CN105964208A - Chemical synthesis device - Google Patents

Chemical synthesis device Download PDF

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Publication number
CN105964208A
CN105964208A CN201610512133.6A CN201610512133A CN105964208A CN 105964208 A CN105964208 A CN 105964208A CN 201610512133 A CN201610512133 A CN 201610512133A CN 105964208 A CN105964208 A CN 105964208A
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CN
China
Prior art keywords
parts
dispersed
casing
mixing
cylinder
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Granted
Application number
CN201610512133.6A
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Chinese (zh)
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CN105964208B (en
Inventor
吴玲玲
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FUJIAN QUANZHOU HUIXIN EPE CO., LTD.
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Huizhou Gregory Technology Co Ltd
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Priority to CN201610512133.6A priority Critical patent/CN105964208B/en
Publication of CN105964208A publication Critical patent/CN105964208A/en
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Publication of CN105964208B publication Critical patent/CN105964208B/en
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    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J19/00Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J19/18Stationary reactors having moving elements inside
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01FMIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
    • B01F27/00Mixers with rotary stirring devices in fixed receptacles; Kneaders
    • B01F27/05Stirrers
    • B01F27/11Stirrers characterised by the configuration of the stirrers
    • B01F27/19Stirrers with two or more mixing elements mounted in sequence on the same axis
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01FMIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
    • B01F27/00Mixers with rotary stirring devices in fixed receptacles; Kneaders
    • B01F27/23Mixers with rotary stirring devices in fixed receptacles; Kneaders characterised by the orientation or disposition of the rotor axis
    • B01F27/232Mixers with rotary stirring devices in fixed receptacles; Kneaders characterised by the orientation or disposition of the rotor axis with two or more rotation axes
    • B01F27/2322Mixers with rotary stirring devices in fixed receptacles; Kneaders characterised by the orientation or disposition of the rotor axis with two or more rotation axes with parallel axes
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01FMIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
    • B01F27/00Mixers with rotary stirring devices in fixed receptacles; Kneaders
    • B01F27/80Mixers with rotary stirring devices in fixed receptacles; Kneaders with stirrers rotating about a substantially vertical axis
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J19/00Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J19/0053Details of the reactor
    • B01J19/0066Stirrers
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J19/00Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J19/02Apparatus characterised by being constructed of material selected for its chemically-resistant properties

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  • Chemical & Material Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Organic Chemistry (AREA)
  • Mixers Of The Rotary Stirring Type (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)

Abstract

The invention discloses a chemical synthesis device which comprises a barrel body, a mixing assembly, a material pre-dispersing assembly and a pressurizing assembly, wherein the two ends of the barrel body are separately provided with an upper end enclosure and a lower end enclosure. The mixing assembly comprises a bracket, a mixing motor, a mixing and stirring shaft and a mixing and stirring paddle. The material pre-dispersing assembly comprises a charging pipe body, a buffer barrel body, a material accommodating box body, a mounting box body, a pre-dispersing mixing motor, a pre-dispersing mixing drive shaft, a pre-dispersing mixing drive paddle and a supporting frame. The pressurizing assembly comprises a pressurizing pump body, a material conveying pipe body and a material containing barrel. According to the chemical synthesis device disclosed by the invention, the barrel body, the mixing assembly and the material pre-dispersing assembly are arranged, so that when materials are needed to be pre-dispersed and mixed, the materials are only needed to be introduced into the charging tube body of the pre-dispersing assembly, and then are thrown out in a centrifugal manner by the pre-dispersing mixing drive paddle, and therefore, pre-dispersing and mixing operations are realized; and moreover, stirring and mixing effect is relatively good.

Description

Chemical industry synthesizer
Technical field
The present invention relates to chemical plant installations technical field, particularly relate to a kind of chemical industry synthesizer.
Background technology
At present, in material production field, after especially various materials mixing reacts, finally produced In the case of product, it usually needs use chemical industry synthesizer, for material being stirred mixing, and make it Successfully react, for obtaining the final products of higher quality.
Common, existing chemical industry synthesizer uses the rabbling mechanism material to being sequentially added into or being simultaneously introduced It is stirred mixing, to obtain the purpose of mix and blend.
But, existing chemical industry synthesizer is all directly to be stirred operation in its cylinder, not to thing Material carries out scatter operation in advance, causes its stirring and mixing effect relatively low, more time-consuming.
Summary of the invention
Based on this, it is necessary to provide one to be capable of pre-dispersion operation and stirring and mixing effect is preferably changed Work synthesizer.
A kind of chemical industry synthesizer, including:
Cylinder, the two ends of described cylinder are respectively arranged with upper cover and low head;
Electric hybrid module, described electric hybrid module includes support, hybrid electric motor, mix and blend axle and mix and blend oar, Described support is fixedly mounted on described upper cover, and described hybrid electric motor is arranged on described support, described mixed Close shaft the first end be connected with the rotary shaft of described hybrid electric motor, the second end of described mix and blend axle and Described mix and blend oar connects, and described mix and blend oar is positioned at inside described low head;
The pre-dispersed assembly of material, the pre-dispersed assembly of described material includes feed body, buffering cylinder, material appearance Put casing, casing, pre-dispersed hybrid electric motor, pre-dispersed combined drive moving axis, pre-dispersed combination drive oar are installed And bracing frame, the first end of described charging body connects with described upper cover, the first end of described buffering cylinder Connecting with the first end of described charging body, described material houses casing and has hollow structure, and it is positioned at institute Stating inside upper cover, described installation casing is arranged on described material and houses on the medial wall of casing, and described The lateral wall of casing is installed and described material houses and forms material containing cavity body between the medial wall of casing, described Second end of buffering cylinder houses casing with described material and is connected, and the second end of described buffering cylinder and institute Stating material and house cavity connection, support frame as described above houses with the medial wall of described upper cover and described material respectively The lateral wall of casing connects, and described pre-dispersed hybrid electric motor is arranged on described installation box house, described pre-point The first end dissipating combined drive moving axis is connected with the rotary shaft of described pre-dispersed hybrid electric motor, described pre-dispersed mixing Second end of drive shaft wears described installation casing successively and described material houses casing, and described pre-dispersed Second end of combined drive moving axis is placed in inside described upper cover, and described pre-dispersed combination drive oar is pre-with described Second end of dispersion mixing drive shaft connects, and described material houses the bottom of casing and offers and hold with described material Put the material spilling hole of cavity connection, and described material spilling hole is towards described pre-dispersed combination drive oar and described low head Direction arrange;
Pressure-applying unit, described pressure-applying unit include the pressurizeing pump housing, conveying body and material holds bucket, described in add The discharge end of press pump body connects with the second end of described charging body, and the feed end of the described pressurization pump housing is with described First end connection of conveying body, the second end of described conveying body holds bucket with described material and connects, described Material holds bucket for holding material.
