CN106009963A - Water-based paint containing graphite and preparation method thereof - Google Patents
Water-based paint containing graphite and preparation method thereof Download PDFInfo
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- CN106009963A CN106009963A CN201610625205.8A CN201610625205A CN106009963A CN 106009963 A CN106009963 A CN 106009963A CN 201610625205 A CN201610625205 A CN 201610625205A CN 106009963 A CN106009963 A CN 106009963A
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D125/00—Coating compositions based on homopolymers or copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and at least one being terminated by an aromatic carbocyclic ring; Coating compositions based on derivatives of such polymers
- C09D125/02—Homopolymers or copolymers of hydrocarbons
- C09D125/04—Homopolymers or copolymers of styrene
- C09D125/08—Copolymers of styrene
- C09D125/14—Copolymers of styrene with unsaturated esters
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D183/00—Coating compositions based on macromolecular compounds obtained by reactions forming in the main chain of the macromolecule a linkage containing silicon, with or without sulfur, nitrogen, oxygen, or carbon only; Coating compositions based on derivatives of such polymers
- C09D183/04—Polysiloxanes
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D5/00—Coating compositions, e.g. paints, varnishes or lacquers, characterised by their physical nature or the effects produced; Filling pastes
- C09D5/08—Anti-corrosive paints
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D5/00—Coating compositions, e.g. paints, varnishes or lacquers, characterised by their physical nature or the effects produced; Filling pastes
- C09D5/18—Fireproof paints including high temperature resistant paints
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D7/00—Features of coating compositions, not provided for in group C09D5/00; Processes for incorporating ingredients in coating compositions
- C09D7/40—Additives
- C09D7/60—Additives non-macromolecular
- C09D7/61—Additives non-macromolecular inorganic
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D7/00—Features of coating compositions, not provided for in group C09D5/00; Processes for incorporating ingredients in coating compositions
- C09D7/40—Additives
- C09D7/60—Additives non-macromolecular
- C09D7/63—Additives non-macromolecular organic
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D7/00—Features of coating compositions, not provided for in group C09D5/00; Processes for incorporating ingredients in coating compositions
- C09D7/40—Additives
- C09D7/65—Additives macromolecular
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
- C08L2201/00—Properties
- C08L2201/08—Stabilised against heat, light or radiation or oxydation
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
- C08L2205/00—Polymer mixtures characterised by other features
- C08L2205/03—Polymer mixtures characterised by other features containing three or more polymers in a blend
- C08L2205/035—Polymer mixtures characterised by other features containing three or more polymers in a blend containing four or more polymers in a blend
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- Chemical & Material Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Engineering & Computer Science (AREA)
- Materials Engineering (AREA)
- Wood Science & Technology (AREA)
- Organic Chemistry (AREA)
- Inorganic Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Paints Or Removers (AREA)
Abstract
The invention discloses a water-based paint containing graphite. The water-based paint is prepared from the following raw materials: graphite powder, a styrene-acrylic emulsion, organic silicon resin, polyurethane resin, fluorocarbon resin, isobutyl alcohol, n-propyl acetate, a synergist, a defoaming agent, a curing agent, glass powder, superfine silica, deionized water, and an epoxy glue. The preparation method comprises the steps of: (1) preparing a mixed solution; (2) preparing a suspension; (3) preparing a solution; and (4) mixing the liquid of the above-mentioned steps evenly, and conducting filtration to obtain a finished product. According to the invention, organic high polymer materials with good comprehensive properties are employed for optimized combination to improve the high temperature resistance and high pressure performance of the composition. The preparation method involved in the invention is simple, realizes full use of resources and energy, the production process is environment-friendly and has pollution, the cost is low, and the production cycle is short, therefore, the water-based paint containing graphite is suitable for industrial batch production, and has good economic and social benefits.
Description
Technical field
The invention belongs to coating industry technical field, relate to a kind of water paint, particularly relate to a kind of graphitiferous water paint and
Its preparation method.
Background technology
Coating, at the entitled paint of Chinese tradition, refer to coat body surface can form thin film under certain conditions and rise protection,
One class I liquid I of decoration or other specific functions (insulation, antirust, mildew-resistant, heat-resisting etc.) or solid material.Because of coating in early days
Mostly with vegetable oil as primary raw material, therefore also referred to as paint.Now synthetic resin instead of vegetable oil, therefore referred to as coating.It is coated with
Material belongs to organic chemical industry's macromolecular material, and the film formed belongs to macromolecular compound type.The chemical industry current according to the modern times produces
The classification of product, coating belongs to fine chemical product.Modern coating the most progressively becomes a polyfunctional engineering material of class, is
An important industry in chemical industry.
