CN105995357A - Innominatam kwai herb healthcare oral liquid for slowing aging - Google Patents
Innominatam kwai herb healthcare oral liquid for slowing aging Download PDFInfo
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- CN105995357A CN105995357A CN201610484345.8A CN201610484345A CN105995357A CN 105995357 A CN105995357 A CN 105995357A CN 201610484345 A CN201610484345 A CN 201610484345A CN 105995357 A CN105995357 A CN 105995357A
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Classifications
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L2/00—Non-alcoholic beverages; Dry compositions or concentrates therefor; Their preparation
- A23L2/38—Other non-alcoholic beverages
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L2/00—Non-alcoholic beverages; Dry compositions or concentrates therefor; Their preparation
- A23L2/70—Clarifying or fining of non-alcoholic beverages; Removing unwanted matter
- A23L2/84—Clarifying or fining of non-alcoholic beverages; Removing unwanted matter using microorganisms or biological material, e.g. enzymes
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23V—INDEXING SCHEME RELATING TO FOODS, FOODSTUFFS OR NON-ALCOHOLIC BEVERAGES AND LACTIC OR PROPIONIC ACID BACTERIA USED IN FOODSTUFFS OR FOOD PREPARATION
- A23V2002/00—Food compositions, function of food ingredients or processes for food or foodstuffs
Abstract
The invention discloses innominatam kwai herb healthcare oral liquid for slowing aging. According to the formula, 1,000 parts of the healthcare oral liquid comprise Chinese herbal medicine raw materials including 40-60 parts of innominatam kwai herbs, 10-15 parts of spirulina, 8-12 parts of herbal portulacae, 10-15 parts of radix polygoni multiflori, 15-20 parts of cordyceps sinensis, 10-13 parts of radix puerariae, 8-12 parts of blueberry leaves, 10-15 parts of roots of rehmannia, 10-16 parts of mulberries, 10-18 parts of cortex acanthopanacis, 5-10 parts of radix scrophulariae, 5-10 parts of radix scutellariae, 10-15 parts of radix glycyrrhizae and 10-15 parts of sweet stevia through the processes of ultrasonic-assisted extraction, volatile oil distillation, decoction with water and alcohol extraction. The oral liquid has the advantages of being good in anti-aging effect, safe, free of side effects, convenient to drink and the like.
Description
Technical field
The present invention relates to the unknown mallow health care oral liquid of a kind of delaying senility, a kind of health care oral liquid made for raw material with vegetable Chinese herbal medicines such as unknown certain herbaceous plants with big flowers, belong to field of health care products.
Background technology
Unknown certain herbaceous plants with big flowers, Malvaceae, draft is annual, the most edible in more than 200 autumn chrysanthemum plants, medicinal, and health-care effect has high value.In addition to viewing and admiring greening environment, treasure part and be none garbage of Herb, bud, Seedling, tender point, alabastrum, tender fruit rich in proteins, high polymerization virgin rubber, Ve, Vc and mineral, market can be supplied as new varieties, family and restaurant can cooking, cross water cold and dressed with sauce, Baoshangs etc., meat and vegetables is the most suitable.Taste flavor is unique, viscous sweet smooth, duplicates with its phase without any vegetable, and that eats is aid digestion, and intestine moistening is regulated the flow of vital energy and made the useless unobstructed discharge of thing of dispelling in gastrointestinal, effective suppression toxin be absorbed, and controls the raising of low-density protein, or the harm that athero is to human body；Especially treatment constipation of old people has the effect got instant result, and frees the hardship of difficult defecation, and strength is cleaned the intestines and stomach and crossed the fat of Sheng, the beneficially physical and mental health of old people.
