performed.
For example, the first strainer 331 is set towards the direction of the second end of material-pumping tube body 310, third strainer 333 is towards reflux Tube body 350 is set.
Referring to Fig. 2, valve 360 is set on reflux tube body 350, when needing to be filtered operation, valve is opened 360, at this point, material is filtered operation in 300 internal circulation flow of material filter, after filter operation is completed, close valve Door 360, at this point, material stops flowing in material filter 300.
The above-mentioned equipment 10 that efficiently synthesizes by setting autoclave body 100, mixing stirring device 200 and material filter 300, and And material filter 300 can carry out material circulating filtration removal impurity operation, go deimpurity operation more simple and convenient, Production efficiency is also higher.
In order to reduce because the excessive generation of material pressure is the problem of impacting screen modules, preferably to protect filter screen The dispersion effect of component and strength imparting material, for example, also referring to Fig. 3 and Fig. 4, the equipment that efficiently synthesizes further includes pressure Buffer unit 400, the pressure buffer device 400 are located at the material-pumping tube body 310 and the first strainer of screen modules 330 Between 331, the pressure buffer device 400 includes several buffering plate bodys 410, and several buffering plate bodys are arranged at intervals at successively In the filter cavity, and madial wall of the edge of several buffering plate bodys with the filter box is connect, the buffering Plate body 410 offers flowing hole 411；For another example, the buffering plate body offers several flowing holes；For another example, several flowing holes Rectangular array is distributed on the buffering plate body；For another example, the flowing hole of the two neighboring buffering plate body shifts to install； For another example, the flowing hole has the cross section of regular polygon structure；For another example, the flowing hole is transversal with regular hexagon structure Face；For another example, the buffering plate body has cuboid shape structure, in this way, when material passes through pressure buffer device 400, can subtract Less because the excessive generation of material pressure is the problem of impacting screen modules, preferably to protect screen modules and stiffener The dispersion effect of material.
In order to preferably dismantle the screen modules, so preferably the screen modules can be cleaned or Replacement operation, for example, also referring to 5, the equipment that efficiently synthesizes further includes activity provision for disengagement 500, the activity dismounting Device 500 includes locking plate body 510, fastener 520 first installs plate body 530 and second and installs plate body 540, the filter box 320 offer dismounting window 322, and at least part of the locking plate body is torn open in the dismounting window described in closing Window is unloaded, the fastener wears the side wall of the locking plate body and the filter box successively, the first installation plate body First side and the latch, which are shown consideration for, to be closed, the second side of the first installation plate body side with first strainer respectively A side connection on side, a side of second strainer and the third strainer, the first side of the second installation plate body Another side with another side of the first strainer, another side of second strainer and the third strainer is connect respectively, The second side and the madial wall of the filter box of the installation plate body support.The locking plate body and the dismounting window It sets and sealing ring is provided at position；For another example, the fastener has threaded portion and head, and the first end of the threaded portion is successively The side wall of the locking plate body and the filter box is worn, the head is connect with the second end of the threaded portion；For another example, institute Stating head has the cross section of regular hexagon structure；For another example, portion is set in the locking plate body setting, and the portion of setting is embedded at institute It states in dismounting window；For another example, the first installation plate body is arranged in parallel with the described second installation plate body；For another example, first filter Net, second strainer and the third strainer are vertically arranged with the described first installation plate body, in this way, being dismantled by the activity Device 500 can preferably dismantle the screen modules, so preferably the screen modules can be cleaned or Replacement operation.
In order to preferably support the screen modules, for preferably protecting the screen modules, for example, please referring to Fig. 6, the equipment that efficiently synthesizes further include filtering support device 600, and the filtering support device 600 includes the first support rack 610 and the second support rack 620, the edge of the first support rack connect with the madial wall of the filter box, described the For one support rack between first strainer and second strainer, the first support rack offers the first mesh, The edge of the second support rack is connect with the madial wall of the filter box, and the second support rack is located at described second Between strainer and the third strainer, the second support rack offers the second mesh.It is the mesh of first strainer, described The filter opening size of the mesh of second strainer and the third strainer is sequentially reduced；For another example, first strainer, first support Rack, second strainer, the second support rack and the third strainer are arranged in parallel；For another example, first mesh Size setting identical with the size of second mesh；For another example, first mesh and second mesh are that diamond shape is poroid Structure；For another example, it is both provided with interval between the first support rack and first strainer and second strainer；For another example, Interval is both provided between the second support rack and second strainer and the third strainer, in this way, by setting the One support rack 610 and second supports rack 620, the screen modules can be preferably supported, for preferably protecting institute State screen modules.