At present, the coating industry of China is the most ripe, and market is close to saturated, in addition under the overall situation of green economy globalization,
People become more concerned with economy the most flourishing after, environment is by great destruction.Along with new " environmental law " promulgates, country is " green
Environmental protection, beautiful China " etc. environmental protection advocate the most no longer to stay on slogan, but implement to perform, implement to promote energetically green
The development of color science and technology industry.Traditional coating is one of important sources of air major pollutants VOC, by the aqueous of environmental protection
Paint replacement paint is the most imperative.Compare traditional paint, and water paint is the one of environment-friendly type paint, and it saves oil
Coal resources, and free from environmental pollution, it is to guide consumption to realize energy-saving and emission-reduction.2015, China's Coating Market sales volume 1500
About ten thousand tons, the industrial paint accounting by 70% converts, and paint consumption then reaches ten million ton, not only wastes 5,000,000 tons of energy,
It is crucial that cause 5,000,000 tons of toxic and harmful discharges to air.Paint consumes the energy and pollutes environment, and it is in the common people consume
Propagate its belief on a large scale, run in the opposite direction with national energy consumption revolution requirement and guide.Along with the enhancing of people's environmental consciousness, water paint
Will be widely used, research and development water paint has the biggest economic benefit and social benefit.Existing water paint
The application in industries such as pharmacy, food, hospital, weaving, chemical industry, electronics can be applied.Water paint is from raw material sources to life
The Life cycle produced and use, the most beneficially sound development of environment.It is the most in process of production by volatile organic molten
Agent substitutes, and when using, coating tool can wash by water, and decreases the consumption of cleaning solvent.The production of organic solvent needs
Consume fossil feedstock, be a major challenge to resource in the present stage of resource scarcity, the appearance of water paint, solve this and ask
Topic.Meanwhile, the reduction of solvent, greatly reduce the discharge of VOC during producing and using, for improving week
Limit atmospheric environment has made positive contribution.
Country curbs environmental pollution severely, and national environmental consciousness promotes, consuming behavior changes, the sealing wax coating industry of energy-conserving and environment-protective
Just welcoming unprecedented opportunity to develop, market presents " blowout formula " Requirement.Efforts To Develop basic research, reduces water
The difficulty of construction of property coating, improve serviceability, be water paint expansive approach field, the task of top priority of extensive popularization and application.
Meanwhile, strengthen policy guides, promotional technique, transformation concept, the elimination public phases such as the prejudice of water paint and misgivings
Close the attention of work, also the application development of water paint will be played the effect of promotion.As Green Product, water paint
Necessarily obtain the accreditation of people and be widely used.The market demand huge in the face of water paint and ever-increasing application prospect, add
Big R&D intensity, updates and promotes the properties of product of water paint, accelerates product quality upgrading, develop technically,
The water paint more showing powerful competitive advantage on cost, in performance has the meaning of reality and the wide market space.
Summary of the invention
The invention aims to overcome the deficiencies in the prior art, it is provided that the water paint of a kind of graphitiferous and preparation thereof
Method, this coating products excellent performance, there are good high temperature resistant, high-voltage performance, and energy-conserving and environment-protective, possess preferable economy
Benefit and social benefit.
For solve above-mentioned technical problem, the present invention by the following technical solutions:
The water paint of a kind of graphitiferous, is prepared by the raw materials in: graphite powder 15～35 parts, styrene-acrylic emulsion 5～20
Part, organic siliconresin 5～20 parts, polyurethane resin 3～15 parts, fluorocarbon resin 3～15 parts, isobutanol 0.3～1.5 parts,
N-propyl acetate 0.5～2 parts, synergist 0.3～1.5 parts, defoamer 0.3～1.2 parts, firming agent 0.2～1 part, glass dust 1～
5 parts, superfine silicon dioxide 2～8 parts, deionized water 20～45 parts, epoxy glue 3～15 parts；
Its preparation method in turn includes the following steps:
(1) graphite powder, styrene-acrylic emulsion, organic siliconresin, polyurethane resin, fluorocarbon resin and isobutanol are put into reaction vessel
In, it is slowly heated to 40～50 DEG C, is stirred continuously and is uniformly completely dissolved to material, obtain mixed liquor standby；
(2) glass dust, superfine silicon dioxide, n-propyl acetate being joined in blender with epoxy glue, being stirred continuously until mixing
Close uniformly, obtain suspension standby；
(3) synergist, defoamer, firming agent are dissolved in deionized water and obtain solution；
(4), after the suspension that mixed liquor step (1) prepared and step (2) prepare is mixed and stirred for uniformly, step is added
(3) solution prepared, continues to stir, and crosses 100～200 mesh sieves, gets product.
