CN105769696A - Chinese herbal toothpaste containing fish collagen protein peptide - Google Patents
Chinese herbal toothpaste containing fish collagen protein peptide Download PDFInfo
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- CN105769696A CN105769696A CN201610236550.2A CN201610236550A CN105769696A CN 105769696 A CN105769696 A CN 105769696A CN 201610236550 A CN201610236550 A CN 201610236550A CN 105769696 A CN105769696 A CN 105769696A
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/64—Proteins; Peptides; Derivatives or degradation products thereof
- A61K8/65—Collagen; Gelatin; Keratin; Derivatives or degradation products thereof
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q11/00—Preparations for care of the teeth, of the oral cavity or of dentures; Dentifrices, e.g. toothpastes; Mouth rinses
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Abstract
Chinese herbal toothpaste containing fish collagen protein peptide contains, by weight, 3-8 parts of fish collagen protein peptide, 1-6 parts of radix scutellariae extract, 1-6 parts of sarcandra glabra extract, 3-8 parts of pseudo-ginseng root powder and 72-92 parts of toothpaste matrix.The multiple kinds of extract are used in a compatibility mode and combined with fish collagen protein peptide for synergic action, and the toothpaste can be used for treating stomatitis, protecting an oral cavity inner membrance and reducing oral diseases and has the refreshing and tasty healthcare effects.
Description
Technical field
The present invention relates to a kind of toothpaste, particularly relate to a kind of Chinese herbal toothpaste containing Isin glue collagen peptide.
Background technology
Oral disease not only affects the performance of oral cavity organs function, and usually affects the absorption of human nutrition and the healthy growth of whole body and growth.Toothpaste is as the requisite dental care products of people's daily life, and its major function is from initial cleaning tooth, and fresh breath gradual perfection, to having antihalitosis, prevents and treat gingival hemorrhage, the effect such as swell and ache.By adding functional component in toothpaste, make toothpaste have auxiliary prevention, prevent and alleviate the function of oral problem or situations of teeth tool is had some improvement.
Collagen peptide is a kind of important functional protein, is the hydrolyzate of collagen protein, has molecular weight low, the feature easily absorbed.The raw material sources of collagen peptide product currently mainly include: the skin of domestic animal and bone, and Fish etc..At present, Isin glue collagen peptide is the wider peptide matters that circulates on the market.Isin glue collagen peptide inherently protein substance, and have no side effect, and it can effectively facilitate promotion calcium carbonate and the absorption of calcium phosphate.
Circulation in the market has multiple Chinese herbal toothpaste, but its prevention and treatment gingival hemorrhage, the effect of gingival swelling and pain is unsatisfactory, and Chinese herbal toothpaste on the market is only the most also using certain several Chinese herbal medicine for as raw material, do not utilize collagen protein as raw material of toothpaste, and existing Isin glue collagen peptide can add in cosmetics or food, so not giving full play to the value with collagen protein.If there being a toothpaste both having contained Isin glue collagen peptide and Chinese herbal medicine, with the effect of dual performance toothpaste, being more beneficial for protecting the tooth of consumer, and solving oral problem.
Summary of the invention
In order to solve problem of the prior art, making full use of Isin glue collagen peptide, the present invention proposes a kind of Chinese herbal toothpaste containing Isin glue collagen peptide, and it is achieved through the following technical solutions:
A kind of Chinese herbal toothpaste containing Isin glue collagen peptide, including the material of following weight portion, Isin glue collagen peptide 3-8 part, Radix Scutellariae extract 1-6 part, Herba Pileae Scriptae extract 1-6 part, Radix Notoginseng powder 3-8 part, toothpaste matrix 72-92 part.
