CN105964208B - Chemical industry synthesis device - Google Patents
Chemical industry synthesis device Download PDFInfo
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- CN105964208B CN105964208B CN201610512133.6A CN201610512133A CN105964208B CN 105964208 B CN105964208 B CN 105964208B CN 201610512133 A CN201610512133 A CN 201610512133A CN 105964208 B CN105964208 B CN 105964208B
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- dispersed
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- cylinder
- babinet
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J19/18—Stationary reactors having moving elements inside
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01F—MIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
- B01F27/00—Mixers with rotary stirring devices in fixed receptacles; Kneaders
- B01F27/05—Stirrers
- B01F27/11—Stirrers characterised by the configuration of the stirrers
- B01F27/19—Stirrers with two or more mixing elements mounted in sequence on the same axis
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01F—MIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
- B01F27/00—Mixers with rotary stirring devices in fixed receptacles; Kneaders
- B01F27/23—Mixers with rotary stirring devices in fixed receptacles; Kneaders characterised by the orientation or disposition of the rotor axis
- B01F27/232—Mixers with rotary stirring devices in fixed receptacles; Kneaders characterised by the orientation or disposition of the rotor axis with two or more rotation axes
- B01F27/2322—Mixers with rotary stirring devices in fixed receptacles; Kneaders characterised by the orientation or disposition of the rotor axis with two or more rotation axes with parallel axes
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01F—MIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
- B01F27/00—Mixers with rotary stirring devices in fixed receptacles; Kneaders
- B01F27/80—Mixers with rotary stirring devices in fixed receptacles; Kneaders with stirrers rotating about a substantially vertical axis
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J19/0053—Details of the reactor
- B01J19/0066—Stirrers
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J19/02—Apparatus characterised by being constructed of material selected for its chemically-resistant properties
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- Chemical & Material Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Organic Chemistry (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Mixers Of The Rotary Stirring Type (AREA)
Abstract
A kind of chemical industry synthesis device, including cylinder, electric hybrid module, the pre-dispersed component of material and pressure-applying unit.The both ends of cylinder are respectively arranged with upper cover and low head.Electric hybrid module includes stent, hybrid electric motor, axis is mixed and paddle is mixed.The pre-dispersed component of material includes charging tube body, buffering cylinder, material and houses babinet, installation casing, pre-dispersed hybrid electric motor, pre-dispersed combined drive moving axis, pre-dispersed combination drive paddle and supporting rack.Pressure-applying unit includes the pressurization pump housing, conveying tube body and material and holds bucket.Above-mentioned chemical industry synthesis device is by setting cylinder, electric hybrid module and the pre-dispersed component of material, when needing material carrying out pre-dispersed hybrid manipulation, material need to be only passed through to the charging tube body of the pre-dispersed component of material, and material centrifugation is thrown away by pre-dispersed combination drive paddle pre-dispersed hybrid manipulation can be realized, and stirring and mixing effect is preferable again.
Description
Technical field
The present invention relates to chemical plant installations technical field, more particularly to a kind of chemical industry synthesis device.
Background technology
At present, in material production field, after especially various materials mixing reacts, the situation of final products is obtained
In, it usually needs using chemical industry synthesis device, for being stirred mixing to material, and it is made successfully to react, be used for
Obtain the final products of higher quality.
Common, existing chemical industry synthesis device stirs the material for sequentially adding or adding in simultaneously using rabbling mechanism
Mixing is mixed, with the purpose being mixed.
However, existing chemical industry synthesis device is all that operation is directly stirred in its cylinder, material is not carried out
Advance scatter operation causes its stirring and mixing effect relatively low, more time-consuming.
Invention content
Based on this, it is necessary to which pre-dispersion operation and the preferable chemical industry synthesis of stirring and mixing effect can be realized by providing one kind
Device.
A kind of chemical industry synthesis device, including：
Cylinder, the both ends of the cylinder are respectively arranged with upper cover and low head；
Electric hybrid module, the electric hybrid module include stent, hybrid electric motor, axis is mixed and paddle, the branch are mixed
Frame is fixedly mounted on the upper cover, and the hybrid electric motor is set on the stent, the first end that axis is mixed
With the rotation axis connection of the hybrid electric motor, the second end that axis is mixed is connect, and described with the mixing paddle
Paddle is mixed to be located inside the low head；
The pre-dispersed component of material, the pre-dispersed component of material includes charging tube body, buffering cylinder, material house babinet,
Installation casing, pre-dispersed hybrid electric motor, pre-dispersed combined drive moving axis, pre-dispersed combination drive paddle and supporting rack, the charge pipe
The first end of body is connected with the upper cover, and the first end of the buffering cylinder is connected with the first end of the charging tube body, institute
It states material and houses babinet with hollow structure, and it is located inside the upper cover, the installation casing is mounted on the material
On the madial wall of accommodating babinet, and the lateral wall of the installation casing and the material house the madial wall of babinet between formed
Material houses cavity, and the second end of the buffering cylinder houses babinet with the material and connect, and described buffers the of cylinder
Two ends house cavity with the material and connect, support frame as described above respectively with the madial wall of the upper cover and the material storage box
The lateral wall connection of body, the pre-dispersed hybrid electric motor are mounted on inside the installation casing, the pre-dispersed combined drive moving axis
First end and the pre-dispersed hybrid electric motor rotation axis connection, the second end of the pre-dispersed combined drive moving axis wears successively
The installation casing and the material house babinet, and the second end of the pre-dispersed combined drive moving axis is placed in the upper envelope
Head is internal, and the pre-dispersed combination drive paddle is connect with the second end of the pre-dispersed combined drive moving axis, the material storage box
The bottom of body offers the material spilling hole for housing cavity with the material and connecting, and the material spilling hole is towards the pre-dispersed combined drive
The setting of the direction of dynamic paddle and the low head；
Pressure-applying unit, the pressure-applying unit include the pressurization pump housing, conveying tube body and material and hold bucket, the pressurization pump housing
Discharge end is connected with the second end of the charging tube body, and the first end of the feed end and the conveying tube body of the pressurization pump housing connects
Logical, the second end of the conveying tube body holds bucket with the material and connects, and the material holds bucket for holding material.
