CN105919871A - Armillaria mellea crude polysaccharide skincare product and preparation method thereof - Google Patents
Armillaria mellea crude polysaccharide skincare product and preparation method thereof Download PDFInfo
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- CN105919871A CN105919871A CN201610402459.3A CN201610402459A CN105919871A CN 105919871 A CN105919871 A CN 105919871A CN 201610402459 A CN201610402459 A CN 201610402459A CN 105919871 A CN105919871 A CN 105919871A
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- armillaria mellea
- crude polysaccharides
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/965—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution of inanimate origin
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/73—Polysaccharides
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/81—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds obtained by reactions involving only carbon-to-carbon unsaturated bonds
- A61K8/8141—Compositions of homopolymers or copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and at least one being terminated by only one carboxyl radical, or of salts, anhydrides, esters, amides, imides or nitriles thereof; Compositions of derivatives of such polymers
- A61K8/8147—Homopolymers or copolymers of acids; Metal or ammonium salts thereof, e.g. crotonic acid, (meth)acrylic acid; Compositions of derivatives of such polymers
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/92—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof
- A61K8/922—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof of vegetable origin
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/08—Anti-ageing preparations
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/80—Process related aspects concerning the preparation of the cosmetic composition or the storage or application thereof
- A61K2800/82—Preparation or application process involves sonication or ultrasonication
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/80—Process related aspects concerning the preparation of the cosmetic composition or the storage or application thereof
- A61K2800/84—Products or compounds obtained by lyophilisation, freeze-drying
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- Life Sciences & Earth Sciences (AREA)
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- Veterinary Medicine (AREA)
- Animal Behavior & Ethology (AREA)
- General Health & Medical Sciences (AREA)
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- Birds (AREA)
- Dermatology (AREA)
- Chemical & Material Sciences (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Gerontology & Geriatric Medicine (AREA)
- Medicines Containing Plant Substances (AREA)
- Cosmetics (AREA)
Abstract
The invention provides an armillaria mellea crude polysaccharide skincare product and a preparation method thereof. The armillaria mellea crude polysaccharide skincare product is prepared from the following raw materials: 15 to 25 weight percent of armillaria mellea crude polysaccharide, 5 to 10 weight percent of a moisturizer, 0.5 to 1 weight percent of a preservative, 0.5 to 1 weight percent of an antioxidant, 2 to 4 weight percent of a nutritional additive, 12 to 14 weight percent of an oily raw material, 1 to 2 weight percent of carbomer, 1 to 2 weight percent of brightening agent, 0.4 to 0.6 weight percent of tea tree essential oil, 0.5 to 2 weight percent of deep ocean water, and the balance of de-ionized water. The preparation method comprises the following steps: adding the armillaria mellea crude polysaccharide to the de-ionized water, continuously stirring, and heating to 50 to 60 DEG C for dissolving; heating and dissolving the oily raw material and the nutritional additive at 80 to 85 DEG C, then mixing the solution and the armillaria mellea crude polysaccharide, homogenizing, emulsifying and stirring to obtain an emulsion; cooling the emulsion to 50 to 60 DEG C; adding the moisturizer, the preservative, the antioxidant and the brightening agent, stirring uniformly, then cooling to 35 to 42 DEG C, adding the carbomer, the tea tree essential oil and the deep ocean water, and stirring uniformly to obtain the armillaria mellea crude polysaccharide skincare product. The skin care product can improve the oxidation resistance of skin, obviously moisturize the skin, increase the elasticity of the skin, enhance the immunity of the skin, and delay skin aging.
Description
Technical field
The invention belongs to technical field of skin care, be specifically related to a kind of Armillaria mellea crude polysaccharides skin care item and preparation thereof
Method.
Background technology
Skin is the natural coat of people, healthy and beautiful skin be mainly manifested in the colour of skin, elasticity, gloss,
Texture and the various aspects of physiological function, and these are played the water content that crucial effect effect is exactly skin.
The generally water content of epidermis and corium is about 75%, and outmost horny layer typically should be not less than 10%, angle
Matter layer water content is that the skin of 10-20% then shows as soft and moist, smooth, flexible, if less than 10%, then
Keratodermatitis can excessively be dried even to be there is squama or ruptures.Therefore, the full-time water keeping skin moistens not
It is only the basic demand of skin protection, is also the basic guarantee of skin beauty of securing good health.
