CN105994000A - Dog-chewing gum and preparation method thereof - Google Patents
Dog-chewing gum and preparation method thereof Download PDFInfo
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- CN105994000A CN105994000A CN201610347886.6A CN201610347886A CN105994000A CN 105994000 A CN105994000 A CN 105994000A CN 201610347886 A CN201610347886 A CN 201610347886A CN 105994000 A CN105994000 A CN 105994000A
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- powder
- bone
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- 238000002360 preparation method Methods 0.000 title claims description 29
- 229940112822 chewing gum Drugs 0.000 title abstract 5
- 239000002994 raw material Substances 0.000 claims abstract description 47
- 239000000843 powder Substances 0.000 claims abstract description 36
- UIIMBOGNXHQVGW-UHFFFAOYSA-M Sodium bicarbonate Chemical compound [Na+].OC([O-])=O UIIMBOGNXHQVGW-UHFFFAOYSA-M 0.000 claims abstract description 32
- 210000000988 bone and bone Anatomy 0.000 claims abstract description 31
- 239000000654 additive Substances 0.000 claims abstract description 28
- 239000003795 chemical substances by application Substances 0.000 claims abstract description 26
- 239000002699 waste material Substances 0.000 claims abstract description 21
- 239000010985 leather Substances 0.000 claims abstract description 18
- 235000012054 meals Nutrition 0.000 claims abstract description 18
- 229910000030 sodium bicarbonate Inorganic materials 0.000 claims abstract description 16
- 235000017557 sodium bicarbonate Nutrition 0.000 claims abstract description 16
- 239000005060 rubber Substances 0.000 claims abstract description 14
- 240000004808 Saccharomyces cerevisiae Species 0.000 claims abstract description 12
- 229920002472 Starch Polymers 0.000 claims abstract description 12
- 239000012752 auxiliary agent Substances 0.000 claims abstract description 12
- 235000013372 meat Nutrition 0.000 claims abstract description 12
- 235000019698 starch Nutrition 0.000 claims abstract description 12
- 239000008107 starch Substances 0.000 claims abstract description 12
- 235000013343 vitamin Nutrition 0.000 claims abstract description 12
- 239000011782 vitamin Substances 0.000 claims abstract description 12
- 229940088594 vitamin Drugs 0.000 claims abstract description 12
- 229930003231 vitamin Natural products 0.000 claims abstract description 12
- 150000003722 vitamin derivatives Chemical class 0.000 claims abstract description 12
- 241001465754 Metazoa Species 0.000 claims abstract description 11
- 239000004280 Sodium formate Substances 0.000 claims abstract description 11
- 229920003063 hydroxymethyl cellulose Polymers 0.000 claims abstract description 11
- 229940031574 hydroxymethyl cellulose Drugs 0.000 claims abstract description 11
- 235000013336 milk Nutrition 0.000 claims abstract description 11
- 239000008267 milk Substances 0.000 claims abstract description 11
- 210000004080 milk Anatomy 0.000 claims abstract description 11
- HLBBKKJFGFRGMU-UHFFFAOYSA-M sodium formate Chemical compound [Na+].[O-]C=O HLBBKKJFGFRGMU-UHFFFAOYSA-M 0.000 claims abstract description 11
- 235000019254 sodium formate Nutrition 0.000 claims abstract description 11
- 244000025254 Cannabis sativa Species 0.000 claims abstract description 7
- 239000004033 plastic Substances 0.000 claims abstract description 7
- OKKJLVBELUTLKV-UHFFFAOYSA-N Methanol Chemical compound OC OKKJLVBELUTLKV-UHFFFAOYSA-N 0.000 claims description 42
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 35
- CSCPPACGZOOCGX-UHFFFAOYSA-N Acetone Chemical compound CC(C)=O CSCPPACGZOOCGX-UHFFFAOYSA-N 0.000 claims description 34
- 235000015111 chews Nutrition 0.000 claims description 34
- RTZKZFJDLAIYFH-UHFFFAOYSA-N Diethyl ether Chemical compound CCOCC RTZKZFJDLAIYFH-UHFFFAOYSA-N 0.000 claims description 28
- 230000000996 additive effect Effects 0.000 claims description 26
- 210000002745 epiphysis Anatomy 0.000 claims description 21
- 239000002671 adjuvant Substances 0.000 claims description 20
- 238000000605 extraction Methods 0.000 claims description 20
- HEDRZPFGACZZDS-UHFFFAOYSA-N Chloroform Chemical compound ClC(Cl)Cl HEDRZPFGACZZDS-UHFFFAOYSA-N 0.000 claims description 18
