CN111686028A - Turtle collagen peptide toothpaste and preparation method thereof - Google Patents
Turtle collagen peptide toothpaste and preparation method thereof Download PDFInfo
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- CN111686028A CN111686028A CN201910341611.5A CN201910341611A CN111686028A CN 111686028 A CN111686028 A CN 111686028A CN 201910341611 A CN201910341611 A CN 201910341611A CN 111686028 A CN111686028 A CN 111686028A
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/64—Proteins; Peptides; Derivatives or degradation products thereof
- A61K8/65—Collagen; Gelatin; Keratin; Derivatives or degradation products thereof
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/19—Cosmetics or similar toiletry preparations characterised by the composition containing inorganic ingredients
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
- A61K8/9706—Algae
- A61K8/9717—Rhodophycota or Rhodophyta [red algae], e.g. Porphyra
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61P—SPECIFIC THERAPEUTIC ACTIVITY OF CHEMICAL COMPOUNDS OR MEDICINAL PREPARATIONS
- A61P1/00—Drugs for disorders of the alimentary tract or the digestive system
- A61P1/02—Stomatological preparations, e.g. drugs for caries, aphtae, periodontitis
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q11/00—Preparations for care of the teeth, of the oral cavity or of dentures; Dentifrices, e.g. toothpastes; Mouth rinses
Abstract
The invention discloses turtle collagen peptide toothpaste and a preparation method thereof, and belongs to the field of toothpaste preparation. The turtle collagen peptide toothpaste comprises the following raw materials in parts by mass: 10-30 parts of sorbitol, 40-60 parts of hydrated silica, 10-30 parts of anion water, 60.1-3 parts of PEG-1, 0.1-2 parts of turtle collagen peptide, 0.5-3 parts of sodium lauryl sulfate, 0.1-3 parts of essence, 0.2-2 parts of cellulose gum, 0.5-3 parts of sodium lauramide creatine and 0.1-3 parts of Chondrus crispus extract; the turtle collagen peptide added in the invention enters a human body through the micromolecular active peptide, is easy to repair gum and oral cells, nourishes and organizes cells, enhances the immunity of organisms in the oral cavity, can directly enter the cells to be fused with cell membranes, prevents the invasion of bacteria and viruses, can enable each organism in the oral cavity to generate more antibodies to resist diseases, is easy to play a role in preventing and repairing oral ulcer, is not easy to damage the oral mucosa, and can be suitable for people of any age group.
Description
Technical Field
The invention relates to the technical field of toothpaste preparation, in particular to turtle collagen peptide toothpaste and a preparation method thereof.
Background
The oral ulcer is a disease with the highest incidence rate in oral mucosa diseases, is a superficial ulcer occurring on the oral mucosa, has obvious peripheral bleeding and pain, has the characteristics of periodicity, recurrence, self-limitation and the like, is a common disease, and is also common, so that many people often ignore the disease. In fact, oral ulcers not only affect nutrient intake, but may also cause canceration.
The toothpaste is frequently used for brushing teeth, the oral hygiene is paid attention to, the oral mucosa is prevented from being damaged, and the most direct prevention mode is provided.
Toothpaste is a common cleaning product in daily life and has a long history. With the continuous development of science and technology, various types of toothpaste come out successively, and the quality and grade of products are improved continuously. The toothpaste is a daily necessity, is full of toothpaste, can play a role in cleaning oral cavity for most of the toothpaste in the market, but can really prevent and repair oral ulcer and protect oral mucosa, and some toothpastes can damage the oral mucosa.
Disclosure of Invention
The invention aims to solve the problems that in the prior art, toothpaste capable of really preventing and repairing dental ulcer and protecting oral mucosa is little, and the oral mucosa can be damaged in some cases, and provides turtle collagen peptide toothpaste and a preparation method thereof.