Armillaria is in Bai Mo section fungus, and its mycelium and mycelia all can be in the dark luminous.Sporophore, mycelia
All can be used as medicine with shoestring, and mushroom body delicious flavour, nutritious, this mushroom is a kind of famous edible medicinal
Fungus.Containing multiple nutritional components such as substantial amounts of protein, fat, carbohydrates in Armillaria mellea, wherein
Armillaria mellea polysaccharide has the multiple physiology such as the generation of anticancer, antitumor, regulation immunologic function and inducing interferon
Regulatory function.Armillaria mellea polysaccharide not only has corresponding medicine effect, and has health product health-care effect,
There is wide market development application prospect.
There is presently no the report in terms of Armillaria mellea crude polysaccharides skin care item.
Summary of the invention
It is an object of the invention to provide a kind of Armillaria mellea crude polysaccharides skin care item, these skin care item can improve skin antioxygen
The property changed, hence it is evident that Glycerin, increases skin elasticity, strengthens skin immunity, slows down skin aging.
The technical scheme is that and be achieved in that:
Armillaria mellea crude polysaccharides 15-25wt%, wetting agent 5-10wt%, preservative 0.5-1wt%, antioxidant
0.5-1wt%, nourishing additive agent 2-4wt%, oiliness raw material 12-14wt%, carbomer 1-2wt%, brighten
Agent 1-2wt%, tea tree ethereal oil 0.4-0.6wt% and deep layer Haiquan water 0.5-2wt%, surplus is deionized water.
Further, described Armillaria mellea crude polysaccharides is prepared via a method which to obtain:
1) obtain powder by carrying out pulverizing after Armillaria mellea vacuum lyophilization, then add 15-20 times of weight
Water carries out ultrasonication process after stirring, and obtains Armillaria mellea homogenate；
2) by step 1) the Armillaria mellea homogenate that obtains adds the water of 26-35 times of weight, and 85-95 DEG C of water-bath carries
Take 0.5-1.2 hour, obtain extracting solution；
3) extracting solution is filtered, and add ethanol in proper amount after filtrate concentration, make second alcohol precipitation concentration reach
85-90%, obtains armillaria mellea polysaccharide precipitation, after armillaria mellea polysaccharide is precipitated vacuum lyophilization.
Further, described wetting agent selected from Butyrospermum parkii fruit fat, tocopherol acetas, trimethyl glycine with
One or more in hyaluronate sodium.
Further, described preservative is phenoxyethanol or Sang Pu K15；Described antioxidant be red wine polyphenols or
Person's oryzanol.
Further, described nourishing additive agent selected from silk fibroin powder, Margarita hydrolyzed solution and is polymerized almond protein
One or more.
Further, described oiliness raw material is Jojoba oil or Oleum Vitis viniferae；Described brightening agent be Trenaxmine with
One or both mixture in vitamin B3.
It is a further object to provide the preparation method of a kind of Armillaria mellea crude polysaccharides skin care item, including with
Lower step:
1) various raw material is weighed according to aforementioned proportion；
2) by Armillaria mellea crude polysaccharides addition deionized water is stirred continuously, dissolve at being heated to 50-60 DEG C；Oil
Property raw material and nourishing additive agent heating for dissolving under the conditions of 80-85 DEG C, then it is mixed with Armillaria mellea crude polysaccharides
Closing, emulsifying is stirred, and obtains emulsion；Emulsion is cooled to 50-60 DEG C, add wetting agent, preservative,
Antioxidant and brightening agent, stir, and is subsequently cooled to 35-42 DEG C, add carbomer, tea tree ethereal oil with
Deep layer Haiquan water stirs.
Beneficial effects of the present invention:
1, Armillaria mellea crude polysaccharides skin care item can significantly improve skin antioxidation, moisturizing and defying age ability, wherein,
The total antioxidant capacity of Armillaria mellea crude polysaccharides skin care item is more than 52mM/g；After using three days continuously, skin
Moisture increases by more than 240%, and skin collagen fiber content increases by more than 80%, and skin elasticity carries
High by more than 180%.
2, the preparation method of Armillaria mellea crude polysaccharides skin care item is simply, easily operate, and raw material is easy to get, low cost, valency
Lattice are cheap, and skin is not only injured by the medicine added in preparation process, and environmentally safe,
Green, environmental protection.