- 238000000034 method Methods 0.000 claims description 13
- 239000010775 animal oil Substances 0.000 claims description 10
- 229940036811 bone meal Drugs 0.000 claims description 10
- 239000002374 bone meal Substances 0.000 claims description 10
- VNWKTOKETHGBQD-UHFFFAOYSA-N methane Chemical compound C VNWKTOKETHGBQD-UHFFFAOYSA-N 0.000 claims description 10
- 239000002904 solvent Substances 0.000 claims description 10
- 238000003756 stirring Methods 0.000 claims description 10
- 238000005406 washing Methods 0.000 claims description 10
- 229920001592 potato starch Polymers 0.000 claims description 8
- 238000000944 Soxhlet extraction Methods 0.000 claims description 7
- 238000000465 moulding Methods 0.000 claims description 7
- 229920001661 Chitosan Polymers 0.000 claims description 6
- 238000001035 drying Methods 0.000 claims description 6
- 238000007493 shaping process Methods 0.000 claims description 6
- 230000001954 sterilising effect Effects 0.000 claims description 6
- 238000004659 sterilization and disinfection Methods 0.000 claims description 6
- 230000005611 electricity Effects 0.000 claims description 5
- 239000003292 glue Substances 0.000 claims description 5
- 239000000463 material Substances 0.000 abstract description 7
- 239000000126 substance Substances 0.000 abstract description 5
- 238000004519 manufacturing process Methods 0.000 abstract description 3
- 235000019737 Animal fat Nutrition 0.000 abstract 1
- 241000282472 Canis lupus familiaris Species 0.000 abstract 1
- 244000061456 Solanum tuberosum Species 0.000 abstract 1
- 235000002595 Solanum tuberosum Nutrition 0.000 abstract 1
- 230000036528 appetite Effects 0.000 abstract 1
- 235000019789 appetite Nutrition 0.000 abstract 1
- RQFQJYYMBWVMQG-IXDPLRRUSA-N chitotriose Chemical compound O[C@@H]1[C@@H](N)[C@H](O)O[C@H](CO)[C@H]1O[C@H]1[C@H](N)[C@@H](O)[C@H](O[C@H]2[C@@H]([C@@H](O)[C@H](O)[C@@H](CO)O2)N)[C@@H](CO)O1 RQFQJYYMBWVMQG-IXDPLRRUSA-N 0.000 abstract 1
- 235000021190 leftovers Nutrition 0.000 abstract 1
- 239000000203 mixture Substances 0.000 abstract 1
- 238000001514 detection method Methods 0.000 description 9
- -1 Phthalic acid ester Chemical group 0.000 description 7
- VLKZOEOYAKHREP-UHFFFAOYSA-N n-Hexane Chemical compound CCCCCC VLKZOEOYAKHREP-UHFFFAOYSA-N 0.000 description 5
- XNGIFLGASWRNHJ-UHFFFAOYSA-N o-dicarboxybenzene Natural products OC(=O)C1=CC=CC=C1C(O)=O XNGIFLGASWRNHJ-UHFFFAOYSA-N 0.000 description 4
- 238000010586 diagram Methods 0.000 description 3
- 241000283690 Bos taurus Species 0.000 description 2
- 239000004803 Di-2ethylhexylphthalate Substances 0.000 description 2
- NIPNSKYNPDTRPC-UHFFFAOYSA-N N-[2-oxo-2-(2,4,6,7-tetrahydrotriazolo[4,5-c]pyridin-5-yl)ethyl]-2-[[3-(trifluoromethoxy)phenyl]methylamino]pyrimidine-5-carboxamide Chemical compound O=C(CNC(=O)C=1C=NC(=NC=1)NCC1=CC(=CC=C1)OC(F)(F)F)N1CC2=C(CC1)NN=N2 NIPNSKYNPDTRPC-UHFFFAOYSA-N 0.000 description 2
- BJQHLKABXJIVAM-UHFFFAOYSA-N bis(2-ethylhexyl) phthalate Chemical group CCCCC(CC)COC(=O)C1=CC=CC=C1C(=O)OCC(CC)CCCC BJQHLKABXJIVAM-UHFFFAOYSA-N 0.000 description 2
- 230000000052 comparative effect Effects 0.000 description 2
- 230000000694 effects Effects 0.000 description 2
- 238000005516 engineering process Methods 0.000 description 2
- 238000002474 experimental method Methods 0.000 description 2
- 235000015097 nutrients Nutrition 0.000 description 2
- 239000013502 plastic waste Substances 0.000 description 2
- 239000002910 solid waste Substances 0.000 description 2
- 235000019750 Crude protein Nutrition 0.000 description 1
- 235000007688 Lycopersicon esculentum Nutrition 0.000 description 1
- 240000003768 Solanum lycopersicum Species 0.000 description 1
- 230000015572 biosynthetic process Effects 0.000 description 1
- 238000010411 cooking Methods 0.000 description 1
- 239000000284 extract Substances 0.000 description 1
- 238000000227 grinding Methods 0.000 description 1
- 238000007654 immersion Methods 0.000 description 1
- 210000000987 immune system Anatomy 0.000 description 1
- 238000007689 inspection Methods 0.000 description 1
- 210000003734 kidney Anatomy 0.000 description 1
- 238000002372 labelling Methods 0.000 description 1