Preferred described Isin glue collagen peptide is prepared from by following technique, is washed with deionized water the most standby by the fish skin that weight portion is 800 parts；Fish skin stripping and slicing after cleaning, after rubbing, puts in the deionized water that weight portion is 1000 parts；It is 121 DEG C in temperature, under the conditions of pressure is 0.15MPa, heating pressurization 40min；Under the temperature conditions of 50-55 DEG C, add the protease hydrolyzed 6h that weight portion is 6 parts；After enzymolysis terminates, it is warming up to 80 DEG C and carries out enzyme denaturing, add the active carbon powder that weight portion is 20 parts and stir, decolour, obtain the serosity of enzyme denaturing decolouring；Under the conditions of temperature is 80 DEG C, the serosity after enzyme denaturing decolours adds the kieselguhr that weight portion is 20 parts and carries out coarse filtration；Under the conditions of temperature is 50 DEG C, adding weight portion is that the active carbon powder of 30 parts stirs and carries out fine straining, obtains semi-finished product；After being concentrated in vacuo by the semi-finished product obtained, then carry out spray dried 80 mesh sieves, obtain Isin glue collagen peptide.
Preferably, described Radix Scutellariae extract, through the following steps that be prepared from, weigh Radix Scutellariae, is added in the ethanol water that volume fraction is 60%-90%, and wherein Radix Scutellariae is 1:4-8 with the mass volume ratio of ethanol water, and reflux 1-3h, filters, obtains filtrate；Continue gained filtering residue to mix backflow 1-3 time, each 1-3h with the ethanol water that volume fraction is 60%-90% of 3-6 times of weight, obtain filtrate；Merge above-mentioned all filtrate, be concentrated into the extractum that relative density is 1.1-1.3 after activated carbon decolorizing, then extractum is spray-dried, obtain Radix Scutellariae extract.
Preferably, described Herba Pileae Scriptae extract is prepared from by following preparation technology: takes after Herba Pileae Scriptae vanes cleans and dry, is ground into Herba Pileae Scriptae coarse powder, crosses 30-50 mesh sieve；Then being joined by above-mentioned coarse powder in the ethanol that volume fraction is 40%-60%, wherein Herba Pileae Scriptae coarse powder is 1:15-20 with the mass volume ratio of ethanol；Supersound extraction 6-8h, is filtrated to get filtrate, filtrate is dried, obtain Herba Pileae Scriptae extract after extraction.
Preferably, described Radix Notoginseng powder is prepared from by following preparation technology, after taking that Radix Notoginseng powder is cleaned and drying, is ground into Radix Notoginseng coarse powder, is then ground by Radix Notoginseng coarse powder, obtain Radix Notoginseng powder after being cut into slices.
Preferably, the molecular weight of the Isin glue collagen peptide obtained is less than 1000 dalton.
Preferably, described fish skin is fish skin or the fish skin of fresh-water fishes of bathypelagic fish.
Preferably, described bathypelagic fish is deep-sea cod.
Preferably, described toothpaste includes the material of following weight portion: Isin glue collagen peptide 5 parts, Radix Scutellariae extract 3 parts, Herba Pileae Scriptae extract 3 parts, 5 parts of Radix Notoginseng powder, toothpaste matrix 84 parts.
Preferably, described toothpaste includes the material of following weight portion: Isin glue collagen peptide 3 parts, Radix Scutellariae extract 1.5 parts, Herba Pileae Scriptae extract 1 part, 3 parts of Radix Notoginseng powder, toothpaste matrix 91.5 parts.
The present invention relative to prior art have the advantage that is: the present invention is by adding in toothpaste by fish collagen, promote calcium carbonate and the absorption of calcium phosphate by little molecule Isin glue collagen peptide below supplementary 1000 dalton in making oral cavity, strengthen tooth antioxidation.Additionally, Isin glue collagen peptide can effectively be repaired oral erosion, preventing canker sore, protects and repair gingiva tissue loss, the people suffering from oral disease had good prevention and repair.
Radix Scutellariae extract can alleviate gingivitis, alleviate gingival hemorrhage, relaxes tooth and meet sour-sweet food and the tender subject caused during ice-cold material, alleviate the oral problem such as halitosis aphtha.
Herba Pileae Scriptae extract have resist rapidly gingival hemorrhage, repair oral ulcer, heat-clearing and toxic substances removing, reducing swelling and alleviating pain, anti-inflammation, there is the effect preventing the problems such as gingivitis, periodontitis, gingival atrophy.
