CN106038587B - A kind of fumed equipment of alumen and calcining systeming method - Google Patents
A kind of fumed equipment of alumen and calcining systeming method Download PDFInfo
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- CN106038587B CN106038587B CN201610635709.8A CN201610635709A CN106038587B CN 106038587 B CN106038587 B CN 106038587B CN 201610635709 A CN201610635709 A CN 201610635709A CN 106038587 B CN106038587 B CN 106038587B
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- fumed
- process chamber
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K33/00—Medicinal preparations containing inorganic active ingredients
- A61K33/06—Aluminium, calcium or magnesium; Compounds thereof, e.g. clay
-
- F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
- F27—FURNACES; KILNS; OVENS; RETORTS
- F27B—FURNACES, KILNS, OVENS, OR RETORTS IN GENERAL; OPEN SINTERING OR LIKE APPARATUS
- F27B17/00—Furnaces of a kind not covered by any preceding group
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- Medicinal Chemistry (AREA)
- Pharmacology & Pharmacy (AREA)
- Epidemiology (AREA)
- Inorganic Chemistry (AREA)
- Animal Behavior & Ethology (AREA)
- General Health & Medical Sciences (AREA)
- Public Health (AREA)
- Veterinary Medicine (AREA)
- Chemical & Material Sciences (AREA)
- Mechanical Engineering (AREA)
- General Engineering & Computer Science (AREA)
- Compositions Of Oxide Ceramics (AREA)
Abstract
The invention discloses a kind of fumed equipment of alumen, belong to Chinese medicine preparation technical field, including shell, process chamber, heating unit, heat-insulation unit and temperature control unit, wherein, the process chamber, heating unit, heat-insulation unit and temperature control unit are respectively positioned in shell, the process chamber is located at the top in shell, the heating unit is located at chamber bottom, the heat-insulation unit is located at the periphery of process chamber and heating unit, the temperature control unit includes temperature sensor, display screen and control button, the temperature sensor is electrically connected with display screen and control button, the invention also discloses carry out the fumed method of alumen using above equipment, using device and method of the invention, fumed efficiency can be made to improve 2 times or more, cost of labor reduces by 68% or more, and product colour is uniform, quality is stablized, it is environmentally protective.
Description
Technical field
The present invention relates to Chinese medicine preparation technical field more particularly to a kind of fumed equipment of alumen and calcining systeming methods.
Background technique
Alumen is to lose the crystallization water after alum is fumed to form, be opaque, white, cellular solids block or fine powder,
Light, loose, hand twirl is frangible, lightly seasoned, there is granular sensation.Alumen stops blooding for eliminating dampness and astringing sores, myogenic, is treatment eczema, wet sore, sore
The common medicine of the illnesss such as ulcer burst for a long time and does not holds back, bleeding.
Traditional alumen calcining systeming method is put into alum in iron pan or other vessel, is calcined and is made with charcoal fire.The method
Phenomena such as often resulting in " dirty bottom ", " half-cooked ", " knot top ", fumed low efficiency；During being calcined with charcoal fire, generate a large amount of
Dense smoke seriously pollutes environment, influences personnel health；This mode keeps pot body persistently overheating because temperature is uncontrollable, leads to pot
Beneath to hang down or perforate, the new pot of a bite is fumed once to that can not reuse twice, causes fumed at high cost；The bottom of a pan iron filings fall off adhesion
Alumen leads to alumen flavescence blackening and influences quality.
For the above-mentioned deficiency of conventional method, also there are many improved methods, such as using the vessel of unlike material, use
Oven is baked method, using electric drying oven with forced convection concocted method, low temperature Constant pressure drying method etc., but efficiently and stably to produce high-quality
The alumen of amount is still relatively difficult, and existing device and method are more difficult to get extensive use.
Summary of the invention
An object of the present invention is to provide a kind of fumed equipment of alumen, to solve the above problems.
To achieve the goals above, the technical solution adopted by the present invention is that it is such: a kind of fumed equipment of alumen, including it is outer
Shell, process chamber, heating unit, heat-insulation unit and temperature control unit, wherein the process chamber, heating unit, heat-insulation unit and
Temperature control unit is respectively positioned in shell, and the process chamber is located at the top in shell, and the heating unit is located at process chamber bottom
Portion, the heat-insulation unit are located at the periphery of process chamber and heating unit, and the temperature control unit includes temperature sensor, display
Screen and control button, the temperature sensor are electrically connected with display screen and control button.
The fumed equipment of the present invention using the above structure, can solve problems existing in the prior art.