3, the Armillaria mellea crude polysaccharides extracting method of the present invention is the most efficient, it is possible to effectively by Polyose extraction out.
Detailed description of the invention
Embodiment 1
Armillaria mellea crude polysaccharides preparation method:
1) obtain powder by carrying out pulverizing after Armillaria mellea vacuum lyophilization, then add the water of 15 times of weight
Carry out ultrasonication process after stirring, obtain Armillaria mellea homogenate；
2) by step 1) the Armillaria mellea homogenate that obtains adds the water of 26 times of weight, and 85 DEG C of water-baths extract 1.2
Hour, obtain extracting solution；
3) extracting solution is filtered, and adds ethanol in proper amount after filtrate concentration, make second alcohol precipitation concentration reach 90%,
Obtain armillaria mellea polysaccharide precipitation, after armillaria mellea polysaccharide is precipitated vacuum lyophilization.
Embodiment 2
Armillaria mellea crude polysaccharides preparation method:
1) obtain powder by carrying out pulverizing after Armillaria mellea vacuum lyophilization, then add the water of 20 times of weight
Carry out ultrasonication process after stirring, obtain Armillaria mellea homogenate；
2) by step 1) the Armillaria mellea homogenate that obtains adds the water of 35 times of weight, and 95 DEG C of water-baths extract 0.5
Hour, obtain extracting solution；
3) extracting solution is filtered, and adds ethanol in proper amount after filtrate concentration, make second alcohol precipitation concentration reach 85%,
Obtain armillaria mellea polysaccharide precipitation, after armillaria mellea polysaccharide is precipitated vacuum lyophilization.
Embodiment 3
A kind of Armillaria mellea crude polysaccharides skin care item, are made up of following raw material:
Armillaria mellea crude polysaccharides 15wt% that embodiment 1 prepares, Butyrospermum parkii fruit fat 10wt%, benzene oxygen second
Alcohol 0.5wt%, oryzanol 1wt%, silk fibroin powder 3wt%, Oleum Vitis viniferae 12wt%, carbomer
1wt%, Trenaxmine 1wt%, tea tree ethereal oil 0.6wt% and deep layer Haiquan water 1wt%, surplus is deionized water.
Preparation method, comprises the following steps:
1) various raw material is weighed according to aforementioned proportion；
2) by Armillaria mellea crude polysaccharides addition deionized water is stirred continuously, it is heated at 50 DEG C dissolving；Fructus Vitis viniferae
Seed oil and silk fibroin powder heating for dissolving under the conditions of 80 DEG C, then mix it with Armillaria mellea crude polysaccharides, all
Matter emulsifying is stirred, and obtains emulsion；Emulsion is cooled to 50 DEG C, add Butyrospermum parkii fruit fat, phenoxyethanol,
Oryzanol and Trenaxmine, stir, and is subsequently cooled to 35 DEG C, adds carbomer, tea tree ethereal oil and deep layer
Haiquan water stirs.
Embodiment 4
A kind of Armillaria mellea crude polysaccharides skin care item, are made up of following raw material:
Armillaria mellea crude polysaccharides 20wt%, hyaluronate sodium 8wt%, Sang Pu K15 that embodiment 1 prepares
1wt%, red wine polyphenols 1wt%, Margarita hydrolyzed solution 2wt%, Jojoba oil 14wt%, carbomer 2wt%,
2wt% vitamin B3, tea tree ethereal oil 0.4wt% and deep layer Haiquan water 0.5wt%, surplus is deionized water.
Preparation method, comprises the following steps:
1) various raw material is weighed according to aforementioned proportion；
2) by Armillaria mellea crude polysaccharides addition deionized water is stirred continuously, it is heated at 60 DEG C dissolving；Lotus lotus
Bar oil and Margarita hydrolyzed solution heating for dissolving under the conditions of 82 DEG C, then mix it with Armillaria mellea crude polysaccharides, all
Matter emulsifying is stirred, and obtains emulsion；Emulsion is cooled to 60 DEG C, adds hyaluronate sodium, Sang Pu K15, red
Wine polyphenol and vitamin B3, stir, and is subsequently cooled to 42 DEG C, adds carbomer, tea tree ethereal oil with deep
Layer Haiquan water stirs.