Radix Notoginseng powder: rich in arasaponin, Radix Notoginseng polysaccharide, flavone effective ingredient, has hemostasis, blood circulation promoting and blood stasis dispelling, subduing swelling and relieving pain, aging resistance, improves immunologic function.
These several extract compatibilities use, and plus the common effect of fish collagen, can be used for treating stomatitis protected oral cavity inner membrance, reduce oral disease, the most tasty and refreshing health-care effect.Oral lesions can effectively be repaired by this toothpaste edible by consumer, preventing canker sore and effectively alleviate gingival hemorrhage.
Detailed description of the invention
Below in conjunction with detailed description of the invention, the invention will be further described.
Embodiment one,
Toothpaste quality obtained by the present embodiment is 1000g, and each composition of this toothpaste and quality thereof are respectively as follows: Isin glue collagen peptide 30g, Radix Scutellariae extract 15g, Herba Pileae Scriptae extract 10g, Radix Notoginseng powder 30g, toothpaste matrix 915g.
The toothpaste preparation method of the present invention: by Radix Scutellariae extract, Herba Pileae Scriptae extract and Radix Notoginseng powder and toothpaste matrix mixing and stirring, through vacuum outgas, fill, sealing and get final product.
Raw material used in the present invention: Isin glue collagen peptide, Radix Scutellariae extract, Herba Pileae Scriptae extract and Radix Notoginseng powder, toothpaste matrix can commercially be buied.
Embodiment two,
Toothpaste quality obtained by the present embodiment is 1000g, and each composition of this toothpaste and quality thereof are respectively as follows: Isin glue collagen peptide 75g, Radix Scutellariae extract 55g, Herba Pileae Scriptae extract 15g, Radix Notoginseng powder 65g, toothpaste matrix 790g.
The toothpaste preparation method of the present embodiment is identical with embodiment one, does not repeats them here.
Embodiment three,
Toothpaste quality obtained by the present embodiment is 1000g, and each composition of this toothpaste and quality thereof are respectively as follows: Isin glue collagen peptide 50g, Radix Scutellariae extract 30g, Herba Pileae Scriptae extract 30g, Radix Notoginseng powder 50g, toothpaste matrix 840g.
So that fish collagen, Radix Scutellariae extract and Herba Pileae Scriptae extract and Radix Notoginseng powder are more beneficial for adding in toothpaste, can mix with toothpaste matrix very well, and ensure that these materials play its effect, ensureing the safety of this toothpaste, in the present embodiment, these materials are obtained by following preparation method respectively simultaneously:
1. fish collagen preparation technology:
(1) deep sea cod skin of 800g is washed with deionized water the most standby；
(2) the fish skin stripping and slicing after cleaning, after rubbing, puts in the deionized water of 1000g；
(3) it is 121 DEG C in temperature, under the conditions of pressure is 0.15MPa, heating pressurization 40min；
(4) under the temperature conditions of 50-55 DEG C, the protease hydrolyzed 6h of 6g is added；
(5) after enzymolysis terminates, it is warming up to 80 DEG C and carries out enzyme denaturing, add 20g active carbon powder and stir, decolour, obtain the serosity of enzyme denaturing decolouring；
(6) under the conditions of temperature is 80 DEG C, the serosity after enzyme denaturing decolours adds 20g kieselguhr and carries out coarse filtration；The filter screen of preferably 180 mesh in this step filters.
(7) under the conditions of temperature is 50 DEG C, the activated carbon of addition 30g stirs and carries out fine straining, obtains semi-finished product；The filter screen of preferably 0.5 mesh in this step filters.
(8) after being concentrated in vacuo by the semi-finished product obtained, then carry out spray dried 80 mesh sieves, obtain Isin glue collagen peptide, thus ensure that the fish collagen adding in toothpaste is fine and smooth, do not affect mouthfeel.Wherein, the inlet temperature being dried is 150-155 DEG C, and outlet temperature is 85-95 DEG C.
