CN105964206A - Kettle type synthesis equipment - Google Patents
Kettle type synthesis equipment Download PDFInfo
- Publication number
- CN105964206A CN105964206A CN201610510922.6A CN201610510922A CN105964206A CN 105964206 A CN105964206 A CN 105964206A CN 201610510922 A CN201610510922 A CN 201610510922A CN 105964206 A CN105964206 A CN 105964206A
- Authority
- CN
- China
- Prior art keywords
- parts
- filter
- filter screen
- kettle
- synthesis device
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
- 230000015572 biosynthetic process Effects 0.000 title claims abstract description 39
- 238000003786 synthesis reaction Methods 0.000 title claims abstract description 39
- 239000000463 material Substances 0.000 claims abstract description 68
- 238000003756 stirring Methods 0.000 claims abstract description 46
- 238000001914 filtration Methods 0.000 claims abstract description 35
- 230000003139 buffering effect Effects 0.000 claims abstract description 30
- 238000005086 pumping Methods 0.000 claims abstract description 30
- 238000002156 mixing Methods 0.000 claims abstract description 20
- 238000009434 installation Methods 0.000 claims description 21
- 239000012535 impurity Substances 0.000 abstract description 12
- 238000004519 manufacturing process Methods 0.000 abstract description 8
- 238000007789 sealing Methods 0.000 abstract description 3
- 239000010410 layer Substances 0.000 description 32
- 229910052706 scandium Inorganic materials 0.000 description 21
- SIXSYDAISGFNSX-UHFFFAOYSA-N scandium atom Chemical compound [Sc] SIXSYDAISGFNSX-UHFFFAOYSA-N 0.000 description 21
- PXHVJJICTQNCMI-UHFFFAOYSA-N Nickel Chemical compound [Ni] PXHVJJICTQNCMI-UHFFFAOYSA-N 0.000 description 20
- 239000002253 acid Substances 0.000 description 18
- 238000006243 chemical reaction Methods 0.000 description 17
- VYZAMTAEIAYCRO-UHFFFAOYSA-N Chromium Chemical compound [Cr] VYZAMTAEIAYCRO-UHFFFAOYSA-N 0.000 description 14
- 229910052804 chromium Inorganic materials 0.000 description 14
- 239000011651 chromium Substances 0.000 description 14
- XEEYBQQBJWHFJM-UHFFFAOYSA-N Iron Chemical compound [Fe] XEEYBQQBJWHFJM-UHFFFAOYSA-N 0.000 description 13
- 229910052712 strontium Inorganic materials 0.000 description 13
- CIOAGBVUUVVLOB-UHFFFAOYSA-N strontium atom Chemical compound [Sr] CIOAGBVUUVVLOB-UHFFFAOYSA-N 0.000 description 13
- 150000001875 compounds Chemical class 0.000 description 12
- 230000000694 effects Effects 0.000 description 12
- 238000009413 insulation Methods 0.000 description 12
- RTAQQCXQSZGOHL-UHFFFAOYSA-N Titanium Chemical compound [Ti] RTAQQCXQSZGOHL-UHFFFAOYSA-N 0.000 description 10
- 229910052759 nickel Inorganic materials 0.000 description 10
- 229910052719 titanium Inorganic materials 0.000 description 10
- 239000010936 titanium Substances 0.000 description 10
- PNEYBMLMFCGWSK-UHFFFAOYSA-N Alumina Chemical compound [O-2].[O-2].[O-2].[Al+3].[Al+3] PNEYBMLMFCGWSK-UHFFFAOYSA-N 0.000 description 9
- 229910052684 Cerium Inorganic materials 0.000 description 9
- ZOKXTWBITQBERF-UHFFFAOYSA-N Molybdenum Chemical compound [Mo] ZOKXTWBITQBERF-UHFFFAOYSA-N 0.000 description 9
- GWXLDORMOJMVQZ-UHFFFAOYSA-N cerium Chemical compound [Ce] GWXLDORMOJMVQZ-UHFFFAOYSA-N 0.000 description 9
- 229910052750 molybdenum Inorganic materials 0.000 description 9
- 239000011733 molybdenum Substances 0.000 description 9
- 239000011241 protective layer Substances 0.000 description 9
- 229910052797 bismuth Inorganic materials 0.000 description 8
- JCXGWMGPZLAOME-UHFFFAOYSA-N bismuth atom Chemical compound [Bi] JCXGWMGPZLAOME-UHFFFAOYSA-N 0.000 description 8
- 229910052792 caesium Inorganic materials 0.000 description 8
- 229910052735 hafnium Inorganic materials 0.000 description 8
- VBJZVLUMGGDVMO-UHFFFAOYSA-N hafnium atom Chemical compound [Hf] VBJZVLUMGGDVMO-UHFFFAOYSA-N 0.000 description 8
- RYGMFSIKBFXOCR-UHFFFAOYSA-N Copper Chemical group [Cu] RYGMFSIKBFXOCR-UHFFFAOYSA-N 0.000 description 7
- 229910052688 Gadolinium Inorganic materials 0.000 description 7
- 229910052782 aluminium Inorganic materials 0.000 description 7
- XAGFODPZIPBFFR-UHFFFAOYSA-N aluminium Chemical compound [Al] XAGFODPZIPBFFR-UHFFFAOYSA-N 0.000 description 7
- 239000011248 coating agent Substances 0.000 description 7
- 238000000576 coating method Methods 0.000 description 7
- 239000010941 cobalt Substances 0.000 description 7
- 229910017052 cobalt Inorganic materials 0.000 description 7
- GUTLYIVDDKVIGB-UHFFFAOYSA-N cobalt atom Chemical compound [Co] GUTLYIVDDKVIGB-UHFFFAOYSA-N 0.000 description 7
- 238000010586 diagram Methods 0.000 description 7
- UIWYJDYFSGRHKR-UHFFFAOYSA-N gadolinium atom Chemical compound [Gd] UIWYJDYFSGRHKR-UHFFFAOYSA-N 0.000 description 7
- 230000036961 partial effect Effects 0.000 description 7
- ZSLUVFAKFWKJRC-IGMARMGPSA-N 232Th Chemical compound [232Th] ZSLUVFAKFWKJRC-IGMARMGPSA-N 0.000 description 6
- ZOXJGFHDIHLPTG-UHFFFAOYSA-N Boron Chemical compound [B] ZOXJGFHDIHLPTG-UHFFFAOYSA-N 0.000 description 6
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 description 6
- OAICVXFJPJFONN-UHFFFAOYSA-N Phosphorus Chemical compound [P] OAICVXFJPJFONN-UHFFFAOYSA-N 0.000 description 6
- XUIMIQQOPSSXEZ-UHFFFAOYSA-N Silicon Chemical compound [Si] XUIMIQQOPSSXEZ-UHFFFAOYSA-N 0.000 description 6
- 229910052776 Thorium Inorganic materials 0.000 description 6
- -1 and e.g. Substances 0.000 description 6
- 229910052796 boron Inorganic materials 0.000 description 6
- TVFDJXOCXUVLDH-UHFFFAOYSA-N caesium atom Chemical compound [Cs] TVFDJXOCXUVLDH-UHFFFAOYSA-N 0.000 description 6
- 229910052799 carbon Inorganic materials 0.000 description 6
- 229910052802 copper Inorganic materials 0.000 description 6
- 239000010949 copper Substances 0.000 description 6
- 229910052741 iridium Inorganic materials 0.000 description 6
- GKOZUEZYRPOHIO-UHFFFAOYSA-N iridium atom Chemical compound [Ir] GKOZUEZYRPOHIO-UHFFFAOYSA-N 0.000 description 6
- GUCVJGMIXFAOAE-UHFFFAOYSA-N niobium atom Chemical compound [Nb] GUCVJGMIXFAOAE-UHFFFAOYSA-N 0.000 description 6
- 229910052698 phosphorus Inorganic materials 0.000 description 6
- 239000011574 phosphorus Substances 0.000 description 6
- 229910052710 silicon Inorganic materials 0.000 description 6
- 239000010703 silicon Substances 0.000 description 6
- WFKWXMTUELFFGS-UHFFFAOYSA-N tungsten Chemical compound [W] WFKWXMTUELFFGS-UHFFFAOYSA-N 0.000 description 6
- WPBNNNQJVZRUHP-UHFFFAOYSA-L manganese(2+);methyl n-[[2-(methoxycarbonylcarbamothioylamino)phenyl]carbamothioyl]carbamate;n-[2-(sulfidocarbothioylamino)ethyl]carbamodithioate Chemical compound [Mn+2].[S-]C(=S)NCCNC([S-])=S.COC(=O)NC(=S)NC1=CC=CC=C1NC(=S)NC(=O)OC WPBNNNQJVZRUHP-UHFFFAOYSA-L 0.000 description 5
- 229910052758 niobium Inorganic materials 0.000 description 5
- 239000010955 niobium Substances 0.000 description 5
- 239000000126 substance Substances 0.000 description 5
- 229910052721 tungsten Inorganic materials 0.000 description 5
- 239000010937 tungsten Substances 0.000 description 5
- NINIDFKCEFEMDL-UHFFFAOYSA-N Sulfur Chemical compound [S] NINIDFKCEFEMDL-UHFFFAOYSA-N 0.000 description 4
- HCHKCACWOHOZIP-UHFFFAOYSA-N Zinc Chemical compound [Zn] HCHKCACWOHOZIP-UHFFFAOYSA-N 0.000 description 4
- QCWXUUIWCKQGHC-UHFFFAOYSA-N Zirconium Chemical compound [Zr] QCWXUUIWCKQGHC-UHFFFAOYSA-N 0.000 description 4
