CN105875604A - Biological preparation capable of degrading pesticide residues - Google Patents

Biological preparation capable of degrading pesticide residues Download PDF

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Publication number
CN105875604A
CN105875604A CN201610283407.9A CN201610283407A CN105875604A CN 105875604 A CN105875604 A CN 105875604A CN 201610283407 A CN201610283407 A CN 201610283407A CN 105875604 A CN105875604 A CN 105875604A
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parts
biologic product
hawthorn
burdock
onion
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丁海伟
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Yantai Minwang Electromechanical Technology Co Ltd
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Yantai Minwang Electromechanical Technology Co Ltd
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Priority to CN201610283407.9A priority Critical patent/CN105875604A/en
Publication of CN105875604A publication Critical patent/CN105875604A/en
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    • A—HUMAN NECESSITIES
    • A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N25/00—Biocides, pest repellants or attractants, or plant growth regulators, characterised by their forms, or by their non-active ingredients or by their methods of application, e.g. seed treatment or sequential application; Substances for reducing the noxious effect of the active ingredients to organisms other than pests
    • A01N25/32—Ingredients for reducing the noxious effect of the active substances to organisms other than pests, e.g. toxicity reducing compositions, self-destructing compositions
    • A—HUMAN NECESSITIES
    • A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N65/00—Biocides, pest repellants or attractants, or plant growth regulators containing material from algae, lichens, bryophyta, multi-cellular fungi or plants, or extracts thereof
    • A—HUMAN NECESSITIES
    • A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N65/00—Biocides, pest repellants or attractants, or plant growth regulators containing material from algae, lichens, bryophyta, multi-cellular fungi or plants, or extracts thereof
    • A01N65/40—Liliopsida [monocotyledons]
    • A01N65/42—Aloeaceae [Aloe family] or Liliaceae [Lily family], e.g. aloe, veratrum, onion, garlic or chives
    • A—HUMAN NECESSITIES
    • A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
    • A23L3/00—Preservation of foods or foodstuffs, in general, e.g. pasteurising, sterilising, specially adapted for foods or foodstuffs
    • A23L3/34—Preservation of foods or foodstuffs, in general, e.g. pasteurising, sterilising, specially adapted for foods or foodstuffs by treatment with chemicals
    • A23L3/3454—Preservation of foods or foodstuffs, in general, e.g. pasteurising, sterilising, specially adapted for foods or foodstuffs by treatment with chemicals in the form of liquids or solids
    • A23L3/3463—Organic compounds; Microorganisms; Enzymes
    • A23L3/3472—Compounds of undetermined constitution obtained from animals or plants
    • C—CHEMISTRY; METALLURGY
    • C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09K—MATERIALS FOR MISCELLANEOUS APPLICATIONS, NOT PROVIDED FOR ELSEWHERE
    • C09K17/00—Soil-conditioning materials or soil-stabilising materials
    • C09K17/14—Soil-conditioning materials or soil-stabilising materials containing organic compounds only
    • A—HUMAN NECESSITIES
    • A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23V—INDEXING SCHEME RELATING TO FOODS, FOODSTUFFS OR NON-ALCOHOLIC BEVERAGES AND LACTIC OR PROPIONIC ACID BACTERIA USED IN FOODSTUFFS OR FOOD PREPARATION
    • A23V2002/00—Food compositions, function of food ingredients or processes for food or foodstuffs
    • C—CHEMISTRY; METALLURGY
    • C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09K—MATERIALS FOR MISCELLANEOUS APPLICATIONS, NOT PROVIDED FOR ELSEWHERE
    • C09K2101/00—Agricultural use
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02A—TECHNOLOGIES FOR ADAPTATION TO CLIMATE CHANGE
    • Y02A50/00—TECHNOLOGIES FOR ADAPTATION TO CLIMATE CHANGE in human health protection, e.g. against extreme weather
    • Y02A50/30—Against vector-borne diseases, e.g. mosquito-borne, fly-borne, tick-borne or waterborne diseases whose impact is exacerbated by climate change

Abstract

The invention discloses a biological preparation capable of degrading pesticide residues. The biological preparation is prepared from the following components: apples, pomegranates, watermelons, oranges, strawberries, shaddocks, star fruits, bananas, kiwi fruits, hawthorn fruits, cherries, water chestnuts, grapes, lemons, tomatoes, chilies, eggplants, wax gourds, carrots, celery, onions, burdocks, Chinese yams, bitter gourds, lotus roots, mushrooms, black fungi and semen juglandis. The biological preparation has the beneficial effects that the pesticide residues in crops can be degraded; soil is improved and the production increasing of the crops is promoted; early maturing of the crops is facilitated; the quality and palatability of the crops are improved; the rice yield of paddy rice is improved; the storage period of agricultural products is prolonged and the soil and water quality can be improved; non-point source pollution is improved.

Description

A kind of biologic product of degrading pesticide residues
Technical field
The present invention relates to biologic product technology field, particularly to the biologic product of a kind of degrading pesticide residues.
Background technology
At Farming, store, the link such as processing uses agricultural chemicals, protective agent, fumigant, additive etc. in a large number, these all may be enriched with by food chain, agricultural chemicals is in fish, fowl, the enrichment of carcass, make pollution by pesticides even more serious, the persistent pesticide being often enriched with larger dose in the human body of extreme higher position it is in food chain, these agricultural chemicals all cannot be used for alimentary crop in terms of its chronic toxicity and residual, all can bring the biggest harm to health.