The molecular weight of the Isin glue collagen peptide prepared by step (8) is less than 1000D.
In this preparation method, collagen peptide generally uses acid hydrolysis or enzymolysis production method, and wherein zymolysis technique is than the method safety of acid hydrolysis gelatin (or animal bone), will not destroy its natural chemical constitution because of strong acid, the effect of highly basic.The method preparing Isin glue collagen peptide of the embodiment of the present invention i.e. uses enzymolysis production method.Additionally, after enzymolysis terminates, add activated carbon in serosity during enzyme denaturing simultaneously, it is achieved that enzyme denaturing and decolouring are carried out simultaneously.With the addition of the most again activated carbon, can decolour further, and filter.Adding the fish collagen in toothpaste in the present invention to and the most do not add preservative, the collagen peptide purity being prepared from is high, without bad smell, it is ensured that the safety of toothpaste.
Certainly this fish skin is also selected from the fish skin of other bathypelagic fishs, such as salmon fish；Or the fish skin of fresh-water fishes, such as tilapia, Cyprinus carpio.
2. Radix Scutellariae extract preparation technology:
(1) weighing Radix Scutellariae, be added in the ethanol water that volume fraction is 60%-90%, wherein Radix Scutellariae: the W:V of ethanol water is 1:4-8, reflux 1-3h, filters, obtains filtrate；The ethanol water of preferably 75% in this step, Radix Scutellariae is preferably 1:6 with the mass volume ratio of ethanol water, and reflux 2h.
(2) gained filtering residue continues to mix with the ethanol water that volume fraction is 60%-90% of 3-6 times of weight backflow 1-3 time, each 1-3h, obtain filtrate.Preferably, being continued by filtering residue in this step with the volume fraction of 4.5 times of weight is that 75% ethanol water mixes backflow 2 times, each 2h.
(3) merge above-mentioned all filtrate, be concentrated into the extractum that relative density is 1.1-1.3 after activated carbon decolorizing, then extractum is spray-dried, be Radix Scutellariae extract.
3. Herba Pileae Scriptae extract preparation technology:
(1) take after Herba Pileae Scriptae vanes cleans and dry, be ground into Herba Pileae Scriptae coarse powder, cross 30-50 mesh sieve；It is preferably 40 mesh sieves.
(2) then above-mentioned coarse powder is joined in the ethanol that volume fraction is 40%-60%, wherein Herba Pileae Scriptae coarse powder: the W:V of ethanol is 1:15-20；In this step.Being preferably joins in the ethanol that volume fraction is 50% by above-mentioned coarse powder, and wherein Herba Pileae Scriptae coarse powder is preferably 1:16 with the mass volume ratio of ethanol.
(3) supersound extraction 6-8h, is filtrated to get filtrate, filtrate is dried, obtain Herba Pileae Scriptae extract after extraction.This production technology is very simple, and only has Herba Pileae Scriptae and two kinds of raw materials of ethanol at whole production link, without other supplementary elements, it is ensured that the safety of Herba Pileae Scriptae extract, is added in toothpaste, it is ensured that the safety of toothpaste.
4. Radix Notoginseng powder preparation technique
After taking that Radix Notoginseng powder is cleaned and drying, it is ground into Radix Notoginseng coarse powder after being cut into slices, then Radix Notoginseng coarse powder is ground, obtain Radix Notoginseng powder.
Embodiment four,
In order to verify the effect of toothpaste of the present invention, being further elaborated below in conjunction with clinical trial, the toothpaste of embodiment is selected in this test.
(1) tested crowd:
Select 300 experimenters suffering from recurrent exerbation oral ulcer to carry out oral ulcer and recover checking test；
Select 300 gingival hemorrhages the experimenter with gingival swelling and pain, carry out the checking test of gingiva situation；
Select the experimenter of 300 odonthemodias, carry out the checking test of odonthemodia recovery.