In order to achieve the purpose, the invention adopts the following technical scheme:
the turtle collagen peptide toothpaste is characterized by comprising the following raw materials in parts by mass: 10-30 parts of sorbitol, 40-60 parts of hydrated silica, 10-30 parts of anion water, 60.1-3 parts of PEG-3, 0.1-2 parts of turtle collagen peptide, 0.5-3 parts of sodium lauryl sulfate, 0.1-3 parts of essence, 0.2-2 parts of cellulose gum, 0.5-3 parts of sodium lauroyl amide creatine, 0.1-3 parts of Chondrus crispus extract, 0.01-0.25 part of sodium saccharin and 0.01-0.1 part of sodium benzoate.
Preferably, the feed is characterized by comprising the following raw materials in parts by mass: 20 parts of sorbitol, 50 parts of hydrated silica, 21.9 parts of anion water, PEG-61 parts, 0.5 part of turtle collagen peptide, 1.5 parts of sodium lauryl sulfate, 1 part of essence, 1 part of cellulose gum, 1.5 parts of sodium lauramide sarcosinate, 1.5 parts of crinkle grass, 0.05 part of saccharin sodium and 0.05 part of sodium benzoate.
Preferably, the turtle collagen peptide toothpaste and the preparation method thereof are characterized by comprising the following operation steps:
the method comprises the following steps: adding anion water into a certain container, adding PEG-6, sodium lauroyl amide sarcosinate and saccharin sodium in a stirring state, mixing and stirring for 30 minutes at the water bath temperature of 30-50 ℃, adding sorbitol after uniformly stirring and dissolving, magnetically stirring for 1-3 hours, and stopping stirring to obtain a mixture a for later use;
step two: adding the carrageen crispus extract and the cellulose gum into another container, stirring to be uniform and colloidal, then adding the essence, stirring and mixing to obtain a uniform mixture b for later use;
step three: putting the prepared mixture b into an oven at 40-60 ℃ for 8-10 hours to age into gel for later use;
step four: adding sodium benzoate, turtle collagen peptide, sodium lauryl sulfate, and hydrated silica into pulverizer, stirring to particle diameter of 0.01-1 μm to obtain mixture c
Step five: pumping the mixture a, the mixture b and the mixture c into a three-in-one paste making machine under vacuum, stirring for 2-48 hours, and discharging to obtain the finished product.
Preferably, the water bath temperature in the first step is 40 ℃.
Preferably, in the first step, the mixture is magnetically stirred for 2 hours.
Preferably, the temperature of the water bath in the third step is 50 ℃.
Preferably, in the third step, the mixture is aged in an oven for 9 hours.
Preferably, the particle diameter in step four is 0.1 micron.
Preferably, the stirring in the fifth step is carried out for 24 hours.
Compared with the prior art, the invention provides the turtle collagen peptide toothpaste and the preparation method thereof, and the turtle collagen peptide toothpaste has the following beneficial effects:
1. the turtle collagen peptide toothpaste enters a human body through the micromolecular active peptide, is easy to repair gum and oral cells, is nutritious, organizes cells, enhances the immunity of organisms in the oral cavity, can directly enter the cells, is fused with cell membranes, prevents the invasion of bacteria and viruses, and can enable the organisms in the oral cavity to generate more antibodies to resist diseases.
2. The turtle collagen peptide toothpaste is easy to activate oral cells and improve the vitality of cells by the intake of liquid anion water; supplementing and repairing cell membrane potential and regulating physiological balance; enhancing hematopoietic function and promoting blood normal; purifying blood and removing blood garbage; the blood viscosity is reduced, and the microcirculation is kept smooth; promoting blood circulation and improving metabolism; promoting weak alkalization of acidic constitution, and improving intra-oral cell ring.
3. The turtle collagen peptide toothpaste is easy to improve the natural water locking function of gum and oral cells by the intake of the carrageen crispus extract, and the carrageen crispus extract is a moisturizing component extracted from natural seaweed and has no toxic or side effect.
The added turtle collagen peptide enters a human body through small molecule active peptide, is easy to repair gum and oral cells, is nutritious and histocyte, enhances the immunity of organisms in an oral cavity, can directly enter the cells, is fused with cell membranes, prevents the invasion of bacteria and viruses, can enable the organisms in the oral cavity to generate more antibodies to resist diseases, is easy to play the effects of preventing and repairing oral ulcer, is not easy to damage the oral mucosa, and can be suitable for people of any age bracket.