It is an important new discovery that the flower put at the beginning of unknown certain herbaceous plants with big flowers and seed core extract biological general flavone, unknown certain herbaceous plants with big flowers flavones content shelter has currently known containing first of flavone plant, the most universally acknowledged Semen Ginkgo and daidzein content are the highest, and newfound unknown certain herbaceous plants with big flowers exceeds Semen Ginkgo and Semen sojae atricolor 500 times.The biological flavone importance to human body, it is raised to very important status already, cancerous cell and hemostasis and anti-inflammation effect are killed in effectively suppression, can prevent comprehensively and wipe out and treat insect pests and plant diseases various " mixed-blood " disease, the powerful profound influence that human body is produced, and there is significant efficacies of tonifying kidney and invigorating yang, because unknown certain herbaceous plants with big flowers is described as natural " viagra "；Meanwhile, VEContent also win than other species, exceed 2000 times of milk, fresh orange-juice 3000 times, come out top；Additionally, the necessary trace element of human body such as Vc, albumen, polysaccharide glue, Plant fiber, non-good fortune mineral selenium, ferrum, zinc are the abundantest.
Aging is the progressive process that each organ of body engenders that along with being continuously increased of age hypofunction and reserve capabillity decline, with advancing age, the same miopragia of various organs of human body, produces various pathological changes, little by little enters ageing state.Therefore prevention and slow down aging have become current social medical research focus.Chinese herbal medicine resource is the rarity of Chinese traditional culture, because its effect is notable, green, safely, have no side effect, the application in field of health care food is the most extensive.Chinese medicine is thought: the main cause of human senility is deficient five internal organs, disorder of QI and blood etc., and by nourishing the five internal organs, QI and blood regulating is the important means of traditional Chinese medical science slow down aging.Chinese medicine research in terms of defying age has the advantage of rich experience and uniqueness.Along with the continuous enhancing of people's prevention and health care consciousness, the demand with function of delaying senility health food is increased by society day by day.Result of study shows, the health product utilizing Chinese herbal medicine development contain abundant nutritional labeling, rich in trace element, vitamin isoreactivity nutritional labelings such as polysaccharide, flavone, aminoacid, potassium calcium, there is the effects such as regulation function of human body, enhancing immunity, nourishing and fit keeping function, life lengthening.
Summary of the invention
For overcoming the deficiency of existing product technology, it is an object of the invention to provide a kind of herbal health care oral liquid with senile-resistant efficacy.
Above-mentioned purpose of the present invention is achieved by the following technical programs:
The present invention provides the unknown mallow health care oral liquid of a kind of delaying senility, it is characterised in that: in 1000 portions of oral liquids, raw material of Chinese medicine and quality proportioning are: unknown certain herbaceous plants with big flowers 40～60 parts, spirulina 10～15 parts, Herba Portulacae 8～12 parts, Radix Polygoni Multiflori 10～15 parts, Cordyceps 15～20 parts, Radix Puerariae 10～13 parts, Blue berry leaf 8～12 parts, the Radix Rehmanniae 10～15 parts, Fructus Mori 10～16 parts, Cortex Acanthopancis 10～18 parts, Radix Scrophulariae 5～10 parts, Radix Scutellariae 5～10 parts, Radix Glycyrrhizae 10～15 parts, Folium Stevlae Rebaudianae 10～15 parts.
The preferred technical solution of the present invention is: the unknown mallow health care oral liquid of a kind of delaying senility, it is characterised in that: its raw material of Chinese medicine and quality proportioning be: unknown certain herbaceous plants with big flowers 50 parts, spirulina 13 parts, Herba Portulacae 12 parts, Radix Polygoni Multiflori 12 parts, Cordyceps 16 parts, Radix Puerariae 12 parts, Blue berry leaf 10 parts, 14 parts of the Radix Rehmanniae, 15 parts of Fructus Mori, Cortex Acanthopancis 15 parts, Radix Scrophulariae 7 parts, Radix Scutellariae 7 parts, 12 parts of Radix Glycyrrhizae, Folium Stevlae Rebaudianae 13 parts.