- 210000004185 liver Anatomy 0.000 description 1
- 210000000653 nervous system Anatomy 0.000 description 1
- 235000016709 nutrition Nutrition 0.000 description 1
- 210000000056 organ Anatomy 0.000 description 1
- XNGIFLGASWRNHJ-UHFFFAOYSA-L phthalate(2-) Chemical compound [O-]C(=O)C1=CC=CC=C1C([O-])=O XNGIFLGASWRNHJ-UHFFFAOYSA-L 0.000 description 1
- 239000004014 plasticizer Substances 0.000 description 1
- 230000001737 promoting effect Effects 0.000 description 1
- 210000004994 reproductive system Anatomy 0.000 description 1
- 210000000952 spleen Anatomy 0.000 description 1
Classifications
-
- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01K—ANIMAL HUSBANDRY; AVICULTURE; APICULTURE; PISCICULTURE; FISHING; REARING OR BREEDING ANIMALS, NOT OTHERWISE PROVIDED FOR; NEW BREEDS OF ANIMALS
- A01K15/00—Devices for taming animals, e.g. nose-rings or hobbles; Devices for overturning animals in general; Training or exercising equipment; Covering boxes
- A01K15/02—Training or exercising equipment, e.g. mazes or labyrinths for animals ; Electric shock devices ; Toys specially adapted for animals
- A01K15/025—Toys specially adapted for animals
- A01K15/026—Chewable toys, e.g. for dental care of pets
Landscapes
- Life Sciences & Earth Sciences (AREA)
- Health & Medical Sciences (AREA)
- Environmental Sciences (AREA)
- Dentistry (AREA)
- General Health & Medical Sciences (AREA)
- Physical Education & Sports Medicine (AREA)
- Animal Behavior & Ethology (AREA)
- Zoology (AREA)
- Animal Husbandry (AREA)
- Biodiversity & Conservation Biology (AREA)
- Fodder In General (AREA)
- Feed For Specific Animals (AREA)
Abstract
The invention provides a dog-chewing gum. The dog-chewing gum comprises the following prepared components in parts by weight: 15 to 40 parts of a raw material, 15 to 25 parts of an auxiliary material, 30 to 45 parts of an addition material and 2 to 5 parts of auxiliary agents, wherein the raw material is one or more selected from the group consisting of leftovers of fresh animal skin, waste leather, waste rubber and waste plastic; the auxiliary material is one or more selected from the group consisting of meat paste, bone powder, shell powder, potato powder and grass meal; the addition material is one or more selected from the group consisting of milk powder, animal fat, starch, hydroxymethyl cellulose, yeast powder, chitosan oligosaccharide and vitamin powder; and the auxiliary agents comprise a chrome-free tanning agent, sodium formate and sodium bicarbonate. The dog-chewing gum provided by the invention is simple in composition and convenient to manufacture; the obtained dog-chewing gum has low content of harmful substances; and functional and flavorful additives are contained, so the requirements of appetite and body of dogs can be met.
Description
Technical field:
The present invention relates to technical field of pet articles, be specifically related to a kind of dog chews and preparation method thereof.
Background technology:
Along with economic growth and the raising of people's living standard, house pet industry has obtained swift and violent discovery,
People's pet feeding has been transformed into a kind of sustenance of people's spirit by simple admiring, and the role of house pet is also
Quietly occur to change, be increasingly becoming companion and the friend of people's life, promoting that harmonious society is sent out
Exhibition plays irreplaceable regulation effect.Therefore, pet supplies industry nowadays its people in economy
Play the most important effect.
As a example by pet toy-dog chews；In prior art, Chinese patent application CN 104472902 A
Disclosing a kind of method that broken Corii Bovis seu Bubali makes pet dog chew, its manufacturing process includes: by Corii Bovis seu Bubali leftover bits and pieces
It is put in 30 DEG C of water-baths immersion；Then rub with meat grinder；Pull an oar with cooking machine again；Serosity is done
Dry；Inject grinding tool；Drying and shaping；Sterilization, although this technology effectively make use of leather leftover pieces, but
It is the failure to other functional or taste additives, does not also use rubber or leather dead meal.