Drawings
Fig. 1 is a schematic structural diagram of turtle collagen peptide toothpaste and a preparation method thereof.
Detailed Description
The technical solutions in the embodiments of the present invention will be clearly and completely described below with reference to the drawings in the embodiments of the present invention, and it is obvious that the described embodiments are only a part of the embodiments of the present invention, and not all of the embodiments.
In the description of the present invention, it is to be understood that the terms "upper", "lower", "front", "rear", "left", "right", "top", "bottom", "inner", "outer", and the like, indicate orientations or positional relationships based on the orientations or positional relationships shown in the drawings, are merely for convenience in describing the present invention and simplifying the description, and do not indicate or imply that the device or element being referred to must have a particular orientation, be constructed and operated in a particular orientation, and thus, should not be construed as limiting the present invention.
Example 1:
the turtle collagen peptide toothpaste is characterized by comprising the following raw materials in parts by mass: 10 parts of sorbitol, 40 parts of hydrated silica, 10 parts of anion water, 60.1 parts of PEG-1, 0.1 part of turtle collagen peptide, 0.5 part of sodium lauryl sulfate, 0.1 part of essence, 0.2 part of cellulose gum, 0.5 part of sodium lauramide sarcosinate, 0.1 part of carrageen crispus extract, 0.01 part of saccharin sodium and 0.01 part of sodium benzoate.
The turtle collagen peptide toothpaste and the preparation method thereof are characterized by comprising the following operation steps:
the method comprises the following steps: adding anion water into a certain container, adding PEG-6, sodium lauroyl amide sarcosinate and saccharin sodium in a stirring state, mixing and stirring for 30 minutes at the water bath temperature of 40 ℃, adding sorbitol after uniformly stirring and dissolving, magnetically stirring for 2 hours, and stopping stirring to obtain a mixture a for later use;
step two: adding the carrageen crispus extract and the cellulose gum into another container, stirring to be uniform and colloidal, then adding the essence, stirring and mixing to obtain a uniform mixture b for later use;
step three: putting the prepared mixture b into a 50 ℃ oven for 9 hours to age into gel for later use;
step four: adding sodium benzoate, turtle collagen peptide, sodium lauryl sulfate, and hydrated silica into pulverizer, stirring to particle diameter of 0.1 micrometer to obtain mixture c for use
Step five: pumping the mixture a, the mixture b and the mixture c into a three-in-one paste making machine under vacuum, stirring for 24 hours, and discharging to obtain the finished product.
Example 2:
the turtle collagen peptide toothpaste is characterized by comprising the following raw materials in parts by mass: 30 parts of sorbitol, 60 parts of hydrated silica, 30 parts of anion water, PEG-63 parts, 2 parts of turtle collagen peptide, 3 parts of sodium lauryl sulfate, 3 parts of essence, 2 parts of cellulose gum, 3 parts of sodium lauramide sarcosinate, 3 parts of a carrageen crispus extract, 0.25 part of saccharin sodium and 0.1 part of sodium benzoate.
The turtle collagen peptide toothpaste and the preparation method thereof are characterized by comprising the following operation steps:
the method comprises the following steps: adding anion water into a certain container, adding PEG-6, sodium lauroyl amide sarcosinate and saccharin sodium in a stirring state, mixing and stirring for 30 minutes at the water bath temperature of 40 ℃, adding sorbitol after uniformly stirring and dissolving, magnetically stirring for 2 hours, and stopping stirring to obtain a mixture a for later use;
step two: adding the carrageen crispus extract and the cellulose gum into another container, stirring to be uniform and colloidal, then adding the essence, stirring and mixing to obtain a uniform mixture b for later use;
step three: putting the prepared mixture b into a 50 ℃ oven for 9 hours to age into gel for later use;
step four: adding sodium benzoate, turtle collagen peptide, sodium lauryl sulfate, and hydrated silica into pulverizer, stirring to particle diameter of 0.1 micrometer to obtain mixture c for use
Step five: pumping the mixture a, the mixture b and the mixture c into a three-in-one paste making machine under vacuum, stirring for 24 hours, and discharging to obtain the finished product.