Wherein in an embodiment, the second end of described conveying body and described material hold the connection position of bucket The place of putting is provided with leakproof glue-line.
Wherein in an embodiment, described material holds bucket and offers connecting hole, the hole wall of described connecting hole Being provided with female thread, the lateral wall of the second end of described conveying body is provided with external screw thread, described female thread with Described external thread bolt connection.
Wherein in an embodiment, described conveying body has round tubular structure.
Wherein in an embodiment, the caliber of described conveying body by the first end of described conveying body to The direction of two ends is gradually increased.
Wherein in an embodiment, described material holds the position of bucket and is provided with and holds platform, described Sheng Set level and be provided with difference in height between platform and described kettle.
Wherein in an embodiment, described in hold platform and be provided with the Sheng holding bucket for holding described material Put face.
Above-mentioned chemical industry synthesizer by arranging the pre-dispersed assembly of cylinder, electric hybrid module and material, when needs by When material carries out pre-dispersed married operation, only material need to be passed through the charging body to the pre-dispersed assembly of material, And by pre-dispersed combination drive oar, centrifugal for material throwing away can be realized pre-dispersed married operation again, and stirring is mixed Conjunction effect is preferable.
Accompanying drawing explanation
Fig. 1 is the structural representation of the chemical industry synthesizer of an embodiment of the present invention;
Fig. 2 is Fig. 1 enlarged drawing at A;
Fig. 3 is the partial structurtes schematic diagram of the chemical industry synthesizer of another embodiment of the present invention;
Fig. 4 is the partial structurtes schematic diagram of the chemical industry synthesizer of another embodiment of the present invention;
Fig. 5 is the partial structurtes schematic diagram of the chemical industry synthesizer of another embodiment of the present invention;
Fig. 6 is the partial structurtes schematic diagram of the chemical industry synthesizer of another embodiment of the present invention;
Fig. 7 is the partial structurtes schematic diagram of the chemical industry synthesizer of another embodiment of the present invention;
Fig. 8 is the partial structurtes schematic diagram of the chemical industry synthesizer of another embodiment of the present invention.
Detailed description of the invention
For the ease of understanding the present invention, below with reference to relevant drawings, the present invention is described more fully. Accompanying drawing gives the better embodiment of the present invention.But, the present invention can come in many different forms Realize, however it is not limited to embodiments described herein.On the contrary, provide the purpose of these embodiments to be Make the disclosure is understood more thorough comprehensively.
It should be noted that when element is referred to as " being fixed on " or " being arranged at " another element, and it can be straight It is connected on another element or element placed in the middle can also be there is.When element be considered as " connection " another Individual element, it can be directly to another element or may be simultaneously present centering elements.Institute herein The term " vertical ", " level ", "left", "right" and the similar statement that use simply to illustrate that mesh , being not offered as is unique embodiment.
Unless otherwise defined, all of technology used herein and scientific terminology and the technology belonging to the present invention The implication that the technical staff in field is generally understood that is identical.The art used the most in the description of the invention Language is intended merely to describe the purpose of specific embodiment, it is not intended that in limiting the present invention.Used herein Term " and/or " include the arbitrary and all of combination of one or more relevant Listed Items.
Such as, a kind of chemical industry synthesizer, including: cylinder, the two ends of described cylinder are respectively arranged with envelope Head and low head;Electric hybrid module, described electric hybrid module includes support, hybrid electric motor, mix and blend axle and mixes Closing stirring paddle, described support is fixedly mounted on described upper cover, and described hybrid electric motor is arranged at described support On, the first end of described mix and blend axle is connected with the rotary shaft of described hybrid electric motor, described mix and blend axle The second end be connected with described mix and blend oar, and described mix and blend oar is positioned at inside described low head;Thing Expect pre-dispersed assembly, the pre-dispersed assembly of described material include feeding body, buffering cylinder, material house casing, Casing, pre-dispersed hybrid electric motor, pre-dispersed combined drive moving axis, pre-dispersed combination drive oar and bracing frame are installed, First end of described charging body connects with described upper cover, the first end of described buffering cylinder and described charging First end connection of body, described material houses casing and has hollow structure, and it is positioned at described upper cover Portion, described installation casing is arranged on described material and houses on the medial wall of casing, and described installation casing Lateral wall and described material house and form material containing cavity body between the medial wall of casing, described buffering cylinder Second end houses casing with described material and is connected, and the second end of described buffering cylinder houses with described material Cavity connects, and support frame as described above houses the outside of casing with the medial wall of described upper cover and described material respectively Wall connects, and described pre-dispersed hybrid electric motor is arranged on described installation box house, described pre-dispersed combination drive First end of axle is connected with the rotary shaft of described pre-dispersed hybrid electric motor, the of described pre-dispersed combined drive moving axis Two ends wear described installation casing successively and described material houses casing, and described pre-dispersed combined drive moving axis The second end be placed in inside described upper cover, described pre-dispersed combination drive oar and described pre-dispersed combined drive Second end of moving axis connects, and described material houses the bottom of casing and offers and house cavity with described material and connect Material spilling hole, and described material spilling hole towards described pre-dispersed combination drive oar and described low head direction arrange; Pressure-applying unit, described pressure-applying unit includes that the pressurization pump housing, conveying body and material hold bucket, described force (forcing) pump The discharge end of body connects with the second end of described charging body, the feed end of the described pressurization pump housing and described conveying First end connection of body, the second end of described conveying body holds bucket with described material and connects, described material Hold bucket for holding material.