(2) test method: all experimenters use toothpaste tooth of each brush sooner or later of embodiment three every day, each 3 minutes, adhere to using 2 months；300 experimenters of each checking test being randomly divided into 3 groups, often organizes 100 people, 3 groups use the toothpaste of embodiment one, the toothpaste of embodiment two, the toothpaste of embodiment three respectively.
(3) result of the test: see following each table
Table 1 oral ulcer recovery situation table
| Oral ulcer changes | Embodiment one number | Embodiment two number | Embodiment three number |
| Total ulcer number significantly reduces | 86 | 88 | 86 |
| Total ulcer number reduces | 12 | 11 | 13 |
| Total ulcer number is without significant change | 2 | 1 | 1 |
| Total ulcer number is unchanged | 0 | 0 | 0 |
Table 2 gingival hemorrhage and gingival swelling and pain glucose recovery information slip
Table 3 odonthemodia symptom recovery situation table
| Odonthemodia symptom variation | Embodiment one number | Embodiment two number | Embodiment three number |
| Odonthemodia transference cure | 93 | 96 | 95 |
| Odonthemodia symptom alleviates | 7 | 4 | 5 |
| Odonthemodia is without significant change | 0 | 0 | 0 |
| Odonthemodia is unchanged | 0 | 0 | 0 |
By above-mentioned three tables, gingival swelling and pain, gingival hemorrhage, oral ulcer and odonthemodia are had and have good elimination and remission effect by this toothpaste, can effectively solve the puzzlement that consumer brings due to oral problem.
Above example is only in order to illustrate technical scheme, rather than is limited；Although the present invention being described in detail with reference to previous embodiment, for the person of ordinary skill of the art, still the technical scheme described in previous embodiment can be modified, or wherein portion of techniques feature is carried out equivalent；And these amendments or replacement, do not make the essence of appropriate technical solution depart from the spirit and scope of claimed technical solution of the invention.
Claims (10)
1. the Chinese herbal toothpaste containing Isin glue collagen peptide, it is characterised in that include the material of following weight portion, Isin glue collagen peptide 3-8 part, Radix Scutellariae extract 1-6 part, Herba Pileae Scriptae extract 1-6 part, Radix Notoginseng powder 3-8 part, toothpaste matrix 72-92 part.
Chinese herbal toothpaste containing Isin glue collagen peptide the most according to claim 1, it is characterised in that described Isin glue collagen peptide is prepared from by following technique,
The fish skin that weight portion is 800 parts is washed with deionized water the most standby；
Fish skin stripping and slicing after cleaning, after rubbing, puts in the deionized water that weight portion is 1000 parts；
It is 121 DEG C in temperature, under the conditions of pressure is 0.15MPa, heating pressurization 40min；
Under the temperature conditions of 50-55 DEG C, add the protease hydrolyzed 6h that weight portion is 6 parts；
After enzymolysis terminates, it is warming up to 80 DEG C and carries out enzyme denaturing, add the active carbon powder that weight portion is 20 parts and stir, decolour, obtain the serosity of enzyme denaturing decolouring；
Under the conditions of temperature is 80 DEG C, the serosity after enzyme denaturing decolours adds the kieselguhr that weight portion is 20 parts and carries out coarse filtration；
Under the conditions of temperature is 50 DEG C, adding weight portion is that the active carbon powder of 30 parts stirs and carries out fine straining, obtains semi-finished product；
After being concentrated in vacuo by the semi-finished product obtained, then carry out spray dried 80 mesh sieves, obtain Isin glue collagen peptide.
Chinese herbal toothpaste containing Isin glue collagen peptide the most according to claim 1, it is characterised in that described Radix Scutellariae extract through the following steps that be prepared from,
Weighing Radix Scutellariae, be added in the ethanol water that volume fraction is 60%-90%, wherein Radix Scutellariae is 1:4-8 with the mass volume ratio of ethanol water, and reflux 1-3 h, filters, obtains filtrate；
Continue gained filtering residue to mix backflow 1-3 time, each 1-3h with the ethanol water that volume fraction is 60%-90% of 3-6 times of weight, obtain filtrate；
Merge above-mentioned all filtrate, be concentrated into the extractum that relative density is 1.1-1. 3 after activated carbon decolorizing, then extractum is spray-dried, obtain Radix Scutellariae extract.