The second end of the conveying tube body is held with the material in one of the embodiments, sets at the communicating position of bucket
It is equipped with leakproof glue-line.
The material holds bucket and offers connecting hole in one of the embodiments, and the hole wall of the connecting hole is provided with
Internal thread, the lateral wall of the second end of the conveying tube body are provided with external screw thread, the internal thread and the external thread bolt connection.
The conveying tube body has round tubular structure in one of the embodiments,.
The caliber of the conveying tube body is from the first end of the conveying tube body to second end in one of the embodiments,
Direction gradually increases.
The material, which holds to be provided at the position of bucket, in one of the embodiments, holds platform, described to hold platform
Difference in height is provided between the cylinder.
In one of the embodiments, it is described hold platform and be provided with hold face for hold that the material holds bucket.
Above-mentioned chemical industry synthesis device by setting cylinder, electric hybrid module and the pre-dispersed component of material, when need by material into
During the pre-dispersed hybrid manipulation of row, material need to be only passed through to the charging tube body of the pre-dispersed component of material, and again by pre-dispersed mixing
Material centrifugation is thrown away and pre-dispersed hybrid manipulation can be realized, and stirring and mixing effect is preferable by driving paddle.
Description of the drawings
Fig. 1 is the structure diagram of the chemical industry synthesis device of an embodiment of the present invention；
Fig. 2 is enlarged drawings of the Fig. 1 at A；
Fig. 3 is the partial structural diagram of the chemical industry synthesis device of another embodiment of the present invention；
Fig. 4 is the partial structural diagram of the chemical industry synthesis device of another embodiment of the present invention；
Fig. 5 is the partial structural diagram of the chemical industry synthesis device of another embodiment of the present invention；
Fig. 6 is the partial structural diagram of the chemical industry synthesis device of another embodiment of the present invention；
Fig. 7 is the partial structural diagram of the chemical industry synthesis device of another embodiment of the present invention；
Fig. 8 is the partial structural diagram of the chemical industry synthesis device of another embodiment of the present invention.
Specific embodiment
For the ease of understanding the present invention, the present invention is described more fully below with reference to relevant drawings.In attached drawing
Give the better embodiment of the present invention.But the present invention can realize in many different forms, however it is not limited to herein
Described embodiment.On the contrary, the purpose of providing these embodiments is that make to understand more the disclosure
Add thorough and comprehensive.
It should be noted that when element is referred to as " being fixed on " or " being set to " another element, it can be directly another
On one element or there may also be elements placed in the middle.When an element is considered as " connection " another element, it can be with
It is directly to another element or may be simultaneously present centering elements.Term as used herein " vertically ", " level
", "left", "right" and similar statement for illustrative purposes only, it is unique embodiment to be not offered as.
Unless otherwise defined, all of technologies and scientific terms used here by the article is with belonging to technical field of the invention
The normally understood meaning of technical staff is identical.Term used in the description of the invention herein is intended merely to description tool
The purpose of the embodiment of body, it is not intended that in the limitation present invention.Term as used herein " and/or " including one or more
The arbitrary and all combination of relevant Listed Items.
For example, a kind of chemical industry synthesis device, including：Cylinder, the both ends of the cylinder are respectively arranged with upper cover and lower envelope
Head；Electric hybrid module, the electric hybrid module include stent, hybrid electric motor, axis are mixed and paddle is mixed, and the stent is fixed
On the upper cover, the hybrid electric motor is set on the stent, it is described be mixed axis first end with it is described
The rotation axis connection of hybrid electric motor, the second end that axis is mixed is connect with the mixing paddle, and the mixing is stirred
Paddle is mixed to be located inside the low head；The pre-dispersed component of material, the pre-dispersed component of material include charging tube body, dsah-pot
Body, material house babinet, installation casing, pre-dispersed hybrid electric motor, pre-dispersed combined drive moving axis, pre-dispersed combination drive paddle and branch
Support, the first end of the charging tube body are connected with the upper cover, the first end of the buffering cylinder and the charging tube body
First end connection, the material houses babinet with hollow structure, and it is located inside the upper cover, the installation casing
On the madial wall for housing babinet mounted on the material, and the lateral wall of the installation casing houses babinet with the material
Material accommodating cavity body is formed between madial wall, the second end of the buffering cylinder houses babinet with the material and connect, and institute
The second end for stating buffering cylinder houses cavity with the material and connects, support frame as described above respectively with the madial wall of the upper cover and
The material houses the lateral wall connection of babinet, and the pre-dispersed hybrid electric motor is mounted on inside the installation casing, described pre-
The first end of dispersion mixing drive shaft and the rotation axis connection of the pre-dispersed hybrid electric motor, the pre-dispersed combined drive moving axis
Second end wears the installation casing successively and the material houses babinet, and the second end of the pre-dispersed combined drive moving axis
It being placed in inside the upper cover, the pre-dispersed combination drive paddle is connect with the second end of the pre-dispersed combined drive moving axis,
The bottom that the material houses babinet offers the material spilling hole for housing cavity with the material and connecting, and the material spilling hole is towards institute
State the direction setting of pre-dispersed combination drive paddle and the low head；Pressure-applying unit, the pressure-applying unit include the pressurization pump housing, defeated
Expects pipe body and material hold bucket, and the discharge end of the pressurization pump housing is connected with the second end of the charging tube body, the force (forcing) pump
The feed end of body is connected with the first end of the conveying tube body, and second end and the material of the conveying tube body hold bucket company
Logical, the material holds bucket for holding material.
In order to which further above-mentioned chemical industry synthesis device is explained, for example, the chemical industry synthesis of another embodiment
Device is as follows：
Referring to Fig. 1, chemical industry synthesis device 10 includes cylinder 100, electric hybrid module 200 and the pre-dispersed component 300 of material, mix
Seaming element 200 and the pre-dispersed component 300 of material may be contained on cylinder 100.