Edible a small amount of remains of pesticide, human body self can be degraded, acute poisoning will not be caused suddenly, but it is eaten for a long time and does not clean up the agricultural product with remains of pesticide, health will necessarily be brought harm greatly, its harm mainly has: one, cause body immunity to decline: to be eaten for a long time the dish with remains of pesticide, after agricultural chemicals is absorbed by the blood, nerve synapse and neuromuscular junction can be distributed to, directly damage neuron, cause nervous centralis dead, cause health each organ immunity degradation.Such as, regular flu, dizziness, palpitaition, night sweat, insomnia, forgetful etc..Two, it is potentially carcinogenic: the chemical substance usually contained in remains of pesticide can promote each tissue inner cell generation canceration.Three, increase the weight of burden of liver: remains of pesticide enter internal, rely primarily on liver manufacture enzyme to absorb these toxin, carry out oxidation Decomposition.If being eaten for a long time the gourd, fruit and vegetable with remains of pesticide, liver will work without cessation and decompose these toxin.Overwork can cause some dry hepatic diseases such as cirrhosis, hydrohepatosis for a long time.Four, enterogastric diseases is caused: owing to pipe intestinal digesting system coat of the stomach fold is more, easily deposit poisonous substance.So remains of pesticide easily accumulates in wherein, cause chronic diarrhea, feel sick etc. symptom.
Additionally the grand nutrition element nitrogen in soil, phosphorus, potassium are generally not capable of meeting the demand of plant growth, current crops need to use chemical fertilizer nitrogenous, phosphorus, potassium and supply, dechlorinating in micronutrient element outside not lacking in soil, the most several nutrients the most all need to use trace-element fertilizer.The use of chemical fertilizer and agricultural chemicals brings a lot of drawback: exploit processing from the raw material of chemical fertilizer, always brings some heavy metal elements or noxious material into chemical fertilizer, is directly detrimental to health, and producing the heavy metal polluted mainly has Zn, Cu, Co and Cr；Can reduce soil microbial activities, material is difficult to convert and degrade；Chronic administration causes soil nutrient to lack of proper care；Chronic administration chemical fertilizer accelerates soil acidification, reduces degree of base saturation and soil fertility；The residues of pesticides of crop can have a strong impact on health；Atmosphere pollution, water environment, cause soil compaction；Strengthen germ, the insect resistance to the action of a drug to agricultural chemicals, murder beneficial organism.
The most effectively degrading the residues of pesticides in agricultural product, improvement soil, reduce the water that causes of chemical fertilizer and pollute, improving pollution of area source becomes and produces one of upper difficult problem the most in the urgent need to address at present.
Summary of the invention
The invention provides a kind of degrading pesticide residues, improvement soil, reduce water and pollute, improve the biologic product of pollution of area source, the plant growth existed to solve prior art uses chemical fertilizer and agricultural chemicals to cause soil nutrient imbalance and the problem of residues of pesticides.
In order to realize foregoing invention purpose, the invention provides the biologic product of a kind of degrading pesticide residues, including following components: apple, pomegranate, watermelon, orange, strawberry, shaddock, carambola, banana, Kiwi berry, hawthorn, cherry, water chestnut, grape, lemon, tomato, capsicum, eggplant, wax gourd, carrot, celery, onion, burdock, Chinese yam, balsam pear, lotus root, mushroom, auricularia auriculajudae and diaphragma juglandis.
nullDescribed biologic product includes the component of following weight portion: apple 10-14 part、Pomegranate 7-12 part、Watermelon 28-32 part、Orange 53-57 part、Strawberry 35-39 part、Shaddock 37-41 part、Carambola 24-28 part、Banana 4-8 part、Kiwi berry 16-24 part、Hawthorn 7-12 part、Cherry 5-9 part、Water chestnut 4-8 part、Grape 28-32 part、Lemon 18-22 part、Tomato 24-28 part、Capsicum 2-6 part、Eggplant 12-18 part、Wax gourd 36-40 part、Carrot 9-15 part、Celery 10-14 part、Onion 10-15 part、Burdock 15-20 part、Chinese yam 19-26 part、Balsam pear 10-17 part、Lotus root 12-17 part、Mushroom 10-15 part、Auricularia auriculajudae 13-19 part and diaphragma juglandis 22-30 part.
Described biologic product includes the component of following weight portion: apple 10 parts, pomegranate 12 parts, watermelon 32 parts, orange 53 parts, strawberry 36 parts, shaddock 38 parts, carambola 24 parts, 8 parts of banana, Kiwi berry 21 parts, hawthorn 11 parts, 5 parts of cherry, water chestnut 4 parts, grape 32 parts, 19 parts of lemon, 26 parts of tomato, 3 parts of capsicum, eggplant 16 parts, 40 parts of wax gourd, 15 parts of carrot, celery 13 parts, onion 10 parts, burdock 20 parts, Chinese yam 19 parts, 15 parts of balsam pear, lotus root 12 parts, mushroom 12 parts, 17 parts of auricularia auriculajudae and diaphragma juglandis 30 parts.
Described biologic product includes the component of following weight portion: apple 14 parts, pomegranate 7 parts, watermelon 28 parts, orange 57 parts, strawberry 35 parts, shaddock 41 parts, carambola 28 parts, 4 parts of banana, Kiwi berry 24 parts, hawthorn 12 parts, 9 parts of cherry, water chestnut 7 parts, grape 30 parts, 22 parts of lemon, 24 parts of tomato, 2 parts of capsicum, eggplant 12 parts, 36 parts of wax gourd, 13 parts of carrot, celery 10 parts, onion 14 parts, burdock 15 parts, Chinese yam 23 parts, 10 parts of balsam pear, lotus root 14 parts, mushroom 15 parts, 13 parts of auricularia auriculajudae and diaphragma juglandis 22 parts.