For another example Chinese patent application CN 105409811 A discloses a kind of dog chews rubber and preparation side thereof
Method.This dog chews skin is made up of Os Bovis seu Bubali, starch, tomato wine, Adeps Bovis seu Bubali, rumen-undegraded fat.And for example China
Patent application CN 105409812 A dog chews and the method making this dog chews, including two layers of cattle
Skin, two layers of Corii Bovis seu Bubali have widthwise edge and the longitudinal edge intersected with widthwise edge, if described two layers of Corii Bovis seu Bubali offer
The dry opening that inweaves, described some openings that inweave parallel with widthwise edge, described in inweave opening by two layers of cattle
Skin is divided into some horizontal woven stripes, described in inweave opening in be equipped with some Thallus Laminariae (Thallus Eckloniae) bars, described Thallus Laminariae (Thallus Eckloniae) bar with
Horizontal woven stripe staggered interting constitutes edible body, described dog chews by edible body along two layers of Corii Bovis seu Bubali arbitrarily
Roll formation cylindrical shape body, and be formed by knots tied at cylindrical shape body two ends.Although both prior aries
Increase functional or taste additive, firmly get dog class and like, but, in its preparation process, nuisance
Matter is more, such as, in toy material, many enterprises, in order to cost-effective, use waste material, feed back (leather
Waste material or rubber scrap) and add phthalate plasticizers increase pliability and glossiness, thus adjacent
Phthalic acid ester use face in toy material is widely.Owing to phthalic acid ester can have a strong impact on
To human reproductive systems, immune system and nervous system, and threaten the existence of the mankind, particularly to place
The organ such as liver,spleen,kidney in the child of growth stage has infringement, the most a lot of countries and regions pair
In toy, the content of phthalic acid ester is all limited.
For solving the problem that in pet toy, phthalic acid ester content is high, Chinese patent CN
The extracting process of phthalate compound and inspection in leather toy material disclosed in 104251789 A
Survey method, the method includes: uses normal hexane to mix as solvent with acetone using 1:1 volume ratio, uses
The mode of soxhlet extraction extracts.The temperature of soxhlet extraction is at 120-150 DEG C, and extraction time is at 6-8
In hour.The present invention is based on above-mentioned prior art, it is desirable to provide a kind of proportioning is simple, easy to make, institute
Obtain product nuisance content low, there is functional and taste additive, it is possible to meet dog class oral erotism and body
Needed for body, and the epiphysis position a kind of dog chews that can be socketed gum cover of dog chews and preparation method thereof.
Summary of the invention:
It is an object of the invention to overcome shortcoming present in prior art, it is provided that a kind of proportioning is simple, system
Facilitating, products obtained therefrom nuisance content is low, has functional and taste additive, it is possible to meet dog
Needed for class oral erotism and health, and the epiphysis position of dog chews can be socketed a kind of dog chews and the preparation thereof of gum cover
Method.
To achieve these goals, the invention provides a kind of dog chews, wherein, join including unit of weight
The following component of system:
Raw material: 15-40 part,
Adjuvant: 15-25 part,
Additive: 30-45 part,
Auxiliary agent: 2-5 part,
Described raw material is: the leftover bits and pieces of the new Cortex Dictamni of animal, and discarded leather, waste rubber, in waste plastic
Any one or a few；
Described adjuvant is: meat paste, bone meal, conch meal, potato starch, any one or a few in grass meal；
Described additive is: milk powder, animal oil, starch, hydroxymethyl cellulose, yeast powder, and shell is few
Sugar, any one or a few in vitamin powder；
Described auxiliary agent is: chrome-free tanning agent, sodium formate, sodium bicarbonate.
The leftover bits and pieces of the new Cortex Dictamni of animal, discarded leather, waste rubber, the weight ratio of waste plastic is 7-20:
3-12:0-6:0-2.
Meat paste, bone meal, conch meal, potato starch, the weight ratio of grass meal is 4-10:3-8:2-5:0-1:0-1.
Milk powder, animal oil, starch, hydroxymethyl cellulose, yeast powder, oligochitosan, vitamin powder
Weight ratio is,
4-8:2-5:10-25:1-3:1-3:0.2-0.5:0.2-0.5。
The preparation method of dog chews, wherein, comprises the steps:
A, by raw material enter 10 times of mass fractions water in, soak 10-20 hour；
Adding deliming agent in B, water, deliming agent is 4:1000 with the mass ratio of water, after step A being soaked
Raw material add and be dissolved with in the water of deliming agent；Water temperature 30-35 degree Celsius, controlling pH value is 8, deliming
1-2 hour time；Adding chrome-free tanning agent 1-3 part, rotary drum turns 120-200 minute；Add sodium formate 0.5-1 again
Part, rotary drum turns 20-40 minute；Adding sodium bicarbonate 0.5-1 part, sodium bicarbonate is opened by 10 times of mass fraction aquations,
Add rotary drum to rotate 40-60 minute；
Raw material after C, step B deliming is washed through warm water, washing time 0.5-1 hour；
D, being rubbed by the raw material after washing, solvent selects chloroform, ether, acetone and methanol, makes
The nuisance in raw material after rubbing with Soxhlet extraction method extraction, temperature 150 DEG C, time 6h, trichlorine
Methane, ether, acetone, the mass ratio of methanol are 1:2:0.8:1.5；
E, adjuvant and additive are added in the raw material after the extraction of step D, add adjuvant, additive,
The water of the 1.2-1.5 mass multiple of the gross weight of the raw material after extraction, stirring becomes serosity；Serosity is at 60-80
DEG C, vacuum is to be evaporated under reduced pressure by motor stirrer stirring under conditions of 0.01-0.09MPa, electricity
Power agitator speed is 450-550 rev/min；
F, step E gains inject in mould, drying and shaping again after molding, dry temperature 40-60 and take the photograph
Family name's degree, humidity 15-20%；
G, wet sterilization 3 hours, vapor (steam) temperature 75-100 degree Celsius.
