CN105768248B - 不着凉内衣及其制备方法 - Google Patents

不着凉内衣及其制备方法 Download PDF

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CN105768248B
CN105768248B CN201610235502.1A CN201610235502A CN105768248B CN 105768248 B CN105768248 B CN 105768248B CN 201610235502 A CN201610235502 A CN 201610235502A CN 105768248 B CN105768248 B CN 105768248B
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underwear
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贾右兵
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Shanghai Xiaolanxiang Garment Co., Ltd.
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Shanghai Ximian Garment Co Ltd
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    • D06M15/19—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment with synthetic macromolecular compounds
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Abstract

本发明公开了一种不着凉内衣及其制备方法，所述不着凉内衣由下述重量份的原料织造而成：0‑100份Thermocool纤维、0‑100份再生纤维素纤维、0‑10份氨纶；所述不着凉内衣在吸湿排汗整理剂中浸渍；所述吸湿排汗整理剂由下述质量百分比的原料组成：0.3‑0.7％聚丙烯酰胺、0.1‑0.5％交联剂、0.1‑0.5％络合剂、余量为水；所述的交联剂由2‑甲基‑2‑丙烯酸‑2,3‑二羟基丙酯、2‑羟丙基异丁烯酸酯、2‑羟基乙基丙烯酸酯混合而成。本发明的不着凉内衣，又称为防感冒内衣，具有很好的吸湿排汗效果，在出现汗时服装不会粘贴皮肤而产生冷湿感，避免着凉，特别具有防感冒的功效。

