CN105994422A - Olive leaf and grape botanical pesticide - Google Patents
Olive leaf and grape botanical pesticide Download PDFInfo
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- CN105994422A CN105994422A CN201610430600.0A CN201610430600A CN105994422A CN 105994422 A CN105994422 A CN 105994422A CN 201610430600 A CN201610430600 A CN 201610430600A CN 105994422 A CN105994422 A CN 105994422A
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- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N65/00—Biocides, pest repellants or attractants, or plant growth regulators containing material from algae, lichens, bryophyta, multi-cellular fungi or plants, or extracts thereof
-
- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N25/00—Biocides, pest repellants or attractants, or plant growth regulators, characterised by their forms, or by their non-active ingredients or by their methods of application, e.g. seed treatment or sequential application; Substances for reducing the noxious effect of the active ingredients to organisms other than pests
- A01N25/32—Ingredients for reducing the noxious effect of the active substances to organisms other than pests, e.g. toxicity reducing compositions, self-destructing compositions
-
- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N65/00—Biocides, pest repellants or attractants, or plant growth regulators containing material from algae, lichens, bryophyta, multi-cellular fungi or plants, or extracts thereof
- A01N65/08—Magnoliopsida [dicotyledons]
- A01N65/36—Rutaceae [Rue family], e.g. lime, orange, lemon, corktree or pricklyash
-
- C—CHEMISTRY; METALLURGY
- C05—FERTILISERS; MANUFACTURE THEREOF
- C05D—INORGANIC FERTILISERS NOT COVERED BY SUBCLASSES C05B, C05C; FERTILISERS PRODUCING CARBON DIOXIDE
- C05D9/00—Other inorganic fertilisers
-
- C—CHEMISTRY; METALLURGY
- C05—FERTILISERS; MANUFACTURE THEREOF
- C05G—MIXTURES OF FERTILISERS COVERED INDIVIDUALLY BY DIFFERENT SUBCLASSES OF CLASS C05; MIXTURES OF ONE OR MORE FERTILISERS WITH MATERIALS NOT HAVING A SPECIFIC FERTILISING ACTIVITY, e.g. PESTICIDES, SOIL-CONDITIONERS, WETTING AGENTS; FERTILISERS CHARACTERISED BY THEIR FORM
- C05G3/00—Mixtures of one or more fertilisers with additives not having a specially fertilising activity
-
- C—CHEMISTRY; METALLURGY
- C05—FERTILISERS; MANUFACTURE THEREOF
- C05G—MIXTURES OF FERTILISERS COVERED INDIVIDUALLY BY DIFFERENT SUBCLASSES OF CLASS C05; MIXTURES OF ONE OR MORE FERTILISERS WITH MATERIALS NOT HAVING A SPECIFIC FERTILISING ACTIVITY, e.g. PESTICIDES, SOIL-CONDITIONERS, WETTING AGENTS; FERTILISERS CHARACTERISED BY THEIR FORM
- C05G3/00—Mixtures of one or more fertilisers with additives not having a specially fertilising activity
- C05G3/60—Biocides or preservatives, e.g. disinfectants, pesticides or herbicides; Pest repellants or attractants
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02A—TECHNOLOGIES FOR ADAPTATION TO CLIMATE CHANGE
- Y02A50/00—TECHNOLOGIES FOR ADAPTATION TO CLIMATE CHANGE in human health protection, e.g. against extreme weather
- Y02A50/30—Against vector-borne diseases, e.g. mosquito-borne, fly-borne, tick-borne or waterborne diseases whose impact is exacerbated by climate change
Abstract
The invention discloses an olive leaf and grape botanical pesticide. The pesticide is prepared from olive leaves, momordica cochinchinensis, melia azedarach leaves, sweet-clover astragalus, agrimonia pilosa ledeb, sanguisorba officinalis, Chinese prickly ash, cinnamon, cortex phellodendri, atractylodes macrocephala koidz and a modified starch solution. Main components of the pesticide are extracted from Chinese herbal medicine. Compared with a traditional organic pesticide, the pesticide has the advantages of being safe, low in toxin and free of pungent smell and pesticide resistance, and after reasonable complexing, the antibacterial and insect-killing effects are remarkable; by adding modified starch, the pesticide is better in stability and difficult to decompose; meanwhile, the modified starch can adsorb excessive components in the pesticide, and pesticide residues of fruits are further reduced; besides, the extraction components of Chinese herbal medicine contain various nutrients and also contain active enzyme, antioxidant, growth promoting factors and the like, quality of grapes is improved, the seedless rate of grapes is increased, and the effect of reducing the cholesterol level of a human body is enhanced.