Described biologic product includes the component of following weight portion: apple 12 parts, pomegranate 11 parts, watermelon 30 parts, orange 54 parts, strawberry 39 parts, shaddock 37 parts, carambola 25 parts, 7 parts of banana, Kiwi berry 16 parts, hawthorn 7 parts, 6 parts of cherry, water chestnut 8 parts, grape 28 parts, 18 parts of lemon, 28 parts of tomato, 6 parts of capsicum, eggplant 18 parts, 38 parts of wax gourd, 9 parts of carrot, celery 14 parts, onion 15 parts, burdock 17 parts, Chinese yam 26 parts, 17 parts of balsam pear, lotus root 17 parts, mushroom 10 parts, 19 parts of auricularia auriculajudae and diaphragma juglandis 26 parts.
In order to goal of the invention is better achieved, the present invention also provides for the preparation method of the biologic product of a kind of degradable residues of pesticides, comprises the following steps:
Step one, take orange, hawthorn, onion, burdock, Chinese yam and balsam pear in proportion and mix to obtain mixture one, it is subsequently adding alcohol immersion 3-8 hour that alcohol volume content is 70-80% being equivalent to mixture one mass 12-14 times, filter, collect filtrate, when filtrate is evaporated under vacuum 0.05～0.06Mpa 60～70 DEG C subsequently, relative density is the lotion of 1.05～1.10, it is spray-dried, the EAT 160 of spray dryer～175 DEG C, leaving air temp 80～85 DEG C, it is ground into powder subsequently, makes dried cream powder；
Step 2, taking diaphragma juglandis in proportion and be subsequently adding the 3 ° of soaking in rice vinegar 30-60min being equivalent to diaphragma juglandis quality 10 times, then intense fire boils and uses slow fire instead and decoct slowly 15-20 minute, filters, obtains filtrate a, standby；
Step 3, take remaining ingredient input pulverizer in proportion to pulverize, after pulverizing, cross 2.0mm sieve to obtain mixture two, the dried cream powder that step one prepares is added in mixture two, the filtrate a that step 2 prepares ferments more than 120 days at 15-35 DEG C after mixing, after taking filtering fermentation liquor, obtain filtrate b and be the biologic product of degradable residues of pesticides.
The technical scheme that the embodiment of the present invention provides has the benefit that
(1) degraded crop Pesticide Residues.Use one day just can residues of pesticides in efficient degradation plant, after 3 days, chemical residual degradation effect is more than 99%, and after 5 days, residues of pesticides do not detect and ensure that vegetable pesticide residue does not exceeds standard.
(2) crop yield is promoted.Experiment field average yield per mu is at more than 500kg, and compares field average yield per mu less than 400kg, and volume increase is more than 40%.Carried out celery, cucumber cultivation experiment in Heilungkiang, effect of increasing production is obvious.
Promote early ripening of the crops.Phytoenzyme in this product has powerful catalytic action, can accelerate biochemical reaction and the photosynthesis of crop, thus realize crop maturation ahead of time.Same kind does sth. in advance ripe about one week, it is achieved that planting across snow change of improved seeds.
Improve paddy rice rice milling yield.It is ripe that the biologic product of the present invention not only promotes paddy rice, and compared with the rice fragrance of a flower of Wuchang City's plantation, rice milling yield improves more than 3%.
(4) crop quality and palatability are improved.Using the paddy rice that this product is planted, detect through National agricultural portion grain quality Supervision Test Center, its gel consistence index is 75, and amylose index is 18.41, and rice taste delicate fragrance, palatability is strong.Using flowers and melon and fruit that this product plants, flowers color and luster beauty is bright-coloured, longer blooming period；Melon and fruit color and luster is bright and new, and sugar content is high.
(5) paddy rice rice milling yield is improved.2013, we used the source activity silicon liquid of standing grain to plant five excellent 4 paddy rice (i.e. Wuchang City's brand paddy rice rice fragrance of a flower, 14 leaves in Jidong County of Heilongjiang Province, it is the first snow change crop), not only promote paddy rice ripe, and compared with the rice fragrance of a flower of Wuchang City's plantation, rice milling yield improves 3%.
(6) agricultural product storage period is extended.The agricultural product using the source activity silicon liquid of standing grain to produce, can make its color and luster bright and new, and shelf-stable extends the freshness date of product.
(7) improvement soil and water quality.The mode using drip irrigation is arranged in field, the rapid amount reproduction of profitable strain in soil can be promoted, sufficient nutrition is provided for plant growth, and can effectively improve soil texture, promote soil remains the decomposition of chemical fertilizer composition, accelerating crop to absorb the effective of the chemical fertilizer composition of residual in soil, improvement soil is gone forward side by side and is improved water quality.
The biologic product of the embodiment of the present invention can significantly hold soil, reduces soil erosion, reduces ammonium nitrogen, total nitrogen and total phosphorus that rainwash is taken away, this is because the unit weight of soil declines, porosity increases, and improves the permeability of soil, decreases flow path surface.The biologic product of the present invention can promote the rapid amount reproduction of profitable strain in soil, sufficient nutrition is provided for plant growth, and can effectively improve soil texture, promote soil remains the decomposition of chemical fertilizer composition, reduce salinity, accelerating crop to absorb the effective of the chemical fertilizer composition of residual in soil, improvement soil is gone forward side by side and is improved water quality and reduce pollution of area source.
The biologic product of the present invention can improve the soil acidification because causing with chemical fertilizer, increases soil fertility；Additionally can also degrade unnecessary salinity.
Detailed description of the invention
High for current crops residues of pesticides, the problems such as the use of agriculture chemical causes soil texture to destroy, environmental pollution, the present invention provides the biologic product of a kind of degrading pesticide residues.