In order to further above-mentioned chemical industry synthesizer be explained, such as, the change of another embodiment Work synthesizer is as follows:
Referring to Fig. 1, chemical industry synthesizer 10 includes that cylinder 100, electric hybrid module 200 and material are pre-dispersed Assembly 300, electric hybrid module 200 and the pre-dispersed assembly of material 300 may be contained within cylinder 100.
Referring to Fig. 1, the two ends of cylinder 100 are respectively arranged with upper cover 110 and low head 120, cylinder 100 For the material of accommodating addition, and give material mix and blend and the offer occasion that reacts.Such as, upper cover 110 be connected with low head 120 after formed cylinder 100.And for example, described cylinder is formed in one structure.And for example, Described cylinder be installed on outside support during, the top of the externally-located support of described upper cover, institute State the bottom of the externally-located support of low head.
Referring to Fig. 1, electric hybrid module 200 includes support 210, hybrid electric motor 220, mix and blend axle 230 And mix and blend oar 240, support 210 is fixedly mounted on the upper cover 110 of cylinder 100, hybrid electric motor 220 are arranged on support 210, and the first end of mix and blend axle 230 is connected with the rotary shaft of hybrid electric motor 220, It is internal that second end of mix and blend axle 230 stretches to cylinder 100, e.g., and the second end of mix and blend axle 230 The low head 120 stretching to cylinder 100 is internal, the second end of mix and blend axle 230 and mix and blend oar 240 Connecting, e.g., the low head 120 that mix and blend oar 240 is positioned at cylinder 100 is internal.Such as, described mixing Stirring paddle is anchor formula stirring paddle or propeller, certainly, can also carry out according to actual needs selecting other The stirring paddle of type.
Referring to Fig. 1, hybrid electric motor 220 is used for driving mix and blend axle 230 to rotate, and then drives and mix The fixing mix and blend oar 240 of shaft 230 rotates.It is stirred when needing the material in cylinder 100 During married operation, control hybrid electric motor 220 and drive mix and blend axle 230 to rotate, and then drive mix and blend Oar 240 rotates, and utilizes the flow-disturbing effect of mix and blend oar 240, can play and preferably stir immixture, And then the material in cylinder 100 can be stirred married operation.
Seeing also Fig. 1 and Fig. 2, the pre-dispersed assembly of material 300 includes feed body 310, buffering cylinder 320, material houses casing 330, installs casing 340, pre-dispersed hybrid electric motor 350, pre-dispersed combination drive Axle 360, pre-dispersed combination drive oar 370 and bracing frame 380, charging body 310 and buffering cylinder 320, Material houses casing 330 and is sequentially connected with, and installation casing 340 is placed in material and houses casing 330 inside, in advance It is internal that dispersion mixing motor 350 is arranged on installation casing 340, pre-dispersed combined drive moving axis 360 respectively with in advance Dispersion mixing motor 350 and pre-dispersed combination drive oar 370 connect, and bracing frame 380 and material house casing 330 connect, and house casing 330 for stationary support material.
Referring to Fig. 2, the first end of charging body 310 connects with the upper cover 110 of cylinder 100, i.e. feeds First end of body 310 is connected fixing with the upper cover 110 of cylinder 100.Such as, described charging body Second end holds bucket with material and connects, and described material holds bucket for adding in charging body 310 or inputting Material.
Referring to Fig. 2, the first end of buffering cylinder 320 connects with the first end of charging body 310, so, The material entered in charging body 310 can flow directly into buffering cylinder 320 internal.
Referring to Fig. 2, material houses casing 330 and has hollow structure, and material houses casing 330 and is positioned at cylinder The upper cover 110 of body 100 is internal, and bracing frame 380 is accommodating with the medial wall of upper cover 110 and material respectively The lateral wall of casing 330 connects, and so, utilizes bracing frame 380 and buffering cylinder 320 preferably to consolidate Determine and support material storage box body 330, for improving the intensity of integrated model.
Referring to Fig. 2, installation casing 340 is arranged on material and houses on the medial wall of casing 330, such as, and institute State installation casing to be arranged on described material and house the bottom of casing.The lateral wall installing case 340 houses with material Between the medial wall of casing 330, material houses cavity 331, the second end of buffering cylinder 320 and material storage box Body 330 connects, and the second end buffering cylinder 320 houses cavity 331 and connects with material, so, and thing Material just can buffer cylinder 320-material along charging body 310-and house the path of cavity 331 and carry.Example As, described material containing cavity intracorporeal site is respectively formed with material conveying passage in the both sides of described installation casing.
Referring to Fig. 2, it is internal that pre-dispersed hybrid electric motor 350 is arranged on installation casing 340, pre-dispersed combined drive First end of moving axis 360 is connected with the rotary shaft of pre-dispersed hybrid electric motor 350, pre-dispersed combined drive moving axis 360 The second end successively wear installation casing 340 and material house casing 330, such as, pre-dispersed combined drive moving axis Second end of 360 wears successively installs the sidewall of casing 340 and material houses the sidewall of casing 330.Pre-dispersed It is internal that second end of combined drive moving axis 360 is placed in upper cover 110, and pre-dispersed combination drive oar 370 is with pre- Second end of dispersion mixing drive shaft 360 connects, and such as, described pre-dispersed combination drive oar is towards described thing The bottom of the accommodating casing of material is arranged.
Referring to Fig. 2, material houses the bottom of casing 330 and offers and house the leakage that cavity 331 connects with material Material hole 332, and material spilling hole 332 is towards the direction setting of pre-dispersed combination drive oar 370 and described low head. Such as, described material houses casing and offers some material spilling holes, and some described material spilling holes are spaced setting successively, Some described material spilling holes are all arranged towards the direction of described pre-dispersed combination drive oar and described low head.