- 229910052787 antimony Inorganic materials 0.000 description 4
- WATWJIUSRGPENY-UHFFFAOYSA-N antimony atom Chemical compound [Sb] WATWJIUSRGPENY-UHFFFAOYSA-N 0.000 description 4
- 229910052725 zinc Inorganic materials 0.000 description 4
- 239000011701 zinc Substances 0.000 description 4
- 229910052726 zirconium Inorganic materials 0.000 description 4
- WYTZZXDRDKSJID-UHFFFAOYSA-N (3-aminopropyl)triethoxysilane Chemical compound CCO[Si](OCC)(OCC)CCCN WYTZZXDRDKSJID-UHFFFAOYSA-N 0.000 description 3
- 229920002748 Basalt fiber Polymers 0.000 description 3
- 229920000742 Cotton Polymers 0.000 description 3
- WHXSMMKQMYFTQS-UHFFFAOYSA-N Lithium Chemical compound [Li] WHXSMMKQMYFTQS-UHFFFAOYSA-N 0.000 description 3
- 239000004743 Polypropylene Substances 0.000 description 3
- OSGAYBCDTDRGGQ-UHFFFAOYSA-L calcium sulfate Chemical compound [Ca+2].[O-]S([O-])(=O)=O OSGAYBCDTDRGGQ-UHFFFAOYSA-L 0.000 description 3
- 230000009514 concussion Effects 0.000 description 3
- 238000005516 engineering process Methods 0.000 description 3
- 239000000835 fiber Substances 0.000 description 3
- 229920001821 foam rubber Polymers 0.000 description 3
- 239000003365 glass fiber Substances 0.000 description 3
- 229910052744 lithium Inorganic materials 0.000 description 3
- 239000011490 mineral wool Substances 0.000 description 3
- 229920002401 polyacrylamide Polymers 0.000 description 3
- 229920001155 polypropylene Polymers 0.000 description 3
- 239000000843 powder Substances 0.000 description 3
- 150000003438 strontium compounds Chemical class 0.000 description 3
- 229910052717 sulfur Inorganic materials 0.000 description 3
- 239000011593 sulfur Substances 0.000 description 3
- 229910052720 vanadium Inorganic materials 0.000 description 3
- LEONUFNNVUYDNQ-UHFFFAOYSA-N vanadium atom Chemical compound [V] LEONUFNNVUYDNQ-UHFFFAOYSA-N 0.000 description 3
- DMYOHQBLOZMDLP-UHFFFAOYSA-N 1-[2-(2-hydroxy-3-piperidin-1-ylpropoxy)phenyl]-3-phenylpropan-1-one Chemical compound C1CCCCN1CC(O)COC1=CC=CC=C1C(=O)CCC1=CC=CC=C1 DMYOHQBLOZMDLP-UHFFFAOYSA-N 0.000 description 2
- UPVYFJALDJUSOV-UHFFFAOYSA-N 3,5-Bis(1,1-dimethylethyl)-4-hydroxy-benzoic acid ethyl ester Chemical compound COC(=O)C1=CC(C(C)(C)C)=C(O)C(C(C)(C)C)=C1 UPVYFJALDJUSOV-UHFFFAOYSA-N 0.000 description 2
- DBMJMQXJHONAFJ-UHFFFAOYSA-M Sodium laurylsulphate Chemical compound [Na+].CCCCCCCCCCCCOS([O-])(=O)=O DBMJMQXJHONAFJ-UHFFFAOYSA-M 0.000 description 2
- 239000004141 Sodium laurylsulphate Substances 0.000 description 2
- 239000006185 dispersion Substances 0.000 description 2
- SNRUBQQJIBEYMU-UHFFFAOYSA-N dodecane Chemical compound CCCCCCCCCCCC SNRUBQQJIBEYMU-UHFFFAOYSA-N 0.000 description 2
- 150000002251 gadolinium compounds Chemical class 0.000 description 2
- 238000010030 laminating Methods 0.000 description 2
- 239000007788 liquid Substances 0.000 description 2
- VTHJTEIRLNZDEV-UHFFFAOYSA-L magnesium dihydroxide Chemical compound [OH-].[OH-].[Mg+2] VTHJTEIRLNZDEV-UHFFFAOYSA-L 0.000 description 2
- 229910001862 magnesium hydroxide Inorganic materials 0.000 description 2
- 239000000347 magnesium hydroxide Substances 0.000 description 2
- 239000000203 mixture Substances 0.000 description 2
- 150000002822 niobium compounds Chemical class 0.000 description 2
- 238000004080 punching Methods 0.000 description 2
- 230000002829 reductive effect Effects 0.000 description 2
- 230000002787 reinforcement Effects 0.000 description 2
- 235000019333 sodium laurylsulphate Nutrition 0.000 description 2
- 229910000640 Fe alloy Inorganic materials 0.000 description 1
- FYYHWMGAXLPEAU-UHFFFAOYSA-N Magnesium Chemical compound [Mg] FYYHWMGAXLPEAU-UHFFFAOYSA-N 0.000 description 1
- PWHULOQIROXLJO-UHFFFAOYSA-N Manganese Chemical compound [Mn] PWHULOQIROXLJO-UHFFFAOYSA-N 0.000 description 1
- 241000220317 Rosa Species 0.000 description 1
- PMZURENOXWZQFD-UHFFFAOYSA-L Sodium Sulfate Chemical compound [Na+].[Na+].[O-]S([O-])(=O)=O PMZURENOXWZQFD-UHFFFAOYSA-L 0.000 description 1
- 239000005864 Sulphur Substances 0.000 description 1
- ADGCGOYTTFAQCH-UHFFFAOYSA-N [Sr].[Gd] Chemical compound [Sr].[Gd] ADGCGOYTTFAQCH-UHFFFAOYSA-N 0.000 description 1
- 230000003044 adaptive effect Effects 0.000 description 1
- 238000013019 agitation Methods 0.000 description 1
- XXHRVGVASCXZLC-UHFFFAOYSA-N bismuth gadolinium Chemical compound [Gd].[Bi] XXHRVGVASCXZLC-UHFFFAOYSA-N 0.000 description 1
- 230000000903 blocking effect Effects 0.000 description 1
- 238000004140 cleaning Methods 0.000 description 1
- 230000001419 dependent effect Effects 0.000 description 1
- 238000006073 displacement reaction Methods 0.000 description 1
- 238000009826 distribution Methods 0.000 description 1
- 229920001971 elastomer Polymers 0.000 description 1
- 230000005611 electricity Effects 0.000 description 1
- 230000003628 erosive effect Effects 0.000 description 1
- 238000005530 etching Methods 0.000 description 1
- 239000004744 fabric Substances 0.000 description 1
- 150000002363 hafnium compounds Chemical class 0.000 description 1
- 230000000670 limiting effect Effects 0.000 description 1
- 239000011777 magnesium Substances 0.000 description 1
- 229910052749 magnesium Inorganic materials 0.000 description 1
- 229910052748 manganese Inorganic materials 0.000 description 1
- 239000011572 manganese Substances 0.000 description 1
- 238000000034 method Methods 0.000 description 1
- 229910052760 oxygen Inorganic materials 0.000 description 1
- 239000001301 oxygen Substances 0.000 description 1
- 230000035484 reaction time Effects 0.000 description 1
- 229910052938 sodium sulfate Inorganic materials 0.000 description 1
- 235000011152 sodium sulphate Nutrition 0.000 description 1
- 150000003586 thorium compounds Chemical class 0.000 description 1
Classifications
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J19/18—Stationary reactors having moving elements inside
- B01J19/1806—Stationary reactors having moving elements inside resulting in a turbulent flow of the reactants, such as in centrifugal-type reactors, or having a high Reynolds-number
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D29/00—Filters with filtering elements stationary during filtration, e.g. pressure or suction filters, not covered by groups B01D24/00 - B01D27/00; Filtering elements therefor
- B01D29/01—Filters with filtering elements stationary during filtration, e.g. pressure or suction filters, not covered by groups B01D24/00 - B01D27/00; Filtering elements therefor with flat filtering elements
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D29/00—Filters with filtering elements stationary during filtration, e.g. pressure or suction filters, not covered by groups B01D24/00 - B01D27/00; Filtering elements therefor
- B01D29/50—Filters with filtering elements stationary during filtration, e.g. pressure or suction filters, not covered by groups B01D24/00 - B01D27/00; Filtering elements therefor with multiple filtering elements, characterised by their mutual disposition
- B01D29/56—Filters with filtering elements stationary during filtration, e.g. pressure or suction filters, not covered by groups B01D24/00 - B01D27/00; Filtering elements therefor with multiple filtering elements, characterised by their mutual disposition in series connection