Referring to Fig. 1, the both ends of cylinder 100 are respectively arranged with upper cover 110 and low head 120, cylinder 100 is used to house
The material of addition, and be mixed and react to material and occasion is provided.For example, after upper cover 110 is connect with low head 120
Form cylinder 100.For another example, the cylinder is an integral molding structure.For another example, in the process for being installed on outside support of the cylinder
In, the upper cover is located at the top of outside support, and the low head is located at the lower part of outside support.
Referring to Fig. 1, electric hybrid module 200 includes stent 210, hybrid electric motor 220, axis 230 is mixed and is mixed
Paddle 240, stent 210 are fixedly mounted on the upper cover 110 of cylinder 100, and hybrid electric motor 220 is set on stent 210, and mixing is stirred
The first end of axis 230 and the rotation axis connection of hybrid electric motor 220 are mixed, the second end that axis 230 is mixed is stretched in cylinder 100
Portion, e.g., the second end that axis 230 is mixed are stretched to inside the low head 120 of cylinder 100, and the second end of axis 230 is mixed
It is connect with paddle 240 is mixed, e.g., paddle 240 is mixed and is located inside the low head 120 of cylinder 100.For example, the mixing
Agitating paddle is anchor formula agitating paddle or propeller, certainly, can also carry out selecting other kinds of stirring according to actual needs
Paddle.
It rotates, and then is driven with axis is mixed referring to Fig. 1, axis 230 is mixed for drive in hybrid electric motor 220
The 230 fixed paddles 240 that are mixed rotate.When needing to be stirred hybrid manipulation to the material in cylinder 100, control mixing
Motor 220, which drives, to be mixed axis 230 and rotates, and then is driven and paddle 240 is mixed is rotated, using disturbing for paddle 240 is mixed
Stream acts on, and can play the role of preferably being stirred, and then can be stirred hybrid manipulation to the material in cylinder 100.
Also referring to Fig. 1 and Fig. 2, the pre-dispersed component 300 of material includes charging tube body 310, buffering cylinder 320, material
Accommodating babinet 330, installation casing 340, pre-dispersed hybrid electric motor 350, pre-dispersed combined drive moving axis 360, pre-dispersed combination drive
Paddle 370 and supporting rack 380, charging tube body 310 and buffering cylinder 320, material house babinet 330 and are sequentially connected, installation casing 340
It is placed in material to house inside babinet 330, pre-dispersed hybrid electric motor 350 is mounted on inside installation casing 340, pre-dispersed combined drive
Moving axis 360 is connect respectively with pre-dispersed hybrid electric motor 350 and pre-dispersed combination drive paddle 370, supporting rack 380 and material storage box
Body 330 connects, and houses babinet 330 for stationary support material.
Referring to Fig. 2, the first end of charging tube body 310 is connected with the upper cover 110 of cylinder 100, that is, feed tube body 310
First end connect fixation with the upper cover 110 of cylinder 100.For example, the second end of the charging tube body holds bucket with material and connects,
The material holds bucket for adding in or inputting material into charging tube body 310.
Referring to Fig. 2, the first end of buffering cylinder 320 is connected with the first end for the tube body 310 that feeds, in this way, from charge pipe
The material entered in body 310 can be flowed directly into buffering cylinder 320.
Referring to Fig. 2, material houses babinet 330 with hollow structure, and material houses babinet 330 and is located at cylinder 100
Inside upper cover 110, the lateral wall that supporting rack 380 houses babinet 330 with the madial wall of upper cover 110 and material respectively is connect,
In this way, can preferably fix and support material using supporting rack 380 and buffering cylinder 320 and house babinet 330, it is whole for improving
The intensity of body mechanism.
Referring to Fig. 2, installation casing 340 is housed mounted on material on the madial wall of babinet 330, for example, the installs case
Body is mounted on the bottom that the material houses babinet.The lateral wall and material of installs case 340 are housed between the madial wall of babinet 330
Material houses cavity 331, and the second end of buffering cylinder 320 houses babinet 330 with material and connect, and buffers the of cylinder 320
Two ends house cavity 331 with material and connect, in this way, material just can be along charging tube body 310- buffering cylinder 320- material accommodating cavities
The path of body 331 is conveyed.For example, the material accommodating cavity intracorporeal site is respectively formed in the both sides of the installation casing
Material conveying passage.
Referring to Fig. 2, pre-dispersed hybrid electric motor 350 is mounted on inside installation casing 340, pre-dispersed combined drive moving axis 360
First end and pre-dispersed hybrid electric motor 350 rotation axis connection, the second end of pre-dispersed combined drive moving axis 360 wears peace successively
Vanning body 340 and material house babinet 330, for example, the second end of pre-dispersed combined drive moving axis 360 wears installation casing successively
340 side wall and material house the side wall of babinet 330.The second end of pre-dispersed combined drive moving axis 360 is placed in upper cover 110
Portion, pre-dispersed combination drive paddle 370 are connect with the second end of pre-dispersed combined drive moving axis 360, for example, the pre-dispersed combined drive
Dynamic paddle houses the bottom setting of babinet towards the material.
Referring to Fig. 2, the bottom that material houses babinet 330 offers the material spilling hole for housing cavity 331 with material and connecting
332, and material spilling hole 332 is set towards the direction of pre-dispersed combination drive paddle 370 and the low head.For example, the material holds
It puts babinet and offers several material spilling holes, several material spilling holes are arranged at intervals successively, and several material spilling holes are towards described pre-
Dispersion mixing drives the setting of the direction of paddle and the low head.