As a preferred technical scheme: the process chamber is the cylindrical shape of bottom flat.
Present inventor has found that the shape of process chamber has important shadow for the fumed effect of alum by many experiments
It rings, comprehensively considers for the material variation of alum and fumed amount and fumed time, it is preferred to use having for bottom flat is certain straight
The cylindrical body of diameter and certain altitude is as process chamber, because of the unreasonable matter that can all influence finished product of fumed amount and fumed time
Amount, and the structure of process chamber and shape have been largely fixed the fumed amount of adjustment and fumed time.
As a preferred technical scheme: the heating unit is resistance wire and E type thermocouple.Use electrically heated side
Formula will not generate a large amount of smog, and be provided with heat-insulation unit, and energy consumption is small, meet the requirement of modernization green production.
As a preferred technical scheme: the heat-insulation unit includes light fire brick, high alumina puts a brick and alumina silicate is kept the temperature
Blanket, wherein light fire brick is paved with the periphery and bottom of process chamber and heating unit, high alumina put a brick be located at chamber bottom with
Between light fire brick, alumina silicate insulation blanket is wrapped on the outside of process chamber and the light fire brick of heating unit periphery.Above-mentioned material
Material and structure, ensure that good refractoriness, high-temperature anti-corrosion ability and thermal insulation property.
The heat-insulation unit can preferably reach the determined temperature of alum physical change during fumed, and control and maintain
In determined temperature, avoids exceeding determined temperature and alumen is caused to be denaturalized.
As a preferred technical scheme: the temperature sensor is two, is located at inner treatment chamber and process chamber bottom
Portion, and respectively connection temperature display and setting button, ensure that the stability to temperature of charge control.
As further preferred technical solution: further including bakelite base, the bakelite base is fixed on the chamber bottom
Light fire brick in；It further include that support is kept a foothold, the support is kept a foothold to be connect with the bottom of the heat-insulation unit, the bakelite base
For the wiring insulating base of heating unit, heat-insulation unit and temperature control unit electrical connection, number is preferably 6.
The fumed method of alumen, the skill of use are carried out using above equipment the second object of the present invention is to provide a kind of
Art scheme are as follows: the following steps are included:
(1) alum raw material is weighed, fumed equipment is opened and inside and the bottom temp of process chamber are set；
(2) by the alum investment process chamber after weighing, when temperature is raised to setting temperature, start fumed timing, it is fumed
Observe into after a certain period of time it is white, loose, in honeycomb, it is light, when hand twists frangible, close fumed equipment, collect finished product alumen
To obtain the final product.
Wherein, with the variation of heating temperature in process chamber physical change occurs for alum, reaches after target temperature and controls
System keeps certain time in target temperature, and alum will constantly be converted into alumen, is not necessarily to any stirring halfway.
As a preferred technical scheme: in step (1), inner treatment chamber temperature setting is 150~200 DEG C, process chamber bottom
Portion's temperature setting is 350~500 DEG C.
Compared with the prior art, the advantages of the present invention are as follows:
A. by Experimental comparison, traditional fumed method of iron pan, everyone fumed 4kg alum per hour, and the invention is used, everyone
Fumed 13kg alum per hour, substantially increases fumed efficiency, and fumed efficiency improves 2 times or more；
B. by Experimental comparison, traditional fumed method of iron pan, artificial unit price is 4.5 yuan/people/kg finished product, and uses this hair
Bright, artificial unit price is 1.4 yuan/people/kg finished product, cost of labor is greatly saved, cost of labor reduces 68% or more；
C. the fumed method of traditional iron pan, security risk is big, may cause fire, damages personnel health, and the invention drops significantly
Low occurrence index, avoids influence of the coal smoke to employee's health；
D. conventional method is lit a fire, and to take pot time long, and hygienic difficulty of clearing out a gathering place is done and time-consuming, and the invention time is short, forges
It makes high-efficient, clears out a gathering place relatively easy, thorough；
E. the fumed finished color out of conventional method is inhomogenous, impure more, and the fumed finished color out of the present invention is uniform,
Quality is stablized；
F. conventional method causes production environment poor, and supervision risk is big, and the invention improves the production environment in workshop, makes
It meets GMP requirement, reduces supervision risk；
G. the invention does not generate a large amount of smog, and fumed equipment is heated by electrothermal, and energy consumption is small, easy to operate, meets existing
The requirement of the environmentally protective production of generationization.