- B01D29/58—Filters with filtering elements stationary during filtration, e.g. pressure or suction filters, not covered by groups B01D24/00 - B01D27/00; Filtering elements therefor with multiple filtering elements, characterised by their mutual disposition in series connection arranged concentrically or coaxially
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J19/0053—Details of the reactor
- B01J19/006—Baffles
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J19/02—Apparatus characterised by being constructed of material selected for its chemically-resistant properties
-
- C—CHEMISTRY; METALLURGY
- C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
- C22C—ALLOYS
- C22C27/00—Alloys based on rhenium or a refractory metal not mentioned in groups C22C14/00 or C22C16/00
- C22C27/04—Alloys based on tungsten or molybdenum
-
- C—CHEMISTRY; METALLURGY
- C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
- C22C—ALLOYS
- C22C30/00—Alloys containing less than 50% by weight of each constituent
-
- C—CHEMISTRY; METALLURGY
- C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
- C22C—ALLOYS
- C22C30/00—Alloys containing less than 50% by weight of each constituent
- C22C30/02—Alloys containing less than 50% by weight of each constituent containing copper
-
- C—CHEMISTRY; METALLURGY
- C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
- C22C—ALLOYS
- C22C38/00—Ferrous alloys, e.g. steel alloys
- C22C38/002—Ferrous alloys, e.g. steel alloys containing In, Mg, or other elements not provided for in one single group C22C38/001 - C22C38/60
-
- C—CHEMISTRY; METALLURGY
- C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
- C22C—ALLOYS
- C22C38/00—Ferrous alloys, e.g. steel alloys
- C22C38/005—Ferrous alloys, e.g. steel alloys containing rare earths, i.e. Sc, Y, Lanthanides
-
- C—CHEMISTRY; METALLURGY
- C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
- C22C—ALLOYS
- C22C38/00—Ferrous alloys, e.g. steel alloys
- C22C38/02—Ferrous alloys, e.g. steel alloys containing silicon
-
- C—CHEMISTRY; METALLURGY
- C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
- C22C—ALLOYS
- C22C38/00—Ferrous alloys, e.g. steel alloys
- C22C38/04—Ferrous alloys, e.g. steel alloys containing manganese
-
- C—CHEMISTRY; METALLURGY
- C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
- C22C—ALLOYS
- C22C38/00—Ferrous alloys, e.g. steel alloys
- C22C38/06—Ferrous alloys, e.g. steel alloys containing aluminium
-
- C—CHEMISTRY; METALLURGY
- C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
- C22C—ALLOYS
- C22C38/00—Ferrous alloys, e.g. steel alloys
- C22C38/08—Ferrous alloys, e.g. steel alloys containing nickel
-
- C—CHEMISTRY; METALLURGY
- C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
- C22C—ALLOYS
- C22C38/00—Ferrous alloys, e.g. steel alloys
- C22C38/10—Ferrous alloys, e.g. steel alloys containing cobalt
- C22C38/105—Ferrous alloys, e.g. steel alloys containing cobalt containing Co and Ni
-
- C—CHEMISTRY; METALLURGY
- C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
- C22C—ALLOYS
- C22C38/00—Ferrous alloys, e.g. steel alloys
- C22C38/12—Ferrous alloys, e.g. steel alloys containing tungsten, tantalum, molybdenum, vanadium, or niobium
-
- C—CHEMISTRY; METALLURGY
- C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
- C22C—ALLOYS
- C22C38/00—Ferrous alloys, e.g. steel alloys
- C22C38/14—Ferrous alloys, e.g. steel alloys containing titanium or zirconium
-
- C—CHEMISTRY; METALLURGY
- C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
- C22C—ALLOYS
- C22C38/00—Ferrous alloys, e.g. steel alloys
- C22C38/18—Ferrous alloys, e.g. steel alloys containing chromium
- C22C38/20—Ferrous alloys, e.g. steel alloys containing chromium with copper
-
- C—CHEMISTRY; METALLURGY
- C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
- C22C—ALLOYS
- C22C38/00—Ferrous alloys, e.g. steel alloys
- C22C38/18—Ferrous alloys, e.g. steel alloys containing chromium
- C22C38/28—Ferrous alloys, e.g. steel alloys containing chromium with titanium or zirconium
-
- C—CHEMISTRY; METALLURGY
- C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
- C22C—ALLOYS
- C22C38/00—Ferrous alloys, e.g. steel alloys
- C22C38/18—Ferrous alloys, e.g. steel alloys containing chromium
- C22C38/30—Ferrous alloys, e.g. steel alloys containing chromium with cobalt
-
- C—CHEMISTRY; METALLURGY
- C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
- C22C—ALLOYS
- C22C38/00—Ferrous alloys, e.g. steel alloys
- C22C38/18—Ferrous alloys, e.g. steel alloys containing chromium
- C22C38/32—Ferrous alloys, e.g. steel alloys containing chromium with boron
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- C—CHEMISTRY; METALLURGY
- C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
- C22C—ALLOYS
- C22C38/00—Ferrous alloys, e.g. steel alloys
- C22C38/60—Ferrous alloys, e.g. steel alloys containing lead, selenium, tellurium, or antimony, or more than 0.04% by weight of sulfur
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J2219/02—Apparatus characterised by their chemically-resistant properties
- B01J2219/0204—Apparatus characterised by their chemically-resistant properties comprising coatings on the surfaces in direct contact with the reactive components
- B01J2219/0236—Metal based
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Engineering & Computer Science (AREA)
- Materials Engineering (AREA)
- Mechanical Engineering (AREA)
- Metallurgy (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Mixers Of The Rotary Stirring Type (AREA)
- Pressure Vessels And Lids Thereof (AREA)
Abstract
The invention provides kettle type synthesis equipment. The kettle type synthesis equipment comprises a kettle body, a stirring and mixing device, a material filtering device and a pressure buffering device. An upper sealing end and a lower sealing end are arranged at the two ends of the kettle body respectively. The stirring and mixing device comprises a mounting rack, a driving motor, a driving shaft and a stirring paddle. The material filtering device comprises a material pumping pipe body, a filtering box body, a filter screen assembly, a filtering pump body, a reflowing pipe body and a valve. The pressure buffering device is located between the material pumping pipe body and a first filter screen; the pressure buffering device comprises a plurality of buffering plate bodies. The kettle type synthesis equipment is provided with the kettle body, the stirring and mixing device and the material filtering device, and the material filtering device can be used for circularly filtering materials to remove impurities; the operation of removing the impurities is relatively simple and convenient, and the production efficiency is relatively high.
Description
Technical field
The present invention relates to chemical industry synthesis device technical field, particularly relate to a kind of autoclave synthesis device.
Background technology
At present, in material production field, after especially various materials mixing reacts, finally produced
In the case of product, it usually needs use chemical industry synthesis device, for material being stirred mixing, and make it
Successfully react, obtain the final products of higher quality for synthesis.
