CN106038587A - Dried alum calcining device and method - Google Patents
Dried alum calcining device and method Download PDFInfo
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- CN106038587A CN106038587A CN201610635709.8A CN201610635709A CN106038587A CN 106038587 A CN106038587 A CN 106038587A CN 201610635709 A CN201610635709 A CN 201610635709A CN 106038587 A CN106038587 A CN 106038587A
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K33/00—Medicinal preparations containing inorganic active ingredients
- A61K33/06—Aluminium, calcium or magnesium; Compounds thereof, e.g. clay
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- F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
- F27—FURNACES; KILNS; OVENS; RETORTS
- F27B—FURNACES, KILNS, OVENS, OR RETORTS IN GENERAL; OPEN SINTERING OR LIKE APPARATUS
- F27B17/00—Furnaces of a kind not covered by any preceding group
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- Inorganic Chemistry (AREA)
- Animal Behavior & Ethology (AREA)
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Abstract
The invention discloses a dried alum calcining device and method and belongs to the technical field of traditional Chinese medicine processing. The dried alum calcining device comprises a housing, a treatment chamber, a heating unit, a thermal insulation unit and a temperature control unit. The treatment chamber, the heating unit, the thermal insulation unit and the temperature control unit are arranged outside the housing. The treatment chamber is located at the upper part in the housing. The heating unit is located at the bottom of the treatment chamber. The thermal insulation unit is located at the peripheries of the treatment chamber and the heating unit. The temperature control unit comprises a temperature senor, a display screen and control buttons. The temperature sensor is electrically connected to the display screen and the control buttons. The invention also discloses a dried alum calcining method. Through the device and method, calcining efficiency is improved by 2 times or more, an artificial cost is reduced by 68% or more, product colors are uniform, product quality is stable and the device and method are environmentally friendly.
Description
Technical field
The present invention relates to Chinese medicine processing technical field, particularly relate to a kind of dried Alumen calcine equipment and calcining systeming method.
Background technology
Dried Alumen, is to lose water of crystallization after Alumen calcine to form, for opaque, white, cellular solids block or fine powder,
Light weight, loose, hands is twisted with the fingers frangible, lightly seasoned, has granular sensation.Dried Alumen is used for eliminating dampness and astringing sores, promoting regeneration of the tissue and arresting bleeding, is treatment eczema, eczema, skin ulcer
Infections burst for a long time do not hold back, the common medicine of the disease such as hemorrhage.
Traditional dried Alumen calcining systeming method is that Alumen is put into iron pan or other vessel, prepares with charcoal fire calcining.The method
Often resulting in the phenomenons such as " the dirty end ", " half-cooked ", " knot top ", calcine efficiency is low；During calcining with charcoal fire, produce a large amount of
Dense smoke, serious environment pollution, affect personnel health；This mode makes pot persistently overheating because temperature is uncontrollable, causes pot
Under hang down or perforation, a bite new pot calcine once re-using to twice, cause calcine cost height；The bottom of a pan iron filings come off adhesion
Dried Alumen, causes dried Alumen flavescence blackening to affect quality.
For the above-mentioned deficiency of traditional method, also occur in that many improved methods, as used the vessel of unlike material, employing
Baking box baking method, employing electric drying oven with forced convection concocted method, low temperature Constant pressure drying method etc., but to produce high-quality efficiently and stably
The dried Alumen of amount is the most relatively difficult, and existing equipment and method are more difficult to get extensively application.
Summary of the invention
An object of the present invention, is to provide a kind of dried Alumen calcine equipment, to solve the problems referred to above.
To achieve these goals, the technical solution used in the present invention is such that a kind of dried Alumen calcine equipment, including shell,
Process chamber, heating unit, heat-insulation unit and temperature control unit, wherein, described process chamber, heating unit, heat-insulation unit and temperature
Degree control unit is respectively positioned in shell, and described process chamber is positioned at the top of shell, and described heating unit is positioned at chamber bottom,
Described heat-insulation unit is positioned at the periphery of process chamber and heating unit, and described temperature control unit includes temperature sensor, display screen
And control knob, described temperature sensor electrically connects with display screen and control knob.
The present invention uses the calcine equipment of said structure, can solve problems present in prior art.
As preferred technical scheme: described process chamber is the cylindrical shape of bottom flat.