Chinese herbal toothpaste containing Isin glue collagen peptide the most according to claim 1, it is characterised in that described Herba Pileae Scriptae extract is prepared from by following preparation technology:
Take after Herba Pileae Scriptae vanes cleans and dry, be ground into Herba Pileae Scriptae coarse powder, cross 30-50 mesh sieve；
Then being joined by above-mentioned coarse powder in the ethanol that volume fraction is 40%-60%, wherein Herba Pileae Scriptae coarse powder is 1:15-20 with the mass volume ratio of ethanol；
Supersound extraction 6-8h, is filtrated to get filtrate, filtrate is dried, obtain Herba Pileae Scriptae extract after extraction.
Chinese herbal toothpaste containing Isin glue collagen peptide the most according to claim 1, it is characterized in that, described Radix Notoginseng powder is prepared from by following preparation technology, after taking that Radix Notoginseng powder is cleaned and drying, Radix Notoginseng coarse powder it is ground into after being cut into slices, then Radix Notoginseng coarse powder is ground, obtains Radix Notoginseng powder.
Chinese herbal toothpaste containing Isin glue collagen peptide the most according to claim 2, it is characterised in that the molecular weight of the Isin glue collagen peptide obtained is less than 1000 dalton.
Chinese herbal toothpaste containing Isin glue collagen peptide the most according to claim 6, it is characterised in that described fish skin is fish skin or the fish skin of fresh-water fishes of bathypelagic fish.
Chinese herbal toothpaste containing fish collagen the most according to claim 7, it is characterised in that described bathypelagic fish is deep-sea cod.
9. according to the Chinese herbal toothpaste containing fish collagen described in claim 1-8 any one, it is characterized in that, described toothpaste includes the material of following weight portion: Isin glue collagen peptide 5 parts, Radix Scutellariae extract 3 parts, Herba Pileae Scriptae extract 3 parts, 5 parts of Radix Notoginseng powder, toothpaste matrix 84 parts.
10. according to the Chinese herbal toothpaste containing Isin glue collagen peptide described in claim 1-8 any one, it is characterized in that, described toothpaste includes the material of following weight portion: Isin glue collagen peptide 3 parts, Radix Scutellariae extract 1.5 parts, Herba Pileae Scriptae extract 1 part, 3 parts of Radix Notoginseng powder, toothpaste matrix 91.5 parts.
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Cited By (6)
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| CN107468631A (en) * | 2017-09-12 | 2017-12-15 | 广州泓生物科技有限公司 | Fish scale collagen biological toothpaste |
| CN107929145A (en) * | 2017-12-19 | 2018-04-20 | 青岛铭芳莲商贸有限公司 | A kind of Shufushang and preparation method thereof |
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| CN110123660A (en) * | 2019-06-21 | 2019-08-16 | 上海利盛生特企业发展有限公司 | Peptides oral health toothpaste containing victory and preparation method thereof |
| CN111686028A (en) * | 2019-04-26 | 2020-09-22 | 山东丁马生物科技有限公司 | Turtle collagen peptide toothpaste and preparation method thereof |
| CN113633604A (en) * | 2021-08-30 | 2021-11-12 | 合肥赛为智慧医疗有限公司 | Mouthwash for preventing and treating gingivitis and preparation method thereof |
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| CN111686028A (en) * | 2019-04-26 | 2020-09-22 | 山东丁马生物科技有限公司 | Turtle collagen peptide toothpaste and preparation method thereof |
| CN110123660A (en) * | 2019-06-21 | 2019-08-16 | 上海利盛生特企业发展有限公司 | Peptides oral health toothpaste containing victory and preparation method thereof |
| CN113633604A (en) * | 2021-08-30 | 2021-11-12 | 合肥赛为智慧医疗有限公司 | Mouthwash for preventing and treating gingivitis and preparation method thereof |
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Application publication date: 20160720 |