The biologic product of the degrading pesticide residues of the present invention, including following components: apple, pomegranate, watermelon, orange, strawberry, shaddock, carambola, banana, Kiwi berry, hawthorn, cherry, water chestnut, grape, lemon, tomato, capsicum, eggplant, wax gourd, carrot, celery, onion, burdock, Chinese yam, balsam pear, lotus root, mushroom, auricularia auriculajudae and diaphragma juglandis.
Wherein:
Mushroom: another name agaricus bisporus, mushroom, ocean gill fungus, ocean bacterium, ocean straw mushroom fine and soft, Western.Mycophyta Basidiomycetes Agaricales Agaricaceae mushroom, is used as medicine with fructification.Sweet, flat.Help digestion, clearly god, flat liver-yang.Cure mainly indigestion, hypertension.
Auricularia auriculajudae: another name, wood, parasitism, gill fungus ear, tree chicken, black fungus, wood fungus, wood moth, cloud ear, the ears or side handles of a utensil, brightness program, wood young pilose antler on mulberry.For Auriculariaceae fungi auricularia auriculajudae, Uricularia polytricha and the fructification of wrinkle auricularia auriculajudae.Sweet；Flat.Return lung；Stomach；Liver；Spleen；Kidney；Large intestine channel.Benefiting qi and nourishing blood;Moisten the lung and relieve the cough;Hemostasis;Step-down;Anticancer.Main Qi and blood deficiency;Chronic cough of deficiency lung;Hemoptysis;Bleeding from five sense organs or subcutaneous tissue;Bloody flux;Hemorrhoid hemorrhage;Woman uterine bleeding;Hypertension;Fundus hemorrhage;Cervix cancer;Carcinoma of vagina;Injuries from falls as well.
Diaphragma juglandis: another name walnut kind every.This product is the wooden barrier film of juglandaceae plant English walnut.Bitter, puckery, flat.The puckery essence of kidney tonifying.For emission due to the kidney deficiency, involuntary emission, the enuresis.
Hereinafter using embodiment to describe embodiments of the present invention in detail, to the present invention, how application technology means solve technical problem whereby, and the process that realizes reaching technique effect can fully understand and implement according to this.
The biologic product 1 of embodiment 1 present invention
Embodiments provide the biologic product of a kind of degrading pesticide residues, biologic product includes the component of following weight portion: apple 10kg, pomegranate 12kg, watermelon 32kg, orange 53kg, strawberry 36kg, shaddock 38kg, carambola 24kg, banana 8kg, Kiwi berry 21kg, hawthorn 11kg, cherry 5kg, water chestnut 4kg, grape 32kg, lemon 19kg, tomato 26kg, capsicum 3kg, eggplant 16kg, wax gourd 40kg, carrot 15kg, celery 13kg, onion 10kg, burdock 20kg, Chinese yam 19kg, balsam pear 15kg, lotus root 12kg, mushroom 12kg, auricularia auriculajudae 17kg and diaphragma juglandis 30kg.
Its preparation method comprises the following steps:
Step one, take orange, hawthorn, onion, burdock, Chinese yam and balsam pear in proportion and mix to obtain mixture one, it is subsequently adding the alcohol immersion that alcohol volume content is 80% 8 hours being equivalent to mixture one mass 12 times, filtering, collect filtrate, it is the lotion of 1.05 that filtrate is evaporated under vacuum 0.06Mpa relative density subsequently when 60 DEG C, it is spray-dried, the EAT of spray dryer 160 DEG C, leaving air temp 85 DEG C, be ground into powder subsequently, make dried cream powder；
Step 2, taking diaphragma juglandis in proportion and be subsequently adding the 3 ° of soaking in rice vinegar 60min being equivalent to diaphragma juglandis quality 10 times, then intense fire boils and uses slow fire instead and decoct slowly 20 minutes, filters, obtains filtrate a, standby；
Step 3, take remaining ingredient input pulverizer in proportion to pulverize, after pulverizing, cross 2.0mm sieve to obtain mixture two, the dried cream powder that step one prepares is added in mixture two, step 2 prepare filtrate a mix after 35 DEG C of spontaneous fermentations 150 days, after taking filtering fermentation liquor, obtain filtrate b and be the biologic product of degradable residues of pesticides.
The biologic product 2 of embodiment 2 present invention
Embodiments provide the biologic product of a kind of degrading pesticide residues, biologic product includes the component of following weight portion: apple 14kg, pomegranate 7kg, watermelon 28kg, orange 57kg, strawberry 35kg, shaddock 41kg, carambola 28kg, banana 4kg, Kiwi berry 24kg, hawthorn 12kg, cherry 9kg, water chestnut 7kg, grape 30kg, lemon 22kg, tomato 24kg, capsicum 2kg, eggplant 12kg, wax gourd 36kg, carrot 13kg, celery 10kg, onion 14kg, burdock 15kg, Chinese yam 23kg, balsam pear 10kg, lotus root 14kg, mushroom 15kg, auricularia auriculajudae 13kg and diaphragma juglandis 22kg.
Its preparation method comprises the following steps:
Step one, take orange, hawthorn, onion, burdock, Chinese yam and balsam pear in proportion and mix to obtain mixture one, it is subsequently adding the alcohol immersion that alcohol volume content is 80% 6 hours being equivalent to mixture one mass 13 times, filtering, collect filtrate, it is the lotion of 1.10 that filtrate is evaporated under vacuum 0.06Mpa relative density subsequently when 70 DEG C, it is spray-dried, the EAT of spray dryer 175 DEG C, leaving air temp 80 DEG C, be ground into powder subsequently, make dried cream powder；
Step 2, taking diaphragma juglandis in proportion and be subsequently adding the 3 ° of soaking in rice vinegar 30min being equivalent to diaphragma juglandis quality 10 times, then intense fire boils and uses slow fire instead and decoct slowly 15 minutes, filters, obtains filtrate a, standby；
Step 3, take remaining ingredient input pulverizer in proportion to pulverize, after pulverizing, cross 2.0mm sieve to obtain mixture two, the dried cream powder that step one prepares is added in mixture two, step 2 prepare filtrate a mix after 25 DEG C of spontaneous fermentations 160 days, after taking filtering fermentation liquor, obtain filtrate b and be the biologic product of degradable residues of pesticides.
