CN105969503A - 一种紫铜高温拉丝用拉丝油 - Google Patents

一种紫铜高温拉丝用拉丝油 Download PDF

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CN105969503A
CN105969503A CN201610309512.5A CN201610309512A CN105969503A CN 105969503 A CN105969503 A CN 105969503A CN 201610309512 A CN201610309512 A CN 201610309512A CN 105969503 A CN105969503 A CN 105969503A
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parts
oil
wire drawing
wiredrawing
red copper
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张军
何孔田
唐兰花
何孔高
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ANHUI JIUHUA KIMRUN COPPER INDUSTRY Co Ltd
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ANHUI JIUHUA KIMRUN COPPER INDUSTRY Co Ltd
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Abstract

一种紫铜高温拉丝用拉丝油，由如下重量份的原料制成：鞘磷脂5‑12份、三酰甘油5‑12份、氢氧化钙2‑5份、甲基环己烷4‑5.5份、月桂酸乙酯4‑5.5份、硬脂酸镁5‑8份、脂肪酸聚氧乙烯酯4‑13份、十六酸甲酯4‑13份、水50‑60份、改性助剂8.5‑16.5份。本发明拉丝油特别适合紫铜在高温下拉丝，高温状态下拉丝油挥发性非常低，而且其运动粘度和比重与常温状态下相比完全没有变化，而且高温状态下拉丝油性质几乎没有变化，没有焦糊碳化现象，能满足紫铜在150℃以内的，拉丝后的紫铜颜色红亮，毫无黑色斑块。