Description
Technical field
The invention belongs to pesticide field, be specifically related to a kind of Folium olive mattae source pesticide.
Background technology
Fructus Vitis viniferae is called: Jambul, grass Herba Tubocapsici Anomali, mountain calabash, Li Tao etc..Belong to the fruit of vitaceae Fructus Vitis viniferae.For defoliation liana, it it is one of the most ancient plant in the world.Fructus Vitis viniferae originates in Europe, West Asia and north African one band.According to archaeological materials, the area of cultivating grape is between the Caspian Sea, Asia Minor and Black Sea and bank area, south the earliest.About before 7000, the regional cultivation having also begun to Fructus Vitis viniferae such as south Caucasus, middle Asia, Syria, Iraq.Most historians think that Persian (i.e. today is Iranian) is the country made grape wine the earliest.Europe early start plantation Fructus Vitis viniferae the country carrying out wine production are Greece.To the north of China Yangtze river basin, all there is product various places.Stem is climing is up to 10 ~ 20 meters.Dan Ye, alternate.Spend little, yellow green, form panicle.Berry is circular or oval, because kind is different, has the different fruit colors such as white, blue or green, red, brown, purple, black.8 ~ October of fructescence, existing more than the 2000 year history of Chinese cultivated Fructus Vitis viniferae, pass on from one to another and introduce for Han dynasty people Zhang Qian.
The growth of most plants now all be unable to do without the applying of pesticide, and the definition of pesticide broad sense refers to for preventing, eliminate or control harm agricultural, the disease of forestry, worm, grass and other harmful organisms and on purpose regulating plant, the chemosynthesis of insect growth or derive from biology, a kind of material of other natural materials or the mixture of several material and preparation thereof.Refer in agricultural production, for ensureing, promote plant and the growth of crops, the parasite killing used, sterilize, kill harmful animal (or weeds)
One class medicine be referred to as.Refer in particular to agriculturally for preventing and treating disease pest and the medicament such as coordinate plant growth, weeding.The growth of mattae is no exception, and the applying of reasonable pesticide can increase yield, and can improve grape quality.But pesticide majority is chemicals now, and tanginess is unpleasant, and easily jeopardizes person poultry safety, has had a strong impact on environmental health and safety, for green, environmental protection, ecology, the most unfavorable.Additionally, apply this type of pesticide to be for a long time easily generated disease resistance, reduce the using effect of pesticide.
Summary of the invention
It is desirable to provide a kind of Folium olive mattae source pesticide.
The present invention is achieved through the following technical solutions:
A kind of Folium olive mattae source pesticide, is made up of the material of following weight portion:
12 parts of Folium olive, 6 parts of Semen Momordicaes, 8 parts of Folium Meliaes, 4 parts of Herba Astragali Melilotoidiss, 5 parts of Herba Agrimoniaes, 3 parts of Radix Sanguisorbaes, 4 parts of Pericarpium Zanthoxylies, 4 parts of Cortex cinnamomi japonici (Ramulus Cinnamomi)s, 7 parts of Cortex Phellodendris, 5 parts of Rhizoma Atractylodis Macrocephalaes, 4 parts of modified starch solutions；Described modified starch solution is made up of the material of following weight portion: 30 parts of starch, 3 parts of modified alta-muds, 0.2 part of dodecylbenzene sodium sulfonate, 0.3 part of Span, 0.6 part of Butylated hydroxyanisole, 1 part of vitamin C, 0.5 part of chitin, 1 part of citric acid, 0.5 part of xylitol.
Further, described method for preparing modified bentonite is: bentonite is first put into soaking and washing 20min in the hydrochloric acid solution that mass fraction is 5%, putting into calcining 2h under 780 DEG C of environment after taking-up, being crushed to granular size with ball mill after taking-up is 400 ~ 500 mesh.Bentonite is through modified, and its adsorptivity, stability are significantly improved, and adds dispersibility and the stability that can strengthen solution in modified starch solution to.
Further, the preparation method of described modified starch solution is:
(1) jointly being mixed by the clear water of starch with its gross mass 2.5 times, heating keeps water temperature to be 80 ~ 88 DEG C, obtains solution A standby after gelatinizing 30 ~ 40min, and period is stirred continuously；
(2) clear water of modified alta-mud with its quality 3 times is mixed jointly, heating keeps water temperature to be 40 ~ 45 DEG C, add dodecylbenzene sodium sulfonate, Span and Butylated hydroxyanisole, after mix and blend 15min, again vitamin C, chitin, citric acid and xylitol are added, continue stirring 15min, obtain solution B standby；
(3) temperature keeping solution B is 40 ~ 45 DEG C, and the temperature keeping solution A is 80 ~ 88 DEG C, solution B is joined in solution A, and is stirred with the rotating speed of 300 ~ 350 turns/min, and, composition constant until solution temperature i.e. obtains modified starch solution after being uniformly dispersed.Solution A, solution B with different temperatures, are carried out mixing and liquidate, utilizes temperature difference to strengthen intermolecular mixing, enhance intermolecular crosslinking fusion degree, and then improve stability and the uniformity of solution.