The biologic product 3 of embodiment 3 present invention
Embodiments provide the biologic product of a kind of degrading pesticide residues, biologic product includes the component of following weight portion: apple 12kg, pomegranate 11kg, watermelon 30kg, orange 54kg, strawberry 39kg, shaddock 37kg, carambola 25kg, banana 7kg, Kiwi berry 16kg, hawthorn 7kg, cherry 6kg, water chestnut 8kg, grape 28kg, lemon 18kg, tomato 28kg, capsicum 6kg, eggplant 18kg, wax gourd 38kg, carrot 9kg, celery 14kg, onion 15kg, burdock 17kg, Chinese yam 26kg, balsam pear 17kg, lotus root 17kg, mushroom 10kg, auricularia auriculajudae 19kg and diaphragma juglandis 26kg.
Its preparation method comprises the following steps:
Step one, take orange, hawthorn, onion, burdock, Chinese yam and balsam pear in proportion and mix to obtain mixture one, it is subsequently adding the alcohol immersion that alcohol volume content is 70% 3 hours being equivalent to mixture one mass 14 times, filtering, collect filtrate, it is the lotion of 1.05 that filtrate is evaporated under vacuum 0.05Mpa relative density subsequently when 60 DEG C, it is spray-dried, the EAT of spray dryer 160 DEG C, leaving air temp 85 DEG C, be ground into powder subsequently, make dried cream powder；
Step 2, taking diaphragma juglandis in proportion and be subsequently adding the 3 ° of soaking in rice vinegar 40min being equivalent to diaphragma juglandis quality 10 times, then intense fire boils and uses slow fire instead and decoct slowly 20 minutes, filters, obtains filtrate a, standby；
Step 3, take remaining ingredient input pulverizer in proportion to pulverize, after pulverizing, cross 2.0mm sieve to obtain mixture two, the dried cream powder that step one prepares is added in mixture two, the filtrate a that step 2 prepares ferments more than 180 days at 15 DEG C after mixing, after taking filtering fermentation liquor, obtain filtrate b and be the biologic product of degradable residues of pesticides.
When preparing biologic product, the method one begun to use is:
Step one, take orange, hawthorn, onion, burdock, Chinese yam and balsam pear in proportion and mix to obtain mixture one, it is subsequently adding alcohol immersion 3-8 hour that alcohol volume content is 70-80% being equivalent to mixture one mass 12-14 times, filter, collect filtrate, when filtrate is evaporated under vacuum 0.05～0.06Mpa 60～70 DEG C subsequently, relative density is the lotion of 1.05～1.10, it is spray-dried, the EAT 160 of spray dryer～175 DEG C, leaving air temp 80～85 DEG C, it is ground into powder subsequently, makes dried cream powder；
Step 2, take remaining ingredient input pulverizer in proportion to pulverize, after pulverizing, cross 2.0mm sieve to obtain mixture two, the dried cream powder that step one prepares is added in mixture two, ferment more than 120 days at 15-35 DEG C after mixing, after taking filtering fermentation liquor, obtain filtrate b and be the biologic product of degradable residues of pesticides.
Finding later, in embodiment in biologic product preparation process, diaphragma juglandis is more preferable by the biologic product effect of preparation after 3 ° of soaking in rice vinegar, and when the biologic product of ratio method one preparation uses, each side effect improves 3-8%.
Contrast test:
The biologic product of the degradable residues of pesticides of the present invention has carried out substantial amounts of Rice Cropping and the experiment of the vegetable growing such as cucumber, celery in Heilungkiang, carry out vegetable growing experiment on Zhangqiu City of Shandong Province, Tai'an and other places, and carried out tealeaves on the ground such as Hubei, Fujian and spray experiment.Test result indicate that the present invention has the effect that
(1) degraded crop Pesticide Residues.This product has carried out the experiment of substantial amounts of Rice Cropping in Heilongjiang Province, from 40,000 mu of the planting experiment base of experimental planting 1300 mu to 2014.
Quarter Design test is divided into 3 process, random alignment, and in triplicate, result takes three mean values, 1. 2. agent degradation district of test medicine district, each process She Liangge community.Within 3 days, spray the biologic product degrading pesticide residues of the present invention every time after dispenser, compare degradation effect with medicament district.The results are shown in Table 1.
The biologic product of table 1 embodiment of the present invention 1 reduces the data of crop Pesticide Residues
Outstanding feature is under the usage amount of normal agricultural chemicals, use one day just can residues of pesticides in efficient degradation plant, after 3 days, chemical residual degradation effect is more than 99%, and after 5 days, residues of pesticides do not detect and ensure that vegetable pesticide residue does not exceeds standard.