In order to reduce vortex phenomenon, and flow-disturbing degree when can improve stirring operation, for example, referring to Fig. 7, The equipment that efficiently synthesizes further includes baffle means 700, and the baffle means 700 include the installation body of rod 710, baffling montant 720 And several baffling cross bars 730, the first end of the installation body of rod 710 are connect with the madial wall of the low head 120, the baffling Montant is connect with the second end of the installation body of rod, and several baffling cross bars are arranged at intervals at successively on the baffling montant, And several baffling cross bars are arranged in parallel.The first end of the installation body of rod is provided with the binding face of arc-shaped curved surface structure, institute The madial wall that binding face is stated with the low head is bonded；For another example, the installation body of rod is provided with reinforcing rib；For another example, the reinforcement The second end of muscle from first end to the installation body of rod of the installation body of rod is extended；For another example, the baffling montant and institute Drive shaft is stated to be arranged in parallel；For another example, the baffling montant has hollow structure；For another example, the end of the baffling cross bar has half Spherical structure in this way, by setting baffle means 700, can reduce vortex phenomenon, and when can improve stirring operation Flow-disturbing degree.
In order to reduce the drive shaft in rotation, the concussion problem of generation, for example, referring to Fig. 8, described efficiently synthesize Equipment further includes stirring limiting device 800, and the stirring limiting device 800 includes limiting body 810 and limiting connecting rod 820, The limiting body 810 is placed on outside the second end of the drive shaft 230, and the limiting body 810 is located at the agitating paddle 240 and the low head 120 bottom between, it is described limiting body madial wall and the drive shaft lateral wall between set There is interval, the first end of the limiting body of rod is connect with the limiting body, the second end and the lower envelope of the limiting body of rod The bottom connection of head, and the extending direction of the limiting body of rod and the extending direction of the drive shaft form angle；For another example, it is described Agitating paddle is propeller；For another example, the limiting body has rounded cylindrical structure；For another example, the center of the limiting body Axis is overlapped with the central axis of the drive shaft；For another example, the stirring limiting device sets several limiting connecting rods, if The dry limiting connecting rod puts distribution so that the center of the drive shaft is radial；For another example, the stirring limiting device setting two A limiting connecting rod, two it is described limiting connecting rods between form angle；For another example, the number of degrees of the angle for 60 degree~ 120 degree, in this way, stirring limiting device 800 by setting, the drive shaft can be reduced in rotation, the concussion problem of generation.
It should be pointed out that when each material that hybrid manipulation is stirred inside the autoclave body carries out combination reaction, and Most of combination reaction is all exothermic reaction, and the yield of rate and the product generation of reaction is also required to what is released during dependent reaction Heat, for improving reaction rate and yield.In addition, in whipping process, the mixing stirring device can do work to material, i.e., Material shows as outwardly releasing heat during agitation is mutually mixed, especially the stronger material of toughness, heat release Phenomenon becomes apparent from, therefore, based on the above situation, for the combination reaction of some dependence higher temperatures, such as dependent on reaction itself Heat release and the combination reaction of stirring heat production, and additional heating unit is not needed to for the reaction that it is heated, it is especially desirable to Ensure the heat-insulating property of the autoclave body.Further, in order to be directed to some acid materials, therefore, to assure that the inside of the autoclave body Wall, i.e., the madial wall of the autoclave body directly contacted with acid material have higher acid etch resistance energy, for prolonging the raw kettle The service life of body and being normally carried out for reaction.Further, the lateral wall of the autoclave body with corrosive materials due to often connecing It touches, e.g., the corrosive materials contact of the forms such as gaseous state or liquid, it is therefore desirable to have preferable corrosion resistance, for more preferable Protect the autoclave body in ground.
In order to improve acid etch resistance energy, heat-insulating property and the corrosion resistance of the autoclave body, for example, referring to Fig. 8, described Autoclave body, e.g., the side wall of the autoclave body include the resistance to acid attack layer 130 being cascading, insulating layer 140, supporting layer 150, counterweight Layer 160 and protective layer 170, the resistance to acid attack layer are located at the madial wall of the autoclave body, and the resistance to acid attack layer is directly and material, Such as, acid material contact, the protective layer are located at the lateral wall of the autoclave body, i.e., described protective layer is directly naked to be exposed on the external.