Present inventor is found by great many of experiments, and the shape of process chamber has important shadow for the calcine effect of Alumen
Ringing, the material for Alumen changes and calcine amount and calcine time consider, it is preferred to use having of bottom flat is certain straight
The cylinder of footpath and certain altitude is as process chamber, because calcine amount and the unreasonable matter that all can affect finished product of calcine time
Amount, and the structure of process chamber and shape have been largely fixed adjustment calcine amount and calcine time.
As preferred technical scheme: described heating unit is resistance wire and E type thermocouple.I.e. use electrically heated side
Formula, will not produce a large amount of smog, and be provided with heat-insulation unit, and energy consumption is little, meets the requirement that modernization green produces.
As preferred technical scheme: described heat-insulation unit includes that light fire brick, high alumina put a brick and aluminium silicate insulation
Blanket, wherein, light fire brick is paved with process chamber and the periphery of heating unit and bottom, high alumina put a brick be positioned at chamber bottom with
Between light fire brick, aluminium silicate insulation blanket is wrapped in outside the light fire brick of process chamber and heating unit periphery.Above-mentioned material
Material and structure, it is ensured that good refractoriness, high-temperature anti-corrosion ability and heat-insulating property.
This heat-insulation unit preferably can reach the determined temperature of Alumen physical change during calcine, and controls to maintain
At determined temperature, it is to avoid exceed determined temperature and cause dried Alumen degeneration.
As preferred technical scheme: described temperature sensor is two, lay respectively at the bottom of inner treatment chamber and process chamber
Portion, and each connect temperature display and settings button, it is ensured that the stability that temperature of charge is controlled.
Technical scheme as further preferred: also include that bakelite base, described bakelite base are fixed on described chamber bottom
Light fire brick in；Also including that support is kept a foothold, the bottom that described support is kept a foothold with described heat-insulation unit is connected, described bakelite base
For the wiring insulating base of heating unit, heat-insulation unit and temperature control unit electrical connection, its number is preferably 6.
The two of the purpose of the present invention, are to provide a kind of method utilizing the said equipment to carry out dried Alumen calcine, the skill of employing
Art scheme is: comprise the following steps:
(1) weigh Alumen raw material, open calcine equipment and inside and the bottom temp of process chamber are set；
(2) Alumen after weighing puts in process chamber, when temperature is raised to arrange temperature, starts calcine timing, and calcine is certain
Observe into after time white, loose, in cellular, light weight, when hands is twisted with the fingers frangible, close calcine equipment, collect finished product dried Alumen and get final product.
Wherein, along with the change of heating temperature, there is physical change in Alumen in process chamber, after reaching target temperature and control
Making and keep certain time at target temperature, Alumen will constantly be converted into dried Alumen, and midway is without any stirring.
As preferred technical scheme: in step (1), inner treatment chamber temperature is set to 150～200 DEG C, at the bottom of process chamber
Portion's temperature is set to 350～500 DEG C.
Compared with prior art, it is an advantage of the current invention that:
A. by Experimental comparison, tradition iron pan calcine method, everyone calcine 4kg Alumen per hour, and use this to invent, everyone is the least
Time calcine 13kg Alumen, substantially increase calcine efficiency, calcine efficiency improves more than 2 times；
B. by Experimental comparison, tradition iron pan calcine method, artificial unit price is 4.5 yuan/people/kg finished product, and uses this to invent, people
Work order valency is 1.4 yuan/people/kg finished product, is greatly saved cost of labor, and cost of labor reduces more than 68%；
C. tradition iron pan calcine method, potential safety hazard is big, can fire hazard, damage personnel health, and this invention greatly reduce
Occurrence index, it is to avoid the impact that coal smoke is on employee healthy；
D. traditional method is lit a fire, and to take pot time long, and health of clearing out a gathering place difficulty is done and time-consumingly, and this invention time is short, and calcine is imitated
Rate is high, clears out a gathering place relatively easy, thorough；
E. the finished color heterogeneity that traditional method calcine goes out, impure many, the finished color that calcine of the present invention goes out is homogeneous, quality
Stable；
F. traditional method causes production environment poor, and supervision risk is big, and this invention improves the production environment in workshop so that it is symbol
Close GMP requirement, reduce supervision risk；
G. this invention does not produce a large amount of smog, and calcine equipment is heated by electric heating, and energy consumption is little, easy to operate, meets modernization
The requirement that environmental protection produces.
Accompanying drawing explanation
Fig. 1 is the structural representation of the calcine equipment of the embodiment of the present invention 1；
Fig. 2 is another view of the calcine equipment of the embodiment of the present invention 1.