Step F injects formed in mould step, particularly as follows: it is bar-shaped and/or be shaped to gum cover shape to be shaped to bone.
Prepare gained bone club shaped structure and include that bone rod, the integrated preparation in two ends of bone rod have epiphysis, prepare institute
Obtaining glue sleeve-like structure and include gum cover, on gum cover, integrated preparation has running-on, and running-on can be socketed in bone
On end and then make gum cover be wrapped on the outer wall of epiphysis.
Advantages of the present invention is: proportioning is simple, and easy to make, products obtained therefrom nuisance content is low, has
Functional and taste additive, it is possible to needed for meeting dog class oral erotism and health, and the epiphysis position of dog chews
Put and can be socketed gum cover.Particularly as follows:
1, the present invention effectively utilizes fresh leather-solid waste, and further with leather waste, rubber and
Plastic waste.
2, the present invention there was added the nutrient substance benefiting dog class health and the interpolation increasing oral erotism in serosity
Thing, it is possible to needed for meeting dog class oral erotism and health.
3, the harmful substance (phthalate compound) in dog chews is reduced by extraction mode,
Reduce pet toy harmfulness.
4, finished product does skeletonization rod moulding, and dog chews preparation can be used in gum cover to be socketed in bone stick end,
Effectively extend product useful life.
Accompanying drawing illustrates:
Fig. 1 is the production procedure schematic diagram of the present invention.
Fig. 2 is the bone club shaped structure schematic diagram after the present invention shapes.
Fig. 3 is for being socketed the gum cover structural representation of epiphysis after the present invention shapes.
Accompanying drawing identifies:
1, bone rod 2, epiphysis 3, running-on
4, gum cover
Detailed description of the invention:
Below in conjunction with the accompanying drawings, the present invention will be described.As Figure 1-3, Fig. 1 is the life of the present invention
Produce schematic flow sheet.Fig. 2 is the bone club shaped structure schematic diagram after the present invention shapes.Fig. 3 is that the present invention is fixed
For being socketed the gum cover structural representation of epiphysis after type.
Example 1, dog chews, wherein, including the following component of unit of weight preparation:
Raw material: 40 parts,
Adjuvant: 25 parts,
Additive: 45 parts,
Auxiliary agent: 5 parts,
Described raw material is: the leftover bits and pieces of the new Cortex Dictamni of animal, discarded leather, waste rubber, waste plastic；
Described adjuvant is: meat paste, bone meal, conch meal, potato starch, grass meal；
Described additive is: milk powder, animal oil, starch, hydroxymethyl cellulose, yeast powder, and shell is few
Sugar, vitamin powder；
Described auxiliary agent is: chrome-free tanning agent 1-3 part, sodium formate 0.5-1 part, sodium bicarbonate 0.5-1 part.
The leftover bits and pieces of the new Cortex Dictamni of animal, discarded leather, waste rubber, the weight ratio of waste plastic is 20:
12:6:2.
Meat paste, bone meal, conch meal, potato starch, the weight ratio of grass meal is 10:8:5:1:1.
Milk powder, animal oil, starch, hydroxymethyl cellulose, yeast powder, oligochitosan, vitamin powder
Weight ratio is, 8:5:25:3:3:0.5:0.5.
The preparation method of dog chews, wherein, comprises the steps:
A, by raw material enter 10 times of mass fractions water in, soak 10-20 hour；
Adding deliming agent in B, water, deliming agent is 4:1000 with the mass ratio of water, after step A being soaked
Raw material add and be dissolved with in the water of deliming agent；Water temperature 30-35 degree Celsius, controlling pH value is 8, deliming
1-2 hour time；Adding chrome-free tanning agent 1-3 part, rotary drum turns 120-200 minute；Add sodium formate 0.5-1 again
Part, rotary drum turns 20-40 minute；Adding sodium bicarbonate 0.5-1 part, sodium bicarbonate is opened by 10 times of mass fraction aquations,
Add rotary drum to rotate 40-60 minute；
Raw material after C, step B deliming is washed through warm water, washing time 0.5-1 hour；
D, being rubbed by the raw material after washing, solvent selects chloroform, ether, acetone and methanol, makes
The nuisance in raw material after rubbing with Soxhlet extraction method extraction, temperature 150 DEG C, time 6h, trichlorine
Methane, ether, acetone, the mass ratio of methanol are 1:2:0.8:1.5；
E, adjuvant and additive are added in the raw material after the extraction of step D, add adjuvant, additive,
The water of the 1.2-1.5 mass multiple of the gross weight of the raw material after extraction, stirring becomes serosity；Serosity is at 60-80
DEG C, vacuum is to be evaporated under reduced pressure by motor stirrer stirring under conditions of 0.01-0.09MPa, electricity
Power agitator speed is 450-550 rev/min；
F, step E gains inject in mould, drying and shaping again after molding, dry temperature 40-60 and take the photograph
Family name's degree, humidity 15-20%；
G, wet sterilization 3 hours, vapor (steam) temperature 75-100 degree Celsius.