For example, the resistance to acid attack layer of an embodiment includes each component of following mass parts：75 parts~88 parts of iron, titanium 30 Part~34 parts, 20 parts~25 parts of chromium, 2.5~3.4 parts of antimony, 2.3~3.4 parts of copper part, 1.5 parts~2.7 parts of zinc, aluminium 0.9~1.4 Part, 0.15 part~0.27 part of carbon, 0.25 part~0.46 part of silicon, 0.12 part~0.18 part of boron, 0.04 part~0.09 part of cobalt, phosphorus 0.001 part~0.03 part, 0.001 part~0.03 part of sulphur, 0.02 part~0.03 part of strontium, 0.03 part~0.04 part of bismuth, 0.01 part of scandium ~0.02 part and 0.001 part~0.002 part of gadolinium.Wherein, scandium is scandium or containing scadium compound, wherein, containing containing scandium in scadium compound Element；Gadolinium is gadolinium or containing gadolinium compound, wherein, containing containing gadolinium element in gadolinium compound；Bismuth be bismuth or bismuth-containing compound, wherein, Contain bismuth element in bismuth gadolinium compound；Strontium is strontium or containing strontium compound, wherein, contain strontium element in strontium gadolinium compound.
Using 75 parts~88 parts of iron, 30 parts~34 parts of titanium and 20 parts of chromium~25 parts of infrastructure elements as resistance to acid attack layer, from And the resistance to acid attack layer can be enable to have certain acid etch resistance, in addition, by adding 2.5~3.4 parts of antimony, 2.3 parts of copper ~3.4 parts, 1.5 parts~2.7 parts of zinc, 0.9~1.4 part of aluminium, 0.04 part~0.09 part of cobalt, 0.02 part~0.03 part of strontium, bismuth 0.03 0.001 part~0.002 part of part~0.04 part, 0.01 part~0.02 part of scandium and gadolinium are compounded, additionally it is possible to be advanced optimized described The properties of resistance to acid attack layer can especially advanced optimize the acid etch resistance energy of the resistance to acid attack layer, so as to more preferable The acid etching of material is resisted on ground, for further improving the service life of the autoclave body and ensuring being normally carried out for reaction.
For another example, the resistance to acid attack layer of another embodiment includes each component of following mass parts：75 parts~80 parts of iron, titanium 33 parts~34 parts, 24 parts~25 parts of chromium, 2.7~3.4 parts of antimony, 2.7 parts~3.4 parts of copper, 1.8 parts~2.5 parts of zinc, aluminium 1.1~1.4 Part, 0.18 part~0.27 part of carbon, 0.27 part~0.46 part of silicon, 0.13 part~0.18 part of boron, 0.04 part~0.09 part of cobalt, phosphorus 0.001 part~0.03 part, 0.001 part~0.03 part of sulphur, 0.02 part~0.03 part of strontium, 0.03 part~0.04 part of bismuth, 0.01 part of scandium ~0.02 part and 0.001 part~0.002 part of gadolinium.
For another example, the resistance to acid attack layer of another embodiment includes each component of following mass parts：77 parts of iron, 33 parts of titanium, 25 parts of chromium, 3.4 parts of antimony, 2.7 parts of copper, 1.9 parts of zinc, 1.3 parts of aluminium, 0.27 part of carbon, 0.46 part of silicon, 0.18 part of boron, 0.04 part of cobalt, phosphorus 0.002 part of 0.03 part, 0.001 part of sulphur, 0.03 part of strontium, 0.04 part of bismuth, 0.01 part of scandium and gadolinium.
For example, the insulating layer of an embodiment includes each component of following mass parts：It is 15 parts~22 parts of land plaster, white 8~20 parts of cotton, 8 parts~15 parts of rock wool, 7 parts~9 parts of glass fibre, 10 parts~20 parts of Lauxite, 3.5 parts of polyacrylamide~ 4.5 parts, 1 part~3 parts of basalt fibre, 3~5 parts of rubber foam, 1 part~2 parts of magnesium hydroxide, aminopropyl triethoxysilane 1 Part~2 parts, 1 part~2 parts of aluminium oxide, 1 part~2 parts of 3,5- di-tert-butyl-4-hydroxybenzoic acids methyl esters, 3~4 parts of polypropylene fiber, 0.2~0.8 part of 1 part~2 parts of polysulfide rubber and lauryl sodium sulfate.