When the material to addition is needed to carry out pre-dispersed hybrid manipulation, material is added in charging tube body 310 first, it
Afterwards, material is entered to by charging tube body 310 inside buffering cylinder 320, and then, material flows into material by buffering cylinder 320 again
The material of accommodating babinet 330 is housed inside cavity 331, and finally, material with material by housing the material spilling hole 332 that cavity 331 connects
Outflow leaks out, at this point, opening pre-dispersed hybrid electric motor 350, opens pre-dispersed hybrid electric motor 350 and drives pre-dispersed combination drive
Axis 360 rotates, and then pre-dispersed combination drive paddle 370 is driven to rotate, when the material for flowing out or leaking out from material spilling hole 332 is through overwinding
Turn during pre-dispersed combination drive paddle 370 when, based on pre-dispersed combination drive paddle 370 to the operating on centrifugal force of material, energy
Enough so that material dispersion is into the material of the dispersing morphologies such as material drop or material particles or material group, these pass through pre-dispersed mixing
The material of operation is thrown away by pre-dispersed combination drive paddle 370, and then is stirred with the unclassified stores in cylinder 100 and is mixed behaviour
Make, for improving stirring and mixing effect.
Above-mentioned chemical industry synthesis device 10 is by setting cylinder 100, electric hybrid module 200 and the pre-dispersed component 300 of material, when need
When material is carried out pre-dispersed hybrid manipulation, material need to be only passed through to the charging tube body 310 of the pre-dispersed component 300 of material,
And material centrifugation is thrown away by pre-dispersed combination drive paddle 370 pre-dispersed hybrid manipulation can be realized, and stirring and mixing effect again
Preferably.
There is the problem of excessively sputtering when carrying out pre-dispersed hybrid manipulation in material in order to prevent, for example, referring to Fig. 3,
The chemical industry synthesis device further includes Anti-splash component 400, the Anti-splash component 400 include the first Anti-splash plate body 410 and
Second Anti-splash plate body 420, the first end of the first Anti-splash plate body 410 and the first of the second Anti-splash plate body 420
The bottom that end houses babinet 330 with the material is connect, and the first Anti-splash plate body 410 and the second Anti-splash plate
Body 420 is placed on the material and houses outside babinet 330, the first Anti-splash plate body 410 and the second Anti-splash plate body
Be set to interval between 420, and the material spilling hole 332 be located at the first Anti-splash plate body and the second Anti-splash plate body it
Between；For another example, the second end of the second Anti-splash plate body is connect with the madial wall of the upper cover；For another example, first splashproof
Plate body is penetrated with the first arcuate structure；For another example, the second Anti-splash plate body has the second arcuate structure；For another example, described first
Plane where Anti-splash plate body houses the bottom of box with the material forms the first angle, the second Anti-splash plate body and institute
It states the plane where material houses the bottom of box and forms the second angle, the number of degrees of first angle are more than second angle
The number of degrees；For another example, the number of degrees of first angle are 135 degree~165 degree；For another example, the number of degrees of second angle are 95 degree~120
Degree, in this way, carrying out certain journey to the material for being sputtered out using the first Anti-splash plate body 410 and the second Anti-splash plate body 420
The blocking operation of degree, can prevent material when carrying out pre-dispersed hybrid manipulation, the problem of excessively sputtering occur.
In order to further improve charging efficiency and pre-dispersed mixed effect, for example, referring to Fig. 4, the chemical industry synthesis
Device further includes pressure-applying unit 500, and the pressure-applying unit 500 includes the pressurization pump housing 510, conveying tube body 520 and material and holds bucket
(not shown), the discharge end of the pressurization pump housing 510 are connected with the second end of the charging tube body 310, the pressurization pump housing
Feed end is connected with the first end of the conveying tube body, and the second end of the conveying tube body holds bucket with the material and connects, institute
It states material and holds bucket for holding material；For another example, the second end of the conveying tube body holds the communicating position of bucket with the material
Place is provided with leakproof glue-line；For another example, the material holds bucket and offers connecting hole, and the hole wall of the connecting hole is provided with interior spiral shell
Line, the lateral wall of the second end of the conveying tube body are provided with external screw thread, the internal thread and the external thread bolt connection；For another example,
The conveying tube body has round tubular structure；For another example, the caliber of the conveying tube body from the conveying tube body first end to
The direction of second end gradually increases；For another example, the material, which holds to be provided at the position of bucket, holds platform, it is described hold platform with
Difference in height is provided between the cylinder；For another example, it is described hold platform and be provided with hold holding for bucket for holding the material
Face in this way, pressurizeing using the material for bucket outflow of pressurizeing the pump housing 510 and held to the material, can further improve charging
Efficiency and pre-dispersed mixed effect.
Babinet is housed in order to more securely install the material, for example, referring to Fig. 5, the chemical industry synthesis device also wraps
Auxiliary fixing assembly 600 is included, the auxiliary fixing assembly 600 includes connecting-rod body 610 and two support rod bodies 620, the company
The first end of extension bar body 610 is connect with the madial wall of the upper cover 110, second end and the object of the connecting-rod body 610
The accommodating babinet 330 of material connects, and the first end of two support rod bodies is connect with the connecting-rod body, two supporting rods
The second end of body houses babinet with the material and connect, and forms angle between two support rod bodies.The supporting rod
Body is provided with reinforcing rib, and second end extension of the reinforcing rib from the first end of the support rod body to the support rod body is set
It puts；For another example, the support rod body has round bar structure；For another example, the support rod body is provided with several reinforcing ribs, Ruo Gansuo
Reinforcing rib is stated to be arranged at intervals successively；For another example, the number of degrees of the angle are 90 degree~130 degree；For another example, two support rod bodies with
The center of the connecting-rod body is centrosymmetric setting；For another example, the first end of the support rod body is embedded at the connecting-rod body
Inside, in this way, can more securely install the material using auxiliary fixing assembly houses babinet.
In order to strengthen the stirring and mixing effect to material, for example, referring to Fig. 6, the chemical industry synthesis device further include it is auxiliary
Electric hybrid module 700 is helped, the auxiliary electric hybrid module 700 includes auxiliary mixing body 710 and several auxiliary mixing paddles 720, institute
It states auxiliary mixing body 710 to be placed on the mixing axis 230, and at the medium position of the cylinder, Ruo Gansuo
It states auxiliary mixing paddle and may be contained within the auxiliary mixing body, and several auxiliary mixing paddles are with the mixing axis
Central axis radially distribute.The auxiliary mixing paddle has distorted-structure；For another example, the auxiliary mixing paddle setting
Meet charge level；For another example, the charge level of meeting has the curved-surface structure of distortion；For another example, the auxiliary mixing paddle is welded in described auxiliary
It helps on mixing body；For another example, the auxiliary electric hybrid module sets at least four auxiliary mixing paddles；For another example, the auxiliary
Mixing body is spirally connected with the mixing axis, is imitated in this way, assisting electric hybrid module 700 that can further strengthen flow-disturbing by setting
Fruit, further to strengthen the stirring and mixing effect to material.