When needing the material added is carried out pre-dispersed married operation, first to charging body 310 admixture Material, afterwards, it is internal that material is entered to buffer cylinder 320 by the body 310 that feeds, and then, material is again by delaying Rush cylinder 320 to flow into material and house the material of casing 330 to house cavity 331 internal, finally, material by House the material spilling hole 332 that cavity 331 connects flow out with material or spill, now, open pre-dispersed mixing electricity Machine 350, opens pre-dispersed hybrid electric motor 350 and drives pre-dispersed combined drive moving axis 360 to rotate, and then drives pre- Dispersion mixing drives oar 370 to rotate, when the material flowed out from material spilling hole 332 or spill is in rotary course Pre-dispersed combination drive oar 370 time, based on the pre-dispersed combination drive oar 370 operating on centrifugal force to material, Enable to material dispersion and become the material of the dispersing morphology such as material drop or material particles or material group, these warps The material crossing pre-dispersed married operation is thrown away by pre-dispersed combination drive oar 370, so with in cylinder 100 Unclassified stores is stirred married operation, is used for improving stirring and mixing effect.
Above-mentioned chemical industry synthesizer 10 is by arranging cylinder 100, electric hybrid module 200 and the pre-dispersed assembly of material 300, when material is carried out pre-dispersed married operation by needs, only material need to be passed through to the pre-dispersed assembly of material The charging body 310 of 300, and again by pre-dispersed combination drive oar 370 by centrifugal for material throw away can realize pre- Dispersive mixing operation, and stirring and mixing effect is preferable.
In order to prevent material when carrying out pre-dispersed married operation, the problem excessively sputtered occurs, such as, asks Refering to Fig. 3, described chemical industry synthesizer also includes that Anti-splash assembly 400, described Anti-splash assembly 400 include First Anti-splash plate body 410 and the second Anti-splash plate body 420, the first end of described first Anti-splash plate body 410 The bottom all housing casing 330 with described material with the first end of described second Anti-splash plate body 420 is connected, And described first Anti-splash plate body 410 and described second Anti-splash plate body 420 are all placed on described material and house Outside casing 330, it is arranged between described first Anti-splash plate body 410 and described second Anti-splash plate body 420 Interval, and described material spilling hole 332 is between described first Anti-splash plate body and described second Anti-splash plate body; And for example, described second end of the second Anti-splash plate body is connected with the medial wall of described upper cover;And for example, described First Anti-splash plate body has the first arcuate structure;And for example, described second Anti-splash plate body has the second arc Structure;And for example, described first Anti-splash plate body and described material house the plane at box bottom place and form the One angle, described second Anti-splash plate body and described material house the plane at box bottom place and form the second folder Angle, the number of degrees of described first angle are more than the number of degrees of described second angle;And for example, the degree of described first angle Number is 135 degree~165 degree;And for example, the number of degrees of described second angle are 95 degree~120 degree, so, utilize Sputtered material out is carried out to a certain degree by the first Anti-splash plate body 410 and the second Anti-splash plate body 420 Stop operation, it is possible to prevent material when carrying out pre-dispersed married operation, the problem excessively sputtered occur.
In order to improve charging efficiency and pre-dispersed mixed effect further, such as, refer to Fig. 4, describedization Work synthesizer also includes that pressure-applying unit 500, described pressure-applying unit 500 include the pressurize pump housing 510, conveying pipeline Body 520 and material hold a barrel (not shown), the discharge end of the described pressurization pump housing 510 and described charging body 310 Second end connection, the feed end of the described pressurization pump housing connects with the first end of described conveying body, described defeated Second end of material body holds bucket with described material and connects, and described material holds bucket for holding material;And for example, Second end of described conveying body and described material hold and are provided with leakproof glue-line at the communicating position of bucket;And for example, Described material holds bucket and offers connecting hole, and the hole wall of described connecting hole is provided with female thread, described conveying pipeline The lateral wall of the second end of body is provided with external screw thread, described female thread and described external thread bolt connection;And for example, institute State conveying body and there is round tubular structure;And for example, the caliber of described conveying body is by described conveying body First end is gradually increased to the direction of the second end;And for example, described material holds the position of bucket and is provided with and holds Platform, described in hold and be provided with difference in height between platform and described kettle;And for example, hold platform described in arrange Have and hold face for hold that described material holds bucket, so, utilize the pressurization pump housing 510 that described material is contained The material putting bucket outflow pressurizes, it is possible to improve charging efficiency and pre-dispersed mixed effect further.
House casing to install described material more securely, such as, refer to Fig. 5, described chemical industry synthesis dress Putting and also include auxiliary fixing assembly 600, described auxiliary fixing assembly 600 includes connecting-rod body 610 and two Strut body 620, the first end of described connecting-rod body 610 is connected with the medial wall of described upper cover 110, described Second end of connecting-rod body 610 houses casing 330 with described material and is connected, the of two described support rod body One end is all connected with described connecting-rod body, the second end of two described support rod body all with described material storage box Body connects, and forms angle between two described support rod body.Described support rod body is provided with reinforcement, institute State reinforcement extended to the second end of described support rod body by the first end of described support rod body;And for example, Described support rod body has circular bar structure;And for example, described support rod body is provided with some reinforcements, if Dry described reinforcement is spaced setting successively;And for example, the number of degrees of described angle are 90 degree~130 degree;And for example, two Individual described support rod body is centrosymmetric setting with the center of described connecting-rod body;And for example, described support rod body The first end be embedded at inside described connecting-rod body, so, utilize auxiliary fixing assembly to pacify more securely Fill described material and house casing.