In figure: 1, process chamber；2, light fire brick；3, aluminium silicate insulation blanket；4, E type thermocouple；5,0Cr25Al5 electric heating
Silk；6, bakelite base；7, support is kept a foothold；8, angle bar；9, shell；10, high alumina puts a brick.
Detailed description of the invention
Below in conjunction with accompanying drawing, the invention will be further described.
Embodiment 1:
A kind of dried Alumen calcine equipment, sees Fig. 1 and Fig. 2, including shell 9, process chamber 1, heating unit, heat-insulation unit and temperature control
Unit processed；
The shell 9 of the present embodiment and process chamber 1 all use stainless steel, process chamber 1 to be the cylindrical shape of bottom flat, and it is straight
Footpath φ 1200mm, height is 150mm；
Heating unit is an E type thermocouple 4 and three 0Cr25Al5 heating wire 5；
Heat-insulation unit includes that high alumina puts a brick 10, light fire brick 2 and aluminium silicate insulation blanket 3, wherein, and light fire brick 2 totally seven
150 pieces, light fire brick 2 is layed in periphery and the bottom of process chamber 1, and light fire brick 2 is layed in E type thermocouple 4 simultaneously
Periphery and the bottom of 0Cr25Al5 heating wire 5, high alumina puts a brick 10 totally six ten pieces, and high alumina is put a brick 10 and is positioned at process chamber 1 end
Between portion and light fire brick 2, aluminium silicate insulation blanket 3 totally 0.5, aluminium silicate insulation blanket 3 is wrapped in process chamber 1 and heating unit
Outside the light fire brick 2 of periphery；
Temperature control unit includes temperature sensor, display screen and control knob, described temperature sensor and display screen and control
Button electrically connects, and described temperature sensor is two, lays respectively at bottom process chamber 1 inside and process chamber 1, and each connects temperature
Degree display screen and settings button；
Wherein, process chamber 1, heating unit, heat-insulation unit and temperature control unit are respectively positioned in shell 9, and process chamber 1 is positioned at shell
Top in 9；The surrounding of shell 9 is provided with A3 angle bar；
0Cr25Al5 heating wire 5 is positioned at bottom process chamber 1, and heat-insulation unit is positioned at the periphery of process chamber 1 and heating unit；
Also include bakelite base 6, bakelite base 6 totally six, bakelite base 6 is fixed in the light fire brick 2 bottom process chamber 1, bakelite,
6 for heating unit, heat-insulation unit and the wiring insulating base of temperature control unit electrical connection；Also include that A3 supports and keep a foothold 7, support
Keep a foothold and 7 be connected with the bottom of heat-insulation unit.
Embodiment 2:
A kind of dried Alumen calcining systeming method, the steps include: to weigh 13kg raw material Alumen, stand-by；Open the calcine equipment of embodiment 1, if
Putting process chamber 1 internal temperature is 200 DEG C, and arranging process chamber 1 bottom temp is 350 DEG C；13kg Alumen is put in process chamber 1,
Temperature display starts calcine timing after reaching target temperature；After calcine 1 hour, become white, loose, in cellular, light weight, hands
Twisting with the fingers frangible, close hull closure, collect finished product dried Alumen, weigh 6.5kg；Calcine efficiency improves more than 2 times, and the finished color obtained is equal
One, steady quality.
Embodiment 3
A kind of dried Alumen calcining systeming method, the steps include: to weigh 13kg raw material Alumen, stand-by；Open the calcine equipment of embodiment 1, if
Putting process chamber 1 internal temperature is 150 DEG C, and arranging process chamber 1 bottom temp is 500 DEG C；13kg Alumen is put in process chamber 1,
Temperature display starts calcine timing after reaching target temperature；After calcine 1.2 hours, become white, loose, in cellular, light weight,
Hands is twisted with the fingers frangible, closes hull closure, collects finished product dried Alumen, and weigh 6.5kg；Calcine efficiency improves more than 2 times, the finished color obtained
Homogeneous, steady quality.
Embodiment 4
A kind of dried Alumen calcining systeming method, the steps include: to weigh 13kg raw material Alumen, stand-by；Open the calcine equipment of embodiment 1, if
Putting process chamber 1 internal temperature is 180 DEG C, and arranging process chamber 1 bottom temp is 450 DEG C；13kg Alumen is put in process chamber 1,
Temperature display starts calcine timing after reaching target temperature；After calcine 1.1 hours, become white, loose, in cellular, light weight,
Hands is twisted with the fingers frangible, closes hull closure, collects finished product dried Alumen, and weigh 6.5kg；Calcine efficiency improves more than 2 times, the finished color obtained
Homogeneous, steady quality.