It can make the insulating layer that there is good heat-insulating property using each component of as above mass parts, when in the autoclave body When exothermic reaction occurs for the material in portion, and after transferring heat to the resistance to acid attack layer, had based on the insulating layer good Heat-insulated and heat-insulating property can limit heat and be further transmitted through the autoclave body, and then heat is avoided to be transferred directly to external environment In, it is ensured that the material inside the autoclave body is reacted at a suitable temperature, for improving the production of reaction rate and product Rate.
For another example, the insulating layer of another embodiment includes each component of following mass parts：17 parts~21 parts of land plaster, White 17~20 parts of cotton, 10 parts~15 parts of rock wool, 7 parts~9 parts of glass fibre, 10 parts~20 parts of Lauxite, polyacrylamide 3.5 Part~4.5 parts, 1 part~2.5 parts of basalt fibre, 3.5~5 parts of rubber foam, 1.5 parts~2 parts of magnesium hydroxide, three second of aminopropyl 1.5 parts~2 parts of oxysilane, 1 part~2 parts of aluminium oxide, 1 part~1.4 parts of 3,5- di-tert-butyl-4-hydroxybenzoic acids methyl esters, third 0.2~0.5 part of 3.3~4 parts of synthetic fibre fiber, 1 part~2 parts of polysulfide rubber and lauryl sodium sulfate.
For another example, the insulating layer of another embodiment includes each component of following mass parts：19 parts of land plaster, white cotton 17 ~20 parts, 15 parts of rock wool, 9 parts of glass fibre, 20 parts of Lauxite, 3.8 parts of polyacrylamide, 2.1 parts of basalt fibre, rubber 4.6 parts of foam, 1.7 parts of magnesium hydroxide, 2 parts of aminopropyl triethoxysilane, 1.8 parts of aluminium oxide, 3,5- di-t-butyl -4- hydroxyls 0.4 part of 1.4 parts of methyl benzoate, 4 parts of polypropylene fiber, 1.9 parts of polysulfide rubber and lauryl sodium sulfate.
For example, the supporting layer of an embodiment includes each component of following mass parts：95 parts~98 parts of iron, manganese 0.4 Part~0.95 part, 0.1 part~0.5 part of molybdenum, 0.01 part~0.05 part of titanium, 0.02 part~0.1 part of aluminium, 0.06 part~0.25 part of carbon, 0.1 part~0.3 part of silicon, 0.05 part~0.1 part of phosphorus, 0.001 part~0.01 part of boron, 0.05 part~0.5 part of hafnium, 0.05 part of scandium~ 0.3 part, 0.05 part~0.3 part of chromium, 0.01 part~0.05 part of nickel, 0.01 part~0.05 part of cerium, 0.01 part~0.05 part of thorium and zirconium 0.01 part~0.05 part.Wherein, hafnium is hafnium or containing hafnium compound, wherein, containing containing hafnium element in hafnium compound；Scandium is scandium or contains Scadium compound, wherein, containing in scadium compound contain scandium element；Thorium is thorium or containing thorium compound, wherein, contain in cerium-containing compound Ce elements；Cerium be cerium or cerium-containing compound, wherein, Ce elements are contained in cerium-containing compound.
It is appreciated that in order to which the autoclave body is made to have preferable heat-insulating property, need to introduce the insulating layer, and the guarantor The mechanical strength of warm layer is poor, in order to strengthen the integrally-built mechanical strength of the autoclave body, needs to introduce the supporting layer, makes it It is in direct contact with the insulating layer, for improving the integrally-built mechanical strength of the autoclave body, to achieve the purpose that safety in production. Based on the above situation, this just necessarily requires the supporting layer to have higher mechanical strength and anti-deformation nature, by using such as It improves quality each component of part, especially described supporting layer contains 0.05 part~0.5 part of hafnium, 0.05 part~0.3 part of scandium, 0.05 part of chromium 0.01 part~0.05 part of~0.3 part, 0.01 part~0.05 part of nickel, 0.01 part~0.05 part of cerium, 0.01 part~0.05 part of thorium and zirconium, The mechanical strength of traditional ferroalloy can be improved, make its mechanical strength and anti-deformation nature more excellent, disclosure satisfy that requirement.