The present invention provides the unknown mallow health care oral liquid of a kind of delaying senility, it is characterised in that prepared by following steps:
(1) sorting weighs: is sorted by Chinese herbal medicine used, goes the removal of impurity etc., weighs according to aforementioned proportion；
(2) pretreatment of raw material: carry out pretreatment of raw material according to property of raw material difference respectively:
1. after spirulina, Herba Portulacae, Radix Polygoni Multiflori, Cordyceps, Blue berry leaf, Radix Puerariae, the Radix Rehmanniae, Cortex Acanthopancis, Radix Scrophulariae, Radix Scutellariae, Radix Glycyrrhizae, Folium Stevlae Rebaudianae mixing, carry out pulverization process, cross 40 mesh sieves；
2. in Fructus Mori, add 2～3 times of pure water, making beating, be subsequently adding 1～2% pectase, enzymolysis 10～20min under the conditions of 40～50 DEG C；
(3) ultrasound-assisted enzymolysis: add raw materials quality after raw material mixing than 3～5 times of pure water, it is subsequently adding raw materials quality than 2～3% cellulase, 1～2% non-starch polysaccharide enzyme, enzymolysis 30～60min under the conditions of ultrasonic assistant, hydrolysis temperature controls at 40～50 DEG C；
(4) centrifugal: centrifugation lixiviating solution and middle medicinal herbs residue；
(5) distillation: add the pure water of 3～5 times amount in Chinese herbal medicine residue, collects volatile oil 8～10h, and volatile oil is collected separately placement, and aqueous solution filters, and merges with lixiviating solution；
(6) volatile oil emulsifying: addition 1.5～the cosolvent tween 80 of 2.0%, heating emulsification in the volatile oil that will collect；
(7) decocting: by adding the water of 2～3 times amount in the Chinese herbal medicine residue after distillation, decocting 3 times, each 1.5～2h, decocting liquid merges with lixiviating solution；
(8) concentrating under reduced pressure: the aqueous solution after merging is concentrated into the clear paste of 1g/ml, lets cool；
(9) precipitate with ethanol: the ethanol adding 95% in clear paste makes alcohol content reach 60～70%, places more than 48h under the conditions of 4 DEG C
(10) alcohol extraction: add 50% ethanol of 4～6 times amount, heating extraction 2 times, extraction time 1～1.5h in the Chinese herbal medicine residue after decocting；
(11) sucking filtration is merged: the liquid after precipitate with ethanol is merged sucking filtration with alcohol extract；
(12) recovered under reduced pressure: sucking filtration liquid is carried out decompression recycling ethanol to without alcohol taste；
(13) mixing: add unknown certain herbaceous plants with big flowers and the good volatile oil of emulsifying while hot in concentrated solution, stir；
(14) adjuvant is added: addition 0.10～the potassium sorbate of 0.15% and 1～the sweeting agent of 2%, add water stirring constant volume；
(15) stand: more than 48h will be stood under oral liquid semi-finished product room temperature；
(16) centrifugal: oral liquid semi-finished product 3000r/min is centrifuged 5～10min；
(17) constant volume subpackage: oral liquid constant volume, subpackage after being centrifuged i.e. obtain oral liquid finished product.
What above-mentioned sweeting agent was selected is the mixture of one or more in xylitol, oligomeric isomaltose, Mel.
The present invention provides the unknown mallow health care oral liquid of a kind of delaying senility, and what described unknown certain herbaceous plants with big flowers raw material was selected is the leaf of unknown certain herbaceous plants with big flowers, stem etc..
The present invention provides the unknown mallow health care oral liquid of a kind of delaying senility, it is advantageous that: one is selected prescription under Traditional Chinese medical theory and practical advice, the unknown certain herbaceous plants with big flowers of scientific compatibility and multiple Chinese herbal medicine, and drug component is through dialectical compatibility, help using mutually assistant, can notable defying age；Two is the technique using " Ultrasonic Wave-Assisted Extraction+volatile matter distillation oil+decocting+alcohol extraction " in the preparation process of oral liquid, fully mixes the functional active components of defying age in Chinese herbal medicine, improves health-care effect；Three is that oral liquid has no side effect safely, drinks conveniently.