Wherein, due to material before the reaction or reaction after, more or less there is some impurity, traditional removal
Impurity mode is first to be taken out from chemical industry synthesis device by the product obtained after reaction, then uses the filtration of outside
Product is filtered by device.
But, above-mentioned go deimpurity mode still exist operation more complicated loaded down with trivial details problem, cause produce effect
Rate is relatively low.
Summary of the invention
Based on this, it is necessary to provide a kind of and go deimpurity operation more simple and convenient and production efficiency is higher
Autoclave synthesis device.
A kind of autoclave synthesis device, including:
Kettle, the two ends of described kettle are respectively arranged with upper cover and low head；
Mixing stirring device, described mixing stirring device includes installation frame, drives motor, drive shaft and stir
Mixing oar, described installation frame is fixedly mounted on described upper cover, and described driving motor is arranged at described installation
In frame, the first end of described drive shaft is connected with the rotary shaft of described driving motor, the of described drive shaft
Two ends are connected with described stirring paddle, and described stirring paddle is positioned at inside described low head；
Material filter, described material filter include material-pumping tube body, filter box, screen modules,
Filtering the pump housing, backflow body and valve, the first end of described material-pumping tube body connects with the bottom of described low head,
Described filter box hollow is arranged, and forms filter cavity, the second end of described material-pumping tube body and described mistake in it
First end of filter box body connects, and the second end of described material-pumping tube body connects with described filter cavity, described mistake
Net-filter assembly includes the first filter screen, the second filter screen and the 3rd filter screen, described first filter screen, described second filter screen
And described 3rd filter screen is arranged at intervals in described filter cavity successively, the edge of described first filter screen, described
The edge of the second filter screen and the edge of described 3rd filter screen all medial walls with described filter box are connected, described
First filter screen is arranged towards the direction of the second end of described material-pumping tube body, the feed end of the described filtration pump housing and institute
The second end stating filter box connects, and described filtration pump housing feed end connects with described filter cavity, described
The discharge end filtering the pump housing connects with the first end of described backflow body, the second end of described backflow body and institute
Stating upper cover connection, described valve is arranged on described backflow body；And
Pressure buffer device, described pressure buffer device between described material-pumping tube body and described first filter screen,
It is described that described pressure buffer device includes that some buffering plate bodys, some described buffering plate bodys are arranged at intervals at successively
In filter cavity, and all medial walls with described filter box, the edge of some described buffering plate bodys are connected, institute
State buffering plate body and offer flowing hole.
Wherein in an embodiment, described buffering plate body offers some flowing holes.
Wherein in an embodiment, some described flowing hole rectangular array are distributed on described buffering plate body.
Wherein in an embodiment, the described flowing hole of adjacent two described buffering plate bodys shifts to install.
Wherein in an embodiment, described flowing hole has the cross section of regular polygon structure.
Wherein in an embodiment, described flowing hole has regular hexagon feature cross-section.
Wherein in an embodiment, described buffering plate body has cuboid shape structure.
Above-mentioned autoclave synthesis device is by arranging kettle, mixing stirring device and material filter, and thing
Material defecator can be circulated filtration and go the removal of impurity to operate material, goes deimpurity operation relatively simple just
Victory, production efficiency is the highest.
Accompanying drawing explanation
Fig. 1 is the structural representation of the autoclave synthesis device of an embodiment of the present invention；
Fig. 2 is Fig. 1 enlarged drawing at A；
Fig. 3 is the partial structurtes schematic diagram of the autoclave synthesis device of another embodiment of the present invention；
Fig. 4 is the partial structurtes schematic diagram of the autoclave synthesis device of another embodiment of the present invention；
Fig. 5 is the partial structurtes schematic diagram of the autoclave synthesis device of another embodiment of the present invention；
Fig. 6 is the partial structurtes schematic diagram of the autoclave synthesis device of another embodiment of the present invention；
Fig. 7 is the partial structurtes schematic diagram of the autoclave synthesis device of another embodiment of the present invention；
Fig. 8 is the partial structurtes schematic diagram of the autoclave synthesis device of another embodiment of the present invention；
Fig. 9 is the partial structurtes schematic diagram of the autoclave synthesis device of another embodiment of the present invention.
Detailed description of the invention
For the ease of understanding the present invention, below with reference to relevant drawings, the present invention is described more fully.
Accompanying drawing gives the better embodiment of the present invention.But, the present invention can come in many different forms
Realize, however it is not limited to embodiments described herein.On the contrary, provide the purpose of these embodiments to be
Make the disclosure is understood more thorough comprehensively.
It should be noted that when element is referred to as " being fixed on " or " being arranged at " another element, and it can be straight
It is connected on another element or element placed in the middle can also be there is.When element be considered as " connection " another
Individual element, it can be directly to another element or may be simultaneously present centering elements.Institute herein
The term " vertical ", " level ", "left", "right" and the similar statement that use simply to illustrate that mesh
, being not offered as is unique embodiment.
Unless otherwise defined, all of technology used herein and scientific terminology and the technology belonging to the present invention
The implication that the technical staff in field is generally understood that is identical.The art used the most in the description of the invention
Language is intended merely to describe the purpose of specific embodiment, it is not intended that in limiting the present invention.Used herein
Term " and/or " include the arbitrary and all of combination of one or more relevant Listed Items.
Such as, a kind of autoclave synthesis device, including: kettle, the two ends of described kettle are respectively arranged with envelope
Head and low head；Mixing stirring device, described mixing stirring device includes installation frame, driving motor, drives
Moving axis and stirring paddle, described installation frame is fixedly mounted on described upper cover, and described driving motor is arranged at
On described installation frame, the first end of described drive shaft is connected with the rotary shaft of described driving motor, described in drive
Second end of moving axis is connected with described stirring paddle, and described stirring paddle is positioned at inside described low head；Material mistake
Filter device, described material filter include material-pumping tube body, filter box, screen modules, the filtration pump housing,
Backflow body and valve, the first end of described material-pumping tube body connects with the bottom of described low head, described filtration
Casing hollow is arranged, and forms filter cavity, the second end of described material-pumping tube body and described filter box in it
First end connects, and the second end of described material-pumping tube body connects with described filter cavity, described screen modules
Including the first filter screen, the second filter screen and the 3rd filter screen, described first filter screen, described second filter screen and described
Three filter screens are arranged at intervals in described filter cavity successively, the edge of described first filter screen, described second filter screen
Edge and all medial walls with described filter box, edge of described 3rd filter screen be connected, described first filter screen
Arrange towards the direction of the second end of described material-pumping tube body, the feed end of the described filtration pump housing and described Rose Box
Second end of body connects, and described filtration pump housing feed end connects with described filter cavity, the described filtration pump housing
Discharge end connect with the first end of described backflow body, the second end of described backflow body and described upper cover
Connection, described valve is arranged on described backflow body；And pressure buffer device, described pressure buffer device
Between described material-pumping tube body and described first filter screen, described pressure buffer device includes some buffering plate bodys,
Some described buffering plate bodys are arranged at intervals in described filter cavity successively, and the limit of some described buffering plate bodys
Edge all medial walls with described filter box are connected, and described buffering plate body offers flowing hole.
In order to further above-mentioned autoclave synthesis device be explained, such as, the still of another embodiment
Formula synthesis device is as follows:
Referring to Fig. 1, autoclave synthesis device 10 includes kettle 100, mixing stirring device 200 and material mistake
Filter device 300, mixing stirring device 200 and material filter 300 may be contained within kettle 100.
Referring to Fig. 1, the two ends of kettle 100 are respectively arranged with upper cover 110 and low head 120, kettle 100
For the material of accommodating addition, and give material mix and blend and the offer occasion that reacts.Such as, upper cover
110 be connected with low head 120 after formed kettle 100.And for example, described kettle is formed in one structure.And for example,
Described kettle be installed on outside support during, the top of the externally-located support of described upper cover, institute
State the bottom of the externally-located support of low head.
Such as, it is hemispherical columnar structured that described kettle has two ends, and certainly, described kettle is all right
Selecting according to practical situation, such as, using two ends is the columnar structured of plane.