Preferably, described synergist is that butyl triphenyl is fluorinated phosphine.
Preferably, described defoamer is polyester modification siloxanes.
Preferably, described firming agent is isocyanates.
The beneficial effects of the present invention is:
The present invention, by using combination property preferably high-molecular organic material and carrying out optimum organization, improves the resistance to height of compositions
Temperature, high-voltage performance, the coating surface using the present invention to obtain is smooth, fine and smooth, smooth, and gloss retention is good, hot strength and fracture
Percentage elongation is superior to common coating, can meet coated-body and use requirement for anticorrosion, weather-proof etc.；Preparation method of the present invention is simple,
Achieving making full use of of resource and the energy, production process is environment friendly and pollution-free, and cost is relatively low, with short production cycle, is suitable to industrialization
Batch production, possesses preferable economic benefit and social benefit.
Detailed description of the invention
Below in conjunction with embodiment, the invention will be further described.
Embodiment 1:
The water paint of a kind of graphitiferous, is prepared by the raw materials in: graphite powder 15 parts, styrene-acrylic emulsion 5 parts, organic
Silicones 5 parts, polyurethane resin 3 parts, fluorocarbon resin 3 parts, isobutanol 0.3 part, n-propyl acetate 0.5 part, synergist
0.3 part, defoamer 0.3 part, 0.2 part of firming agent, 1 part of glass dust, superfine silicon dioxide 2 parts, deionized water 20 parts, ring
3 parts of oxygen glue；
Its preparation method in turn includes the following steps:
(1) graphite powder, styrene-acrylic emulsion, organic siliconresin, polyurethane resin, fluorocarbon resin and isobutanol are put into reaction vessel
In, it is slowly heated to 40～50 DEG C, is stirred continuously and is uniformly completely dissolved to material, obtain mixed liquor standby；
(2) glass dust, superfine silicon dioxide, n-propyl acetate being joined in blender with epoxy glue, being stirred continuously until mixing
Close uniformly, obtain suspension standby；
(3) synergist, defoamer, firming agent are dissolved in deionized water and obtain solution；
(4), after the suspension that mixed liquor step (1) prepared and step (2) prepare is mixed and stirred for uniformly, step is added
(3) solution prepared, continues to stir, and crosses 100 mesh sieves, gets product.
Embodiment 2:
The water paint of a kind of graphitiferous, is prepared by the raw materials in: graphite powder 35 parts, styrene-acrylic emulsion 20 parts, have
Machine silicones 20 parts, polyurethane resin 15 parts, fluorocarbon resin 15 parts, isobutanol 1.5 parts, n-propyl acetate 2 parts, potentiation
Agent 1.5 parts, defoamer 1.2 parts, 1 part of firming agent, 5 parts of glass dust, superfine silicon dioxide 8 parts, deionized water 45 parts,
Epoxy glue 15 parts；
Its preparation method in turn includes the following steps:
(1) graphite powder, styrene-acrylic emulsion, organic siliconresin, polyurethane resin, fluorocarbon resin and isobutanol are put into reaction vessel
In, it is slowly heated to 40～50 DEG C, is stirred continuously and is uniformly completely dissolved to material, obtain mixed liquor standby；
(2) glass dust, superfine silicon dioxide, n-propyl acetate being joined in blender with epoxy glue, being stirred continuously until mixing
Close uniformly, obtain suspension standby；
(3) synergist, defoamer, firming agent are dissolved in deionized water and obtain solution；
(4), after the suspension that mixed liquor step (1) prepared and step (2) prepare is mixed and stirred for uniformly, step is added
(3) solution prepared, continues to stir, and crosses 150 mesh sieves, gets product.
In the above embodiment of the present invention:
Described synergist is that butyl triphenyl is fluorinated phosphine；
Described defoamer is polyester modification siloxanes；
Described firming agent is isocyanates.
During the present invention implements, by using combination property preferably high-molecular organic material and carrying out optimum organization, improve combination
High temperature resistant, the high-voltage performance of thing, the coating surface using the present invention to obtain is smooth, fine and smooth, smooth, and gloss retention is good, and stretching is strong
Degree and elongation at break are superior to common coating, can meet coated-body and use requirement for anticorrosion, weather-proof etc.；The present invention side of preparation
Method is simple, and production process is environment friendly and pollution-free, and cost is relatively low, with short production cycle, is suitable to industrialized mass production.
