CN105967921A - Modified-Chinese-chestnut-protein-coated slow-release medicinal fertilizer - Google Patents
Modified-Chinese-chestnut-protein-coated slow-release medicinal fertilizer Download PDFInfo
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- CN105967921A CN105967921A CN201610103219.3A CN201610103219A CN105967921A CN 105967921 A CN105967921 A CN 105967921A CN 201610103219 A CN201610103219 A CN 201610103219A CN 105967921 A CN105967921 A CN 105967921A
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- fertilizer
- semen castaneae
- chestnut
- minute
- slow
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- C—CHEMISTRY; METALLURGY
- C05—FERTILISERS; MANUFACTURE THEREOF
- C05G—MIXTURES OF FERTILISERS COVERED INDIVIDUALLY BY DIFFERENT SUBCLASSES OF CLASS C05; MIXTURES OF ONE OR MORE FERTILISERS WITH MATERIALS NOT HAVING A SPECIFIC FERTILISING ACTIVITY, e.g. PESTICIDES, SOIL-CONDITIONERS, WETTING AGENTS; FERTILISERS CHARACTERISED BY THEIR FORM
- C05G3/00—Mixtures of one or more fertilisers with additives not having a specially fertilising activity
- C05G3/60—Biocides or preservatives, e.g. disinfectants, pesticides or herbicides; Pest repellants or attractants
-
- C—CHEMISTRY; METALLURGY
- C05—FERTILISERS; MANUFACTURE THEREOF
- C05D—INORGANIC FERTILISERS NOT COVERED BY SUBCLASSES C05B, C05C; FERTILISERS PRODUCING CARBON DIOXIDE
- C05D3/00—Calcareous fertilisers
-
- C—CHEMISTRY; METALLURGY
- C05—FERTILISERS; MANUFACTURE THEREOF
- C05G—MIXTURES OF FERTILISERS COVERED INDIVIDUALLY BY DIFFERENT SUBCLASSES OF CLASS C05; MIXTURES OF ONE OR MORE FERTILISERS WITH MATERIALS NOT HAVING A SPECIFIC FERTILISING ACTIVITY, e.g. PESTICIDES, SOIL-CONDITIONERS, WETTING AGENTS; FERTILISERS CHARACTERISED BY THEIR FORM
- C05G3/00—Mixtures of one or more fertilisers with additives not having a specially fertilising activity
-
- C—CHEMISTRY; METALLURGY
- C05—FERTILISERS; MANUFACTURE THEREOF
- C05G—MIXTURES OF FERTILISERS COVERED INDIVIDUALLY BY DIFFERENT SUBCLASSES OF CLASS C05; MIXTURES OF ONE OR MORE FERTILISERS WITH MATERIALS NOT HAVING A SPECIFIC FERTILISING ACTIVITY, e.g. PESTICIDES, SOIL-CONDITIONERS, WETTING AGENTS; FERTILISERS CHARACTERISED BY THEIR FORM
- C05G5/00—Fertilisers characterised by their form
- C05G5/30—Layered or coated, e.g. dust-preventing coatings
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- Chemical & Material Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Pest Control & Pesticides (AREA)
- Organic Chemistry (AREA)
- Plant Pathology (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Inorganic Chemistry (AREA)
- Fertilizers (AREA)
Abstract
The invention discloses a modified-Chinese-chestnut-protein-coated slow-release medicinal fertilizer. The fertilizer is made from the following raw materials, by weight part, 26-28 of rice husks, 10-12 of herba houttuyniae, 2-3 of oligochitosan, 3-4 of calcium sulfate, 14-15 of elodea nuttallii, 2-3 of wheat gluten powder, 0.4-0.6 of benthiocarb sodium salt having a concentration being 95%, 76-80 of fresh Chinese chestnuts, 17-18 of fruits of ficus pumila, 1.2-1.3 of a glutamine transaminase preparation and a proper amount of water. In the fertilizer, a slow-release fertilizer is combined with Chinese herbal medicines and pesticides, and the slow-release effect of fertilizer particles is utilized to gradually produce the pesticide effect. Durability of the pesticide effect is ensured, pests and diseases can be prevented, and the problem that an extremely-high local concentration of pesticides which are singly applied results in pollution of the soil and damage to plants is solved. The fertilizer is high in nutritional content, and has a double effect of fertilizer application and disease control.
Description
Technical field
The present invention relates to slow release fertilizer technical field, particularly relate to a kind of modified slow-releasing medicated fertilizer of Semen Castaneae protein envelope.