Referring to Fig. 1, mixing stirring device 200 includes installation frame 210, drives motor 220, drive shaft
230 and stirring paddle 240, installation frame 210 is fixedly mounted on the upper cover 110 of kettle 100, drives electricity
Machine 220 is arranged on installation frame 210, the first end of drive shaft 230 and the rotary shaft driving motor 220
Connecting, it is internal that the second end of drive shaft 230 stretches to kettle 100, and e.g., the second end of drive shaft 230 is stretched
Entering to the low head 120 of kettle 100 internal, the second end of drive shaft 230 is connected with stirring paddle 240, e.g.,
The low head 120 that stirring paddle 240 is positioned at kettle 100 is internal.
Such as, described stirring paddle is anchor formula stirring paddle or propeller, certainly, the most also may be used
To carry out selecting other kinds of stirring paddle.
Refer to Fig. 1, drive motor 220 to be used for driving drive shaft 230 to rotate, and then drive and drive shaft
230 fixing stirring paddles 240 rotate.When needing the material in kettle 100 is stirred married operation,
Control to drive motor 220 to drive drive shaft 230 to rotate, and then drive stirring paddle 240 to rotate, utilize stirring
The flow-disturbing effect of oar 240, can play and preferably stir immixture, and then can be in kettle 100
Material is stirred married operation.
See also Fig. 1 and Fig. 2, material filter 300 include material-pumping tube body 310, filter box 320,
Screen modules 330, filter the pump housing 340, backflow body 350 and valve 360, low head 120, take out material
Body 310, filter box 320, the filtration pump housing 340, backflow body 350 and upper cover 110 are sequentially communicated,
It is internal that screen modules 330 is placed in filter box 320, and valve 360 is arranged on backflow body 350.
Seeing also Fig. 1 and Fig. 2, the first end of material-pumping tube body 310 connects with the bottom of low head 120,
So, when the material in kettle 100 is when reacting, material can flow in low head 120 and take out
In material body 310, and then carry out follow-up filter operation.
Referring to Fig. 2, filter box 320 hollow is arranged, and forms filter cavity 321 in filter box 320,
Second end of material-pumping tube body 310 is connected with the first end of filter box 320, and the second of material-pumping tube body 310
End connects with filter cavity 321, and so, the material to be filtered flowed in material-pumping tube body 310 just can flow
Enter to filter cavity 321 internal, and complete filter operation in filter cavity 321.
Referring to Fig. 2, screen modules 330 includes the first filter screen the 331, second filter screen 332 and the 3rd filter screen
333, first filter screen the 331, second filter screen 332 and the 3rd filter screen 333 are arranged at intervals at filter cavity 321 successively
In, the edge 332 of edge 331, second filter screen of the first filter screen and the edge of the 3rd filter screen 333 all with filtration
The medial wall of casing 320 connects, and so, the material flowed out in material-pumping tube body 310 is successively through the first filter
Net the 331, second filter screen 332 and the 3rd filter screen 333, so that material completes filter operation, it is possible to preferably
Remove the impurity in material, operate more convenient simply.Such as, first filter screen the 331, second filter screen 332 and
Three filter screens 333 are spaced setting successively, so that leave gap between filter screen, in such manner, it is possible to more preferably land productivity
Accommodate the impurity being filtered out with described gap, and for example, carry out clearly at interval of the Preset Time impurity to being filtered out
Reason, to reduce the problem generation of filter screen or casing blocking.
In order to preferably improve the filter effect of described screen modules, such as, described first filter screen, described
The filter opening aperture of the second filter screen and described 3rd filter screen is sequentially reduced, and so, takes three layers of effect progressively filtered
Really, it is possible to for the impurity of different-grain diameter, to optimize filtration path, and then can preferably improve described mistake
The filter effect of net-filter assembly.
Seeing also Fig. 1 and Fig. 2, the second end of the feed end and filter box 320 that filter the pump housing 340 connects
Connect, and the filtration pump housing 340 feed end connects with filter cavity 321, filters the discharge end of the pump housing 340 and returns
First end connection of flow tube body 350, the second end of backflow body 350 connects with upper cover 110.So,
Based on filter the pump housing 340 when normally working, the suction of generation, material can by filter the pump housing 340 under
End socket 120 is pumped in material-pumping tube body 310, then is sucked up in filter box 320 by material-pumping tube body 310,
And the first filter screen the 331, second filter screen 332 and the 3rd filter screen that material is in described filter box 320
When 333, complete filter operation, i.e. complete deimpurity operation, after material completes filter operation, then,
Through the described filtration pump housing 340 and by the material after filtering, under the effect filtering the pump housing 340, it is drawn into
To backflow body 350, finally, then it is back in upper cover 110, i.e. be back to kettle 100 internal,
Now, material completes a filter operation, certainly, in order to improve the removal effect of impurity further, according to
Practical situation, it is also possible to perform circulating filtration operation.
Such as, the first filter screen 331 is arranged towards the direction of the second end of material-pumping tube body 310, the 3rd filter screen 333
Arrange towards backflow body 350.
Referring to Fig. 2, valve 360 is arranged on backflow body 350, when needs carry out filter operation, beats
Valve opening door 360, now, material carries out filter operation at material filter 300 internal circulation flow, when completing
After filter operation, closing valve 360, now, material stops flowing in material filter 300.
Above-mentioned autoclave synthesis device 10 fills by arranging kettle 100, mixing stirring device 200 and material filtering
Put 300, and material filter 300 can be circulated filtration and go the removal of impurity to operate material, goes remove impurity
The operation of matter is more simple and convenient, and production efficiency is the highest.
In order to reduce the problem to screen modules impact because of the excessive generation of material pressure, preferably to protect
Screen modules and the dispersion effect of strength imparting material, such as, see also Fig. 3 and Fig. 4, described autoclave
Synthesis device also includes that pressure buffer device 400, described pressure buffer device 400 are positioned at described material-pumping tube body
310 and screen modules 330 the first filter screen 331 between, described pressure buffer device 400 includes some slow
Punching body 410, some described buffering plate bodys are arranged at intervals in described filter cavity successively, and some described slow
All medial walls with described filter box, the edge of punching body are connected, and described buffering plate body 410 offered stream
Hole 411；And for example, described buffering plate body offers some flowing holes；And for example, some described flowing holes are rectangular
Array distribution is on described buffering plate body；And for example, the described flowing hole dislocation of adjacent two described buffering plate bodys
Arrange；And for example, described flowing hole has the cross section of regular polygon structure；And for example, described flowing hole has
Regular hexagon feature cross-section；And for example, described buffering plate body has cuboid shape structure, so, works as material
When pressure buffer device 400, it is possible to reduce screen modules being impacted because of the excessive generation of material pressure
Problem, preferably to protect the dispersion effect of screen modules and strength imparting material.
In order to preferably dismantle described screen modules, and then can preferably described screen modules be carried out
Cleaning or replacement operation, such as, see also 5, described autoclave synthesis device also includes activity provision for disengagement
500, described activity provision for disengagement 500 includes locking plate body 510, plate body 530 installed by securing member 520 first
And second install plate body 540, described filter box 320 offer dismounting window 322, described locking plate body
At least partly being embedded in described dismounting window, and close described dismounting window, described securing member wears successively
Described locking plate body and the sidewall of described filter box, described first installs the first side of plate body and described lock
Tight plate body laminating, described first install the second side of plate body respectively with a side, the institute of described first filter screen
One side of a side and described 3rd filter screen of stating the second filter screen connects, and described second installs the first of plate body
Side respectively with another side of the first filter screen, another side of described second filter screen and described 3rd filter screen
Another side connects, and the second side of described installation plate body supports with the medial wall of described filter box.Described
Locking plate body is provided with sealing ring with the position of setting of described dismounting window；And for example, described securing member has
Threaded portion and head, the first end of described threaded portion wears described locking plate body and described filter box successively
Sidewall, described head is connected with the second end of described threaded portion；And for example, described head has regular hexagon knot
The cross section of structure；And for example, described locking plate body arrange set portion, described in the portion of setting be embedded at described dismounting window
In mouthful；And for example, described first installation plate body be arranged in parallel with described second installation plate body；And for example, described
One filter screen, described second filter screen and described 3rd filter screen are installed plate body with described first and are vertically arranged, so,
By described activity provision for disengagement 500, it is possible to preferably dismantle described screen modules, and then can be preferably
Described screen modules is carried out or replacement operation.