Example 3:
the turtle collagen peptide toothpaste is characterized by comprising the following raw materials in parts by mass: 20 parts of sorbitol, 50 parts of hydrated silica, 21.9 parts of water, 61 parts of PEG-7, 0.5 part of turtle collagen peptide, 1.5 parts of sodium lauryl sulfate, 1 part of essence, 1 part of cellulose gum, 1.5 parts of sodium lauramide sarcosinate, 1.5 parts of carrageen crispus, 0.05 part of saccharin sodium and 0.05 part of sodium benzoate.
The turtle collagen peptide toothpaste and the preparation method thereof are characterized by comprising the following operation steps:
the method comprises the following steps: adding anion water into a certain container, adding PEG-6, sodium lauroyl amide sarcosinate and saccharin sodium in a stirring state, mixing and stirring for 30 minutes at the water bath temperature of 40 ℃, adding sorbitol after uniformly stirring and dissolving, magnetically stirring for 2 hours, and stopping stirring to obtain a mixture a for later use;
step two: adding the carrageen crispus extract and the cellulose gum into another container, stirring to be uniform and colloidal, then adding the essence, stirring and mixing to obtain a uniform mixture b for later use;
step three: putting the prepared mixture b into a 50 ℃ oven for 9 hours to age into gel for later use;
step four: adding sodium benzoate, turtle collagen peptide, sodium lauryl sulfate, and hydrated silica into pulverizer, stirring to particle diameter of 0.1 micrometer to obtain mixture c for use
Step five: pumping the mixture a, the mixture b and the mixture c into a three-in-one paste making machine under vacuum, stirring for 24 hours, and discharging to obtain the finished product.
Sorbitol, also known as sorbitol. The molecular formula is C6H14O6, and the molecular weight is 182.17. Is white hygroscopic powder or crystalline powder, tablet or granule, and has no odor. The melting point varies from 88 to 102 ℃ depending on the crystallization conditions, and the relative density is about 1.49. Readily soluble in water (1g in about 0.45mL water), slightly soluble in ethanol and acetic acid. Has cool sweet taste, the sweetness of the sugar is about half of that of the cane sugar, and the calorific value of the sugar is similar to that of the cane sugar. In the food industry, sorbitol solution with the content of 69-71% is mostly used. Toxicity tests show that excessive oral administration can cause diarrhea and digestive disorders.
The liquid anion water has small molecular groups, and the molecular chains of the liquid anion water are shorter, narrower and smaller, so that the liquid anion water can permeate cell membranes more easily, carry active oxygen and nutrient substances more easily and provide nutrition and energy for cells. This water has a strong physiological function and is called "active functional water". The water solubility of the small molecular groups is strong, and the mineral substances in the water are more easily dissolved in body fluid or blood and can be absorbed and utilized by the human body. Therefore, the water molecules can be saved and the original functions can be recovered by only adopting proper physical technology to 'break' the large water molecule groups into small water molecule groups. The liquid anion water has the following effects: activating cells and enhancing the permeability of cell membranes; supplementing and repairing cell membrane potential and regulating physiological balance; enhancing hematopoietic function and promoting blood normal; purifying blood and removing blood garbage; the high-concentration negative ions can rapidly supplement and increase the membrane potential of blood cells and regulate physiological balance; the blood viscosity is reduced, and the microcirculation is kept smooth; promoting blood circulation and improving metabolism; activating brain cells, and preventing senile dementia; skin care, skin care and skin resistance enhancement; promoting weak basification of acidic constitution, and improving intracellular encytosis.
Hydrated silica is a non-metallic mineral based on minerals rich in silicon dioxide. The silica ore comprises quartz sandstone, quartzite, quartz sand, vein quartz, intergrown siliceous hornstone and the like. The main minerals are quartz and chalcedony. The chemical industry requires that the silica content of quartzite and vein quartz be greater than or equal to 90%, and that the smaller the water absorption and porosity, the better, and the best is zero. All are open pit mining. The mineral separation is mainly performed by a flotation method, and also by a scrubbing method or a gravity separation method. The product is used for manufacturing silica gel, water glass and various silicides and silicates, and is used as a filler of plastics, rubber, paint and coating; the better one can utilize its acid resistance as a packing in the sulfuric acid absorption column. It is also widely used in glass, petroleum, ceramics, machinery, metallurgy, casting, building materials and other departments.