In order to further strengthen the stirring and mixing effect to material, for example, referring to Fig. 7, the chemical industry synthesis device also
Including strengthening electric hybrid module 800, the reinforcing electric hybrid module 800 includes several strengthen and mixes muscle group 810, the mixing paddle
240a has several mixing blade 241a, for example, the mixing paddle includes anchor formula agitating paddle or propeller,
In this embodiment, the mixing paddle is propeller；It is each it is described strengthen mixing muscle group 810 be arranged in a one-to-one correspondence in
The one mixing blade 241a, the mixing muscle group 810 of strengthening include several reinforcing mixing muscle 811, several reinforcings
Mixing muscle is arranged at intervals at the one side that blade is mixed successively, and the mixing muscle of strengthening has arcuate structure；For another example,
It is described to strengthen at least three reinforcing mixing muscle of mixing muscle group setting；For another example, the mixing muscle group of strengthening is set described in three
Strengthen mixing muscle；For another example, the mixing muscle of strengthening has the cross section of regular polygon structure；For another example, it is described to strengthen mixing muscle tool
There is the cross section of equilateral triangle structure；For another example, the mixing muscle of strengthening has the cross section of regular hexagon structure；For another example, it is described
Strengthening mixing muscle has the arcuate structure of distortion, in this way, can further strengthen flow-disturbing effect using the reinforcing electric hybrid module,
Further to strengthen the stirring and mixing effect to material.
It should be pointed out that when each material that the inner barrel is stirred hybrid manipulation carries out combination reaction, and
Most of combination reaction is all exothermic reaction, and the yield of rate and the product generation of reaction is also required to what is released during dependent reaction
Heat, for improving reaction rate and yield.In addition, in whipping process, the electric hybrid module can do work to material, i.e. material
It during agitation is mutually mixed, shows as outwardly releasing heat, especially the stronger material of toughness, exothermic phenomenon
It becomes apparent from, therefore, based on the above situation, for the combination reaction of some dependence higher temperatures, such as dependent on reaction self-heat generation
With the combination reaction of stirring heat production, and additional heating unit is not needed to for the reaction that it is heated, it is especially desirable to ensure
The heat-insulating property of the cylinder.Further, in order to be directed to some acid materials, therefore, to assure that the madial wall of the cylinder, i.e.,
The madial wall of the cylinder directly contacted with acid material has higher acid etch resistance energy, for prolonging making for the raw cylinder
It is normally carried out with the service life with what is reacted.Further, the lateral wall of the cylinder with corrosive materials due to often contacting, e.g.,
The corrosive materials contact of the forms such as gaseous state or liquid, it is therefore desirable to have preferable corrosion resistance, for preferably protecting
The cylinder.
In order to improve acid etch resistance energy, heat-insulating property and the corrosion resistance of the cylinder, for example, referring to Fig. 8, described
Cylinder, e.g., the side wall of the cylinder include the resistance to acid attack layer 130 being cascading, insulating layer 140, supporting layer 150, counterweight
Layer 160 and protective layer 170, the resistance to acid attack layer are located at the madial wall of the cylinder, and the resistance to acid attack layer is directly and material,
Such as, acid material contact, the protective layer are located at the lateral wall of the cylinder, i.e., described protective layer is directly naked to be exposed on the external.
For example, the resistance to acid attack layer of an embodiment includes each component of following mass parts：75 parts~88 parts of iron, titanium 30
Part~34 parts, 20 parts~25 parts of chromium, 2.5~3.4 parts of antimony, 2.3~3.4 parts of copper part, 1.5 parts~2.7 parts of zinc, aluminium 0.9~1.4
Part, 0.15 part~0.27 part of carbon, 0.25 part~0.46 part of silicon, 0.12 part~0.18 part of boron, 0.04 part~0.09 part of cobalt, phosphorus
0.001 part~0.03 part, 0.001 part~0.03 part of sulphur, 0.02 part~0.03 part of strontium, 0.03 part~0.04 part of bismuth, 0.01 part of scandium
~0.02 part and 0.001 part~0.002 part of gadolinium.Wherein, scandium is scandium or containing scadium compound, wherein, containing containing scandium in scadium compound
Element；Gadolinium is gadolinium or containing gadolinium compound, wherein, containing containing gadolinium element in gadolinium compound；Bismuth be bismuth or bismuth-containing compound, wherein,
Contain bismuth element in bismuth gadolinium compound；Strontium is strontium or containing strontium compound, wherein, contain strontium element in strontium gadolinium compound.
Using 20 parts~25 parts 75 parts~88 parts of iron, 30 parts~34 parts of titanium and chromium the basis basis members as resistance to acid attack layer
Element, so as to which the resistance to acid attack layer is enable to have certain acid etch resistance, in addition, by adding 2.5~3.4 parts of antimony, copper
2.3 parts~3.4 parts, 1.5 parts~2.7 parts of zinc, 0.9~1.4 part of aluminium, 0.04 part~0.09 part of cobalt, 0.02 part~0.03 part of strontium, bismuth
0.001 part~0.002 part of 0.03 part~0.04 part, 0.01 part~0.02 part of scandium and gadolinium are compounded, additionally it is possible to be advanced optimized
The properties of the resistance to acid attack layer can especially advanced optimize the acid etch resistance energy of the resistance to acid attack layer, so as to
Better against the acid etching of material, for further improving the service life of the cylinder and ensuring being normally carried out for reaction.