Finally it should be noted that above example only in order to illustrative not limiting technical scheme, although with reference to above-mentioned reality
Execute example the present invention has been described in detail, it will be appreciated by those skilled in the art that still the present invention can be modified or
Equivalent, any modification or partial replacement without departing from the spirit and scope of the present invention, it all should contain the power in the present invention
In profit claimed range.
Claims (4)
1. the water paint of a graphitiferous, it is characterised in that be prepared by the raw materials in: graphite powder 15～35 parts,
Styrene-acrylic emulsion 5～20 parts, organic siliconresin 5～20 parts, polyurethane resin 3～15 parts, fluorocarbon resin 3～15 parts, isobutyl
Alcohol 0.3～1.5 parts, n-propyl acetate 0.5～2 parts, synergist 0.3～1.5 parts, defoamer 0.3～1.2 parts, firming agent 0.2～
1 part, glass dust 1～5 parts, superfine silicon dioxide 2～8 parts, deionized water 20～45 parts, epoxy glue 3～15 parts；
Its preparation method in turn includes the following steps:
(1) graphite powder, styrene-acrylic emulsion, organic siliconresin, polyurethane resin, fluorocarbon resin and isobutanol are put into reaction vessel
In, it is slowly heated to 40～50 DEG C, is stirred continuously and is uniformly completely dissolved to material, obtain mixed liquor standby；
(2) glass dust, superfine silicon dioxide, n-propyl acetate being joined in blender with epoxy glue, being stirred continuously until mixing
Close uniformly, obtain suspension standby；
(3) synergist, defoamer, firming agent are dissolved in deionized water and obtain solution；
(4), after the suspension that mixed liquor step (1) prepared and step (2) prepare is mixed and stirred for uniformly, step is added
(3) solution prepared, continues to stir, and crosses 100～200 mesh sieves, gets product.
The water paint of a kind of graphitiferous the most according to claim 1, it is characterised in that described synergist is butyl triphen
Base fluorination phosphine.
The water paint of a kind of graphitiferous the most according to claim 1, it is characterised in that described defoamer is polyester modification
Siloxanes.
The water paint of a kind of graphitiferous the most according to claim 1, it is characterised in that described firming agent is isocyanates.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201610625205.8A CN106009963A (en) | 2016-08-01 | 2016-08-01 | Water-based paint containing graphite and preparation method thereof |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201610625205.8A CN106009963A (en) | 2016-08-01 | 2016-08-01 | Water-based paint containing graphite and preparation method thereof |
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| Publication Number | Publication Date |
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| CN106009963A true CN106009963A (en) | 2016-10-12 |
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Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201610625205.8A Pending CN106009963A (en) | 2016-08-01 | 2016-08-01 | Water-based paint containing graphite and preparation method thereof |
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Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101508855A (en) * | 2009-03-27 | 2009-08-19 | 南京工业大学 | Watersoluble plumbago electrically-conducting paint and method for producing the same |
| CN101691470A (en) * | 2009-10-12 | 2010-04-07 | 东莞市艾斯迪新材料有限公司 | Conductive and fire-retardant waterborne coating |
| CN103132079A (en) * | 2013-02-07 | 2013-06-05 | 睿纳能源科技（上海）有限公司 | Additive for acid texturing of diamond-wire-cutting polycrystalline silicon slices and application method thereof |
| CN104877524A (en) * | 2015-06-28 | 2015-09-02 | 任碧龙 | High-temperature-resistant and antistatic coating |
-
2016
- 2016-08-01 CN CN201610625205.8A patent/CN106009963A/en active Pending
Patent Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101508855A (en) * | 2009-03-27 | 2009-08-19 | 南京工业大学 | Watersoluble plumbago electrically-conducting paint and method for producing the same |
| CN101691470A (en) * | 2009-10-12 | 2010-04-07 | 东莞市艾斯迪新材料有限公司 | Conductive and fire-retardant waterborne coating |
| CN103132079A (en) * | 2013-02-07 | 2013-06-05 | 睿纳能源科技（上海）有限公司 | Additive for acid texturing of diamond-wire-cutting polycrystalline silicon slices and application method thereof |
| CN104877524A (en) * | 2015-06-28 | 2015-09-02 | 任碧龙 | High-temperature-resistant and antistatic coating |
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Application publication date: 20161012 |
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