Detect through National agricultural portion grain quality Supervision Test Center, use the paddy rice of biologic product output of the present invention, can the effectively chemical fertilizer of use and farm chemical ingredients in degrading rice planting process, paddy does not has any residues of pesticides；And the paddy rice of the biologic product output being provided without the present invention of correspondence, its paddy has obvious agricultural chemicals.The growing vegetables such as the celery carried out in Shandong Province, potato test result indicate that do not have any residues of pesticides in addition to tomato in other vegetables；Tomato the most only detects a small amount of residual of a kind of agricultural chemicals.The results are shown in Table 2-table 7
Table 2 uses the paddy rice testing result of the biologic product 2 of the present invention
Detection project Unit Standard-required Testing result Method detection limit Individual event judges The method of inspection
DDVP mg/kg ≤0.05 Do not detect <0.01 Qualified GB/T 5009.20—2003
Rogor mg/kg ≤0.02 Do not detect <0.01 Qualified GB/T 5009.20—2003
Malathion mg/kg ≤0.1 Do not detect <0.01 Qualified GB/T 5009.20—2003
Fenifrothion mg/kg ≤1.0 Do not detect <0.01 Qualified GB/T 5009.20—2003
Entex mg/kg Must not detect (< 0.01) Do not detect <0.01 Qualified GB/T 5009.20—2003
Hostathion mg/kg ≤0.05 Do not detect <0.01 Qualified GB/T 5009.20—2003
Chlopyrifos mg/kg ≤0.1 Do not detect <0.01 Qualified GB/T 5009.20—2003
Chlorpyrifos-methyl mg/kg ≤5 Do not detect <0.01 Qualified GB/T 5009.20—2003
Acephatemet mg/kg Must not detect (< 0.004) Do not detect <0.004 Qualified GB/T 5009.103—2003
Tricyclazole mg/kg ≤1.0 Do not detect <0.05 Qualified GB/T 5009.115—2003
Dimehypo mg/kg ≤0.1 Do not detect <0.05 Qualified GB/T 5009.114—2003
BHC mg/kg ≤0.05 Do not detect <0.00016 Qualified GB/T 5009.19—2008
DDT mg/kg ≤0.05 Do not detect <0.0024 Qualified GB/T 5009.19—2008
Decis mg/kg ≤0.5 Do not detect <0.00088 Qualified GB/T 5009.110—2003
Table 3 contrast groups uses the paddy rice testing result of other preparations
Detection project Unit Standard-required Testing result Method detection limit Individual event judges The method of inspection
DDVP mg/kg ≤0.05 Do not detect <0.01 Qualified GB/T 5009.20—2003
Rogor mg/kg ≤0.02 Do not detect <0.01 Qualified GB/T 5009.20—2003
Malathion mg/kg ≤0.1 Do not detect <0.01 Qualified GB/T 5009.20—2003
Fenifrothion mg/kg ≤1.0 Do not detect <0.01 Qualified GB/T 5009.20—2003
Entex mg/kg Must not detect (< 0.01) Do not detect <0.01 Qualified GB/T 5009.20—2003
Hostathion mg/kg ≤0.05 0.07 <0.01 Defective GB/T 5009.20—2003
Chlopyrifos mg/kg ≤0.1 0.03 <0.01 Defective GB/T 5009.20—2003
Chlorpyrifos-methyl mg/kg ≤5 Do not detect <0.01 Qualified GB/T 5009.20—2003
Acephatemet mg/kg Must not detect (< 0.004) Do not detect <0.004 Qualified GB/T 5009.103—2003
Tricyclazole mg/kg ≤1.0 2.12 <0.05 Defective GB/T 5009.115—2003
Dimehypo mg/kg ≤0.1 Do not detect <0.05 Qualified GB/T 5009.114—2003
BHC mg/kg ≤0.05 Do not detect <0.00016 Qualified GB/T 5009.19—2008
DDT mg/kg ≤0.05 Do not detect <0.0024 Qualified GB/T 5009.19—2008
Decis mg/kg ≤0.5 0.82 <0.00088 Defective GB/T 5009.110—2003
Table 4 uses the testing result detection of the wheat of the biologic product 3 of the present invention according to NY/T 421 2012
Detection project Unit Standard-required Testing result Single item evaluation
Total arsenic mg/kg ≤0.5 Do not detect Qualified
Lead mg/kg ≤0.05 Do not detect Qualified
Cadmium mg/kg ≤0.1 0.008 Qualified
Carbofuran mg/kg ≤0.05 Do not detect Qualified
Aphox mg/kg ≤0.05 Do not detect Qualified
Phoxim mg/kg ≤0.05 Do not detect Qualified
Pyrrole worm mg/kg ≤0.05 Do not detect Qualified
Thimet mg/kg ≤0.01 Do not detect Qualified
Triazolone mg/kg ≤0.1 Do not detect Qualified
Cypermethrin mg/kg ≤0.2 Do not detect Qualified
Decis mg/kg ≤0.2 Do not detect Qualified
Fenvalerate mg/kg ≤2 Do not detect Qualified
The dead tick of element mg/kg ≤0.1 Do not detect Qualified
Rogor mg/kg ≤0.05 Do not detect Qualified
Phosphide mg/kg ≤0.05 Negative reaction Qualified
Chloropicrin mg/kg ≤0.1 Do not detect Qualified
Aflatoxins element B1 μg/kg ≤5 Do not detect Qualified
Zearalenone μg/kg ≤60 Do not detect Qualified
Deoxynivalenol μg /kg ≤1000 Do not detect Qualified
Table 5 uses the Vegetable testing result of the biologic product of the present invention
Table 6 uses the Vegetable testing result of the biologic product of the present invention
Table 7 uses the Vegetable testing result of the biologic product of the present invention
(2) crop yield is promoted
This product is at Rice in Hei Longjiang Province planting experiment, and experiment water in field rice base fertilizer can suitably consider minimizing with topdressing, and in rice tillering, booting, grouting three stage, carries out liquid level in 1:300 ratio with the biologic product of the water dilution present invention and sprays；Comparison field is normally arranged base fertilizer and topdresses.The results are shown in Table 8.
The biologic product of table 8 present invention promotes crop yield statistics
Result: experiment field average yield per mu is at more than 570kg, and compares field average yield per mu less than 400kg, and volume increase (667 square metres every mu, test 1000 mu of field) more than 45%, effect of increasing production is obvious.