For another example, the resistance to acid attack layer of another embodiment includes each component of following mass parts：75 parts~80 parts of iron, titanium
33 parts~34 parts, 24 parts~25 parts of chromium, 2.7~3.4 parts of antimony, 2.7 parts~3.4 parts of copper, 1.8 parts~2.5 parts of zinc, aluminium 1.1~1.4
Part, 0.18 part~0.27 part of carbon, 0.27 part~0.46 part of silicon, 0.13 part~0.18 part of boron, 0.04 part~0.09 part of cobalt, phosphorus
0.001 part~0.03 part, 0.001 part~0.03 part of sulphur, 0.02 part~0.03 part of strontium, 0.03 part~0.04 part of bismuth, 0.01 part of scandium
~0.02 part and 0.001 part~0.002 part of gadolinium.
For another example, the resistance to acid attack layer of another embodiment includes each component of following mass parts：77 parts of iron, 33 parts of titanium,
25 parts of chromium, 3.4 parts of antimony, 2.7 parts of copper, 1.9 parts of zinc, 1.3 parts of aluminium, 0.27 part of carbon, 0.46 part of silicon, 0.18 part of boron, 0.04 part of cobalt, phosphorus
0.002 part of 0.03 part, 0.001 part of sulphur, 0.03 part of strontium, 0.04 part of bismuth, 0.01 part of scandium and gadolinium.
For example, the insulating layer of an embodiment includes each component of following mass parts：It is 15 parts~22 parts of land plaster, white
8~20 parts of cotton, 8 parts~15 parts of rock wool, 7 parts~9 parts of glass fibre, 10 parts~20 parts of Lauxite, 3.5 parts of polyacrylamide~
4.5 parts, 1 part~3 parts of basalt fibre, 3~5 parts of rubber foam, 1 part~2 parts of magnesium hydroxide, aminopropyl triethoxysilane 1
Part~2 parts, 1 part~2 parts of aluminium oxide, 1 part~2 parts of 3,5- di-tert-butyl-4-hydroxybenzoic acids methyl esters, 3~4 parts of polypropylene fiber,
0.2~0.8 part of 1 part~2 parts of polysulfide rubber and lauryl sodium sulfate.
It can make the insulating layer that there is good heat-insulating property using each component of as above mass parts, when in the cylinder
When exothermic reaction occurs for the material in portion, and after transferring heat to the resistance to acid attack layer, had based on the insulating layer good
Heat-insulated and heat-insulating property can limit heat and be further transmitted through the cylinder, and then heat is avoided to be transferred directly to external environment
In, it is ensured that the material of the inner barrel is reacted at a suitable temperature, for improving the production of reaction rate and product
Rate.
For another example, the insulating layer of another embodiment includes each component of following mass parts：17 parts~21 parts of land plaster,
White 17~20 parts of cotton, 10 parts~15 parts of rock wool, 7 parts~9 parts of glass fibre, 10 parts~20 parts of Lauxite, polyacrylamide 3.5
Part~4.5 parts, 1 part~2.5 parts of basalt fibre, 3.5~5 parts of rubber foam, 1.5 parts~2 parts of magnesium hydroxide, three second of aminopropyl
1.5 parts~2 parts of oxysilane, 1 part~2 parts of aluminium oxide, 1 part~1.4 parts of 3,5- di-tert-butyl-4-hydroxybenzoic acids methyl esters, third
0.2~0.5 part of 3.3~4 parts of synthetic fibre fiber, 1 part~2 parts of polysulfide rubber and lauryl sodium sulfate.
For another example, the insulating layer of another embodiment includes each component of following mass parts：19 parts of land plaster, white cotton 17
~20 parts, 15 parts of rock wool, 9 parts of glass fibre, 20 parts of Lauxite, 3.8 parts of polyacrylamide, 2.1 parts of basalt fibre, rubber
4.6 parts of foam, 1.7 parts of magnesium hydroxide, 2 parts of aminopropyl triethoxysilane, 1.8 parts of aluminium oxide, 3,5- di-t-butyl -4- hydroxyls
0.4 part of 1.4 parts of methyl benzoate, 4 parts of polypropylene fiber, 1.9 parts of polysulfide rubber and lauryl sodium sulfate.
For example, the supporting layer of an embodiment includes each component of following mass parts：95 parts~98 parts of iron, manganese 0.4
Part~0.95 part, 0.1 part~0.5 part of molybdenum, 0.01 part~0.05 part of titanium, 0.02 part~0.1 part of aluminium, 0.06 part~0.25 part of carbon,
0.1 part~0.3 part of silicon, 0.05 part~0.1 part of phosphorus, 0.001 part~0.01 part of boron, 0.05 part~0.5 part of hafnium, 0.05 part of scandium~
0.3 part, 0.05 part~0.3 part of chromium, 0.01 part~0.05 part of nickel, 0.01 part~0.05 part of cerium, 0.01 part~0.05 part of thorium and zirconium
0.01 part~0.05 part.Wherein, hafnium is hafnium or containing hafnium compound, wherein, containing containing hafnium element in hafnium compound；Scandium is scandium or contains
Scadium compound, wherein, containing in scadium compound contain scandium element；Thorium is thorium or containing thorium compound, wherein, contain in cerium-containing compound
Ce elements；Cerium be cerium or cerium-containing compound, wherein, Ce elements are contained in cerium-containing compound.
It is appreciated that in order to which the cylinder is made to have preferable heat-insulating property, need to introduce the insulating layer, and the guarantor
The mechanical strength of warm layer is poor, in order to strengthen the integrally-built mechanical strength of the cylinder, needs to introduce the supporting layer, makes it
It is in direct contact with the insulating layer, for improving the integrally-built mechanical strength of the cylinder, to achieve the purpose that safety in production.
Based on the above situation, this just necessarily requires the supporting layer to have higher mechanical strength and anti-deformation nature, by using such as
It improves quality each component of part, especially described supporting layer contains 0.05 part~0.5 part of hafnium, 0.05 part~0.3 part of scandium, 0.05 part of chromium
0.01 part~0.05 part of~0.3 part, 0.01 part~0.05 part of nickel, 0.01 part~0.05 part of cerium, 0.01 part~0.05 part of thorium and zirconium,
The mechanical strength of traditional ferroalloy can be improved, make its mechanical strength and anti-deformation nature more excellent, disclosure satisfy that requirement.