Step F injects formed in mould step, particularly as follows: it is bar-shaped and/or be shaped to gum cover shape to be shaped to bone.
Preparing gained bone club shaped structure and include bone rod 1, the integrated preparation in two ends of bone rod 1 has epiphysis 2,
Preparing gained glue sleeve-like structure and include gum cover 4, on gum cover 4, integrated preparation has running-on 3, running-on 3
Can be socketed on epiphysis 2 and then make gum cover 4 to be wrapped on the outer wall of epiphysis 2.
Example 2, dog chews, wherein, including the following component of unit of weight preparation:
Raw material: 20 parts,
Adjuvant: 18 parts,
Additive: 32 parts,
Auxiliary agent: 3 parts,
Described raw material is: the leftover bits and pieces of the new Cortex Dictamni of animal, discarded leather, waste rubber；
Described adjuvant is: meat paste, bone meal, conch meal, potato starch；
Described additive is: milk powder, animal oil, starch, hydroxymethyl cellulose, yeast powder, and shell is few
Sugar, vitamin powder；
Described auxiliary agent is: chrome-free tanning agent 1-3 part, sodium formate 0.5-1 part, sodium bicarbonate 0.5-1 part.
The leftover bits and pieces of the new Cortex Dictamni of animal, discarded leather, the weight ratio of waste rubber is 10:6:4.
Meat paste, bone meal, conch meal, potato starch weight ratio is 8:6:3:1.
Milk powder, animal oil, starch, hydroxymethyl cellulose, yeast powder, oligochitosan, vitamin powder
Weight ratio is, 5:2:22:1:1:0.5:0.5.
The preparation method of dog chews, wherein, comprises the steps:
A, by raw material enter 10 times of mass fractions water in, soak 10-20 hour；
Adding deliming agent in B, water, deliming agent is 4:1000 with the mass ratio of water, after step A being soaked
Raw material add and be dissolved with in the water of deliming agent；Water temperature 30-35 degree Celsius, controlling pH value is 8, deliming
1-2 hour time；Adding chrome-free tanning agent 1-3 part, rotary drum turns 120-200 minute；Add sodium formate 0.5-1 again
Part, rotary drum turns 20-40 minute；Adding sodium bicarbonate 0.5-1 part, sodium bicarbonate is opened by 10 times of mass fraction aquations,
Add rotary drum to rotate 40-60 minute；
Raw material after C, step B deliming is washed through warm water, washing time 0.5-1 hour；
D, being rubbed by the raw material after washing, solvent selects chloroform, ether, acetone and methanol, makes
The nuisance in raw material after rubbing with Soxhlet extraction method extraction, temperature 150 DEG C, time 6h, trichlorine
Methane, ether, acetone, the mass ratio of methanol are 1:2:0.8:1.5；
E, adjuvant and additive are added in the raw material after the extraction of step D, add adjuvant, additive,
The water of the 1.2-1.5 mass multiple of the gross weight of the raw material after extraction, stirring becomes serosity；Serosity is at 60-80
DEG C, vacuum is to be evaporated under reduced pressure by motor stirrer stirring under conditions of 0.01-0.09MPa, electricity
Power agitator speed is 450-550 rev/min；
F, step E gains inject in mould, drying and shaping again after molding, dry temperature 40-60 and take the photograph
Family name's degree, humidity 15-20%；
G, wet sterilization 3 hours, vapor (steam) temperature 75-100 degree Celsius.
Step F injects formed in mould step, particularly as follows: it is bar-shaped and/or be shaped to gum cover shape to be shaped to bone.
Prepare gained bone club shaped structure and include that bone rod, the integrated preparation in two ends of bone rod have epiphysis, prepare institute
Obtaining glue sleeve-like structure and include gum cover, on gum cover, integrated preparation has running-on, and running-on can be socketed in bone
On end and then make gum cover be wrapped on the outer wall of epiphysis.
Example 3, dog chews, wherein, including the following component of unit of weight preparation:
Raw material: 18 parts,
Adjuvant: 20 parts,
Additive: 35 parts,
Auxiliary agent: 2-5 part,
Described raw material is: the leftover bits and pieces of the new Cortex Dictamni of animal, discarded leather；
Described adjuvant is: meat paste, bone meal, conch meal；
Described additive is: milk powder, animal oil, starch, hydroxymethyl cellulose, yeast powder, and shell is few
Sugar, vitamin powder；
Described auxiliary agent is: chrome-free tanning agent 1-3 part, sodium formate 0.5-1 part, sodium bicarbonate 0.5-1 part..
The leftover bits and pieces of the new Cortex Dictamni of animal, the weight ratio of discarded leather is 11:7.