In order to strengthen the stirring and mixing effect to material, such as, referring to Fig. 6, described chemical industry synthesizer is also Including auxiliary electric hybrid module 700, described auxiliary electric hybrid module 700 includes auxiliary mixing body 710 and some auxiliary Mixing paddle 720, described auxiliary mixing body 710 is helped to be placed on described mix and blend axle 230, and be positioned at At the medium position of described cylinder, some described auxiliary mixing paddles may be contained within described auxiliary mixing body, And some described auxiliary mixing paddles radially distributes with the central axis of described mix and blend axle.Described auxiliary Mixing paddle is helped to have distorted-structure;And for example, described auxiliary mixing paddle is provided with and meets charge level;And for example, institute State and meet charge level there is the curved-surface structure of distortion;And for example, described auxiliary mixing paddle is welded in described auxiliary mixing On body;And for example, described auxiliary electric hybrid module arranges auxiliary mixing paddle described at least four;And for example, institute State auxiliary mixing body to be spirally connected with described mix and blend axle, so, by arranging auxiliary electric hybrid module 700 energy Enough reinforcement flow-disturbing effects further, to strengthen the stirring and mixing effect to material further.
In order to strengthen the stirring and mixing effect to material further, such as, referring to Fig. 7, described chemical industry synthesizes Device also includes strengthening electric hybrid module 800, and described strengthening electric hybrid module 800 includes some strengthening mixing muscle groups 810, described mix and blend oar 240a has some mix and blend blade 241a, such as, described mix and blend Oar includes anchor formula stirring paddle or propeller, and in this embodiment, described mix and blend oar is that spiral stirs Mix oar;Each described strengthening mixing muscle group 810 one_to_one corresponding is arranged at mix and blend blade 241a described in, Described strengthening mixing muscle group 810 includes that some strengthening mixing muscle 811, some described strengthening mixing muscle are spaced successively Being arranged at the one side of described mix and blend blade, described strengthening mixing muscle has arcuate structure;And for example, institute State strengthening mixing muscle group and strengthening mixing muscle described at least three is set;And for example, described strengthening mixing muscle group is arranged Three described strengthening mixing muscle;And for example, described strengthening mixing muscle has the cross section of regular polygon structure;Again As, described strengthening mixing muscle has the cross section of equilateral triangle structure;And for example, described strengthening mixing muscle has The cross section of regular hexagon structure;And for example, described strengthening mixing muscle has an arcuate structure of distortion, so, Utilize described strengthening electric hybrid module can strengthen flow-disturbing effect further, to strengthen the stirring to material further Mixed effect.
It is pointed out that being stirred each material of married operation in described inner barrel carries out combination reaction Time, and most combination reaction is all exothermic reaction, the productivity that the speed of reaction and product generate is also required to Liberated heat during dependent reaction, is used for improving reaction rate and productivity.Additionally, in whipping process, institute Stating electric hybrid module to do work material, i.e. material is during being mutually mixed agitation, shows as outwardly putting Go out heat, the material that especially toughness is stronger, its exothermic phenomenon becomes apparent from, therefore, based on above-mentioned situation, The combination reaction of higher temperature is relied on, as depended on reaction self-heat generation and the chemical combination of stirring heat production for some Reaction, and need not extra heater for the reaction that it heats, it is especially desirable to guarantee described cylinder The heat-insulating property of body.Further, in order to for some acid materials, therefore, to assure that the inner side of described cylinder Wall, the medial wall of the described cylinder i.e. directly contacted with acid material possesses higher resistance to acid attack performance, is used for Prolong the raw service life of described cylinder and being normally carried out of reaction.Further, the lateral wall of described cylinder by In often contacting with corrosive materials, e.g., the corrosive materials contact of the form such as gaseous state or liquid, therefore need Possesses preferable decay resistance, for preferably protecting described cylinder.
In order to improve resistance to acid attack performance, heat-insulating property and the decay resistance of described cylinder, such as, refer to Fig. 8, described cylinder, e.g., the sidewall of described cylinder includes resistance to acid attack layer 130, the insulation being cascading Layer 140, supporting layer 150, weight coating 160 and protective layer 170, described resistance to acid attack layer is positioned at described cylinder Medial wall, and described resistance to acid attack layer is direct and material, and e.g., acid material contact, described protective layer is positioned at The lateral wall of described cylinder, the most described protective layer is the most naked to be exposed on the external.
Such as, the described resistance to acid attack layer of an embodiment includes each component of following mass parts: ferrum 75 parts~88 Part, titanium 30 parts~34 parts, chromium 20 parts~25 parts, antimony 2.5~3.4 parts, copper part 2.3~3.4 parts, 1.5 parts of zinc ~2.7 parts, aluminum 0.9~1.4 parts, 0.15 part~0.27 part of carbon, silicon 0.25 part~0.46 part, boron 0.12 part~0.18 Part, cobalt 0.04 part~0.09 part, 0.001 part~0.03 part of phosphorus, sulfur 0.001 part~0.03 part, 0.02 part of strontium~0.03 Part, bismuth 0.03 part~0.04 part, scandium 0.01 part~0.02 part and gadolinium 0.001 part~0.002 part.Wherein, scandium is Scandium or containing scadium compound, wherein, is contained within scandium element containing scadium compound;Gadolinium is gadolinium or contains gadolinium compound, its In, it is contained within gadolinium element containing gadolinium compound;Bismuth is bismuth or bismuth-containing compound, and wherein, bismuth gadolinium compound includes There is bismuth element;Strontium is strontium or contains strontium compound, and wherein, strontium gadolinium compound is contained within strontium element.
Use ferrum 75 parts~88 parts, titanium 30 parts~34 parts and 20 parts~25 parts basic bases as resistance to acid attack layer of chromium Plinth element such that it is able to make described resistance to acid attack layer possess certain resistance to acid attack performance, additionally, by adding Antimony 2.5~3.4 parts, copper 2.3 parts~3.4 parts, 1.5 parts~2.7 parts of zinc, aluminum 0.9~1.4 parts, cobalt 0.04 part~0.09 Part, 0.02 part~0.03 part of strontium, bismuth 0.03 part~0.04 part, scandium 0.01 part~0.02 part and gadolinium 0.001 part~0.002 Part compounds, additionally it is possible to optimize the properties of described resistance to acid attack layer further, especially can be further Optimize the resistance to acid attack performance of described resistance to acid attack layer such that it is able to better against the acid etching of material, be used for into one Step improves the service life of described cylinder and guarantees being normally carried out of reaction.