Description

一种紫铜高温拉丝用拉丝油
技术领域
本发明涉及拉丝油领域，具体涉及一种紫铜高温拉丝用拉丝油。
背景技术
拉丝油，它也是跟黄油一样，起到润滑作用的一种油，但是它的粘稠度非常的高，拉扯的话都能拉出丝来，所以简称为拉丝油。拉丝油是一类重要的工业助剂，在金属线拉丝、拉拔工艺过程中做高效润滑油用，具有润滑、清洗、冷却、防锈等功效，协助金属流动，避免模具拖花拉线，提高成品率，降低生产损耗。现有的拉丝油主要分为油性拉丝油和水性拉丝油，这两类拉丝油在实际使用时各有利弊，如油性拉丝油存在散热性能差，清洗排屑困难，废液难降解等问题，而水性的拉丝油虽然散热性能较油性拉丝油优良，但是润滑效果却不尽如人意，难以满足多种金属线的拉丝拉拨工艺要求。
紫铜用途非常广泛，目前紫铜在高温拉丝时经常由于温度较高导致拉丝油不稳定，严重影响拉丝品质。
发明内容
本发明所要解决的技术问题在于提供一种紫铜高温拉丝用拉丝油。
本发明所要解决的技术问题采用以下技术方案来实现：
一种紫铜高温拉丝用拉丝油，由如下重量份的原料制成：鞘磷脂5-12份、三酰甘油5-12份、氢氧化钙2-5份、甲基环己烷4-5.5份、月桂酸乙酯4-5.5份、硬脂酸镁5-8份、脂肪酸聚氧乙烯酯4-13份、十六酸甲酯4-13份、水50-60份、改性助剂8.5-16.5份；
所述的改性助剂由以下重量份的原料制成：滑石粉1-4份、二氧化硅1-4份、氧化钡1-4份、氧化钙1-4份、葡萄花酸6-18份、二甲基甲酰胺6-18份、没食子酸钠6-18份、聚L-醇单月桂酸酯6-18份、二月桂酸二丁基锡5.5-10.2份、磷脂酰乙醇胺5.5-10.2份、四氢呋喃5.5-10.2份、棕榈酸异丙酯5.5-10.2份、丁酸纤维素5.5-10.2份、环氧油酸酯4-5份、蒸馏水30-35份、去离子水30-35份；
所述的改性助剂的制备方法是，先将滑石粉在450-500℃高温下煅烧30-50分钟，冷却后研磨成300目粉末，粉末与二氧化硅、氧化钡、氧化钙混合磨碎成20-50目粉末；将丁酸纤维素和蒸馏水混合，混合液加热至100℃蒸汽，蒸汽喷射葡萄花酸、二甲基甲酰胺、没食子酸钠、聚L-醇单月桂酸酯、二月桂酸二丁基锡、磷脂酰乙醇胺、四氢呋喃、棕榈酸异丙酯、环氧油酸酯，获得乳化液，乳化液放入-20℃冷库冷冻1小时，取出后加热融化，边融化边加入去离子水，待完全融化即得改性助剂。
一种紫铜高温拉丝用拉丝油，制备方法如下：
(1)将鞘磷脂、甲基环己烷、月桂酸乙酯混合加热至80℃，然后加入氢氧化钙和硬脂酸镁再加热到90℃并保持该温度3分钟，冷却后备用；
(2)将水加热至70℃，然后加入脂肪酸三酰甘油、聚氧乙烯酯、十六酸甲酯，再使用高剪切乳化机分散处理40min，得混合溶液备用；
(3)将步骤(1)和步骤(2)所得物料与改性助剂混合，搅拌静置后即得拉丝油。
本发明的有益效果是：本发明拉丝油特别适合紫铜在高温下拉丝，高温状态下拉丝油挥发性非常低，而且其运动粘度和比重与常温状态下相比完全没有变化，而且高温状态下拉丝油性质几乎没有变化，没有焦糊碳化现象，能满足紫铜在150℃以内的，拉丝后的紫铜颜色红亮，毫无黑色斑块。
具体实施方式
为了使本发明实现的技术手段、创作特征、达成目的与功效易于明白了解，下面结合具体实施例，进一步阐述本发明。
实施例1
一种紫铜高温拉丝用拉丝油，由如下重量份的原料制成：鞘磷脂8份、三酰甘油8份、氢氧化钙4份、甲基环己烷5份、月桂酸乙酯5份、硬脂酸镁6份、脂肪酸聚氧乙烯酯9份、十六酸甲酯9份、水55份、改性助剂12份；
所述的改性助剂由以下重量份的原料制成：滑石粉3份、二氧化硅3份、氧化钡3份、氧化钙3份、葡萄花酸12份、二甲基甲酰胺12份、没食子酸钠12份、聚L-醇单月桂酸酯12份、二月桂酸二丁基锡8份、磷脂酰乙醇胺8份、四氢呋喃8份、棕榈酸异丙酯8份、丁酸纤维素8份、环氧油酸酯4份、蒸馏水32份、去离子水32份；
所述的改性助剂的制备方法是，先将滑石粉在450-500℃高温下煅烧30-50分钟，冷却后研磨成300目粉末，粉末与二氧化硅、氧化钡、氧化钙混合磨碎成20-50目粉末；将丁酸纤维素和蒸馏水混合，混合液加热至100℃蒸汽，蒸汽喷射葡萄花酸、二甲基甲酰胺、没食子酸钠、聚L-醇单月桂酸酯、二月桂酸二丁基锡、磷脂酰乙醇胺、四氢呋喃、棕榈酸异丙酯、环氧油酸酯，获得乳化液，乳化液放入-20℃冷库冷冻1小时，取出后加热融化，边融化边加入去离子水，待完全融化即得改性助剂。