For another example, the supporting layer of another embodiment includes each component of following mass parts：97 parts~98 parts of iron, manganese
0.55 part~0.95 part, 0.35 part~0.5 part of molybdenum, 0.01 part~0.05 part of titanium, 0.02 part~0.1 part of aluminium, 0.17 part of carbon~
0.25 part, 0.1 part~0.25 part of silicon, 0.05 part~0.1 part of phosphorus, 0.008 part~0.01 part of boron, 0.1 part~0.5 part of hafnium, scandium 0.1
Part~0.3 part, 0.1 part~0.3 part of chromium, 0.02 part~0.05 part of nickel, 0.02 part~0.05 part of cerium, 0.02 part~0.05 part of thorium and
0.02 part~0.05 part of zirconium.
For another example, the supporting layer of another embodiment includes each component of following mass parts：97 parts of iron, 0.75 part of manganese,
0.5 part of molybdenum, 0.05 part of titanium, 0.02 part of aluminium, 0.17 part of carbon, 0.25 part of silicon, 0.1 part of phosphorus, 0.008 part of boron, 0.5 part of hafnium, scandium 0.2
Part, 0.2 part of chromium, 0.05 part of nickel, 0.05 part of cerium, 0.05 part of thorium and 0.05 part of zirconium.
For example, the weight coating of an embodiment includes each component of following mass parts：85 parts~95 parts of tungsten, 30 parts of nickel
0.5 part~5 parts of~60 parts, 15 parts~40 parts of iron, 1.5 parts~10 parts of chromium, 1.5 parts~10 parts of lead, 1 part~6 parts of copper and molybdenum.
It is appreciated that in reaction process is produced, need to carry out the material in the cylinder the higher stirring behaviour of intensity
Make, and since thickness is larger and the presence of the insulating layer of lighter weight, in order to avoid the integrally-built matter of the cylinder
Amount kicks the beam, and then reduces influence of the external impacts to the cylinder, you can concussion or displacement problem occurs to reduce the cylinder.
The weight coating can be made to have excellent counterweight performance using each component of as above mass parts, can effectively increase the cylinder
The integrally-built weight of body makes its weight with traditional cylinder identical or is adapted to, so as to improve the peace in production process
Full performance.
For another example, the weight coating of another embodiment includes each component of following mass parts：90 parts~95 parts of tungsten, nickel 30
0.5 part of part~45 parts, 27 parts~40 parts of iron, 1.5 parts~2.3 parts of chromium, 1.5 parts~3.3 parts of lead, 1 part~5.5 parts of copper and molybdenum~
4.9 part.
For another example, the weight coating of another embodiment includes each component of following mass parts：92 parts of tungsten, 38 parts of nickel, iron
3.8 parts of 29 parts, 2.1 parts of chromium, 2.1 parts of lead, 3.5 parts of copper and molybdenum.
For example, the protective layer of an embodiment includes each component of following mass parts：65 parts~80 parts of iron, lithium 16~
18 parts, 18 parts~25 parts of nickel, 3.5 parts~4 parts of molybdenum, 2 parts~5 parts of chromium, 1 part~5 parts of cobalt, 1 part~5 parts of vanadium, 1 part~2 parts of manganese, iridium
0.8 part~2.5 parts, 0.5 part~2.5 parts of niobium, 0.3 part~2.5 parts of scandium, 0.2 part~2.5 parts of strontium, 0.2 part~2.5 parts of caesium, tungsten
0.2 part~2.5 parts and 0.2 part~2.5 parts of titanium.Wherein, caesium is caesium or containing cesium compound, wherein, containing containing caesium in cesium compound
Element；Wherein, strontium is strontium or containing strontium compound, wherein, containing containing strontium element in strontium compound；Wherein, scandium is for scandium or containing scandium
Close object, wherein, containing in scadium compound contain scandium element；Wherein, niobium is niobium or containing niobium compound, wherein, it is included containing niobium compound
There is niobium element；Wherein, iridium is iridium or containing iridic compound, wherein, containing containing iridium in iridic compound.
It is appreciated that the lateral wall of the cylinder is with corrosive materials due to often contacting, and e.g., the forms such as gaseous state or liquid
Corrosive materials contact, it is therefore desirable to have preferable corrosion resistance, for preferably protecting the cylinder.By as above
The each component of mass parts can make the protective layer have good Corrosion Protection, and then preferably protect the cylinder, use
In the service life for extending the cylinder.
For another example, the protective layer of another embodiment includes each component of following mass parts：65 parts~70 parts of iron, lithium 16
Part~16.5 parts, 18~21 parts of nickel, 3.5 parts~3.9 parts of molybdenum, 2 parts~4.4 parts of chromium, 1 part~3.9 parts of cobalt, 1 part~4.5 parts of vanadium,
1 part~1.7 parts of manganese, 0.8 part~2.3 parts of iridium, 0.5 part~2.2 parts of niobium, 0.3 part~2.3 parts of scandium, 0.2 part~2.3 parts of strontium, caesium
0.2 part~1.9 parts of 0.2 part~2.4 parts, 0.2 part~2.1 parts of tungsten and titanium.
For another example, the protective layer of another embodiment includes each component of following mass parts：65 parts of iron, 16.5 parts of lithium,
21 parts of nickel, 3.5 parts of molybdenum, 3.5 parts of chromium, 2.8 parts of cobalt, 3.7 parts of vanadium, 1.5 parts of manganese, 2.3 parts of iridium, 2.2 parts of niobium, 2.3 parts of scandium, strontium 2.3
Part, 2.4 parts of caesium, 0.2 part of tungsten and 0.2 part of titanium.
In order to advanced optimize the cylinder, e.g., the structure of the side wall of the cylinder, for example, the resistance to acid attack layer, described
Insulating layer, the supporting layer, the weight coating and the protective layer thickness ratio be (1~1.5)：(15~20)：(5~5.5)：
(8~9.8)：(0.5~1.2)；For another example, the thickness ratio of the weight coating and the protective layer is 1：15：5：9.5：1.1.