Turtles are important freshwater reptiles and are cultivated in many countries and regions of asia, such as the mainland and taiwan, japan, korea, vietnam. Since ancient times, turtles are deeply favored by Chinese people due to their delicious taste and nutrition. The connective soft tissue surrounding the turtle shell is commonly referred to as the "skirt," which is quite rich in collagen and serves as a source of high quality, superior collagen. So far, no turtle collagen gene and recombinant protein thereof are reported.
Sodium lauryl sulfate is white powder, has characteristic smell, is easy to dissolve in water, has strong foaming force, plump, white and fine foam and excellent emulsifying property and washing capacity, and is used as a raw material of a washing agent, a leveling agent in printing and dyeing industry, a flotation agent of minerals, a cleaning agent and a foaming agent.
The cellulose gel is easy to mix and use various functionalized ionic liquids, and endows the ionic liquid system with multifunctional characteristics. The mixed ionic liquid can dissolve and fragment cellulose, and a microenvironment is formed around cellulose molecules after water is added, so that cellulose is prevented from crystallizing in the conversion process, and a cellulose colloid is constructed. The microcrystalline cellulose particles are broken up into innumerable ionic liquid solution units of fine cellulose, which increase the affinity for water due to the increase of the surface area to result in an increase of the viscosity and finally form a colloid. The cellulose in the cellulose colloid prepared by the invention is completely dissolved, the dispersion is very uniform, and the concentration of the cellulose is high. The biocompatibility is good, so the cellulose colloid prepared by the method can be used for biocatalytic reaction. The process for preparing the cellulose colloid is green and environment-friendly, and cellulose can not be converted into toxic byproducts such as furfural and the like. Has great social significance and application value.
The lauroyl sarcosine sodium is colorless liquid, and has cleaning effect.
Chondrus crispus extract is moisture keeping component extracted from natural seaweed. Chondrus crispus belongs to Rhodophyta, Gigartinales, Gigartinaceae, Chondrus, is naturally distributed in coastal regions of Atlantic ocean and south east coast of China, Qingdao, Dalian and other sea areas, and is an important economic seaweed in China. Carrageenans are not only important raw algae for carrageenan production, but also have been increasingly used in the medical field in recent years, and have attracted much attention.
According to the invention, the small molecule active peptide enters a human body, so that the gum and oral cells are easily repaired, the cells are nourished and organized, the immunity of organisms in the oral cavity is enhanced, the small molecule active peptide can directly enter the cells and be fused with cell membranes, the invasion of bacteria and viruses is prevented, and each organism in the oral cavity can generate more antibodies to resist diseases; oral cells are easily activated and the cell life activity is improved by taking in liquid negative ion water; supplementing and repairing cell membrane potential and regulating physiological balance; enhancing hematopoietic function and promoting blood normal; purifying blood and removing blood garbage; the blood viscosity is reduced, and the microcirculation is kept smooth; promoting blood circulation and improving metabolism; promoting weak basification of acidic constitution, and improving intra-oral cell ring; the natural water locking function of gum and oral cells is easily improved by the intake of the carrageen crispus extract, and the carrageen crispus extract is a moisturizing component extracted from natural seaweed and has no toxic or side effect; the invention has the advantages of easy prevention and repair of oral ulcer, no damage to oral mucosa, and suitability for people of any age.
The above description is only for the preferred embodiment of the present invention, but the scope of the present invention is not limited thereto, and any person skilled in the art should be considered to be within the technical scope of the present invention, and the technical solutions and the inventive concepts thereof according to the present invention should be equivalent or changed within the scope of the present invention.