Detailed description of the invention
Fig. 1 is the structural schematic diagram of the fumed equipment of the embodiment of the present invention 1；
Fig. 2 is another view of the fumed equipment of the embodiment of the present invention 1.
In figure: 1, process chamber；2, light fire brick；3, alumina silicate insulation blanket；4, E type thermocouple；5,0Cr25Al5 electric heating
Silk；6, bakelite base；7, support is kept a foothold；8, angle bar；9, shell；10, high alumina puts a brick.
Specific embodiment
The present invention will be further described with reference to the accompanying drawings.
Embodiment 1:
A kind of fumed equipment of alumen, referring to Fig. 1 and Fig. 2, including shell 9, process chamber 1, heating unit, heat-insulation unit and temperature
Spend control unit；
The shell 9 and process chamber 1 of the present embodiment are all made of stainless steel material, and process chamber 1 is the cylindrical shape of bottom flat,
Its diameter phi 1200mm is highly 150mm；
Heating unit is an E type thermocouple 4 and three 0Cr25Al5 heating wire 5；
Heat-insulation unit includes that high alumina puts a brick 10, light fire brick 2 and alumina silicate insulation blanket 3, wherein light fire brick 2
Totally seven hundred five ten pieces, light fire brick 2 is layed in the periphery and bottom of process chamber 1, and light fire brick 2 is layed in E type heat simultaneously
The periphery of galvanic couple 4 and the bottom of 0Cr25Al5 heating wire 5, high alumina put totally six ten pieces of a brick 10, and high alumina puts a brick 10 and is located at processing
Between 1 bottom of room and light fire brick 2, totally 0.5 ㎡, alumina silicate insulation blanket 3 are wrapped in process chamber 1 and add alumina silicate insulation blanket 3
2 outside of light fire brick of hot cell periphery；
Temperature control unit includes temperature sensor, display screen and control button, the temperature sensor and display screen and
Control button electrical connection, the temperature sensor are two, are located at 1 inside of process chamber and 1 bottom of process chamber, and respectively connect
Jointing temp display screen and setting button；
Wherein, process chamber 1, heating unit, heat-insulation unit and temperature control unit are respectively positioned in shell 9, and process chamber 1 is located at
Top in shell 9；The surrounding of shell 9 is provided with A3 angle bar；
0Cr25Al5 heating wire 5 is located at 1 bottom of process chamber, and heat-insulation unit is located at the periphery of process chamber 1 and heating unit；
It further include bakelite base 6, bakelite base 6 totally six, bakelite base 6 is fixed in the light fire brick 2 of 1 bottom of process chamber,
Bakelite, 6 for heating unit, the wiring insulating base of heat-insulation unit and temperature control unit electrical connection；It further include that A3 support is kept a foothold
7, support is kept a foothold 7 to be connect with the bottom of heat-insulation unit.
Embodiment 2:
A kind of alumen calcining systeming method the steps include: to weigh 13kg raw material alum, for use；The fumed of embodiment 1 is opened to set
Standby, setting 1 internal temperature of process chamber is 200 DEG C, and setting 1 bottom temp of process chamber is 350 DEG C；13kg alum is put into process chamber
In 1, temperature display starts fumed timing after reaching target temperature；After fumed 1 hour, Cheng Baise, it is loose, be in honeycomb, matter
Gently, hand twists frangible, pass hull closure, collects finished product alumen, and weigh 6.5kg；Fumed efficiency improves 2 times or more, obtained finished product
Color is uniform, and quality is stablized.
Embodiment 3
A kind of alumen calcining systeming method the steps include: to weigh 13kg raw material alum, for use；The fumed of embodiment 1 is opened to set
Standby, setting 1 internal temperature of process chamber is 150 DEG C, and setting 1 bottom temp of process chamber is 500 DEG C；13kg alum is put into process chamber
In 1, temperature display starts fumed timing after reaching target temperature；After fumed 1.2 hours, Cheng Baise, it is loose, be in honeycomb,
Light, hand twists frangible, pass hull closure, collects finished product alumen, and weigh 6.5kg；Fumed efficiency improves 2 times or more, obtain at
Product color is uniform, and quality is stablized.
Embodiment 4
A kind of alumen calcining systeming method the steps include: to weigh 13kg raw material alum, for use；The fumed of embodiment 1 is opened to set
Standby, setting 1 internal temperature of process chamber is 180 DEG C, and setting 1 bottom temp of process chamber is 450 DEG C；13kg alum is put into process chamber
In 1, temperature display starts fumed timing after reaching target temperature；After fumed 1.1 hours, Cheng Baise, it is loose, be in honeycomb,
Light, hand twists frangible, pass hull closure, collects finished product alumen, and weigh 6.5kg；Fumed efficiency improves 2 times or more, obtain at
Product color is uniform, and quality is stablized.