Meat paste, bone meal, conch meal weight ratio is 10:5:5.
Milk powder, animal oil, starch, hydroxymethyl cellulose, yeast powder, oligochitosan, vitamin powder
Weight ratio is, 6:4:20:2:2:0.5:0.5.
The preparation method of dog chews, wherein, comprises the steps:
A, by raw material enter 10 times of mass fractions water in, soak 10-20 hour；
Adding deliming agent in B, water, deliming agent is 4:1000 with the mass ratio of water, after step A being soaked
Raw material add and be dissolved with in the water of deliming agent；Water temperature 30-35 degree Celsius, controlling pH value is 8, deliming
1-2 hour time；Adding chrome-free tanning agent 1-3 part, rotary drum turns 120-200 minute；Add sodium formate 0.5-1 again
Part, rotary drum turns 20-40 minute；Adding sodium bicarbonate 0.5-1 part, sodium bicarbonate is opened by 10 times of mass fraction aquations,
Add rotary drum to rotate 40-60 minute；
Raw material after C, step B deliming is washed through warm water, washing time 0.5-1 hour；
D, being rubbed by the raw material after washing, solvent selects chloroform, ether, acetone and methanol, makes
The nuisance in raw material after rubbing with Soxhlet extraction method extraction, temperature 150 DEG C, time 6h, trichlorine
Methane, ether, acetone, the mass ratio of methanol are 1:2:0.8:1.5；
E, adjuvant and additive are added in the raw material after the extraction of step D, add adjuvant, additive,
The water of the 1.2-1.5 mass multiple of the gross weight of the raw material after extraction, stirring becomes serosity；Serosity is at 60-80
DEG C, vacuum is to be evaporated under reduced pressure by motor stirrer stirring under conditions of 0.01-0.09MPa, electricity
Power agitator speed is 450-550 rev/min；
F, step E gains inject in mould, drying and shaping again after molding, dry temperature 40-60 and take the photograph
Family name's degree, humidity 15-20%；
G, wet sterilization 3 hours, vapor (steam) temperature 75-100 degree Celsius.
Step F injects formed in mould step, particularly as follows: it is bar-shaped and/or be shaped to gum cover shape to be shaped to bone.
Prepare gained bone club shaped structure and include that bone rod, the integrated preparation in two ends of bone rod have epiphysis, prepare institute
Obtaining glue sleeve-like structure and include gum cover, on gum cover, integrated preparation has running-on, and running-on can be socketed in bone
On end and then make gum cover be wrapped on the outer wall of epiphysis.
Note: above-mentioned example 1-3, after bone rod two ends epiphysis is gnawed by dog class and breakage is occurred, it is possible to use
Gum cover is enclosed within the epiphysis of bone rod two ends, forms new dog chews.
Comparative experiments 1:
Example 1-3 of the present invention and prior art CN 104472902 A is contrasted nutritional labeling list
| Group | Crude protein content | Moisture | Yeast | Oligochitosan | Vitamin |
| Example 1 of the present invention | 86% | 10% | Detection | Detection | Detection |
| Example 2 of the present invention | 82% | 10% | Detection | Detection | Detection |
| Example 3 of the present invention | 84% | 11% | Detection | Detection | Detection |
| CN 104472902A | The highest by 80% | The highest by 8% | -- | -- | -- |
Comparative experiments 2:
Using surname extraction (150 DEG C, 6h), leather sample is DEHP content in different solvents proportioning
(mg/kg), contrast such as following table with prior art CN 104251789 A:
The solvent of the present invention uses chloroform, ether, acetone, the mass ratio of methanol to be 1:2:0.8:1.5；
Documents 1 uses solvent hexane: acetone 1:1.
| Group | Solvent | DEHP | Extraction time |
| Example 1 of the present invention | Chloroform, ether, acetone, methanol | 115.2 | 6h |
| Example 2 of the present invention | Chloroform, ether, acetone, methanol | 113.7 | 6h |
| Example 3 of the present invention | Chloroform, ether, acetone, methanol | 112.8 | 6h |
| CN 104251789A | Normal hexane, acetone | 108.0 | 6h |
Being contrasted by above-mentioned list, proportioning of the present invention is simple, easy to make, products obtained therefrom nuisance content
Low, there is functional and taste additive, it is possible to needed for meeting dog class oral erotism and health, and dog chews
Epiphysis position can be socketed gum cover.Particularly as follows: the present invention effectively utilizes fresh leather-solid waste, and enter one
Step make use of leather waste, rubber and plastic waste.The present invention there was added in serosity and benefits dog class health
Nutrient substance and increase the additive of oral erotism, it is possible to needed for meeting dog class oral erotism and health.By extraction
Mode reduces the harmful substance (phthalate compound) in dog chews, and reducing pet toy has
Evil property.Finished product does skeletonization rod moulding, and dog chews preparation can be used in gum cover to be socketed in bone stick end,
Effectively extend product useful life.