The present invention provides the unknown mallow health care oral liquid of a kind of delaying senility, is carried out toxicology test and the safety evaluatio of health care oral liquid by animal experiment.Chmice acute Oral toxicity result of the test shows, this health care oral liquid is more than high dose group 75mg/kg bw to chmice acute per os maximum tolerated dose；Genetic toxicity test mouse marrow cell micro nuclear test and two result of the tests of mouse inbred strain are feminine gender, show that this health care oral liquid is without mutagenic action；From rat 30d feeding trial, rat sign behavior is normal, figure is healthy, blood and blood parameters change the most without exception, and therefore the dosage (150 times of human body recommended amounts) of 75mg/kg bw belongs to safe dose；Genetic toxicity test and rat 30d feeding trial result are feminine gender, it is thus determined that this health beverage belongs to non-toxic type food, people can be safe relieved edible.
The present invention provides the unknown mallow health care oral liquid of a kind of delaying senility, different Chinese herbal medicine nature and flavor are different, effect also exists huge difference, the interaction relationship of complexity is there is after different Chinese herbal medicine combinations, and proportioning between Chinese herbal medicine is closer, different ratio also will make monarch relation that substantial change occurs, so that the relation generation material alterations of composite Chinese herbal.The interaction relationship of complexity is there is to each other in the application by Chinese herbal medicine such as unknown certain herbaceous plants with big flowers, spirulina, Herba Portulacae, Radix Polygoni Multiflori, Cordyceps, Radix Puerariae, Blue berry leaf, the Radix Rehmanniae, Fructus Mori, Cortex Acanthopancis, Radix Scrophulariae, Radix Scutellariae, Radix Glycyrrhizae, Folium Stevlae Rebaudianae, rational proportion, achieve unforeseeable technique effect, make the relation generation material alterations of defying age herbal health care oral liquid.According to " function of health food assessment process and the method for inspection ", the application product is carried out Evaluation of Functional, rat test is utilized to measure health care oral liquid to the impact on one of aging index peroxidation lipid, after result shows to feed 3 months, experimental group serum MDA value is less than matched group, liver homogenate MDA and brain homogenate MDA relatively matched group reduce by 30.32% and 29.64%, relatively matched group significant difference (p < 0.01), illustrates that product has preferable activity of fighting against senium；Additionally, result of the test shows, changing unknown certain herbaceous plants with big flowers and the composition of Chinese herbal medicine and significantly reduce effect of product than regular meeting, result difference is notable (p < 0.01), illustrates that the synergism between unknown certain herbaceous plants with big flowers and Chinese herbal medicine serves the effect being obviously improved oral liquid functional activity.
Detailed description of the invention
Below in conjunction with embodiment, the present invention will be further described.
Embodiment 1:
The unknown mallow health care oral liquid of a kind of delaying senility, is prepared by following steps:
(1) sorting weighs: sorted by Chinese herbal medicine used, go the removal of impurity etc., weigh according to unknown certain herbaceous plants with big flowers 50 parts, spirulina 13 parts, Herba Portulacae 12 parts, Radix Polygoni Multiflori 12 parts, Cordyceps 16 parts, Radix Puerariae 12 parts, Blue berry leaf 10 parts, 14 parts of the Radix Rehmanniae, 15 parts of Fructus Mori, Cortex Acanthopancis 15 parts, Radix Scrophulariae 7 parts, Radix Scutellariae 7 parts, 12 parts of Radix Glycyrrhizae, 13 parts of ratios of Folium Stevlae Rebaudianae in every 1000 portions of oral liquids；