一种紫铜高温拉丝用拉丝油，制备方法如下：
(1)将鞘磷脂、甲基环己烷、月桂酸乙酯混合加热至80℃，然后加入氢氧化钙和硬脂酸镁再加热到90℃并保持该温度3分钟，冷却后备用；
(2)将水加热至70℃，然后加入脂肪酸三酰甘油、聚氧乙烯酯、十六酸甲酯，再使用高剪切乳化机分散处理40min，得混合溶液备用；
(3)将步骤(1)和步骤(2)所得物料与改性助剂混合，搅拌静置后即得拉丝油。
实施例2
一种紫铜高温拉丝用拉丝油，由如下重量份的原料制成：鞘磷脂5份、三酰甘油5份、氢氧化钙2份、甲基环己烷4份、月桂酸乙酯4份、硬脂酸镁5份、脂肪酸聚氧乙烯酯4份、十六酸甲酯4份、水50份、改性助剂8.5份；
所述的改性助剂由以下重量份的原料制成：滑石粉1份、二氧化硅1份、氧化钡1份、氧化钙1份、葡萄花酸6份、二甲基甲酰胺6份、没食子酸钠6份、聚L-醇单月桂酸酯6份、二月桂酸二丁基锡5.5份、磷脂酰乙醇胺5.5份、四氢呋喃5.5份、棕榈酸异丙酯5.5份、丁酸纤维素5.5份、环氧油酸酯4份、蒸馏水30份、去离子水30份；
所述的改性助剂的制备方法是，先将滑石粉在450-500℃高温下煅烧30-50分钟，冷却后研磨成300目粉末，粉末与二氧化硅、氧化钡、氧化钙混合磨碎成20-50目粉末；将丁酸纤维素和蒸馏水混合，混合液加热至100℃蒸汽，蒸汽喷射葡萄花酸、二甲基甲酰胺、没食子酸钠、聚L-醇单月桂酸酯、二月桂酸二丁基锡、磷脂酰乙醇胺、四氢呋喃、棕榈酸异丙酯、环氧油酸酯，获得乳化液，乳化液放入-20℃冷库冷冻1小时，取出后加热融化，边融化边加入去离子水，待完全融化即得改性助剂。
一种紫铜高温拉丝用拉丝油，制备方法如下：
(1)将鞘磷脂、甲基环己烷、月桂酸乙酯混合加热至80℃，然后加入氢氧化钙和硬脂酸镁再加热到90℃并保持该温度3分钟，冷却后备用；
(2)将水加热至70℃，然后加入脂肪酸三酰甘油、聚氧乙烯酯、十六酸甲酯，再使用高剪切乳化机分散处理40min，得混合溶液备用；
(3)将步骤(1)和步骤(2)所得物料与改性助剂混合，搅拌静置后即得拉丝油。
实施例3
一种紫铜高温拉丝用拉丝油，由如下重量份的原料制成：鞘磷脂12份、三酰甘油12份、氢氧化钙5份、甲基环己烷5.5份、月桂酸乙酯5.5份、硬脂酸镁8份、脂肪酸聚氧乙烯酯13份、十六酸甲酯13份、水60份、改性助剂16.5份；
所述的改性助剂由以下重量份的原料制成：滑石粉4份、二氧化硅4份、氧化钡4份、氧化钙4份、葡萄花酸18份、二甲基甲酰胺18份、没食子酸钠18份、聚L-醇单月桂酸酯18份、二月桂酸二丁基锡10.2份、磷脂酰乙醇胺10.2份、四氢呋喃10.2份、棕榈酸异丙酯10.2份、丁酸纤维素10.2份、环氧油酸酯5份、蒸馏水35份、去离子水35份；
所述的改性助剂的制备方法是，先将滑石粉在450-500℃高温下煅烧30-50分钟，冷却后研磨成300目粉末，粉末与二氧化硅、氧化钡、氧化钙混合磨碎成20-50目粉末；将丁酸纤维素和蒸馏水混合，混合液加热至100℃蒸汽，蒸汽喷射葡萄花酸、二甲基甲酰胺、没食子酸钠、聚L-醇单月桂酸酯、二月桂酸二丁基锡、磷脂酰乙醇胺、四氢呋喃、棕榈酸异丙酯、环氧油酸酯，获得乳化液，乳化液放入-20℃冷库冷冻1小时，取出后加热融化，边融化边加入去离子水，待完全融化即得改性助剂。
一种紫铜高温拉丝用拉丝油，制备方法如下：
(1)将鞘磷脂、甲基环己烷、月桂酸乙酯混合加热至80℃，然后加入氢氧化钙和硬脂酸镁再加热到90℃并保持该温度3分钟，冷却后备用；
(2)将水加热至70℃，然后加入脂肪酸三酰甘油、聚氧乙烯酯、十六酸甲酯，再使用高剪切乳化机分散处理40min，得混合溶液备用；
(3)将步骤(1)和步骤(2)所得物料与改性助剂混合，搅拌静置后即得拉丝油。
以上显示和描述了本发明的基本原理和主要特征和本发明的优点。本行业的技术人员应该了解，本发明不受上述实施例的限制，上述实施例和说明书中描述的只是说明本发明的原理，在不脱离本发明精神和范围的前提下，本发明还会有各种变化和改进，这些变化和改进都落入要求保护的本发明范围内。本发明要求保护范围由所附的权利要求书及其等效物界定。