Improve paddy rice rice milling yield.It is ripe that the biologic product of the present invention not only promotes paddy rice, and compared with the rice fragrance of a flower of Wuchang City's plantation, rice milling yield improves more than 5%.
Table 9 uses the biologic product 2 of the present invention and does not uses the paddy rice testing result of biologic product control group of the present invention
Detection project Unit Use the biologic product 2 of the present invention Control group The method of inspection
Brown rice yield % 79.8 75.5 GB/T 5495—2008
Head rice rate % 67.4 66.7 GB/T 21719—2008
Chalky grain rate % 4.0 8.0 GB/T 17891—1999
Chalkiness degree % 0.9 1.3 GB/T 17891—1999
Amylose (accounts for sample dry weight) % 18.41 18.90 NY/T 55—1987
Gel consistence mm 75.0 70.0 GB/T 17,891 1999 appendix A
Taste evaluation Point 81 73 GB/T 17,891 1999 Appendix B
(3) early ripening of the crops is promoted.Phytoenzyme in this product has powerful catalytic action, can accelerate biochemical reaction and the photosynthesis of crop, thus realize crop maturation ahead of time.We are at area, crescent moon lake, Hulin City, Heilongjiang Province fragrant No. 2 paddy rice (13 leaves of the loose round-grained rice of (the 3rd snow change lower limit) experimental planting, it is the first snow change crop) 1300 mus, the most ripe 7 days of the kind more same than Heilongjiang Province Wuchang City (the first snow change), it is achieved that planting across snow change of improved seeds.
(4) crop quality and palatability are improved.Using the paddy rice that this product is planted, detect through National agricultural portion grain quality Supervision Test Center, its gel consistence index is 75, and amylose index is 18.41, and rice taste delicate fragrance, palatability is strong.Using flowers and melon and fruit that this product plants, flowers color and luster beauty is bright-coloured, longer blooming period；Melon and fruit color and luster is bright and new, and sugar content is high.
(5) agricultural product storage period is extended.The agricultural product using biologic product of the present invention to produce, can make its color and luster bright and new, shelf-stable, extend the freshness date of product.
(6) improvement soil and water quality.
Experimental design: wheat paddock, area 2hm are selected in test2.Take split plot experiment to design, if 4 process, plant respectively and use embodiment 1, embodiment 2, the biologic product of embodiment 3, and blank.The biologic product of the present invention is pressed the dilution of 1:300 ratios with water, uses the mode of drip irrigation to arrange in field, every kind of processing area 0.5hm2, check plot 0.4hm2.Along gutter, field, 9 areas are selected to be 1m at each treatment region2The community of (1m × 1m), the gradient is about 7 °.Face, community three is inserted perpendicularly into plastic plate, embedded depth 10cm, and aerial part, away from ground 10cm, an opening, is connected with gutter, field.In gutter, lay plastic sheeting, be used for collecting rainwater.Film is paved with sward district joining place soil, it is ensured that rainwater Channel Group, ne-leakage.In 9 communities that each sward district selects, being randomly provided 3 nitrogen fertilizer applications (urea) and process, dose is respectively 300kg/hm2；Fertilization mode uses the method for foliage-spray, to reach the purpose of uniform of application.Each fertilizer treatment repeats for 3 times, and fertilizer treatment, after 1 week, starts artificially-simulated rainfall process.
Artificially-simulated rainfall designs: for ensureing the collection of artificial rainfall runoff, rainfall is designed as heavy rain level.Rainfall is about 1mm/min.Use watering can simulated rainfall, time 10min, water consumption 15L.After simulated rainfall terminates, collect and collect in the water laying in plastic sheeting, calculate run-off, take 50ml water simultaneously, measure for nitrogen, phosphorus, potassium content.The results are shown in Table 10.
The impact on water pollution of area source of table 10 biologic product of the present invention
Biologic product Flow path surface ml Ammonium nitrogen mg/l Total nitrogen mg/l Total phosphorus mg/l
Control group 2104 15.6 16.9 4.3
Embodiment 1 1365 6.5 11.2 2.4
Embodiment 2 1270 6.8 11.3 2.7
Embodiment 3 1033 8.2 12.1 2.6
During it addition, do not use this biologic product of the present invention (before wheat field planting), the soil salt initial value of mensuration is respectively 6.07g/kg, 6.03 g/kg, 6.05 g/kg, and mean value is 6.05g/kg.Rear result is used to see table 11.
Disease index is the overall target comprehensively considering the incidence of disease and severity.If in units of blade.When severity is expressed as a percentage, disease index computing formula is: the disease index=incidence of disease × severity.
Its root density is measured during wheat 35-43cm.
* indicating: in a, 4 process, each process uses 3 point samplings, and every some investigation plant strain number is 50, and indices test value is every sampling point 50 strain number mean value；
The effect to wheat paddock of the biologic product of table 11 present invention
The biologic product of the embodiment of the present invention can significantly hold soil, reduces soil erosion, reduces ammonium nitrogen, total nitrogen and total phosphorus that rainwash is taken away, this is because the unit weight of soil declines, porosity increases, and improves the permeability of soil, decreases flow path surface.The biologic product of the present invention can promote the rapid amount reproduction of profitable strain in soil, sufficient nutrition is provided for plant growth, and can effectively improve soil texture, promote soil remains the decomposition of chemical fertilizer composition, reduce salinity, accelerating crop to absorb the effective of the chemical fertilizer composition of residual in soil, improvement soil is gone forward side by side and is improved water quality and reduce pollution of area source.
The foregoing is only presently preferred embodiments of the present invention, not in order to limit the present invention, all within the spirit and principles in the present invention, any modification, equivalent substitution and improvement etc. made, should be included within the scope of the present invention.