And for example, the described resistance to acid attack layer of another embodiment includes each component of following mass parts: ferrum 75 parts~80 Part, titanium 33 parts~34 parts, chromium 24 parts~25 parts, antimony 2.7~3.4 parts, copper 2.7 parts~3.4 parts, 1.8 parts of zinc ~2.5 parts, aluminum 1.1~1.4 parts, 0.18 part~0.27 part of carbon, silicon 0.27 part~0.46 part, boron 0.13 part~0.18 Part, cobalt 0.04 part~0.09 part, 0.001 part~0.03 part of phosphorus, sulfur 0.001 part~0.03 part, 0.02 part of strontium~0.03 Part, bismuth 0.03 part~0.04 part, scandium 0.01 part~0.02 part and gadolinium 0.001 part~0.002 part.
And for example, the described resistance to acid attack layer of another embodiment includes each component of following mass parts: ferrum 77 parts, Titanium 33 parts, chromium 25 parts, 3.4 parts of antimony, copper 2.7 parts, 1.9 parts of zinc, 1.3 parts of aluminum, 0.27 part of carbon, silicon 0.46 part, boron 0.18 part, cobalt 0.04 part, 0.03 part of phosphorus, sulfur 0.001 part, 0.03 part of strontium, bismuth 0.04 Part, scandium 0.01 part and gadolinium 0.002 part.
Such as, the described heat-insulation layer of an embodiment includes each component of following mass parts: Gypsum Fibrosum powder 15 parts~22 Part, white cotton 8~20 parts, rock wool 8 parts~15 parts, glass fibre 7 parts~9 parts, Lauxite 10 parts~20 Part, polyacrylamide 3.5 parts~4.5 parts, basalt fibre 1 part~3 parts, rubber foam 3~5 parts, hydrogen-oxygen Change 1 part~2 parts of magnesium, aminopropyl triethoxysilane 1 part~2 parts, aluminium oxide 1 part~2 parts, the tertiary fourth of 3,5-bis- Base-4-HBA methyl ester 1 part~2 parts, polypropylene fiber 3~4 parts, thiorubber. 1 part~2 parts and dodecane Base sodium sulfate 0.2~0.8 part.
The each component using as above mass parts can make described heat-insulation layer have good heat-insulating property, when described During the material generation exothermic reaction of inner barrel, and after transferring heat to described resistance to acid attack layer, based on described Heat-insulation layer has good heat insulation and heat-insulating property, can limit heat and be further transmitted through described cylinder, and then Heat is avoided to be transferred directly in external environment, it is ensured that the material of described inner barrel is at a suitable temperature React, for improving the productivity of reaction rate and product.
And for example, the described heat-insulation layer of another embodiment includes each component of following mass parts: Gypsum Fibrosum powder 17 parts ~21 parts, white cotton 17~20 parts, rock wool 10 parts~15 parts, glass fibre 7 parts~9 parts, Lauxite 10 Part~20 parts, polyacrylamide 3.5 parts~4.5 parts, basalt fibre 1 part~2.5 parts, rubber foam 3.5~5 Part, 1.5 parts~2 parts of magnesium hydroxide, aminopropyl triethoxysilane 1.5 parts~2 parts, aluminium oxide 1 part~2 parts, 3,5-di-tert-butyl-4-hydroxybenzoic acid methyl ester 1 part~1.4 parts, polypropylene fiber 3.3~4 parts, thiorubber. 1 part ~2 parts and sodium lauryl sulphate 0.2~0.5 part.
And for example, the described heat-insulation layer of another embodiment includes each component of following mass parts: Gypsum Fibrosum powder 19 parts, White cotton 17~20 parts, rock wool 15 parts, glass fibre 9 parts, Lauxite 20 parts, polyacrylamide 3.8 parts, Basalt fibre 2.1 parts, rubber foam 4.6 parts, 1.7 parts of magnesium hydroxide, aminopropyl triethoxysilane 2 Part, aluminium oxide 1.8 parts, 3,5-di-tert-butyl-4-hydroxybenzoic acid methyl ester 1.4 parts, polypropylene fiber 4 parts, poly- Sulphur rubber 1.9 parts and sodium lauryl sulphate 0.4 part.
Such as, the described supporting layer of an embodiment includes each component of following mass parts: ferrum 95 parts~98 parts, 0.4 part~0.95 part of manganese, molybdenum 0.1 part~0.5 part, titanium 0.01 part~0.05 part, 0.02 part~0.1 part of aluminum, carbon 0.06 part~0.25 part, silicon 0.1 part~0.3 part, 0.05 part~0.1 part of phosphorus, boron 0.001 part~0.01 part, hafnium 0.05 part~0.5 part, scandium 0.05 part~0.3 part, chromium 0.05 part~0.3 part, 0.01 part~0.05 part of nickel, cerium 0.01 Part~0.05 part, thorium 0.01 part~0.05 part and zirconium 0.01 part~0.05 part.Wherein, hafnium is hafnium or the chemical combination Han hafnium Thing, wherein, is contained within hafnium element containing hafnium compound;Scandium is scandium or contains scadium compound, wherein, containing scandium chemical combination Thing is contained within scandium element;Thorium is thorium or contains thorium compound, and wherein, cerium-containing compound is contained within Ce elements;Cerium For cerium or cerium-containing compound, wherein, cerium-containing compound is contained within Ce elements.