The preparation method of a kind of Folium olive mattae source pesticide, comprises the steps:
(1) Folium olive, Semen Momordicae, Folium Meliae, Herba Astragali Melilotoidis, Herba Agrimoniae, Radix Sanguisorbae, Pericarpium Zanthoxyli, Cortex cinnamomi japonici (Ramulus Cinnamomi), Cortex Phellodendri and the Rhizoma Atractylodis Macrocephalae jointly being put in cellar, the temperature keeping cellar is 40 ~ 45 DEG C, takes out standby after placing 5 ~ 7 days；Mentioned component is put into middle temperature storage a period of time in cellar, zest and the toxic component of Chinese medicine can be dispelled, be avoided that again the infringement to beneficiating ingredient simultaneously；
(2) with clear water to step (1) process after composition be rinsed, dry standby；
(3) Semen Momordicae, Pericarpium Zanthoxyli and Cortex cinnamomi japonici (Ramulus Cinnamomi) are put into jointly fill fry sand marmite in, heating keep temperature be 100 ~ 105 DEG C, constantly stir-fry, take out after 15 ~ 18min parch medicine A is standby；
(4) Herba Astragali Melilotoidis, Cortex Phellodendri and the Rhizoma Atractylodis Macrocephalae are put in the marmite filling Testa Tritici jointly, heating keep temperature be 95 ~ 100 DEG C, constantly stir-fry, take out after 10 ~ 15min parch medicine B is standby；The property of medicine for medicine carries out stir-baking with sand and parched with bran, can improve, promote the property of medicine of medicine, and follow-up extraction operation；
(5) Folium olive, Folium Meliae, Herba Agrimoniae, Radix Sanguisorbae and parch medicine A, parch medicine B are mixed jointly, after pulverizing, cross 60 mesh, be then placed in the ethanol solution that mass fraction is 75% of its gross mass 3 times circulating extraction 20 ~ 24h, obtain extracting solution standby；Extract with ethanol solution after medicine is pulverized, the content of beneficiating ingredient can not only be improved, be avoided that again tradition water puies forward the problem of infringement beneficiating ingredient, further ensure the using effect of extract；
(6) by common with modified starch solution for the extracting solution of step (5) gained mix homogeneously get product.
There is advantages that pesticide main component of the present invention is to extract from Chinese herbal medicine and obtain, compared with tradition organic agricultural chemicals, there is safety, low toxicity, the advantage that has no irritating odor, will not develop immunity to drugs, after the most compounding, its disinfection and deinsectization effect is notable, coordinates the interpolation of modified starch, its stability more preferably, be not easily decomposed, modified starch can adsorb again the excess ingredients in medicine simultaneously, reduces the drug residue of fruit further；Additionally, the extract component of Chinese herbal medicine contains various nutritional labeling, contain again the compositions such as organized enzyme, polyphenoils, positive growth factor, grape quality can be improved, improve the no seed rate of Fructus Vitis viniferae, enhance its effect reducing body's cholesterol level.
Detailed description of the invention
Embodiment 1
A kind of Folium olive mattae source pesticide, is made up of the material of following weight portion:
12 parts of Folium olive, 6 parts of Semen Momordicaes, 8 parts of Folium Meliaes, 4 parts of Herba Astragali Melilotoidiss, 5 parts of Herba Agrimoniaes, 3 parts of Radix Sanguisorbaes, 4 parts of Pericarpium Zanthoxylies, 4 parts of Cortex cinnamomi japonici (Ramulus Cinnamomi)s, 7 parts of Cortex Phellodendris, 5 parts of Rhizoma Atractylodis Macrocephalaes, 4 parts of modified starch solutions；Described modified starch solution is made up of the material of following weight portion: 30 parts of starch, 3 parts of modified alta-muds, 0.2 part of dodecylbenzene sodium sulfonate, 0.3 part of Span, 0.6 part of Butylated hydroxyanisole, 1 part of vitamin C, 0.5 part of chitin, 1 part of citric acid, 0.5 part of xylitol.