In order to preferably support described screen modules, for preferably protecting described screen modules, such as,
Referring to Fig. 6, described autoclave synthesis device also includes filtering support means 600, described filtration support means 600
Supporting rack 620 including the first support rack 610 and second, described first supports the edge of rack and described mistake
The medial wall of filter box body connects, described first support rack be positioned at described first filter screen and described second filter screen it
Between, described first supports rack offers the first mesh, and described second supports the edge of rack and described filtration
The medial wall of casing connects, and described second supports rack between described second filter screen and described 3rd filter screen,
Described second supports rack offers the second mesh.The mesh of described first filter screen, the net of described second filter screen
The filter opening size of hole and described 3rd filter screen is sequentially reduced；And for example, described first filter screen, described first support
Rack, described second filter screen, described second support rack and described 3rd filter screen be arranged in parallel；And for example, institute
State the size of the first mesh and the identical setting of size of described second mesh；And for example, described first mesh and institute
State the second mesh and be rhombus cavernous structure；And for example, described first rack and described first filter screen and institute are supported
State and be provided with interval between the second filter screen；And for example, described second rack and described second filter screen and institute are supported
State and be provided with interval between the 3rd filter screen, so, support by arranging the first support rack 610 and second
Rack 620, it is possible to preferably support described screen modules, for preferably protecting described screen modules.
In order to minimizing vortex phenomenon, and flow-disturbing degree when can improve stirring operation, such as, please
Refering to Fig. 7, described autoclave synthesis device also includes that baffle means 700, described baffle means 700 include installing
The body of rod 710, baffling montant 720 and some baffling cross bars 730, the first end of the described installation body of rod 710 and institute
The medial wall stating low head 120 connects, and described baffling montant is connected with the second end of the described installation body of rod, if
Dry described baffling cross bar is arranged at intervals on described baffling montant successively, and some described baffling cross bars are parallel sets
Put.First end of the described installation body of rod is provided with the binding face of arc-shaped curved surface structure, and described binding face is with described
The medial wall laminating of low head；And for example, the described installation body of rod is provided with reinforcement；And for example, described reinforcement
Extended to the second end of the described installation body of rod by the first end of the described installation body of rod；And for example, described baffling
Montant be arranged in parallel with described drive shaft；And for example, described baffling montant has hollow structure；And for example, described
The end of baffling cross bar has hemispherical structure, so, by arranging baffle means 700, it is possible to reduce whirlpool
Rotation phenomenon, and flow-disturbing degree when can improve stirring operation.
In order to reduce described drive shaft rotate time, the concussion problem of generation, such as, refer to Fig. 8, described
Autoclave synthesis device also includes stirring stopping means 800, and described stirring stopping means 800 includes spacing body
810 and spacing connecting rod 820, described spacing body 810 is placed on outside the second end of described drive shaft 230,
And described spacing body 810 is between described stirring paddle 240 and the bottom of described low head 120, described
Interval it is provided with, the of the described spacing body of rod between medial wall and the lateral wall of described drive shaft of spacing body
One end is connected with described spacing body, and the second end of the described spacing body of rod is connected with the bottom of described low head,
And the bearing of trend of the bearing of trend of the described spacing body of rod and described drive shaft forms angle；And for example, stir described in
Mixing oar is propeller；And for example, described spacing body has rounded cylindrical structure；And for example, described spacing
The central axis of body and the central axes of described drive shaft；And for example, described stirring stopping means is arranged
Some described spacing connecting rods, some described spacing connecting rods are radially put point with the center of described drive shaft
Cloth；And for example, described stirring stopping means arranges two described spacing connecting rods, two described spacing connecting rods
Between formed angle；And for example, the number of degrees of described angle are 60 degree～120 degree, so, by arranging stirring limit
Position device 800, it is possible to reduce described drive shaft rotate time, the concussion problem of generation.
It is pointed out that each material being stirred married operation inside described kettle carries out combination reaction
Time, and most combination reaction is all exothermic reaction, the productivity that the speed of reaction and product generate is also required to
Liberated heat during dependent reaction, is used for improving reaction rate and productivity.Additionally, in whipping process, institute
Stating mixing stirring device to do work material, i.e. material is during being mutually mixed agitation, outwards shows as
Boundary releases the material that heat, especially toughness are stronger, and its exothermic phenomenon becomes apparent from, therefore, based on above-mentioned
Situation, relies on the combination reaction of higher temperature for some, as depended on reaction self-heat generation and stirring heat production
Combination reaction, and need not extra heater for the reaction that it heats, it is especially desirable to guarantee
The heat-insulating property of described kettle.Further, in order to for some acid materials, therefore, to assure that described kettle
Medial wall, the medial wall of the described kettle i.e. directly contacted with acidity material possesses higher resistance to acid attack performance,
For prolonging the raw service life of described kettle and being normally carried out of reaction.Further, the outside of described kettle
Wall is owing to often contacting with corrosive materials, e.g., and the corrosive materials contact of the form such as gaseous state or liquid, because of
This needs possess preferable decay resistance, for preferably protecting described kettle.
In order to improve resistance to acid attack performance, heat-insulating property and the decay resistance of described kettle, such as, refer to
Fig. 8, described kettle, e.g., the sidewall of described kettle includes resistance to acid attack layer 130, the insulation being cascading
Layer 140, supporting layer 150, weight coating 160 and protective layer 170, described resistance to acid attack layer is positioned at described kettle
Medial wall, and described resistance to acid attack layer is direct and material, and e.g., acid material contact, described protective layer is positioned at
The lateral wall of described kettle, the most described protective layer is the most naked to be exposed on the external.
Such as, the described resistance to acid attack layer of an embodiment includes each component of following mass parts: ferrum 75 parts～88
Part, titanium 30 parts～34 parts, chromium 20 parts～25 parts, antimony 2.5～3.4 parts, copper part 2.3～3.4 parts, 1.5 parts of zinc
～2.7 parts, aluminum 0.9～1.4 parts, 0.15 part～0.27 part of carbon, silicon 0.25 part～0.46 part, boron 0.12 part～0.18
Part, cobalt 0.04 part～0.09 part, 0.001 part～0.03 part of phosphorus, sulfur 0.001 part～0.03 part, 0.02 part of strontium～0.03
Part, bismuth 0.03 part～0.04 part, scandium 0.01 part～0.02 part and gadolinium 0.001 part～0.002 part.Wherein, scandium is
Scandium or containing scadium compound, wherein, is contained within scandium element containing scadium compound；Gadolinium is gadolinium or contains gadolinium compound, its
In, it is contained within gadolinium element containing gadolinium compound；Bismuth is bismuth or bismuth-containing compound, and wherein, bismuth gadolinium compound includes
There is bismuth element；Strontium is strontium or contains strontium compound, and wherein, strontium gadolinium compound is contained within strontium element.
Use ferrum 75 parts～88 parts, titanium 30 parts～34 parts and chromium 20 parts～25 parts as the basis unit of resistance to acid attack layer
Element such that it is able to make described resistance to acid attack layer possess certain resistance to acid attack performance, additionally, by adding antimony
2.5～3.4 parts, copper 2.3 parts～3.4 parts, 1.5 parts～2.7 parts of zinc, aluminum 0.9～1.4 parts, cobalt 0.04 part～0.09
Part, 0.02 part～0.03 part of strontium, bismuth 0.03 part～0.04 part, scandium 0.01 part～0.02 part and gadolinium 0.001 part～0.002
Part compounds, additionally it is possible to optimize the properties of described resistance to acid attack layer further, especially can be further
Optimize the resistance to acid attack performance of described resistance to acid attack layer such that it is able to better against the acid etching of material, be used for into one
Step improves the service life of described kettle and guarantees being normally carried out of reaction.
And for example, the described resistance to acid attack layer of another embodiment includes each component of following mass parts: ferrum 75 parts～80
Part, titanium 33 parts～34 parts, chromium 24 parts～25 parts, antimony 2.7～3.4 parts, copper 2.7 parts～3.4 parts, 1.8 parts of zinc
～2.5 parts, aluminum 1.1～1.4 parts, 0.18 part～0.27 part of carbon, silicon 0.27 part～0.46 part, boron 0.13 part～0.18
Part, cobalt 0.04 part～0.09 part, 0.001 part～0.03 part of phosphorus, sulfur 0.001 part～0.03 part, 0.02 part of strontium～0.03
Part, bismuth 0.03 part～0.04 part, scandium 0.01 part～0.02 part and gadolinium 0.001 part～0.002 part.