The foregoing is merely illustrative of the preferred embodiments of the present invention, is not intended to limit the invention, all in essence of the invention
Made any modifications, equivalent replacements, and improvements etc., should all be included in the protection scope of the present invention within mind and principle.
Claims (7)
1. a kind of fumed equipment of alumen, it is characterised in that: controlled including shell, process chamber, heating unit, heat-insulation unit and temperature
Unit, wherein the process chamber, heating unit, heat-insulation unit and temperature control unit are respectively positioned in shell, the process chamber position
In the top in shell, the heating unit is located at chamber bottom, and the heat-insulation unit is located at process chamber and heating unit
Periphery, the temperature control unit include temperature sensor, display screen and control button, the temperature sensor and display screen and
Control button electrical connection;The heat-insulation unit includes that light fire brick, high alumina put a brick and alumina silicate insulation blanket, wherein lightweight
Refractory brick is paved with the periphery and bottom of process chamber and heating unit, high alumina put a brick be located at chamber bottom and light fire brick it
Between, alumina silicate insulation blanket is wrapped on the outside of process chamber and the light fire brick of heating unit periphery.
2. the fumed equipment of alumen according to claim 1, it is characterised in that: the process chamber is the cylindrical body of bottom flat
Shape.
3. the fumed equipment of alumen according to claim 1, it is characterised in that: the heating unit is resistance wire and E type heat
Galvanic couple.
4. the fumed equipment of alumen according to claim 1, it is characterised in that: the temperature sensor is two, respectively position
In inner treatment chamber and chamber bottom.
5. the fumed equipment of alumen according to claim 1, it is characterised in that: further include bakelite base, the bakelite base is fixed
In in the light fire brick of the chamber bottom；It further include that support is kept a foothold, it is described to support the bottom kept a foothold with the heat-insulation unit
Portion's connection.
6. a kind of equipment using claim 1-5 any one carries out the fumed method of alumen, which is characterized in that including following
Step:
(1) alum raw material is weighed, fumed equipment is opened and inside and the bottom temp of process chamber are set；
(2) by the alum investment process chamber after weighing, when temperature is raised to setting temperature, start fumed timing, it is fumed certain
After time observation at it is white, loose, be in honeycomb, it is light, when hand twists frangible, close fumed equipment, collection finished product alumen to obtain the final product.
7. calcining systeming method according to claim 6, it is characterised in that: in step (1), inner treatment chamber temperature setting is
150~200 DEG C, chamber bottom temperature setting is 350~500 DEG C.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201610635709.8A CN106038587B (en) | 2016-08-05 | 2016-08-05 | A kind of fumed equipment of alumen and calcining systeming method |
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| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201610635709.8A CN106038587B (en) | 2016-08-05 | 2016-08-05 | A kind of fumed equipment of alumen and calcining systeming method |
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| CN106038587A CN106038587A (en) | 2016-10-26 |
| CN106038587B true CN106038587B (en) | 2019-03-12 |
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| Application Number | Title | Priority Date | Filing Date |
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| CN201610635709.8A Active CN106038587B (en) | 2016-08-05 | 2016-08-05 | A kind of fumed equipment of alumen and calcining systeming method |
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Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN2292261Y (en) * | 1996-08-10 | 1998-09-23 | 刘赞清 | Temp.-controlled medicine calcining oven |
| CN201727740U (en) * | 2009-12-11 | 2011-02-02 | 杭州海善制药设备有限公司 | High-temperature control traditional Chinese medicament calcining furnace |
| CN202709727U (en) * | 2012-07-07 | 2013-01-30 | 刘永秋 | Small-sized alum openly-calcining furnace |
-
2016
- 2016-08-05 CN CN201610635709.8A patent/CN106038587B/en active Active
Patent Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN2292261Y (en) * | 1996-08-10 | 1998-09-23 | 刘赞清 | Temp.-controlled medicine calcining oven |
| CN201727740U (en) * | 2009-12-11 | 2011-02-02 | 杭州海善制药设备有限公司 | High-temperature control traditional Chinese medicament calcining furnace |
| CN202709727U (en) * | 2012-07-07 | 2013-01-30 | 刘永秋 | Small-sized alum openly-calcining furnace |
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| Publication number | Publication date |
|---|---|
| CN106038587A (en) | 2016-10-26 |
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