Claims (6)

1. the biologic product of a degrading pesticide residues, it is characterized in that, including following components: apple, pomegranate, watermelon, orange, strawberry, shaddock, carambola, banana, Kiwi berry, hawthorn, cherry, water chestnut, grape, lemon, tomato, capsicum, eggplant, wax gourd, carrot, celery, onion, burdock, Chinese yam, balsam pear, lotus root, mushroom, auricularia auriculajudae and diaphragma juglandis.
nullThe biologic product of degrading pesticide residues the most according to claim 1，It is characterized in that，Described biologic product includes the component of following weight portion: apple 10-14 part、Pomegranate 7-12 part、Watermelon 28-32 part、Orange 53-57 part、Strawberry 35-39 part、Shaddock 37-41 part、Carambola 24-28 part、Banana 4-8 part、Kiwi berry 16-24 part、Hawthorn 7-12 part、Cherry 5-9 part、Water chestnut 4-8 part、Grape 28-32 part、Lemon 18-22 part、Tomato 24-28 part、Capsicum 2-6 part、Eggplant 12-18 part、Wax gourd 36-40 part、Carrot 9-15 part、Celery 10-14 part、Onion 10-15 part、Burdock 15-20 part、Chinese yam 19-26 part、Balsam pear 10-17 part、Lotus root 12-17 part、Mushroom 10-15 part、Auricularia auriculajudae 13-19 part and diaphragma juglandis 22-30 part.
The biologic product of degrading pesticide residues the most according to claim 1 and 2, it is characterized in that, described biologic product includes the component of following weight portion: apple 10 parts, pomegranate 12 parts, watermelon 32 parts, orange 53 parts, strawberry 36 parts, shaddock 38 parts, carambola 24 parts, 8 parts of banana, Kiwi berry 21 parts, hawthorn 11 parts, 5 parts of cherry, water chestnut 4 parts, grape 32 parts, 19 parts of lemon, 26 parts of tomato, 3 parts of capsicum, eggplant 16 parts, 40 parts of wax gourd, 15 parts of carrot, celery 13 parts, onion 10 parts, burdock 20 parts, Chinese yam 19 parts, 15 parts of balsam pear, lotus root 12 parts, mushroom 12 parts, 17 parts of auricularia auriculajudae and diaphragma juglandis 30 parts.
4. according to the biologic product of the arbitrary described degrading pesticide residues of claim 1-3, it is characterized in that, described biologic product includes the component of following weight portion: apple 14 parts, pomegranate 7 parts, watermelon 28 parts, orange 57 parts, strawberry 35 parts, shaddock 41 parts, carambola 28 parts, 4 parts of banana, Kiwi berry 24 parts, hawthorn 12 parts, 9 parts of cherry, water chestnut 7 parts, grape 30 parts, 22 parts of lemon, 24 parts of tomato, 2 parts of capsicum, eggplant 12 parts, 36 parts of wax gourd, 13 parts of carrot, celery 10 parts, onion 14 parts, burdock 15 parts, Chinese yam 23 parts, 10 parts of balsam pear, lotus root 14 parts, mushroom 15 parts, 13 parts of auricularia auriculajudae and diaphragma juglandis 22 parts.
5. according to the biologic product of the arbitrary described degrading pesticide residues of claim 1-4, it is characterized in that, described biologic product includes the component of following weight portion: apple 12 parts, pomegranate 11 parts, watermelon 30 parts, orange 54 parts, strawberry 39 parts, shaddock 37 parts, carambola 25 parts, 7 parts of banana, Kiwi berry 16 parts, hawthorn 7 parts, 6 parts of cherry, water chestnut 8 parts, grape 28 parts, 18 parts of lemon, 28 parts of tomato, 6 parts of capsicum, eggplant 18 parts, 38 parts of wax gourd, 9 parts of carrot, celery 14 parts, onion 15 parts, burdock 17 parts, Chinese yam 26 parts, 17 parts of balsam pear, lotus root 17 parts, mushroom 10 parts, 19 parts of auricularia auriculajudae and diaphragma juglandis 26 parts.
6. according to the preparation method of the biologic product of the arbitrary described degradable residues of pesticides of claim 1-5, it is characterised in that comprise the following steps:
Step one, take orange, hawthorn, onion, burdock, Chinese yam and balsam pear in proportion and mix to obtain mixture one, it is subsequently adding alcohol immersion 3-8 hour that alcohol volume content is 70-80% being equivalent to mixture one mass 12-14 times, filter, collect filtrate, when filtrate is evaporated under vacuum 0.05～0.06Mpa 60～70 DEG C subsequently, relative density is the lotion of 1.05～1.10, it is spray-dried, the EAT 160 of spray dryer～175 DEG C, leaving air temp 80～85 DEG C, it is ground into powder subsequently, makes dried cream powder；
Step 2, taking diaphragma juglandis in proportion and be subsequently adding the 3 ° of soaking in rice vinegar 30-60min being equivalent to diaphragma juglandis quality 10 times, then intense fire boils and uses slow fire instead and decoct slowly 15-20 minute, filters, obtains filtrate a, standby；
Step 3, take remaining ingredient input pulverizer in proportion to pulverize, after pulverizing, cross 2.0mm sieve to obtain mixture two, the dried cream powder that step one prepares is added in mixture two, the filtrate a that step 2 prepares ferments more than 120 days at 15-35 DEG C after mixing, after taking filtering fermentation liquor, obtain filtrate b and be the biologic product of degradable residues of pesticides.
CN201610283407.9A 2016-05-03 2016-05-03 Biological preparation capable of degrading pesticide residues Pending CN105875604A (en)

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