And for example, the described resistance to acid attack layer of another embodiment includes each component of following mass parts: ferrum 77 parts,
Titanium 33 parts, chromium 25 parts, 3.4 parts of antimony, copper 2.7 parts, 1.9 parts of zinc, 1.3 parts of aluminum, 0.27 part of carbon, silicon
0.46 part, boron 0.18 part, cobalt 0.04 part, 0.03 part of phosphorus, sulfur 0.001 part, 0.03 part of strontium, bismuth 0.04
Part, scandium 0.01 part and gadolinium 0.002 part.
Such as, the described heat-insulation layer of an embodiment includes each component of following mass parts: Gypsum Fibrosum powder 15 parts～22
Part, white cotton 8～20 parts, rock wool 8 parts～15 parts, glass fibre 7 parts～9 parts, Lauxite 10 parts～20
Part, polyacrylamide 3.5 parts～4.5 parts, basalt fibre 1 part～3 parts, rubber foam 3～5 parts, hydrogen-oxygen
Change 1 part～2 parts of magnesium, aminopropyl triethoxysilane 1 part～2 parts, aluminium oxide 1 part～2 parts, the tertiary fourth of 3,5-bis-
Base-4-HBA methyl ester 1 part～2 parts, polypropylene fiber 3～4 parts, thiorubber. 1 part～2 parts and dodecane
Base sodium sulfate 0.2～0.8 part.
The each component using as above mass parts can make described heat-insulation layer have good heat-insulating property, when described
During material generation exothermic reaction within kettle, and after transferring heat to described resistance to acid attack layer, based on described
Heat-insulation layer has good heat insulation and heat-insulating property, can limit heat and be further transmitted through described kettle, and then
Heat is avoided to be transferred directly in external environment, it is ensured that the material within described kettle is at a suitable temperature
React, for improving the productivity of reaction rate and product.
And for example, the described heat-insulation layer of another embodiment includes each component of following mass parts: Gypsum Fibrosum powder 17 parts
～21 parts, white cotton 17～20 parts, rock wool 10 parts～15 parts, glass fibre 7 parts～9 parts, Lauxite 10
Part～20 parts, polyacrylamide 3.5 parts～4.5 parts, basalt fibre 1 part～2.5 parts, rubber foam 3.5～5
Part, 1.5 parts～2 parts of magnesium hydroxide, aminopropyl triethoxysilane 1.5 parts～2 parts, aluminium oxide 1 part～2 parts,
3,5-di-tert-butyl-4-hydroxybenzoic acid methyl ester 1 part～1.4 parts, polypropylene fiber 3.3～4 parts, thiorubber. 1 part
～2 parts and sodium lauryl sulphate 0.2～0.5 part.
And for example, the described heat-insulation layer of another embodiment includes each component of following mass parts: Gypsum Fibrosum powder 19 parts,
White cotton 17～20 parts, rock wool 15 parts, glass fibre 9 parts, Lauxite 20 parts, polyacrylamide 3.8 parts,
Basalt fibre 2.1 parts, rubber foam 4.6 parts, 1.7 parts of magnesium hydroxide, aminopropyl triethoxysilane 2
Part, aluminium oxide 1.8 parts, 3,5-di-tert-butyl-4-hydroxybenzoic acid methyl ester 1.4 parts, polypropylene fiber 4 parts, poly-
Sulphur rubber 1.9 parts and sodium lauryl sulphate 0.4 part.
Such as, the described supporting layer of an embodiment includes each component of following mass parts: ferrum 95 parts～98 parts,
0.4 part～0.95 part of manganese, molybdenum 0.1 part～0.5 part, titanium 0.01 part～0.05 part, 0.02 part～0.1 part of aluminum, carbon
0.06 part～0.25 part, silicon 0.1 part～0.3 part, 0.05 part～0.1 part of phosphorus, boron 0.001 part～0.01 part, hafnium
0.05 part～0.5 part, scandium 0.05 part～0.3 part, chromium 0.05 part～0.3 part, 0.01 part～0.05 part of nickel, cerium 0.01
Part～0.05 part, thorium 0.01 part～0.05 part and zirconium 0.01 part～0.05 part.Wherein, hafnium is hafnium or the chemical combination Han hafnium
Thing, wherein, is contained within hafnium element containing hafnium compound；Scandium is scandium or contains scadium compound, wherein, containing scandium chemical combination
Thing is contained within scandium element；Thorium is thorium or contains thorium compound, and wherein, cerium-containing compound is contained within Ce elements；Cerium
For cerium or cerium-containing compound, wherein, cerium-containing compound is contained within Ce elements.
It is appreciated that to make described kettle possess preferable heat-insulating property, needs to introduce described heat-insulation layer,
And the mechanical strength of described heat-insulation layer is poor, in order to strengthen the integrally-built mechanical strength of described kettle, need
Introduce described supporting layer so that it is directly contact with described heat-insulation layer, be used for improving described kettle integrally-built
Mechanical strength, to reach the purpose of safety in production.Based on above-mentioned situation, this is necessary for requiring described supporting layer
Possess higher mechanical strength and anti-deformation nature, by using each component of as above mass parts, especially institute
State supporting layer and contain hafnium 0.05 part～0.5 part, scandium 0.05 part～0.3 part, chromium 0.05 part～0.3 part, nickel 0.01
Part～0.05 part, cerium 0.01 part～0.05 part, thorium 0.01 part～0.05 part and zirconium 0.01 part～0.05 part, Ke Yigai
The mechanical strength of kind conventional iron alloy so that it is mechanical strength and anti-deformation nature are more excellent, it is possible to meet and want
Ask.
And for example, the described supporting layer of another embodiment includes each component of following mass parts: ferrum 97 parts～98
Part, 0.55 part～0.95 part of manganese, molybdenum 0.35 part～0.5 part, titanium 0.01 part～0.05 part, 0.02 part of aluminum～0.1
Part, 0.17 part～0.25 part of carbon, silicon 0.1 part～0.25 part, 0.05 part～0.1 part of phosphorus, boron 0.008 part～0.01
Part, hafnium 0.1 part～0.5 part, scandium 0.1 part～0.3 part, chromium 0.1 part～0.3 part, 0.02 part～0.05 part of nickel,
Cerium 0.02 part～0.05 part, thorium 0.02 part～0.05 part and zirconium 0.02 part～0.05 part.
And for example, the described supporting layer of another embodiment includes each component of following mass parts: ferrum 97 parts, manganese
0.75 part, molybdenum 0.5 part, titanium 0.05 part, 0.02 part of aluminum, 0.17 part of carbon, silicon 0.25 part, 0.1 part of phosphorus,
Boron 0.008 part, hafnium 0.5 part, scandium 0.2 part, chromium 0.2 part, 0.05 part of nickel, cerium 0.05 part, thorium 0.05 part
With zirconium 0.05 part.
Such as, the described weight coating of an embodiment includes each component of following mass parts: 85 parts～95 parts of tungsten,
30 parts～60 parts of nickel, ferrum 15 parts～40 parts, chromium 1.5 parts～10 parts, 1.5 parts～10 parts of lead, copper 1 part～6
Part and molybdenum 0.5 part～5 parts.
It is appreciated that in producing course of reaction, needs that the material in described kettle is carried out intensity higher
Stirring operation, and the existence of the described heat-insulation layer of and lighter weight relatively big due to thickness, in order to avoid described still
The integrally-built quality of body kicks the beam, and then reduces the external impacts impact on described kettle, i.e. can reduce
There is concussion or displacement problem in described kettle.The each component using as above mass parts can make described weight coating have
Standby excellent counterweight performance, it is possible to effectively increase the integrally-built weight of described kettle so that it is with traditional
The weight of kettle is identical or adaptive, such that it is able to the security performance improved in production process.
And for example, the described weight coating of another embodiment includes each component of following mass parts: 90 parts of tungsten～95
Part, 30 parts～45 parts of nickel, ferrum 27 parts～40 parts, chromium 1.5 parts～2.3 parts, 1.5 parts～3.3 parts of lead, copper 1
Part～5.5 parts and molybdenum 0.5 part～4.9 parts.
And for example, the described weight coating of another embodiment includes each component of following mass parts: 92 parts of tungsten, nickel
38 parts, ferrum 29 parts, chromium 2.1 parts, 2.1 parts of lead, copper 3.5 parts and molybdenum 3.8 parts.