Further, described method for preparing modified bentonite is: bentonite is first put into soaking and washing 20min in the hydrochloric acid solution that mass fraction is 5%, putting into calcining 2h under 780 DEG C of environment after taking-up, being crushed to granular size with ball mill after taking-up is 400 ~ 500 mesh.
Further, the preparation method of described modified starch solution is:
(1) jointly being mixed by the clear water of starch with its gross mass 2.5 times, heating keeps water temperature to be 80 ~ 88 DEG C, obtains solution A standby after gelatinizing 30 ~ 40min, and period is stirred continuously；
(2) clear water of modified alta-mud with its quality 3 times is mixed jointly, heating keeps water temperature to be 40 ~ 45 DEG C, add dodecylbenzene sodium sulfonate, Span and Butylated hydroxyanisole, after mix and blend 15min, again vitamin C, chitin, citric acid and xylitol are added, continue stirring 15min, obtain solution B standby；
(3) temperature keeping solution B is 40 ~ 45 DEG C, and the temperature keeping solution A is 80 ~ 88 DEG C, solution B is joined in solution A, and is stirred with the rotating speed of 300 ~ 350 turns/min, and, composition constant until solution temperature i.e. obtains modified starch solution after being uniformly dispersed.
The preparation method of a kind of Folium olive mattae source pesticide, comprises the steps:
(1) Folium olive, Semen Momordicae, Folium Meliae, Herba Astragali Melilotoidis, Herba Agrimoniae, Radix Sanguisorbae, Pericarpium Zanthoxyli, Cortex cinnamomi japonici (Ramulus Cinnamomi), Cortex Phellodendri and the Rhizoma Atractylodis Macrocephalae jointly being put in cellar, the temperature keeping cellar is 40 ~ 45 DEG C, takes out standby after placing 5 ~ 7 days；
(2) with clear water to step (1) process after composition be rinsed, dry standby；
(3) Semen Momordicae, Pericarpium Zanthoxyli and Cortex cinnamomi japonici (Ramulus Cinnamomi) are put into jointly fill fry sand marmite in, heating keep temperature be 100 ~ 105 DEG C, constantly stir-fry, take out after 15 ~ 18min parch medicine A is standby；
(4) Herba Astragali Melilotoidis, Cortex Phellodendri and the Rhizoma Atractylodis Macrocephalae are put in the marmite filling Testa Tritici jointly, heating keep temperature be 95 ~ 100 DEG C, constantly stir-fry, take out after 10 ~ 15min parch medicine B is standby；
(5) Folium olive, Folium Meliae, Herba Agrimoniae, Radix Sanguisorbae and parch medicine A, parch medicine B are mixed jointly, after pulverizing, cross 60 mesh, be then placed in the ethanol solution that mass fraction is 75% of its gross mass 3 times circulating extraction 20 ~ 24h, obtain extracting solution standby；
(6) by common with modified starch solution for the extracting solution of step (5) gained mix homogeneously get product.
Comparative example 1
Compared with Example 1, in addition to not containing modified starch solution, remaining method step is the most identical for this comparative example 1.
Matched group
Commercially available common pesticide.
In order to contrast using effect of the present invention, selecting the experimental plot that three pieces of conditions are identical and suitable, in experimental plot, plantation is all four ages " Teng Nian " grape variety, carries out pest management with above-mentioned three kinds of pesticide respectively, and following table is corresponding correction data:
| Embodiment 1 | Comparative example 1 | Matched group | |
| Fructus Vitis viniferae per mu yield (kg) | 4010 | 3900 | 3500 |
| Fructus Vitis viniferae no seed rate (%) | 15.7 | 8.6 | 0.5 |
| Every hectogram edible portion Vitamin C content (mg) | 42 | 37 | 26 |
| Bitter rot or anthracnose of grape cure rate (%) | 92.7 | 89.3 | 88.6 |
| Downy mildew of garpe cure rate (%) | 91.8 | 85.4 | 92.5 |
| Fructus Vitis viniferae maize ear rot cure rate (%) | 93.6 | 89.7 | 94.3 |
As can be seen from the above table, pesticide of the present invention can well promote the yield and quality of Fructus Vitis viniferae, the no seed rate of Fructus Vitis viniferae can be increased again, eliminate people and tell the trouble of seed, improve the edible impression of people, in addition, its to the cure rate of Fructus Vitis viniferae commonly encountered diseases compared with tradition pesticide, effect is very nearly the same, but has the advantage of safe noresidue, and life-time service will not develop immunity to drugs again；And it being not added with a group of modified starch solution, its effect is compared pesticide of the present invention in every respect and has been declined.