Claims (2)

1.一种紫铜高温拉丝用拉丝油，其特征在于，由如下重量份的原料制成：鞘磷脂5-12份、三酰甘油5-12份、氢氧化钙2-5份、甲基环己烷4-5.5份、月桂酸乙酯4-5.5份、硬脂酸镁5-8份、脂肪酸聚氧乙烯酯4-13份、十六酸甲酯4-13份、水50-60份、改性助剂8.5-16.5份；
所述的改性助剂由以下重量份的原料制成：滑石粉1-4份、二氧化硅1-4份、氧化钡1-4份、氧化钙1-4份、葡萄花酸6-18份、二甲基甲酰胺6-18份、没食子酸钠6-18份、聚L-醇单月桂酸酯6-18份、二月桂酸二丁基锡5.5-10.2份、磷脂酰乙醇胺5.5-10.2份、四氢呋喃5.5-10.2份、棕榈酸异丙酯5.5-10.2份、丁酸纤维素5.5-10.2份、环氧油酸酯4-5份、蒸馏水30-35份、去离子水30-35份；
所述的改性助剂的制备方法是，先将滑石粉在450-500℃高温下煅烧30-50分钟，冷却后研磨成300目粉末，粉末与二氧化硅、氧化钡、氧化钙混合磨碎成20-50目粉末；将丁酸纤维素和蒸馏水混合，混合液加热至100℃蒸汽，蒸汽喷射葡萄花酸、二甲基甲酰胺、没食子酸钠、聚L-醇单月桂酸酯、二月桂酸二丁基锡、磷脂酰乙醇胺、四氢呋喃、棕榈酸异丙酯、环氧油酸酯，获得乳化液，乳化液放入-20℃冷库冷冻1小时，取出后加热融化，边融化边加入去离子水，待完全融化即得改性助剂。
2.如权利要求1所述的一种紫铜高温拉丝用拉丝油，其特征在于，制备方法如下：
(1)将鞘磷脂、甲基环己烷、月桂酸乙酯混合加热至80℃，然后加入氢氧化钙和硬脂酸镁再加热到90℃并保持该温度3分钟，冷却后备用；
(2)将水加热至70℃，然后加入脂肪酸三酰甘油、聚氧乙烯酯、十六酸甲酯，再使用高剪切乳化机分散处理40min，得混合溶液备用；
(3)将步骤(1)和步骤(2)所得物料与改性助剂混合，搅拌静置后即得拉丝油。
CN201610309512.5A 2016-05-10 2016-05-10 一种紫铜高温拉丝用拉丝油 Pending CN105969503A (zh)

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Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN107603714A (zh) * 2017-11-07 2018-01-19 刘兴满 磁力泵轴承用润滑液
CN107603715A (zh) * 2017-11-07 2018-01-19 刘兴满 水泵用润滑液
CN107892977A (zh) * 2017-11-07 2018-04-10 刘兴满 潜水泵转子用润滑液

Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN107603714A (zh) * 2017-11-07 2018-01-19 刘兴满 磁力泵轴承用润滑液
CN107603715A (zh) * 2017-11-07 2018-01-19 刘兴满 水泵用润滑液
CN107892977A (zh) * 2017-11-07 2018-04-10 刘兴满 潜水泵转子用润滑液

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