(2) pretreatment of raw material: carry out pretreatment of raw material according to property of raw material difference respectively:
1. after spirulina, Herba Portulacae, Radix Polygoni Multiflori, Cordyceps, Blue berry leaf, the Radix Rehmanniae, Cortex Acanthopancis, Radix Puerariae, Radix Scrophulariae, Radix Scutellariae, Radix Glycyrrhizae, Folium Stevlae Rebaudianae mixing, carry out pulverization process, cross 40 mesh sieves；
2. in Fructus Mori, add 2.5 times of pure water, making beating, be subsequently adding 1.5% pectase, enzymolysis 15min under the conditions of 40～50 DEG C；
(3) ultrasound-assisted enzymolysis: adding raw materials quality after raw material mixing than 4 times of pure water, be subsequently adding raw materials quality than 2.5% cellulase, 1.5% non-starch polysaccharide enzyme, enzymolysis 45min under the conditions of ultrasonic assistant, hydrolysis temperature controls at 40～50 DEG C；
(4) centrifugal: centrifugation lixiviating solution and middle medicinal herbs residue；
(5) distillation: add the pure water of 4 times amount in Chinese herbal medicine residue, collects volatile oil 9h, and volatile oil is collected separately placement, and aqueous solution filters, and merges with lixiviating solution；
(6) volatile oil emulsifying: add the cosolvent tween 80 of 1.8%, heating emulsification in the volatile oil that will collect；
(7) decocting: by adding the water of 2.5 times amount in the Chinese herbal medicine residue after distillation, decocting 3 times, each 1.8h, decocting liquid merges with lixiviating solution；
(8) concentrating under reduced pressure: the aqueous solution after merging is concentrated into the clear paste of 1g/ml, lets cool；
(9) precipitate with ethanol: the ethanol adding 95% in clear paste makes alcohol content reach 60～70%, places more than 48h under the conditions of 4 DEG C
(10) alcohol extraction: add 50% ethanol of 5 times amount, heating extraction 2 times, extraction time 1.2h in the Chinese herbal medicine residue after decocting；
(11) sucking filtration is merged: the liquid after precipitate with ethanol is merged sucking filtration with alcohol extract；
(12) recovered under reduced pressure: sucking filtration liquid is carried out decompression recycling ethanol to without alcohol taste；
(13) mixing: add unknown certain herbaceous plants with big flowers and the good volatile oil of emulsifying while hot in concentrated solution, stir；
(14) adjuvant is added: adding potassium sorbate and the xylitol of 1.5% of 0.12%, add water stirring constant volume；
(15) stand: more than 48h will be stood under oral liquid semi-finished product room temperature；
(16) centrifugal: oral liquid semi-finished product 3000r/min is centrifuged 8min；
(17) constant volume subpackage: oral liquid constant volume, subpackage after being centrifuged i.e. obtain oral liquid finished product.
Embodiment 2:
The unknown mallow health care oral liquid of a kind of delaying senility, is prepared by following steps:
(1) sorting weighs: sorted by Chinese herbal medicine used, go the removal of impurity etc., weigh according to unknown certain herbaceous plants with big flowers 60 parts, spirulina 10 parts, Herba Portulacae 12 parts, Radix Polygoni Multiflori 10 parts, Cordyceps 20 parts, Radix Puerariae 10 parts, Blue berry leaf 12 parts, 10 parts of the Radix Rehmanniae, 16 parts of Fructus Mori, Cortex Acanthopancis 10 parts, Radix Scrophulariae 5 parts, Radix Scutellariae 10 parts, 15 parts of Radix Glycyrrhizae, 10 parts of ratios of Folium Stevlae Rebaudianae in every 1000 portions of oral liquids；