Background technology
Along with the specialization of China's agricultural production, industrialization, the development of scale, agricultural is constantly upgraded for the requirement of fertilizer, soil fertility, and conventional fertilizers is low due to plant recovery of nutrient, constrains the sustainable development of agricultural planting.The application of coated slow release fertilizer is then the effective way solving this problem.But the coated fertilizer of current common coated slow release fertilizer is to use the non-degradable high molecular polymer of chemosynthesis, easily remain in soil and cause soil degradation and pollution, the function singleness of coated fertilizer simultaneously, generally only there is slow controlled-release effect, do not account for the effects such as water suction, antibacterial, antioxidation and the practicality for different soils environment.
The rich in nutrition content of Semen Castaneae, there are substantial amounts of starch, protein, fat etc., contain multi mineral prime element simultaneously, the most important macroelement N, P, K, Ca etc. and trace element Fe, Cu, Zn, Mn etc., Semen Castaneae also has the functional component useful to plant growing, if the polyphenol substance in Semen Castaneae is a kind of natural antioxidant, gallic acid therein, ellagic acid, elladitannin have powerful antioxidation, antibacterial characteristics.In Semen Castaneae, protein content is high simultaneously, accounts for 5%-11%, rich amino acids in Semen Castaneae albumen, and plant can absorb aminoacid, therefore can improve the trophic structure in growing process, and potentiality to be exploited is very big.
Semen Castaneae albumen has preferable dissolubility and viscosity in the pH range of 7.0-8.0, and by combining the common effect of water, hydrodynamics water and Physical entrapment water, it is allowed to that there is fabulous moisture holding capacity, the number of dropouts of moisture can be reduced, the most in the basic conditions, Semen Castaneae albumen also has preferable emulsibility, foaming characteristic and foam stability, meets the condition needed for coated fertilizer in slow release fertilizer.
Semen Castaneae all has plantation, wide material sources in various places, utilizes the slow-release fertilizer that the exploitation of Semen Castaneae albumen is novel, gives the function that slow release fertilizer is new simultaneously, and the development for slow release fertilizer opens new approach.
Summary of the invention
The object of the invention is contemplated to make up the defect of prior art, it is provided that a kind of modified slow-releasing medicated fertilizer of Semen Castaneae protein envelope.
The present invention is achieved by the following technical solutions:
A kind of modified slow-releasing medicated fertilizer of Semen Castaneae protein envelope, is prepared by the raw materials in: rice husk 26-28, Herba Houttuyniae 10-12, oligo-chitosan 2-3, calcium sulfate 3-4, waterweed 14-15, wheat gluten flour 2-3,95% benthiocarb sodium salt 0.4-0.6, fresh Semen Castaneae 76-80, Receptaculum Fici Pumilae 17-18, glutamine transaminage preparation 1.2-1.3, water are appropriate.
Specifically comprising the following steps that of the described modified slow-releasing medicated method for preparing fertilizer of Semen Castaneae protein envelope
(1) cut into slices after going bud to shell fresh Semen Castaneae, pulverize levigate after drying at 48-50 DEG C, rice-chestnut powder is joined in the water of 10 times of its quality, and use 1mol/L sodium hydroxide solution to regulate PH to 9.8-10.0, through Ultrasonic Pulverization 14-15 minute under 35-40kHz, it is heated to 44-46 DEG C afterwards, is incubated 80-90 minute, cross leaching supernatant, after vacuum lyophilization, obtain Semen Castaneae egg albumen powder;
(2) step 1 is discarded Semen Castaneae bud, chestnut shell mixing is placed in calcining furnace; it is warming up to 530-550 DEG C with 20-25 DEG C/minute; take out after calcining 120-130 minute; obtain chestnut powdered carbon standby; again by rice husk, waterweed, Herba Houttuyniae mixing retting fermentation; post-drying for the treatment of fully to become thoroughly decomposed is pulverized and mixes with chestnut powdered carbon, 95% benthiocarb sodium salt, is placed in pelletize in comminutor;
(3) squeeze the juice clean for the Receptaculum Fici Pumilae and filter, filtrate being mixed with oligo-chitosan, is heated to 72-75 DEG C, be cooled to 40-42 DEG C and add calcium sulfate after stirring 5 minutes, be again stirring for 10 minutes, obtain nutritional solution standby;
(4) step 1 gained Semen Castaneae egg albumen powder is added in the water of 12-15 times of its quality, and regulate PH to 7.3-7.7 with 1mol/L sodium hydroxide solution, add glutamine transaminage preparation, wheat gluten flour, be heated to 49-51 DEG C, it is incubated 3.5-4 hour, obtains modified Semen Castaneae protein liquid;
(5) step 2 gained granule is placed in bottom and has in the cylinder of heater, barrel is heated to 55-60 DEG C, rolling process sprays into by the way of spraying sprays in cylinder step 3 gained nutritional solution, continue after having sprayed to roll 10-15 minute, spray into step 4 gained modification Semen Castaneae protein liquid again, continue to roll 10-15 minute, take out and i.e. obtain coated fertilizer granule of the present invention.