Embodiment 5
A kind of Armillaria mellea crude polysaccharides skin care item, are made up of following raw material:
Armillaria mellea crude polysaccharides 25wt% that embodiment 2 prepares, trimethyl glycine 5wt%, benzene oxygen second
Alcohol 0.5wt%, red wine polyphenols 0.5wt%, polymerization almond protein 4wt%, Jojoba oil 12wt%, card ripple
Nurse 2wt%, Trenaxmine 2wt%, tea tree ethereal oil 0.4wt% and deep layer Haiquan water 2wt%, surplus for go from
Sub-water.
Preparation method, comprises the following steps:
1) various raw material is weighed according to aforementioned proportion；
2) by Armillaria mellea crude polysaccharides addition deionized water is stirred continuously, it is heated at 60 DEG C dissolving；Lotus lotus
Bar oil be polymerized almond protein heating for dissolving under the conditions of 85 DEG C, then it is mixed with Armillaria mellea crude polysaccharides,
Emulsifying is stirred, and obtains emulsion；Emulsion is cooled to 60 DEG C, add trimethyl glycine, phenoxyethanol,
Red wine polyphenols and Trenaxmine, stir, and is subsequently cooled to 42 DEG C, adds carbomer, tea tree ethereal oil with deep
Layer Haiquan water stirs.
Embodiment 6
Armillaria mellea crude polysaccharides skin care item embodiment 3-5 prepared carry out total antioxidation test, use FRAP
Method measures total antioxidant capacity, and test result is as follows: the total antioxidant capacity of embodiment 3-5 is respectively
52.33mM/g, 52.57mM/g, 52.15mM/g.
Moisturizing and defying age performance test
Before test, inside experimenter's arm of cleaning, and with wet gauze (with deionized water) scrub, water
Temperature is room temperature, carries out measurement markers at experimenter's both hands inner forearm after cleaning, and each test zone is spaced 1cm,
Often place's pilot region is 4cm*4cm, within before recipient site 2-3 days, can not use any cosmetic product；Experimenter
Room temperature environment is sat quietly after 30min, use capacitance method moisture of skin analyzer (SG-5D) to measure each district
The moisture value in territory, by 2,000,000 pixel CCD50X portable high-definition intelligent skin detection instrument (EH-800U)
Measure skin collagen fiber content and elasticity indexes.Afterwards test product uniform application is tested in arm
In district, after 40min, carry out measurement and the observation in tested region, sequentially parallel assay five times of each region, draw
Meansigma methods.Tested region METHOD FOR CONTINUOUS DETERMINATION six days, every day measures after product smears 40min and observes.
After result shows and uses six days continuously, the moisture of embodiment 3-5 increases by 240% respectively, 241%,
245%.The collagen fabric content of embodiment 3-5 increases by 81%, 83%, 82% respectively.Embodiment 3-5
Elastic improve 183%, 182%, 185%.
The foregoing is only presently preferred embodiments of the present invention, not in order to limit the present invention, all at this
Within bright spirit and principle, any modification, equivalent substitution and improvement etc. made, should be included in this
Within bright protection domain.
Claims (8)
1. Armillaria mellea crude polysaccharides skin care item, it is characterised in that be made up of following raw material:
Armillaria mellea crude polysaccharides 15-25wt%, wetting agent 5-10wt%, preservative 0.5-1wt%, antioxidant
0.5-1wt%, nourishing additive agent 2-4wt%, oiliness raw material 12-14wt%, carbomer 1-2wt%, brighten
Agent 1-2wt%, tea tree ethereal oil 0.4-0.6wt% and deep layer Haiquan water 0.5-2wt%, surplus is deionized water.
Armillaria mellea crude polysaccharides skin care item the most according to claim 1, it is characterised in that described Armillaria mellea
Crude polysaccharides is prepared via a method which to obtain:
1) obtain powder by carrying out pulverizing after Armillaria mellea vacuum lyophilization, then add 15-20 times of weight
Water carries out ultrasonication process after stirring, and obtains Armillaria mellea homogenate；
2) by step 1) the Armillaria mellea homogenate that obtains adds the water of 26-35 times of weight, and 85-95 DEG C of water-bath carries
Take 0.5-1.2 hour, obtain extracting solution；
3) extracting solution is filtered, and add ethanol in proper amount after filtrate concentration, make second alcohol precipitation concentration reach
85-90%, obtains armillaria mellea polysaccharide precipitation, after armillaria mellea polysaccharide is precipitated vacuum lyophilization.