The foregoing is only presently preferred embodiments of the present invention, not in order to limit the present invention, all essences in the present invention
Any amendment, equivalent and the improvement etc. made within god and principle, should be included within the scope of the present invention.
Claims (8)
1. a dried Alumen calcine equipment, it is characterised in that: include that shell, process chamber, heating unit, heat-insulation unit and temperature control
Unit, wherein, described process chamber, heating unit, heat-insulation unit and temperature control unit are respectively positioned in shell, described process chamber position
Top in shell, described heating unit is positioned at chamber bottom, and described heat-insulation unit is positioned at process chamber and heating unit
Periphery, described temperature control unit includes temperature sensor, display screen and control knob, described temperature sensor and display screen and
Control knob electrically connects.
Dried Alumen calcine equipment the most according to claim 1, it is characterised in that: described process chamber is the cylinder of bottom flat
Shape.
Dried Alumen calcine equipment the most according to claim 1, it is characterised in that: described heating unit is resistance wire and E type heat
Galvanic couple.
Dried Alumen calcine equipment the most according to claim 1, it is characterised in that: described heat-insulation unit include light fire brick,
High alumina puts a brick and aluminium silicate insulation blanket, and wherein, light fire brick is paved with process chamber and the periphery of heating unit and bottom, high alumina
Putting a brick between chamber bottom and light fire brick, aluminium silicate insulation blanket is wrapped in process chamber and heating unit periphery
Outside light fire brick.
Dried Alumen calcine equipment the most according to claim 1, it is characterised in that: described temperature sensor is two, respectively position
In inner treatment chamber and chamber bottom.
Dried Alumen calcine equipment the most according to claim 4, it is characterised in that: also include that bakelite base, described bakelite base are fixed
In the light fire brick of described chamber bottom；Also including that support is kept a foothold, described support is kept a foothold at the end with described heat-insulation unit
Portion connects.
7. the method that the equipment utilizing claim 1-6 any one carries out dried Alumen calcine, it is characterised in that include following
Step:
(1) weigh Alumen raw material, open calcine equipment and inside and the bottom temp of process chamber are set；
(2) Alumen after weighing puts in process chamber, when temperature is raised to arrange temperature, starts calcine timing, and calcine is certain
Observe into after time white, loose, in cellular, light weight, when hands is twisted with the fingers frangible, close calcine equipment, collect finished product dried Alumen and get final product.
Calcining systeming method the most according to claim 7, it is characterised in that: in step (1), inner treatment chamber temperature is set to
150～200 DEG C, chamber bottom temperature is set to 350～500 DEG C.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201610635709.8A CN106038587B (en) | 2016-08-05 | 2016-08-05 | A kind of fumed equipment of alumen and calcining systeming method |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201610635709.8A CN106038587B (en) | 2016-08-05 | 2016-08-05 | A kind of fumed equipment of alumen and calcining systeming method |
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| Publication Number | Publication Date |
|---|---|
| CN106038587A true CN106038587A (en) | 2016-10-26 |
| CN106038587B CN106038587B (en) | 2019-03-12 |
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| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201610635709.8A Active CN106038587B (en) | 2016-08-05 | 2016-08-05 | A kind of fumed equipment of alumen and calcining systeming method |
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Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN2292261Y (en) * | 1996-08-10 | 1998-09-23 | 刘赞清 | Temp.-controlled medicine calcining oven |
| CN201727740U (en) * | 2009-12-11 | 2011-02-02 | 杭州海善制药设备有限公司 | High-temperature control traditional Chinese medicament calcining furnace |
| CN202709727U (en) * | 2012-07-07 | 2013-01-30 | 刘永秋 | Small-sized alum openly-calcining furnace |
-
2016
- 2016-08-05 CN CN201610635709.8A patent/CN106038587B/en active Active
Patent Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN2292261Y (en) * | 1996-08-10 | 1998-09-23 | 刘赞清 | Temp.-controlled medicine calcining oven |
| CN201727740U (en) * | 2009-12-11 | 2011-02-02 | 杭州海善制药设备有限公司 | High-temperature control traditional Chinese medicament calcining furnace |
| CN202709727U (en) * | 2012-07-07 | 2013-01-30 | 刘永秋 | Small-sized alum openly-calcining furnace |
Non-Patent Citations (1)
| Title |
|---|
| 高天爱等: "《矿物药真伪图鉴及应用》", 28 February 2014 * |
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| CN106038587B (en) | 2019-03-12 |
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