The invention have the advantage that
Semen Castaneae egg albumen powder acts on modification under the conditions of glutamine transaminage and alkalescence jointly, be conducive to the expansion of protein molecule, and catalytic proteins polypeptide generation intramolecular and intermolecular generation covalent cross-linking, it is embodied in viscosity to increase, there is higher shearing force repellence and gumminess, can stably be attached to fertiliser granulates surface, the retentiveness coordinating egg albumen powder ensures being dried of fertiliser granulates, will not make moist in short time disintegrate, extend action period, during slow release, albumin layer slowly decomposes, it is alternatively arranged as plant nitrogen source, and aminoacid-cation-polyphosphoric acid complex can be formed, reduce the mobility of heavy metal in soil ion, alleviate heavy metal ion to poison.Slow-release fertilizer is combined by fertilizer of the present invention with Chinese herbal medicine, parasite killing, and utilize the slow release effect of fertiliser granulates progressively to discharge drug effect, both can guarantee that the persistence of drug effect was to control worm diseases prevention, turn avoid single pesticide grown causes local concentration too high and contaminated soil, infringement plant, fertilizer nutrient content is high simultaneously, can realize the double effects of fertilizer and disease control.
Detailed description of the invention
A kind of modified slow-releasing medicated fertilizer of Semen Castaneae protein envelope, is made up of the raw material of following weight portion (kg): rice husk 26, Herba Houttuyniae 10, oligo-chitosan 2, calcium sulfate 3, waterweed 14, wheat gluten flour 2,95% benthiocarb sodium salt 0.4, fresh Semen Castaneae 76, the Receptaculum Fici Pumilae 17, glutamine transaminage preparation 1.2, water are appropriate.
Specifically comprising the following steps that of the described modified slow-releasing medicated method for preparing fertilizer of Semen Castaneae protein envelope
(1) cut into slices after going bud to shell fresh Semen Castaneae, pulverize levigate after drying at 48 DEG C, rice-chestnut powder is joined in the water of 10 times of its quality, and use 1mol/L sodium hydroxide solution to regulate PH to 9.8, through Ultrasonic Pulverization 14 minutes under 35kHz, it is heated to 44 DEG C afterwards, is incubated 80 minutes, cross leaching supernatant, after vacuum lyophilization, obtain Semen Castaneae egg albumen powder;
(2) step 1 is discarded Semen Castaneae bud, chestnut shell mixing is placed in calcining furnace; it is warming up to 530 DEG C with 20 DEG C/minute; take out after calcining 120 minutes; obtain chestnut powdered carbon standby; again by rice husk, waterweed, Herba Houttuyniae mixing retting fermentation; post-drying for the treatment of fully to become thoroughly decomposed is pulverized and mixes with chestnut powdered carbon, 95% benthiocarb sodium salt, is placed in pelletize in comminutor;
(3) squeeze the juice clean for the Receptaculum Fici Pumilae and filter, filtrate being mixed with oligo-chitosan, is heated to 72 DEG C, be cooled to 40 DEG C after stirring 5 minutes and add calcium sulfate, being again stirring for 10 minutes, obtain nutritional solution standby;
(4) step 1 gained Semen Castaneae egg albumen powder is added in the water of 12 times of its quality, and regulate PH to 7.3 with 1mol/L sodium hydroxide solution, add glutamine transaminage preparation, wheat gluten flour, be heated to 49 DEG C, be incubated 3.5 hours, obtain modified Semen Castaneae protein liquid;
(5) step 2 gained granule is placed in bottom and has in the cylinder of heater, barrel is heated to 55 DEG C, rolling process sprays into by the way of spraying sprays in cylinder step 3 gained nutritional solution, continue after having sprayed to roll 10 minutes, spray into step 4 gained modification Semen Castaneae protein liquid again, continue to roll 10 minutes, take out and i.e. obtain coated fertilizer granule of the present invention.