Such as, the described protective layer of an embodiment includes each component of following mass parts: ferrum 65 parts～80 parts,
Lithium 16～18 parts, 18 parts～25 parts of nickel, molybdenum 3.5 parts～4 parts, chromium 2 parts～5 parts, cobalt 1 part～5 parts, vanadium 1
Part～5 parts, 1 part～2 parts of manganese, 0.8 part～2.5 parts of iridium, niobium 0.5 part～2.5 parts, scandium 0.3 part～2.5 parts,
0.2 part～2.5 parts of strontium, caesium 0.2 part～2.5 parts, 0.2 part～2.5 parts of tungsten and titanium 0.2 part～2.5 parts.Wherein,
Caesium is caesium or contains cesium compound, wherein, is contained within cesium element containing cesium compound；Wherein, strontium is strontium or contains strontium
Compound, wherein, is contained within strontium element containing strontium compound；Wherein, scandium is scandium or contains scadium compound, wherein,
It is contained within scandium element containing scadium compound；Wherein, niobium is niobium or contains niobium compound, wherein, containing in niobium compound
Containing niobium element；Wherein, iridium is iridium or contains iridic compound, wherein, is contained within iridium containing iridic compound.
Be appreciated that the lateral wall of described kettle owing to often contacting with corrosive materials, e.g., gaseous state or liquid
The corrosive materials contact of the forms such as state, it is therefore desirable to possess preferable decay resistance, for preferably protecting
Protect described kettle.By each component of as above mass parts, described protective layer can be made to possess good anticorrosion
Performance, and then preferably protect described kettle, for extending the service life of described kettle.
And for example, the described protective layer of another embodiment includes each component of following mass parts: ferrum 65 parts～70
Part, lithium 16 parts～16.5 parts, nickel 18～21 parts, molybdenum 3.5 parts～3.9 parts, chromium 2 parts～4.4 parts, cobalt 1 part
～3.9 parts, vanadium 1 part～4.5 parts, 1 part～1.7 parts of manganese, 0.8 part～2.3 parts of iridium, niobium 0.5 part～2.2 parts, scandium
0.3 part～2.3 parts, 0.2 part～2.3 parts of strontium, caesium 0.2 part～2.4 parts, 0.2 part～2.1 parts of tungsten and titanium 0.2 part～1.9
Part.
And for example, the described protective layer of another embodiment includes each component of following mass parts: ferrum 65 parts, lithium
16.5 parts, 21 parts of nickel, molybdenum 3.5 parts, chromium 3.5 parts, cobalt 2.8 parts, vanadium 3.7 parts, 1.5 parts of manganese, iridium 2.3
Part, niobium 2.2 parts, scandium 2.3 parts, 2.3 parts of strontium, caesium 2.4 parts, 0.2 part of tungsten and titanium 0.2 part.
In order to optimize described kettle further, e.g., the structure of the sidewall of described kettle, such as, described acidproof
The thickness ratio of erosion layer, described heat-insulation layer, described supporting layer, described weight coating and described protective layer is (1～1.5):
(15～20): (5～5.5): (8～9.8): (0.5～1.2)；And for example, described weight coating and the thickness of described protective layer
Degree ratio is 1:15:5:9.5:1.1.
It should be noted that other embodiments of the present invention also include the technical characteristic phase in the various embodiments described above
Combination can be formed mutually, and the autoclave synthesis device that can implement.
Each technical characteristic of embodiment described above can combine arbitrarily, for making description succinct, the most right
The all possible combination of each technical characteristic in above-described embodiment is all described, but, if these skills
There is not contradiction in the combination of art feature, is all considered to be the scope that this specification is recorded.
The above embodiment only have expressed the several embodiments of the present invention, and it describes more concrete and detailed
Carefully, but therefore can not be interpreted as the restriction to the scope of the claims of the present invention.It should be pointed out that, for this
For the those of ordinary skill in field, without departing from the inventive concept of the premise, it is also possible to make some changes
Shape and improvement, these broadly fall into protection scope of the present invention.Therefore, the protection domain of patent of the present invention should be with
Claims are as the criterion.
Claims (7)
1. an autoclave synthesis device, it is characterised in that including:
Kettle, the two ends of described kettle are respectively arranged with upper cover and low head；
Mixing stirring device, described mixing stirring device includes installation frame, drives motor, drive shaft and stir
Mixing oar, described installation frame is fixedly mounted on described upper cover, and described driving motor is arranged at described installation
In frame, the first end of described drive shaft is connected with the rotary shaft of described driving motor, the of described drive shaft
Two ends are connected with described stirring paddle, and described stirring paddle is positioned at inside described low head；
Material filter, described material filter include material-pumping tube body, filter box, screen modules,
Filtering the pump housing, backflow body and valve, the first end of described material-pumping tube body connects with the bottom of described low head,
Described filter box hollow is arranged, and forms filter cavity, the second end of described material-pumping tube body and described mistake in it
First end of filter box body connects, and the second end of described material-pumping tube body connects with described filter cavity, described mistake
Net-filter assembly includes the first filter screen, the second filter screen and the 3rd filter screen, described first filter screen, described second filter screen
And described 3rd filter screen is arranged at intervals in described filter cavity successively, the edge of described first filter screen, described
The edge of the second filter screen and the edge of described 3rd filter screen all medial walls with described filter box are connected, described
First filter screen is arranged towards the direction of the second end of described material-pumping tube body, the feed end of the described filtration pump housing and institute
The second end stating filter box connects, and described filtration pump housing feed end connects with described filter cavity, described
The discharge end filtering the pump housing connects with the first end of described backflow body, the second end of described backflow body and institute
Stating upper cover connection, described valve is arranged on described backflow body；And
Pressure buffer device, described pressure buffer device between described material-pumping tube body and described first filter screen,
It is described that described pressure buffer device includes that some buffering plate bodys, some described buffering plate bodys are arranged at intervals at successively
In filter cavity, and all medial walls with described filter box, the edge of some described buffering plate bodys are connected, institute
State buffering plate body and offer flowing hole.
Autoclave synthesis device the most according to claim 1, it is characterised in that described buffering plate body is offered
There are some flowing holes.
Autoclave synthesis device the most according to claim 2, it is characterised in that some described flowing holes in
Rectangular array is distributed on described buffering plate body.
Autoclave synthesis device the most according to claim 3, it is characterised in that adjacent two described bufferings
The described flowing hole of plate body shifts to install.
Autoclave synthesis device the most according to claim 1, it is characterised in that described flowing hole just has
The cross section of polygonized structure.
Autoclave synthesis device the most according to claim 5, it is characterised in that described flowing hole just has
Hexagonal structure cross section.
Autoclave synthesis device the most according to claim 1, it is characterised in that described buffering plate body has
Cuboid shape structure.
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| CN201610510922.6A CN105964206B (en) | 2016-06-30 | 2016-06-30 | Autoclave synthesis device |
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|---|---|---|---|
| CN201610510922.6A CN105964206B (en) | 2016-06-30 | 2016-06-30 | Autoclave synthesis device |
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Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN108014729A (en) * | 2017-12-20 | 2018-05-11 | 苏州市锐翊电子科技有限公司 | A kind of high-strength durable reaction kettle |
| CN114561582A (en) * | 2022-02-22 | 2022-05-31 | 中国长江三峡集团有限公司 | Alloy powder material, preparation method thereof and application of alloy powder material in corrosion resistance and rust resistance of bolt |
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| CN103083973A (en) * | 2011-11-05 | 2013-05-08 | 海门市大生水处理设备（厂）有限公司 | Air-liquid pipeline filter |
| CN205055928U (en) * | 2015-09-15 | 2016-03-02 | 山东东源新材料科技有限公司 | Produce no vanadium tombarthite base titanium and tungsten powder's stirring mixing apparatus |
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- 2016-06-30 CN CN201610510922.6A patent/CN105964206B/en active Active
Patent Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
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| CN103083973A (en) * | 2011-11-05 | 2013-05-08 | 海门市大生水处理设备（厂）有限公司 | Air-liquid pipeline filter |
| CN205055928U (en) * | 2015-09-15 | 2016-03-02 | 山东东源新材料科技有限公司 | Produce no vanadium tombarthite base titanium and tungsten powder's stirring mixing apparatus |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN108014729A (en) * | 2017-12-20 | 2018-05-11 | 苏州市锐翊电子科技有限公司 | A kind of high-strength durable reaction kettle |
| CN114561582A (en) * | 2022-02-22 | 2022-05-31 | 中国长江三峡集团有限公司 | Alloy powder material, preparation method thereof and application of alloy powder material in corrosion resistance and rust resistance of bolt |
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| CN105964206B (en) | 2018-04-27 |
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