It is appreciated that to make described cylinder possess preferable heat-insulating property, needs to introduce described heat-insulation layer, And the mechanical strength of described heat-insulation layer is poor, in order to strengthen the integrally-built mechanical strength of described cylinder, need Introduce described supporting layer so that it is directly contact with described heat-insulation layer, be used for improving described cylinder integrally-built Mechanical strength, to reach the purpose of safety in production.Based on above-mentioned situation, this is necessary for requiring described supporting layer Possess higher mechanical strength and anti-deformation nature, by using each component of as above mass parts, especially institute State supporting layer and contain hafnium 0.05 part~0.5 part, scandium 0.05 part~0.3 part, chromium 0.05 part~0.3 part, nickel 0.01 Part~0.05 part, cerium 0.01 part~0.05 part, thorium 0.01 part~0.05 part and zirconium 0.01 part~0.05 part, Ke Yigai The mechanical strength of kind conventional iron alloy so that it is mechanical strength and anti-deformation nature are more excellent, it is possible to meet and want Ask.
And for example, the described supporting layer of another embodiment includes each component of following mass parts: ferrum 97 parts~98 Part, 0.55 part~0.95 part of manganese, molybdenum 0.35 part~0.5 part, titanium 0.01 part~0.05 part, 0.02 part of aluminum~0.1 Part, 0.17 part~0.25 part of carbon, silicon 0.1 part~0.25 part, 0.05 part~0.1 part of phosphorus, boron 0.008 part~0.01 Part, hafnium 0.1 part~0.5 part, scandium 0.1 part~0.3 part, chromium 0.1 part~0.3 part, 0.02 part~0.05 part of nickel, Cerium 0.02 part~0.05 part, thorium 0.02 part~0.05 part and zirconium 0.02 part~0.05 part.
And for example, the described supporting layer of another embodiment includes each component of following mass parts: ferrum 97 parts, manganese 0.75 part, molybdenum 0.5 part, titanium 0.05 part, 0.02 part of aluminum, 0.17 part of carbon, silicon 0.25 part, 0.1 part of phosphorus, Boron 0.008 part, hafnium 0.5 part, scandium 0.2 part, chromium 0.2 part, 0.05 part of nickel, cerium 0.05 part, thorium 0.05 part With zirconium 0.05 part.
Such as, the described weight coating of an embodiment includes each component of following mass parts: 85 parts~95 parts of tungsten, 30 parts~60 parts of nickel, ferrum 15 parts~40 parts, chromium 1.5 parts~10 parts, 1.5 parts~10 parts of lead, copper 1 part~6 Part and molybdenum 0.5 part~5 parts.
It is appreciated that in producing course of reaction, needs that the material in described cylinder is carried out intensity higher Stirring operation, and the existence of the described heat-insulation layer of and lighter weight relatively big due to thickness, in order to avoid described cylinder The integrally-built quality of body kicks the beam, and then reduces the external impacts impact on described cylinder, i.e. can reduce There is concussion or displacement problem in described cylinder.The each component using as above mass parts can make described weight coating have Standby excellent counterweight performance, it is possible to effectively increase the integrally-built weight of described cylinder so that it is with traditional The weight of cylinder is identical or adaptive, such that it is able to the security performance improved in production process.
And for example, the described weight coating of another embodiment includes each component of following mass parts: 90 parts of tungsten~95 Part, 30 parts~45 parts of nickel, ferrum 27 parts~40 parts, chromium 1.5 parts~2.3 parts, 1.5 parts~3.3 parts of lead, copper 1 Part~5.5 parts and molybdenum 0.5 part~4.9 parts.
And for example, the described weight coating of another embodiment includes each component of following mass parts: 92 parts of tungsten, nickel 38 parts, ferrum 29 parts, chromium 2.1 parts, 2.1 parts of lead, copper 3.5 parts and molybdenum 3.8 parts.
Such as, the described protective layer of an embodiment includes each component of following mass parts: ferrum 65 parts~80 parts, Lithium 16~18 parts, 18 parts~25 parts of nickel, molybdenum 3.5 parts~4 parts, chromium 2 parts~5 parts, cobalt 1 part~5 parts, vanadium 1 Part~5 parts, 1 part~2 parts of manganese, 0.8 part~2.5 parts of iridium, niobium 0.5 part~2.5 parts, scandium 0.3 part~2.5 parts, 0.2 part~2.5 parts of strontium, caesium 0.2 part~2.5 parts, 0.2 part~2.5 parts of tungsten and titanium 0.2 part~2.5 parts.Wherein, Caesium is caesium or contains cesium compound, wherein, is contained within cesium element containing cesium compound;Wherein, strontium is strontium or contains strontium Compound, wherein, is contained within strontium element containing strontium compound;Wherein, scandium is scandium or contains scadium compound, wherein, It is contained within scandium element containing scadium compound;Wherein, niobium is niobium or contains niobium compound, wherein, containing in niobium compound Containing niobium element;Wherein, iridium is iridium or contains iridic compound, wherein, is contained within iridium containing iridic compound.
Be appreciated that the lateral wall of described cylinder owing to often contacting with corrosive materials, e.g., gaseous state or liquid The corrosive materials contact of the forms such as state, it is therefore desirable to possess preferable decay resistance, for preferably protecting Protect described cylinder.By each component of as above mass parts, described protective layer can be made to possess good anticorrosion Performance, and then preferably protect described cylinder, for extending the service life of described cylinder.
And for example, the described protective layer of another embodiment includes each component of following mass parts: ferrum 65 parts~70 Part, lithium 16 parts~16.5 parts, nickel 18~21 parts, molybdenum 3.5 parts~3.9 parts, chromium 2 parts~4.4 parts, cobalt 1 part ~3.9 parts, vanadium 1 part~4.5 parts, 1 part~1.7 parts of manganese, 0.8 part~2.3 parts of iridium, niobium 0.5 part~2.2 parts, scandium 0.3 part~2.3 parts, 0.2 part~2.3 parts of strontium, caesium 0.2 part~2.4 parts, 0.2 part~2.1 parts of tungsten and titanium 0.2 part~1.9 Part.