For another example, the supporting layer of another embodiment includes each component of following mass parts：97 parts~98 parts of iron, manganese 0.55 part~0.95 part, 0.35 part~0.5 part of molybdenum, 0.01 part~0.05 part of titanium, 0.02 part~0.1 part of aluminium, 0.17 part of carbon~ 0.25 part, 0.1 part~0.25 part of silicon, 0.05 part~0.1 part of phosphorus, 0.008 part~0.01 part of boron, 0.1 part~0.5 part of hafnium, scandium 0.1 Part~0.3 part, 0.1 part~0.3 part of chromium, 0.02 part~0.05 part of nickel, 0.02 part~0.05 part of cerium, 0.02 part~0.05 part of thorium and 0.02 part~0.05 part of zirconium.
For another example, the supporting layer of another embodiment includes each component of following mass parts：97 parts of iron, 0.75 part of manganese, 0.5 part of molybdenum, 0.05 part of titanium, 0.02 part of aluminium, 0.17 part of carbon, 0.25 part of silicon, 0.1 part of phosphorus, 0.008 part of boron, 0.5 part of hafnium, scandium 0.2 Part, 0.2 part of chromium, 0.05 part of nickel, 0.05 part of cerium, 0.05 part of thorium and 0.05 part of zirconium.
For example, the weight coating of an embodiment includes each component of following mass parts：85 parts~95 parts of tungsten, 30 parts of nickel 0.5 part~5 parts of~60 parts, 15 parts~40 parts of iron, 1.5 parts~10 parts of chromium, 1.5 parts~10 parts of lead, 1 part~6 parts of copper and molybdenum.
It is appreciated that in reaction process is produced, need to carry out the material in the autoclave body the higher stirring behaviour of intensity Make, and since thickness is larger and the presence of the insulating layer of lighter weight, in order to avoid the integrally-built matter of the autoclave body Amount kicks the beam, and then reduces influence of the external impacts to the autoclave body, you can concussion or displacement problem occurs to reduce the autoclave body. The weight coating can be made to have excellent counterweight performance using each component of as above mass parts, can effectively increase the kettle The integrally-built weight of body makes its weight with traditional autoclave body identical or is adapted to, so as to improve the peace in production process Full performance.
For another example, the weight coating of another embodiment includes each component of following mass parts：90 parts~95 parts of tungsten, nickel 30 0.5 part of part~45 parts, 27 parts~40 parts of iron, 1.5 parts~2.3 parts of chromium, 1.5 parts~3.3 parts of lead, 1 part~5.5 parts of copper and molybdenum~ 4.9 part.
For another example, the weight coating of another embodiment includes each component of following mass parts：92 parts of tungsten, 38 parts of nickel, iron 3.8 parts of 29 parts, 2.1 parts of chromium, 2.1 parts of lead, 3.5 parts of copper and molybdenum.
For example, the protective layer of an embodiment includes each component of following mass parts：65 parts~80 parts of iron, lithium 16~ 18 parts, 18 parts~25 parts of nickel, 3.5 parts~4 parts of molybdenum, 2 parts~5 parts of chromium, 1 part~5 parts of cobalt, 1 part~5 parts of vanadium, 1 part~2 parts of manganese, iridium 0.8 part~2.5 parts, 0.5 part~2.5 parts of niobium, 0.3 part~2.5 parts of scandium, 0.2 part~2.5 parts of strontium, 0.2 part~2.5 parts of caesium, tungsten 0.2 part~2.5 parts and 0.2 part~2.5 parts of titanium.Wherein, caesium is caesium or containing cesium compound, wherein, containing containing caesium in cesium compound Element；Wherein, strontium is strontium or containing strontium compound, wherein, containing containing strontium element in strontium compound；Wherein, scandium is for scandium or containing scandium Close object, wherein, containing in scadium compound contain scandium element；Wherein, niobium is niobium or containing niobium compound, wherein, it is included containing niobium compound There is niobium element；Wherein, iridium is iridium or containing iridic compound, wherein, containing containing iridium in iridic compound.