(2) pretreatment of raw material: carry out pretreatment of raw material according to property of raw material difference respectively:
1. after spirulina, Herba Portulacae, Radix Polygoni Multiflori, Cordyceps, Blue berry leaf, the Radix Rehmanniae, Cortex Acanthopancis, Radix Puerariae, Radix Scrophulariae, Radix Scutellariae, Radix Glycyrrhizae, Folium Stevlae Rebaudianae mixing, carry out pulverization process, cross 40 mesh sieves；
2. in Fructus Mori, add 3 times of pure water, making beating, be subsequently adding 2% pectase, enzymolysis 10min under the conditions of 40～50 DEG C；
(3) ultrasound-assisted enzymolysis: adding raw materials quality after raw material mixing than 5 times of pure water, be subsequently adding raw materials quality than 3% cellulase, 2% non-starch polysaccharide enzyme, enzymolysis 30min under the conditions of ultrasonic assistant, hydrolysis temperature controls at 40～50 DEG C；
(4) centrifugal: centrifugation lixiviating solution and middle medicinal herbs residue；
(5) distillation: add the pure water of 5 times amount in Chinese herbal medicine residue, collects volatile oil 8h, and volatile oil is collected separately placement, and aqueous solution filters, and merges with lixiviating solution；
(6) volatile oil emulsifying: add the cosolvent tween 80 of 2.0%, heating emulsification in the volatile oil that will collect；
(7) decocting: by adding the water of 3 times amount in the Chinese herbal medicine residue after distillation, decocting 3 times, each 1.5h, decocting liquid merges with lixiviating solution；
(8) concentrating under reduced pressure: the aqueous solution after merging is concentrated into the clear paste of 1g/ml, lets cool；
(9) precipitate with ethanol: the ethanol adding 95% in clear paste makes alcohol content reach 60～70%, places more than 48h under the conditions of 4 DEG C
(10) alcohol extraction: add 50% ethanol of 6 times amount, heating extraction 2 times, extraction time 1h in the Chinese herbal medicine residue after decocting；
(11) sucking filtration is merged: the liquid after precipitate with ethanol is merged sucking filtration with alcohol extract；
(12) recovered under reduced pressure: sucking filtration liquid is carried out decompression recycling ethanol to without alcohol taste；
(13) mixing: add unknown certain herbaceous plants with big flowers and the good volatile oil of emulsifying while hot in concentrated solution, stir；
(14) adjuvant is added: adding potassium sorbate and the oligomeric isomaltose of 2% of 0.15%, add water stirring constant volume；
(15) stand: more than 48h will be stood under oral liquid semi-finished product room temperature；
(16) centrifugal: oral liquid semi-finished product 3000r/min is centrifuged 10min；
(17) constant volume subpackage: oral liquid constant volume, subpackage after being centrifuged i.e. obtain oral liquid finished product.
Embodiment 3:
The unknown mallow health care oral liquid of a kind of delaying senility, is prepared by following steps:
(1) sorting weighs: sorted by Chinese herbal medicine used, go the removal of impurity etc., weigh according to unknown certain herbaceous plants with big flowers 40 parts, spirulina 15 parts, Herba Portulacae 8 parts, Radix Polygoni Multiflori 15 parts, Cordyceps 15 parts, Radix Puerariae 13 parts, Blue berry leaf 8 parts, 15 parts of the Radix Rehmanniae, 10 parts of Fructus Mori, Cortex Acanthopancis 18 parts, Radix Scrophulariae 10 parts, Radix Scutellariae 5 parts, 10 parts of Radix Glycyrrhizae, 15 parts of ratios of Folium Stevlae Rebaudianae in every 1000 portions of oral liquids；
(2) pretreatment of raw material: carry out pretreatment of raw material according to property of raw material difference respectively:
1. after spirulina, Herba Portulacae, Radix Polygoni Multiflori, Cordyceps, Blue berry leaf, the Radix Rehmanniae, Cortex Acanthopancis, Radix Puerariae, Radix Scrophulariae, Radix Scutellariae, Radix Glycyrrhizae, Folium Stevlae Rebaudianae mixing, carry out pulverization process, cross 40 mesh sieves；
2. in Fructus Mori, add 2 times of pure water, making beating, be subsequently adding 1% pectase, enzymolysis 20min under the conditions of 40～50 DEG C；
(3) ultrasound-assisted enzymolysis: adding raw materials quality after raw material mixing than 3 times of pure water, be subsequently adding raw materials quality than 2% cellulase, 1% non-starch polysaccharide enzyme, enzymolysis 60min under the conditions of ultrasonic assistant, hydrolysis temperature controls at 40～50 DEG C；
(4) centrifugal: centrifugation lixiviating solution and middle medicinal herbs residue；
(5) distillation: add the pure water of 3 times amount in Chinese herbal medicine residue, collects volatile oil 10h, and volatile oil is collected separately placement, and aqueous solution filters, and merges with lixiviating solution；
(6) volatile oil emulsifying: add the cosolvent tween 80 of 1.5%, heating emulsification in the volatile oil that will collect；
(7) decocting: by adding the water of 2 times amount in the Chinese herbal medicine residue after distillation, decocting 3 times, each 2h, decocting liquid merges with lixiviating solution；
(8) concentrating under reduced pressure: the aqueous solution after merging is concentrated into the clear paste of 1g/ml, lets cool；
(9) precipitate with ethanol: the ethanol adding 95% in clear paste makes alcohol content reach 60～70%, places more than 48h under the conditions of 4 DEG C
(10) alcohol extraction: add 50% ethanol of 4 times amount, heating extraction 2 times, extraction time 1.5h in the Chinese herbal medicine residue after decocting；
(11) sucking filtration is merged: the liquid after precipitate with ethanol is merged sucking filtration with alcohol extract；
(12) recovered under reduced pressure: sucking filtration liquid is carried out decompression recycling ethanol to without alcohol taste；
(13) mixing: add unknown certain herbaceous plants with big flowers and the good volatile oil of emulsifying while hot in concentrated solution, stir；
(14) adjuvant is added: adding potassium sorbate and the Mel of 1% of 0.10%, add water stirring constant volume；
(15) stand: more than 48h will be stood under oral liquid semi-finished product room temperature；
(16) centrifugal: oral liquid semi-finished product 3000r/min is centrifuged 5～10min；
(17) constant volume subpackage: oral liquid constant volume, subpackage after being centrifuged i.e. obtain oral liquid finished product.
Above example is merely to illustrate technical scheme, rather than is limited；Although being described in detail by invention with reference to previous embodiment, but for the person of ordinary skill of the art, still the technical scheme described in previous embodiment can be modified, or wherein portion of techniques feature is carried out equivalent；And to these amendments or replacement, do not make the essence of appropriate technical solution depart from the spirit and scope of claimed technical solution of the invention.
Claims (3)
1. the unknown mallow health care oral liquid of a delaying senility, it is characterised in that: in 1000 portions of oral liquids, raw material of Chinese medicine and quality proportioning are: unknown certain herbaceous plants with big flowers 40～60 parts, spirulina 10～15 parts, Herba Portulacae 8～12 parts, Radix Polygoni Multiflori 10～15 parts, Cordyceps 15～20 parts, Radix Puerariae 10～13 parts, Blue berry leaf 8～12 parts, the Radix Rehmanniae 10～15 parts, Fructus Mori 10～16 parts, Cortex Acanthopancis 10～18 parts, Radix Scrophulariae 5～10 parts, Radix Scutellariae 5～10 parts, Radix Glycyrrhizae 10～15 parts, Folium Stevlae Rebaudianae 10～15 parts.