In order to further illustrate the using value of the present invention, inventor chooses two pieces of areas and is the Oryza sativa L. experiment field of 10 mu, and is divided into matched group and experimental group, matched group uses common fertilizer, and experimental group uses slow-release fertilizer of the present invention, and every mu is 70kg with fertilizer, during plantation, field management pattern is the most identical, results statistics, matched group per mu yield 481kg, sickness rate 11.3% after maturation, experimental group per mu yield 527kg, sickness rate 4.2%, and experimental group rice grain is relatively big, condition is preferable.
Claims (2)
1. the modified slow-releasing medicated fertilizer of Semen Castaneae protein envelope, it is characterized in that, be prepared by the raw materials in: rice husk 26-28, Herba Houttuyniae 10-12, oligo-chitosan 2-3, calcium sulfate 3-4, waterweed 14-15, wheat gluten flour 2-3,95% benthiocarb sodium salt 0.4-0.6, fresh Semen Castaneae 76-80, Receptaculum Fici Pumilae 17-18, glutamine transaminage preparation 1.2-1.3, water are appropriate.
2. according to the modified slow-releasing medicated fertilizer of Semen Castaneae protein envelope described in claims 1, it is characterised in that specifically comprising the following steps that of preparation method
(1) cut into slices after going bud to shell fresh Semen Castaneae, pulverize levigate after drying at 48-50 DEG C, rice-chestnut powder is joined in the water of 10 times of its quality, and use 1mol/L sodium hydroxide solution to regulate PH to 9.8-10.0, through Ultrasonic Pulverization 14-15 minute under 35-40kHz, it is heated to 44-46 DEG C afterwards, is incubated 80-90 minute, cross leaching supernatant, after vacuum lyophilization, obtain Semen Castaneae egg albumen powder;
(2) step 1 is discarded Semen Castaneae bud, chestnut shell mixing is placed in calcining furnace; it is warming up to 530-550 DEG C with 20-25 DEG C/minute; take out after calcining 120-130 minute; obtain chestnut powdered carbon standby; again by rice husk, waterweed, Herba Houttuyniae mixing retting fermentation; post-drying for the treatment of fully to become thoroughly decomposed is pulverized and mixes with chestnut powdered carbon, 95% benthiocarb sodium salt, is placed in pelletize in comminutor;
(3) squeeze the juice clean for the Receptaculum Fici Pumilae and filter, filtrate being mixed with oligo-chitosan, is heated to 72-75 DEG C, be cooled to 40-42 DEG C and add calcium sulfate after stirring 5 minutes, be again stirring for 10 minutes, obtain nutritional solution standby;
(4) step 1 gained Semen Castaneae egg albumen powder is added in the water of 12-15 times of its quality, and regulate PH to 7.3-7.7 with 1mol/L sodium hydroxide solution, add glutamine transaminage preparation, wheat gluten flour, be heated to 49-51 DEG C, it is incubated 3.5-4 hour, obtains modified Semen Castaneae protein liquid;
(5) step 2 gained granule is placed in bottom and has in the cylinder of heater, barrel is heated to 55-60 DEG C, rolling process sprays into by the way of spraying sprays in cylinder step 3 gained nutritional solution, continue after having sprayed to roll 10-15 minute, spray into step 4 gained modification Semen Castaneae protein liquid again, continue to roll 10-15 minute, take out and i.e. obtain coated fertilizer granule of the present invention.
Priority Applications (1)
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CN201610103219.3A CN105967921A (en) | 2016-02-25 | 2016-02-25 | Modified-Chinese-chestnut-protein-coated slow-release medicinal fertilizer |
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Citations (8)
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CN1887827A (en) * | 2006-07-25 | 2007-01-03 | 天津大学 | Slow released urea fertilizer and its prepn |
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2016
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Patent Citations (8)
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CN102351606A (en) * | 2011-09-17 | 2012-02-15 | 山东喜丰田生态肥业有限公司 | Environment-friendly coated fertilizer and preparation method thereof |
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CN104086318A (en) * | 2014-07-30 | 2014-10-08 | 河南力浮科技有限公司 | Production method of biomass coated controlled-release fertilizer |
CN104193502A (en) * | 2014-07-30 | 2014-12-10 | 马鞍山市四季果业有限公司 | Special strawberry organic fertilizer for protecting flowers and fruits and preparation method thereof |
CN104521667A (en) * | 2014-12-04 | 2015-04-22 | 安徽汇丰园生物科技有限公司 | Method for planting pomegranates rich in organic selenium |
CN105175132A (en) * | 2015-09-16 | 2015-12-23 | 安徽省陆虎生物科技有限公司 | Functional residue-free slow-release protein peptide fertilizer |
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Application publication date: 20160928 |