It is appreciated that the lateral wall of the autoclave body is with corrosive materials due to often contacting, and e.g., the forms such as gaseous state or liquid Corrosive materials contact, it is therefore desirable to have preferable corrosion resistance, for preferably protecting the autoclave body.By as above The each component of mass parts can make the protective layer have good Corrosion Protection, and then preferably protect the autoclave body, use In the service life for extending the autoclave body.
For another example, the protective layer of another embodiment includes each component of following mass parts：65 parts~70 parts of iron, lithium 16 Part~16.5 parts, 18~21 parts of nickel, 3.5 parts~3.9 parts of molybdenum, 2 parts~4.4 parts of chromium, 1 part~3.9 parts of cobalt, 1 part~4.5 parts of vanadium, 1 part~1.7 parts of manganese, 0.8 part~2.3 parts of iridium, 0.5 part~2.2 parts of niobium, 0.3 part~2.3 parts of scandium, 0.2 part~2.3 parts of strontium, caesium 0.2 part~1.9 parts of 0.2 part~2.4 parts, 0.2 part~2.1 parts of tungsten and titanium.
For another example, the protective layer of another embodiment includes each component of following mass parts：65 parts of iron, 16.5 parts of lithium, 21 parts of nickel, 3.5 parts of molybdenum, 3.5 parts of chromium, 2.8 parts of cobalt, 3.7 parts of vanadium, 1.5 parts of manganese, 2.3 parts of iridium, 2.2 parts of niobium, 2.3 parts of scandium, strontium 2.3 Part, 2.4 parts of caesium, 0.2 part of tungsten and 0.2 part of titanium.
In order to advanced optimize the autoclave body, e.g., the structure of the side wall of the autoclave body, for example, the resistance to acid attack layer, described Insulating layer, the supporting layer, the weight coating and the protective layer thickness ratio be (1~1.5)：(15~20)：(5~5.5)： (8~9.8)：(0.5~1.2)；For another example, the thickness ratio of the weight coating and the protective layer is 1：15：5：9.5：1.1.
It should be noted that the technical characteristic that the other embodiment of the present invention is further included in the various embodiments described above be combined with each other It can be formed, and what can be implemented efficiently synthesizes equipment.
Each technical characteristic of embodiment described above can be combined arbitrarily, to make description succinct, not to above-mentioned reality It applies all possible combination of each technical characteristic in example to be all described, as long as however, the combination of these technical characteristics is not deposited In contradiction, it is all considered to be the range of this specification record.
Embodiment described above only expresses the several embodiments of the present invention, and description is more specific and detailed, but Can not the limitation to the scope of the claims of the present invention therefore be interpreted as.It should be pointed out that the ordinary skill people for this field For member, without departing from the inventive concept of the premise, various modifications and improvements can be made, these belong to the present invention's Protection domain.Therefore, the protection domain of patent of the present invention should be determined by the appended claims.

Claims (7)

1. one kind efficiently synthesizes equipment, which is characterized in that including：
Autoclave body, the both ends of the autoclave body are respectively arranged with upper cover and low head；
Mixing stirring device, the mixing stirring device include installation frame, driving motor, drive shaft and agitating paddle, the peace Installation frame is fixedly mounted on the upper cover, and the driving motor is set on the installation frame, and the of the drive shaft One end and the rotation axis connection of the driving motor, the second end of the drive shaft is connect with the agitating paddle, and the stirring Paddle is located inside the low head；
Material filter, the material filter include material-pumping tube body, filter box, screen modules, the filtering pump housing, return Flow tube body and valve, the first end of the material-pumping tube body are connected with the bottom of the low head, the hollow setting of filter box, Filter cavity is formed in it, the second end of the material-pumping tube body is connect with the first end of the filter box, and the material-pumping tube The second end of body is connected with the filter cavity, and the screen modules include the first strainer, the second strainer and third strainer, institute It states the first strainer, second strainer and the third strainer to be arranged at intervals at successively in the filter cavity, first filter Madial wall of the edge at the edge of net, the edge of second strainer and the third strainer with the filter box is connect, First strainer is set towards the direction of the second end of the material-pumping tube body, the feed end of the filtering pump housing and the filtering The second end connection of babinet, and the filtering pump housing feed end is connected with the filter cavity, the discharge end of the filtering pump housing It is connected with the first end of the reflux tube body, the second end of the reflux tube body is connected with the upper cover, the valve setting In on the reflux tube body；And
Baffle means, the baffle means include the installation body of rod, baffling montant and several baffling cross bars, and the of the installation body of rod One end is connect with the madial wall of the low head, and the baffling montant is connect with the second end of the installation body of rod, several described Baffling cross bar is arranged at intervals at successively on the baffling montant, and several baffling cross bars are arranged in parallel；