And for example, the described protective layer of another embodiment includes each component of following mass parts: ferrum 65 parts, lithium 16.5 parts, 21 parts of nickel, molybdenum 3.5 parts, chromium 3.5 parts, cobalt 2.8 parts, vanadium 3.7 parts, 1.5 parts of manganese, iridium 2.3 Part, niobium 2.2 parts, scandium 2.3 parts, 2.3 parts of strontium, caesium 2.4 parts, 0.2 part of tungsten and titanium 0.2 part.
In order to optimize described cylinder further, e.g., the structure of the sidewall of described cylinder, such as, described acidproof The thickness ratio of erosion layer, described heat-insulation layer, described supporting layer, described weight coating and described protective layer is (1~1.5): (15~20): (5~5.5): (8~9.8): (0.5~1.2);And for example, described weight coating and the thickness of described protective layer Degree ratio is 1:15:5:9.5:1.1.
It should be noted that other embodiments of the present invention also include the technical characteristic phase in the various embodiments described above Combination can be formed mutually, and the chemical industry synthesizer that can implement.
Each technical characteristic of embodiment described above can combine arbitrarily, for making description succinct, the most right The all possible combination of each technical characteristic in above-described embodiment is all described, but, if these skills There is not contradiction in the combination of art feature, is all considered to be the scope that this specification is recorded.
The above embodiment only have expressed the several embodiments of the present invention, and it describes more concrete and detailed Carefully, but therefore can not be interpreted as the restriction to the scope of the claims of the present invention.It should be pointed out that, for this For the those of ordinary skill in field, without departing from the inventive concept of the premise, it is also possible to make some changes Shape and improvement, these broadly fall into protection scope of the present invention.Therefore, the protection domain of patent of the present invention should be with Claims are as the criterion.

Claims (7)

1. a chemical industry synthesizer, it is characterised in that including:
Cylinder, the two ends of described cylinder are respectively arranged with upper cover and low head;
Electric hybrid module, described electric hybrid module includes support, hybrid electric motor, mix and blend axle and mix and blend oar, Described support is fixedly mounted on described upper cover, and described hybrid electric motor is arranged on described support, described mixed Close shaft the first end be connected with the rotary shaft of described hybrid electric motor, the second end of described mix and blend axle and Described mix and blend oar connects, and described mix and blend oar is positioned at inside described low head;
The pre-dispersed assembly of material, the pre-dispersed assembly of described material includes feed body, buffering cylinder, material appearance Put casing, casing, pre-dispersed hybrid electric motor, pre-dispersed combined drive moving axis, pre-dispersed combination drive oar are installed And bracing frame, the first end of described charging body connects with described upper cover, the first end of described buffering cylinder Connecting with the first end of described charging body, described material houses casing and has hollow structure, and it is positioned at institute Stating inside upper cover, described installation casing is arranged on described material and houses on the medial wall of casing, and described The lateral wall of casing is installed and described material houses and forms material containing cavity body between the medial wall of casing, described Second end of buffering cylinder houses casing with described material and is connected, and the second end of described buffering cylinder and institute Stating material and house cavity connection, support frame as described above houses with the medial wall of described upper cover and described material respectively The lateral wall of casing connects, and described pre-dispersed hybrid electric motor is arranged on described installation box house, described pre-point The first end dissipating combined drive moving axis is connected with the rotary shaft of described pre-dispersed hybrid electric motor, described pre-dispersed mixing Second end of drive shaft wears described installation casing successively and described material houses casing, and described pre-dispersed Second end of combined drive moving axis is placed in inside described upper cover, and described pre-dispersed combination drive oar is pre-with described Second end of dispersion mixing drive shaft connects, and described material houses the bottom of casing and offers and hold with described material Put the material spilling hole of cavity connection, and described material spilling hole is towards described pre-dispersed combination drive oar and described low head Direction arrange;
Pressure-applying unit, described pressure-applying unit include the pressurizeing pump housing, conveying body and material holds bucket, described in add The discharge end of press pump body connects with the second end of described charging body, and the feed end of the described pressurization pump housing is with described First end connection of conveying body, the second end of described conveying body holds bucket with described material and connects, described Material holds bucket for holding material.
Chemical industry synthesizer the most according to claim 1, it is characterised in that the of described conveying body Two ends and described material hold and are provided with leakproof glue-line at the communicating position of bucket.
Chemical industry synthesizer the most according to claim 1, it is characterised in that described material holds bucket and opens Being provided with connecting hole, the hole wall of described connecting hole is provided with female thread, the outside of the second end of described conveying body Wall is provided with external screw thread, described female thread and described external thread bolt connection.
Chemical industry synthesizer the most according to claim 1, it is characterised in that described conveying body has Round tubular structure.
Chemical industry synthesizer the most according to claim 4, it is characterised in that the pipe of described conveying body Footpath is gradually increased to the direction of the second end by the first end of described conveying body.
Chemical industry synthesizer the most according to claim 1, it is characterised in that described material holds bucket Position is provided with and holds platform, described in hold and be provided with difference in height between platform and described kettle.
Chemical industry synthesizer the most according to claim 6, it is characterised in that described in hold platform arrange Have and hold face for hold that described material holds bucket.
CN201610512133.6A 2016-06-30 2016-06-30 Chemical industry synthesis device Active CN105964208B (en)

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Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US4578449A (en) * 1983-03-25 1986-03-25 General Electric Company Two-stage process for preparation of polyphenylene oxides
CN204933452U (en) * 2015-07-09 2016-01-06 涟水新源生物科技有限公司 The feed arrangement of sulfonating reaction
CN206046009U (en) * 2016-06-30 2017-03-29 惠州市格雷戈里科技有限公司 Chemical industry synthesis device

Patent Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US4578449A (en) * 1983-03-25 1986-03-25 General Electric Company Two-stage process for preparation of polyphenylene oxides
CN204933452U (en) * 2015-07-09 2016-01-06 涟水新源生物科技有限公司 The feed arrangement of sulfonating reaction
CN206046009U (en) * 2016-06-30 2017-03-29 惠州市格雷戈里科技有限公司 Chemical industry synthesis device

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