Claims (9)
1. The turtle collagen peptide toothpaste is characterized by comprising the following raw materials in parts by mass: 10-30 parts of sorbitol, 40-60 parts of hydrated silica, 10-30 parts of anion water, 60.1-3 parts of PEG-3, 0.1-2 parts of turtle collagen peptide, 0.5-3 parts of sodium lauryl sulfate, 0.1-3 parts of essence, 0.2-2 parts of cellulose gum, 0.5-3 parts of sodium lauroyl amide creatine, 0.1-3 parts of Chondrus crispus extract, 0.01-0.25 part of sodium saccharin and 0.01-0.1 part of sodium benzoate.
2. The turtle collagen peptide toothpaste as claimed in claim 1, which comprises the following raw materials in parts by mass: 20 parts of sorbitol, 50 parts of hydrated silica, 21.9 parts of anion water, PEG-61 parts, 0.5 part of turtle collagen peptide, 1.5 parts of sodium lauryl sulfate, 1 part of essence, 1 part of cellulose gum, 1.5 parts of sodium lauramide sarcosinate, 1.5 parts of crinkle grass, 0.05 part of saccharin sodium and 0.05 part of sodium benzoate.
3. The turtle collagen peptide toothpaste and the preparation method thereof according to claim 1, wherein the method comprises the following steps:
the method comprises the following steps: adding anion water into a certain container, adding PEG-6, sodium lauroyl amide sarcosinate and saccharin sodium in a stirring state, mixing and stirring for 30 minutes at the water bath temperature of 30-50 ℃, adding sorbitol after uniformly stirring and dissolving, magnetically stirring for 1-3 hours, and stopping stirring to obtain a mixture a for later use;
step two: adding the carrageen crispus extract and the cellulose gum into another container, stirring to be uniform and colloidal, then adding the essence, stirring and mixing to obtain a uniform mixture b for later use;
step three: putting the prepared mixture b into an oven at 40-60 ℃ for 8-10 hours to age into gel for later use;
step four: adding sodium benzoate, turtle collagen peptide, sodium lauryl sulfate, and hydrated silica into pulverizer, stirring to particle diameter of 0.01-1 μm to obtain mixture c
Step five: pumping the mixture a, the mixture b and the mixture c into a three-in-one paste making machine under vacuum, stirring for 2-48 hours, and discharging to obtain the finished product.
4. The turtle collagen peptide toothpaste as claimed in claim 1, wherein the temperature of the water bath in the first step is 40 ℃.
5. The turtle collagen peptide toothpaste as claimed in claim 1, wherein the first step is a step of magnetic stirring for 2 hours.
6. The turtle collagen peptide toothpaste and the preparation method thereof according to claim 1, wherein the water bath temperature in step three is 50 ℃.
7. The turtle collagen peptide toothpaste and the preparation method thereof according to claim 1, wherein in the third step, the toothpaste is aged in an oven for 9 hours.
8. The turtle collagen peptide toothpaste as claimed in claim 1, wherein the diameter of the particles in step four is 0.1 μm.
9. The turtle collagen peptide toothpaste as claimed in claim 1, wherein in step five, the toothpaste is stirred for 24 hours.
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| CN201910341611.5A CN111686028A (en) | 2019-04-26 | 2019-04-26 | Turtle collagen peptide toothpaste and preparation method thereof |
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Citations (5)
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| CN103550123A (en) * | 2013-11-07 | 2014-02-05 | 广西奥奇丽股份有限公司 | Chinese medicinal toothpaste containing pseudo-ginseng total saponins and saponin extracts and tortoise shell extracts |
| CN104127340A (en) * | 2014-07-23 | 2014-11-05 | 浙江森宇实业有限公司 | Dendrobium officinale toothpaste and preparation method |
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2019
- 2019-04-26 CN CN201910341611.5A patent/CN111686028A/en active Pending
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| CN103550123A (en) * | 2013-11-07 | 2014-02-05 | 广西奥奇丽股份有限公司 | Chinese medicinal toothpaste containing pseudo-ginseng total saponins and saponin extracts and tortoise shell extracts |
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| CN105063140A (en) * | 2015-07-29 | 2015-11-18 | 浙江万里学院 | Preparation method and application of pelodiscus sinensis collagen peptide |
| CN105769696A (en) * | 2016-04-15 | 2016-07-20 | 山东天欣生物科技有限公司 | Chinese herbal toothpaste containing fish collagen protein peptide |
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