It should be noted that the technical characteristic that the other embodiment of the present invention is further included in the various embodiments described above be combined with each other
It can be formed, and the chemical industry synthesis device that can implement.
Each technical characteristic of embodiment described above can be combined arbitrarily, to make description succinct, not to above-mentioned reality
It applies all possible combination of each technical characteristic in example to be all described, as long as however, the combination of these technical characteristics is not deposited
In contradiction, it is all considered to be the range of this specification record.
Embodiment described above only expresses the several embodiments of the present invention, and description is more specific and detailed, but
Can not the limitation to the scope of the claims of the present invention therefore be interpreted as.It should be pointed out that the ordinary skill people for this field
For member, without departing from the inventive concept of the premise, various modifications and improvements can be made, these belong to the present invention's
Protection domain.Therefore, the protection domain of patent of the present invention should be determined by the appended claims.
Claims (7)
1. a kind of chemical industry synthesis device, which is characterized in that including：
Cylinder, the both ends of the cylinder are respectively arranged with upper cover and low head；
Electric hybrid module, the electric hybrid module include stent, hybrid electric motor, axis are mixed and paddle is mixed, and the stent is consolidated
On the upper cover, the hybrid electric motor is set on the stent for Dingan County, the first end that axis is mixed and institute
The rotation axis connection of hybrid electric motor is stated, the second end that axis is mixed is connect, and the mixing with the mixing paddle
Agitating paddle is located inside the low head；
The pre-dispersed component of material, the pre-dispersed component of material include charging tube body, buffering cylinder, material and house babinet, installation
Babinet, pre-dispersed hybrid electric motor, pre-dispersed combined drive moving axis, pre-dispersed combination drive paddle and supporting rack, the charging tube body
First end is connected with the upper cover, and the first end of the buffering cylinder is connected with the first end of the charging tube body, the object
The accommodating babinet of material has hollow structure, and it is located inside the upper cover, and the installation casing is housed mounted on the material
On the madial wall of babinet, and the lateral wall of the installation casing and the material house the madial wall of babinet between form material
Accommodating cavity, the second end of the buffering cylinder house babinet with the material and connect, and the second end of the buffering cylinder
Cavity is housed with the material to connect, support frame as described above houses babinet with the madial wall of the upper cover and the material respectively
Lateral wall connects, and the pre-dispersed hybrid electric motor is mounted on inside the installation casing, and the of the pre-dispersed combined drive moving axis
The rotation axis connection of one end and the pre-dispersed hybrid electric motor, the second end of the pre-dispersed combined drive moving axis wear described successively
Installation casing and the material house babinet, and the second end of the pre-dispersed combined drive moving axis is placed in the upper cover
Portion, the pre-dispersed combination drive paddle are connect with the second end of the pre-dispersed combined drive moving axis, and the material houses babinet
Bottom offers the material spilling hole for housing cavity with the material and connecting, and the material spilling hole is towards the pre-dispersed combination drive paddle
And the direction setting of the low head；
Pressure-applying unit, the pressure-applying unit include the pressurization pump housing, conveying tube body and material and hold bucket, the discharging of the pressurization pump housing
The second end with the charging tube body is held to connect, the feed end of the pressurization pump housing is connected with the first end of the conveying tube body,
The second end of the conveying tube body holds bucket with the material and connects, and the material holds bucket for holding material；
Wherein, the chemical industry synthesis device further includes auxiliary fixing assembly, and the auxiliary fixing assembly includes connecting-rod body and two
A support rod body, the first end of the connecting-rod body are connect with the madial wall of the upper cover, the second end of the connecting-rod body
Babinet is housed with the material to connect, the first end of two support rod bodies is connect with the connecting-rod body, described in two
The second end of support rod body houses babinet with the material and connect, and forms angle between two support rod bodies；It is described
Support rod body is provided with reinforcing rib, and the second end of the reinforcing rib from first end to the support rod body of the support rod body is prolonged
Stretch setting.
2. chemical industry synthesis device according to claim 1, which is characterized in that the second end of the conveying tube body and the object
Material holds and is provided with leakproof glue-line at the communicating position of bucket.
3. chemical industry synthesis device according to claim 1, which is characterized in that the material holds bucket and offers connecting hole,
The hole wall of the connecting hole is provided with internal thread, and the lateral wall of the second end of the conveying tube body is provided with external screw thread, described interior
Screw thread and the external thread bolt connection.
4. chemical industry synthesis device according to claim 1, which is characterized in that the conveying tube body has round tubular knot
Structure.
5. chemical industry synthesis device according to claim 4, which is characterized in that the caliber of the conveying tube body is by the conveying
The first end of tube body gradually increases to the direction of second end.
6. chemical industry synthesis device according to claim 1, which is characterized in that the material holds and is provided at the position of bucket
Platform is held, described hold is provided with difference in height between platform and the cylinder.
7. chemical industry synthesis device according to claim 6, which is characterized in that the platform that holds is provided with for holding
That states that material holds bucket holds face.
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Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US4578449A (en) * | 1983-03-25 | 1986-03-25 | General Electric Company | Two-stage process for preparation of polyphenylene oxides |
| CN204933452U (en) * | 2015-07-09 | 2016-01-06 | 涟水新源生物科技有限公司 | The feed arrangement of sulfonating reaction |
| CN206046009U (en) * | 2016-06-30 | 2017-03-29 | 惠州市格雷戈里科技有限公司 | Chemical industry synthesis device |
-
2016
- 2016-06-30 CN CN201610512133.6A patent/CN105964208B/en active Active
Patent Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US4578449A (en) * | 1983-03-25 | 1986-03-25 | General Electric Company | Two-stage process for preparation of polyphenylene oxides |
| CN204933452U (en) * | 2015-07-09 | 2016-01-06 | 涟水新源生物科技有限公司 | The feed arrangement of sulfonating reaction |
| CN206046009U (en) * | 2016-06-30 | 2017-03-29 | 惠州市格雷戈里科技有限公司 | Chemical industry synthesis device |
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