Claims (7)
1. a dog chews, it is characterised in that include the following component that unit of weight is prepared:
Raw material: 15-40 part,
Adjuvant: 15-25 part,
Additive: 30-45 part,
Auxiliary agent: 2-5 part,
Described raw material is: the leftover bits and pieces of the new Cortex Dictamni of animal, and discarded leather, waste rubber, in waste plastic
Any one or a few；
Described adjuvant is: meat paste, bone meal, conch meal, potato starch, any one or a few in grass meal；
Described additive is: milk powder, animal oil, starch, hydroxymethyl cellulose, yeast powder, and shell is few
Sugar, any one or a few in vitamin powder；
Described auxiliary agent is: chrome-free tanning agent, sodium formate, sodium bicarbonate.
Dog chews the most according to claim 1, it is characterised in that: the leftover bits and pieces of the new Cortex Dictamni of animal,
Discarded leather, waste rubber, the weight ratio of waste plastic is 7-20:3-12:0-6:0-2.
Dog chews the most according to claim 1, it is characterised in that: meat paste, bone meal, conch meal,
Potato starch, the weight ratio of grass meal is 4-10:3-8:2-5:0-1:0-1.
Dog chews the most according to claim 1, it is characterised in that: milk powder, animal oil, starch,
Hydroxymethyl cellulose, yeast powder, oligochitosan, the weight ratio of vitamin powder is,
4-8:2-5:10-25:1-3:1-3:0.2-0.5:0.2-0.5。
5. according to the preparation method of the arbitrary described dog chews of claim 1-4, it is characterised in that include as
Lower step:
A, by raw material enter 10 times of mass fractions water in, soak 10-20 hour；
Adding deliming agent in B, water, deliming agent is 4:1000 with the mass ratio of water, after step A being soaked
Raw material add and be dissolved with in the water of deliming agent；Water temperature 30-35 degree Celsius, controlling pH value is 8, deliming
1-2 hour time；Adding chrome-free tanning agent 1-3 part, rotary drum turns 120-200 minute；Add sodium formate 0.5-1 again
Part, rotary drum turns 20-40 minute；Adding sodium bicarbonate 0.5-1 part, sodium bicarbonate is opened by 10 times of mass fraction aquations,
Add rotary drum to rotate 40-60 minute；
Raw material after C, step B deliming is washed through warm water, washing time 0.5-1 hour；
D, being rubbed by the raw material after washing, solvent selects chloroform, ether, acetone and methanol, makes
The nuisance in raw material after rubbing with Soxhlet extraction method extraction, temperature 150 DEG C, time 6h, trichlorine
Methane, ether, acetone, the mass ratio of methanol are 1:2:0.8:1.5；
E, adjuvant and additive are added in the raw material after the extraction of step D, add adjuvant, additive,
The water of the 1.2-1.5 mass multiple of the gross weight of the raw material after extraction, stirring becomes serosity；Serosity is at 60-80
DEG C, vacuum is to be evaporated under reduced pressure by motor stirrer stirring under conditions of 0.01-0.09MPa, electricity
Power agitator speed is 450-550 rev/min；
F, step E gains inject in mould, drying and shaping again after molding, dry temperature 40-60 and take the photograph
Family name's degree, humidity 15-20%；
G, wet sterilization 3 hours, vapor (steam) temperature 75-100 degree Celsius.
The preparation method of dog chews the most according to claim 5, it is characterised in that step F is injected
Formed in mould step, particularly as follows: it is bar-shaped and/or be shaped to gum cover shape to be shaped to bone.
The preparation method of dog chews the most according to claim 6, it is characterised in that prepare gained bone
Club shaped structure includes that bone rod (1), the integrated preparation in two ends of bone rod (1) have epiphysis (2),
Preparing gained glue sleeve-like structure and include gum cover (4), the upper integrated preparation of gum cover (4) has running-on (3),
Running-on (3) can be socketed in epiphysis (2) above and then makes gum cover (4) be wrapped in the outer wall of epiphysis (2)
On.
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| CN106857300A (en) * | 2017-03-03 | 2017-06-20 | 苏美盛 | Dog chewing animal skin gum |
| CN107279546A (en) * | 2017-07-10 | 2017-10-24 | 青岛远飞宠物食品有限公司 | A kind of pet dog teeth grinding teeth and preparation method thereof |
| CN110972988A (en) * | 2019-12-23 | 2020-04-10 | 苏州锦华宠物用品有限公司 | Pet chew and preparation method thereof |
| CN114304384A (en) * | 2021-12-02 | 2022-04-12 | 石玲青 | Animal chew food and preparation method thereof |
| CN117770157A (en) * | 2023-12-29 | 2024-03-29 | 江苏多肯新材料有限公司 | Small dog chew and preparation method thereof |
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| CN117770157A (en) * | 2023-12-29 | 2024-03-29 | 江苏多肯新材料有限公司 | Small dog chew and preparation method thereof |
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|---|---|
| CN105994000B (en) | 2019-08-20 |
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