Armillaria mellea crude polysaccharides skin care item the most according to claim 1 and 2, it is characterised in that described guarantor
Humectant is selected from Butyrospermum parkii fruit fat, tocopherol acetas, trimethyl glycine and the one in hyaluronate sodium
Or it is multiple.
Armillaria mellea crude polysaccharides skin care item the most according to claim 1 and 2, it is characterised in that described anti-
Rotten agent is phenoxyethanol or Sang Pu K15；Described antioxidant is red wine polyphenols or oryzanol.
Armillaria mellea crude polysaccharides skin care item the most according to claim 1 and 2, it is characterised in that described battalion
Support additive selected from silk fibroin powder, Margarita hydrolyzed solution and be polymerized almond protein one or more.
Armillaria mellea crude polysaccharides skin care item the most according to claim 1 and 2, it is characterised in that described oil
Property raw material is Jojoba oil or Oleum Vitis viniferae；Described brightening agent be Trenaxmine with the one in vitamin B3 or
The mixture of two kinds.
7. the preparation method of Armillaria mellea crude polysaccharides skin care item as claimed in claim 1, it is characterised in that
Comprise the following steps:
1) various raw material as claimed in claim 1 is weighed；
2) by Armillaria mellea crude polysaccharides addition deionized water is stirred continuously, dissolve at being heated to 50-60 DEG C；Oil
Property raw material and nourishing additive agent heating for dissolving under the conditions of 80-85 DEG C, then it is mixed with Armillaria mellea crude polysaccharides
Closing, emulsifying is stirred, and obtains emulsion；Emulsion is cooled to 50-60 DEG C, add wetting agent, preservative,
Antioxidant and brightening agent, stir, and is subsequently cooled to 35-42 DEG C, add carbomer, tea tree ethereal oil with
Deep layer Haiquan water stirs.
The preparation method of Armillaria mellea crude polysaccharides skin care item the most according to claim 7, it is characterised in that
Described Armillaria mellea crude polysaccharides is prepared via a method which to obtain:
1) obtain powder by carrying out pulverizing after Armillaria mellea vacuum lyophilization, then add 15-20 times of weight
Water carries out ultrasonication process after stirring, and obtains Armillaria mellea homogenate；
2) by step 1) the Armillaria mellea homogenate that obtains adds the water of 26-35 times of weight, and 85-95 DEG C of water-bath carries
Take 0.5-1.2 hour, obtain extracting solution；
3) extracting solution is filtered, and add ethanol in proper amount after filtrate concentration, make second alcohol precipitation concentration reach
85-90%, obtains armillaria mellea polysaccharide precipitation, after armillaria mellea polysaccharide is precipitated vacuum lyophilization.
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| CN201610402459.3A CN105919871A (en) | 2016-06-01 | 2016-06-01 | Armillaria mellea crude polysaccharide skincare product and preparation method thereof |
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| CN201610402459.3A CN105919871A (en) | 2016-06-01 | 2016-06-01 | Armillaria mellea crude polysaccharide skincare product and preparation method thereof |
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Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN116019737A (en) * | 2023-03-29 | 2023-04-28 | 天齐(内蒙古)生物科技有限公司 | Preparation process and application of easily absorbable bovine and sheep skin collagen peptide |
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| CN103059162A (en) * | 2013-01-14 | 2013-04-24 | 胡玮 | Novel method for effectively extracting lentinan |
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2016
- 2016-06-01 CN CN201610402459.3A patent/CN105919871A/en active Pending
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| CN103059162A (en) * | 2013-01-14 | 2013-04-24 | 胡玮 | Novel method for effectively extracting lentinan |
| CN103800247A (en) * | 2014-02-27 | 2014-05-21 | 上海海洋大学 | Agar crude polysaccharide cream and preparation method thereof |
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Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN116019737A (en) * | 2023-03-29 | 2023-04-28 | 天齐(内蒙古)生物科技有限公司 | Preparation process and application of easily absorbable bovine and sheep skin collagen peptide |
| CN116019737B (en) * | 2023-03-29 | 2023-06-02 | 天齐(内蒙古)生物科技有限公司 | Preparation process and application of easily absorbable bovine and sheep skin collagen peptide |
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Application publication date: 20160907 |