Wherein, the equipment that efficiently synthesizes further includes stirring limiting device, and the stirring limiting device includes limiting body and limit Position connecting rod, the limiting body are placed on outside the second end of the drive shaft, and the stop collar body is located at the agitating paddle And between the bottom of the low head, between being provided between the madial wall of the limiting body and the lateral wall of the drive shaft Every the first end of the limiting body of rod is connect with the limiting body, the second end of the limiting body of rod and the low head Bottom connects, and the extending direction of the limiting body of rod and the extending direction of the drive shaft form angle；The agitating paddle is Propeller；The limiting body has rounded cylindrical structure；The central axis of the limiting body and the drive shaft Central axis overlaps；The stirring limiting device sets several limiting connecting rods, and several limiting connecting rods are with described The center of drive shaft is radial to put distribution；The stirring limiting device sets two limiting connecting rods, two limits Angle is formed between the connecting rod of position；The number of degrees of the angle are 60 degree~120 degree；
The filter opening aperture of first strainer, second strainer and the third strainer is sequentially reduced；Described efficiently synthesize sets It is standby to further include pressure buffer device, the pressure buffer device be located at the material-pumping tube body and screen modules the first strainer it Between, the pressure buffer device includes several buffering plate bodys, and several buffering plate bodys are arranged at intervals at the filter chamber successively In vivo, and madial wall of the edge of several buffering plate bodys with the filter box is connect, and the buffering plate body offers Flowing hole；The buffering plate body offers several flowing holes；Several flowing hole rectangular arrays are distributed in the buffer board On body；The flowing hole of the two neighboring buffering plate body shifts to install；The flowing hole has the horizontal stroke of regular polygon structure Section；The buffering plate body has cuboid shape structure；The equipment that efficiently synthesizes further includes activity provision for disengagement, the activity Provision for disengagement includes locking plate body, fastener, the first installation plate body and the second installation plate body, the filter box and offers dismounting Window, at least part of the locking plate body close the dismounting window, the fastener in the dismounting window The side wall of the locking plate body and the filter box, the first side of the first installation plate body and the locking are worn successively Plate body is bonded, the second side of the first installation plate body respectively with a side of first strainer, second strainer A side and the connection of a side of the third strainer, the first side of the second installation plate body are another with the first strainer respectively Another side connection of a side, another side of second strainer and the third strainer, the second of the installation plate body Side and the madial wall of the filter box support；It is described locking plate body with it is described dismantle window set be provided at position it is close Seal；The fastener has threaded portion and a head, and the first end of the threaded portion wears the locking plate body and described successively The side wall of filter box, the head are connect with the second end of the threaded portion；The head has the horizontal stroke of regular hexagon structure Section；Portion is set in the locking plate body setting, and the portion of setting is in the dismounting window；It is described first installation plate body with The second installation plate body is arranged in parallel；First strainer, second strainer and the third strainer and the described first peace Loading board body is vertically arranged.
2. according to claim 1 efficiently synthesize equipment, which is characterized in that the first end of the installation body of rod is provided with arc The binding face of shape curved-surface structure, the binding face are bonded with the madial wall of the low head.
3. according to claim 1 efficiently synthesize equipment, which is characterized in that the installation body of rod is provided with reinforcing rib.
4. according to claim 3 efficiently synthesize equipment, which is characterized in that the reinforcing rib is by the of the installation body of rod The second end of one end to the installation body of rod is extended.
5. according to claim 1 efficiently synthesize equipment, which is characterized in that the baffling montant is parallel with the drive shaft Setting.
6. according to claim 1 efficiently synthesize equipment, which is characterized in that the baffling montant has hollow structure.
7. according to claim 1 efficiently synthesize equipment, which is characterized in that the end of the baffling cross bar has hemispherical Structure.
CN201610514340.5A 2016-06-30 2016-06-30 Efficiently synthesize equipment Active CN105964209B (en)

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CN201810553773.0A CN108479672A (en) 2016-06-30 2016-06-30 Improving production efficiency efficiently synthesizes equipment

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