The unknown mallow health care oral liquid of a kind of delaying senility the most according to claim 1, it is characterised in that described oral liquid is prepared as follows:
(1) sorting weighs: is sorted by Chinese herbal medicine used, goes the removal of impurity, proportionally weighs；
(2) pretreatment of raw material: carry out pretreatment of raw material according to property of raw material difference respectively:
1. after spirulina, Herba Portulacae, Radix Polygoni Multiflori, Cordyceps, Blue berry leaf, Radix Puerariae, the Radix Rehmanniae, Cortex Acanthopancis, Radix Scrophulariae, Radix Scutellariae, Radix Glycyrrhizae, Folium Stevlae Rebaudianae mixing, carry out pulverization process, cross 40 mesh sieves；
2. in Fructus Mori, add 2～3 times of pure water, making beating, be subsequently adding 1～2% pectase, enzymolysis 10～20min under the conditions of 40～50 DEG C；
(3) ultrasound-assisted enzymolysis: add raw materials quality after raw material mixing than 3～5 times of pure water, it is subsequently adding raw materials quality than 2～3% cellulase, 1～2% non-starch polysaccharide enzyme, enzymolysis 30～60min under the conditions of ultrasonic assistant, hydrolysis temperature controls at 40～50 DEG C；
(4) centrifugal: centrifugation lixiviating solution and middle medicinal herbs residue；
(5) distillation: add the pure water of 3～5 times amount in Chinese herbal medicine residue, collects volatile oil 8～10h, and volatile oil is collected separately placement, and aqueous solution filters, and merges with lixiviating solution；
(6) volatile oil emulsifying: addition 1.5～the cosolvent tween 80 of 2.0%, heating emulsification in the volatile oil that will collect；
(7) decocting: by adding the water of 2～3 times amount in the Chinese herbal medicine residue after distillation, decocting 3 times, each 1.5～2h, decocting liquid merges with lixiviating solution；
(8) concentrating under reduced pressure: the aqueous solution after merging is concentrated into the clear paste of 1g/ml, lets cool；
(9) precipitate with ethanol: the ethanol adding 95% in clear paste makes alcohol content reach 60～70%, places more than 48h under the conditions of 4 DEG C
(10) alcohol extraction: add 50% ethanol of 4～6 times amount, heating extraction 2 times, extraction time 1～1.5h in the Chinese herbal medicine residue after decocting；
(11) sucking filtration is merged: the liquid after precipitate with ethanol is merged sucking filtration with alcohol extract；
(12) recovered under reduced pressure: sucking filtration liquid is carried out decompression recycling ethanol to without alcohol taste；
(13) mixing: add unknown certain herbaceous plants with big flowers and the good volatile oil of emulsifying while hot in concentrated solution, stir；
(14) adjuvant is added: addition 0.10～the potassium sorbate of 0.15% and 1～the sweeting agent of 2%, add water stirring constant volume；
(15) stand: more than 48h will be stood under oral liquid semi-finished product room temperature；
(16) centrifugal: oral liquid semi-finished product 3000r/min is centrifuged 5～10min；
(17) constant volume subpackage: oral liquid constant volume, subpackage after being centrifuged i.e. obtain oral liquid finished product.
The unknown mallow health care oral liquid of a kind of delaying senility, it is characterised in that what described sweeting agent was selected is the mixture of one or more in xylitol, oligomeric isomaltose, Mel.
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| CN105029608A (en) * | 2015-07-05 | 2015-11-11 | 青岛浩大海洋保健食品有限公司 | Marine functional health beverage with ageing delaying efficacy |
| CN105477369A (en) * | 2015-12-21 | 2016-04-13 | 青岛浩大海洋保健食品有限公司 | Anti-aging Chinese herbal medicinal health oral liquid containing seaweed protein and preparation method of anti-aging Chinese herbal medicinal health oral liquid |
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| Publication number | Priority date | Publication date | Assignee | Title |
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| JP2002293711A (en) * | 2001-03-23 | 2002-10-09 | General Topics Srl | Active ingredient based on lipoic acid and polyenol fatty acid |
| CN103518842A (en) * | 2013-09-27 | 2014-01-22 | 安徽省林锦记食品工业有限公司 | Honey, lucid ganoderma, fruit and vegetable yoghurt and preparation method thereof |
| CN105029608A (en) * | 2015-07-05 | 2015-11-11 | 青岛浩大海洋保健食品有限公司 | Marine functional health beverage with ageing delaying efficacy |
| CN104957331A (en) * | 2015-07-07 | 2015-10-07 | 北京尚亭正毅科技开发有限公司 | Innominatam kwai mixed tea and preparing method of innominatam kwai mixed tea |
| CN105477369A (en) * | 2015-12-21 | 2016-04-13 | 青岛浩大海洋保健食品有限公司 | Anti-aging Chinese herbal medicinal health oral liquid containing seaweed protein and preparation method of anti-aging Chinese herbal medicinal health oral liquid |
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