Claims (4)
1. a Folium olive mattae source pesticide, it is characterised in that be made up of the material of following weight portion:
12 parts of Folium olive, 6 parts of Semen Momordicaes, 8 parts of Folium Meliaes, 4 parts of Herba Astragali Melilotoidiss, 5 parts of Herba Agrimoniaes, 3 parts of Radix Sanguisorbaes, 4 parts of Pericarpium Zanthoxylies, 4 parts of Cortex cinnamomi japonici (Ramulus Cinnamomi)s, 7 parts of Cortex Phellodendris, 5 parts of Rhizoma Atractylodis Macrocephalaes, 4 parts of modified starch solutions；Described modified starch solution is made up of the material of following weight portion: 30 parts of starch, 3 parts of modified alta-muds, 0.2 part of dodecylbenzene sodium sulfonate, 0.3 part of Span, 0.6 part of Butylated hydroxyanisole, 1 part of vitamin C, 0.5 part of chitin, 1 part of citric acid, 0.5 part of xylitol.
A kind of Folium olive mattae source pesticide the most according to claim 1, it is characterized in that, described method for preparing modified bentonite is: bentonite is first put into soaking and washing 20min in the hydrochloric acid solution that mass fraction is 5%, putting into calcining 2h under 780 DEG C of environment after taking-up, being crushed to granular size with ball mill after taking-up is 400 ~ 500 mesh.
A kind of Folium olive mattae source pesticide the most according to claim 1, it is characterised in that the preparation method of described modified starch solution is:
(1) jointly being mixed by the clear water of starch with its gross mass 2.5 times, heating keeps water temperature to be 80 ~ 88 DEG C, obtains solution A standby after gelatinizing 30 ~ 40min, and period is stirred continuously；
(2) clear water of modified alta-mud with its quality 3 times is mixed jointly, heating keeps water temperature to be 40 ~ 45 DEG C, add dodecylbenzene sodium sulfonate, Span and Butylated hydroxyanisole, after mix and blend 15min, again vitamin C, chitin, citric acid and xylitol are added, continue stirring 15min, obtain solution B standby；
(3) temperature keeping solution B is 40 ~ 45 DEG C, and the temperature keeping solution A is 80 ~ 88 DEG C, solution B is joined in solution A, and is stirred with the rotating speed of 300 ~ 350 turns/min, and, composition constant until solution temperature i.e. obtains modified starch solution after being uniformly dispersed.
4. the preparation method of a Folium olive mattae source pesticide as claimed in claim 1, it is characterised in that comprise the steps:
(1) Folium olive, Semen Momordicae, Folium Meliae, Herba Astragali Melilotoidis, Herba Agrimoniae, Radix Sanguisorbae, Pericarpium Zanthoxyli, Cortex cinnamomi japonici (Ramulus Cinnamomi), Cortex Phellodendri and the Rhizoma Atractylodis Macrocephalae jointly being put in cellar, the temperature keeping cellar is 40 ~ 45 DEG C, takes out standby after placing 5 ~ 7 days；
(2) with clear water to step (1) process after composition be rinsed, dry standby；
(3) Semen Momordicae, Pericarpium Zanthoxyli and Cortex cinnamomi japonici (Ramulus Cinnamomi) are put into jointly fill fry sand marmite in, heating keep temperature be 100 ~ 105 DEG C, constantly stir-fry, take out after 15 ~ 18min parch medicine A is standby；
(4) Herba Astragali Melilotoidis, Cortex Phellodendri and the Rhizoma Atractylodis Macrocephalae are put in the marmite filling Testa Tritici jointly, heating keep temperature be 95 ~ 100 DEG C, constantly stir-fry, take out after 10 ~ 15min parch medicine B is standby；
(5) Folium olive, Folium Meliae, Herba Agrimoniae, Radix Sanguisorbae and parch medicine A, parch medicine B are mixed jointly, after pulverizing, cross 60 mesh, be then placed in the ethanol solution that mass fraction is 75% of its gross mass 3 times circulating extraction 20 ~ 24h, obtain extracting solution standby；
(6) by common with modified starch solution for the extracting solution of step (5) gained mix homogeneously get product.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201610430600.0A CN105994422A (en) | 2016-06-17 | 2016-06-17 | Olive leaf and grape botanical pesticide |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201610430600.0A CN105994422A (en) | 2016-06-17 | 2016-06-17 | Olive leaf and grape botanical pesticide |
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| CN105994422A true CN105994422A (en) | 2016-10-12 |
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| CN201610430600.0A Pending CN105994422A (en) | 2016-06-17 | 2016-06-17 | Olive leaf and grape botanical pesticide |
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Application publication date: 20161012 |
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