Description

不着凉内衣及其制备方法
技术领域
本发明涉及一种面料，具体涉及一种不着凉内衣及其制备方法。
背景技术
近年来，人们对服装面料的舒适性、健康性、安全性和环保性等要求越来越高，既要求有良好的舒适性，又要求能在出现汗时服装不会粘贴皮肤而产生冷湿感。
众所周知，天然纤维以棉为例，其吸湿性能好，穿着舒适，但当人的出汗量稍大时，棉纤维会因吸湿膨胀，其运气性下降并粘贴在皮肤上，同时，水份发散速度也较慢，从而给人体造成一种冷湿感；合成纤维以涤纶为例，其吸水性小，透湿性能差，由于其静电积累而容易引起穿着时产生纠缠的麻烦，尤其在活动时容易产生闷热感。
然而，现有技术中并没有具有吸湿排汗性能的内衣，本申请开创性的发明了一种不着凉内衣。
发明内容
本发明要解决的技术问题之一是提供一种不着凉内衣，之二是提供上述不着凉内衣的制备方法。
为解决上述问题，本发明采用如下技术方案：
一种不着凉内衣(又称为防感冒内衣)，由下述重量份的原料织造而成：0-100份Thermocool纤维、0-100份再生纤维素纤维、0-10份氨纶。
一种不着凉内衣，由下述重量份的原料织造而成：21-39份Thermocool纤维、61-79份莫代尔纤维、1-4份氨纶。
所述不着凉内衣再经过吸湿排汗处理步骤而得；
所述吸湿排汗处理步骤为将所述不着凉内衣在吸湿排汗整理剂中浸渍；
所述吸湿排汗整理剂由下述质量百分比的原料组成：0.3-0.7％聚丙烯酰胺、0.1-0.5％交联剂、0.1-0.5％络合剂、余量为水；
所述的交联剂由2-甲基-2-丙烯酸-2,3-二羟基丙酯、2-羟丙基异丁烯酸酯、2-羟基乙基丙烯酸酯混合而成，所述2-甲基-2-丙烯酸-2,3-二羟基丙酯、2-羟丙基异丁烯酸酯、2-羟基乙基丙烯酸酯的质量比为(1-3)：(1-3)：(1-3)。
优选地，所述的络合剂由40-60wt％羟基乙叉二膦酸钠和40-60wt％乙二胺四甲叉膦酸五钠盐组成。
所述再生纤维素纤维，包括铜氨纤维、甲壳素纤维、竹纤维、Modal纤维、Tencel纤维等。
Modal纤维又称木代尔纤维、莫代尔纤维，是一种全新的纤维素纤维，Modal纤维的原料来自于大自然的木材，使用后可以自然降解。由于这类纤维是采用天然纤维素为原料，具有生物降解性，并且在纤维生产过程中不产生类似粘胶纤维的严重污染环境问题，是21世纪的新型环保纤维。Modal纤维价格是Tencel纤维的一半，系第二代再生纤维素纤维。Modal纤维可与多种纤维混纺、交织，发挥各自纤维的特点，达到更佳的效果。Modal纤维面料吸湿性能、透气性能优于纯棉织物，其手感柔软，悬垂性好，穿着舒适，色泽光亮，是一种天然的丝光面料。正因为莫代尔面料舒适，弹性好，透气性佳等特性，它被很多知名的内衣品牌像七匹狼、纤丝鸟、健将、富妮来、David archy等用在了内衣生产中，也有越来越多的国内消费者喜爱莫代尔内衣。但是也因为这些特性，莫代尔面料用在成衣中的较少，因为它较难达到定型塑形的效果。
Thermocool,是欧洲公司ADVANSA的产品，在体育运动过程中或者炎热的天气里，ADVANSA ThermoCool较其它材料相比能够更快地蒸发掉湿汽。这一纤维材料在设计之初就采用了增加表面积的方式，并且多微细凹槽表面的纤维帮助将湿气快速地从皮肤传导到面料表面，而中空纤维使得空气流通增强进而将热能都集中消耗在蒸发过程中，借此达到蒸发降温效果的最大化。在寒冷的天气里或是运动过后，中空的纤维成为热阻隔介质，它保护穿着者的身体和肌肉以预防运动后的寒热。
本发明还提供了上述不着凉内衣的制备方法，包括以下步骤：(1)采用常规方法将Thermocool纤维、莫代尔纤维和氨纶织造成面料，裁剪缝制成内衣；(2)将上述内衣进行亲水处理。
所述吸湿排汗整理剂由下述质量百分比的原料组成：0.3-0.7％聚丙烯酰胺、0.1-0.5％交联剂、0.1-0.5％络合剂、余量为水。
优选地，所述步骤(2)为在75-95℃条件下，将内衣在吸湿排汗整理剂中浸渍20-30min，脱水后，在80-100℃条件下烘干5-10min。
具体的，在本发明中：
2-甲基-2-丙烯酸-2,3-二羟基丙酯，CAS号：5919-74-4。
2-羟丙基异丁烯酸酯，CAS号：923-26-2。
2-羟基乙基丙烯酸酯，CAS号：818-61-1。
羟基乙叉二膦酸钠，CAS号：29329-71-3。
乙二胺四甲叉膦酸五钠盐，CAS号：7651-99-2。
本发明的不着凉内衣，为内衣的一种，又称为防感冒内衣，具有很好的吸湿排汗效果，在出现汗时服装不会粘贴皮肤而产生冷湿感，避免着凉，特别具有防感冒的功效。
具体实施方式
下面是对本发明的优选实施例进行详细阐述，以使本发明的优点和特征能更易于被本领域技术人员理解，从而对本发明的保护范围做出更为清楚明确的界定。
聚丙烯酰胺，CAS号：9003-05-8。采用山东省聊城市宏鑫化工有限公司提供的分子量为500-800万的非离子型聚丙烯酰胺。
实施例1
不着凉内衣原料(重量份)：36份Thermocool纤维(采用ADVANSA公司Thermocool纤维，75D)、61份莫代尔纤维(采用细绒棉,规格：1.8dtex×30mm)、3份氨纶(采用杜邦氨纶丝，70D)。
吸湿排汗整理剂原料(质量百分比)：0.5％聚丙烯酰胺、0.1％2-甲基-2-丙烯酸-2,3-二羟基丙酯、0.1％2-羟丙基异丁烯酸酯、0.1％2-羟基乙基丙烯酸酯、0.15％羟基乙叉二膦酸钠、0.15％乙二胺四甲叉膦酸五钠盐、98.9％去离子水。
不着凉内衣的制备方法：
(1)将Thermocool纤维与竹纤维混纺成混纺纱线，再用混纺纱线与氨纶使用针织纬编大圆机进行针织织造，得到面料(平纹织物，面料克重为200克/平方米)，按照制作内衣的工艺和要求，将面料裁剪后，加工成内衣。
(2)将聚乙烯吡咯烷酮、交联剂、络合剂加入去离子水中混合均匀，得到吸湿排汗整理剂；
在90℃条件下，将内衣在吸湿排汗整理剂中浸渍25min，脱水后，在90℃条件下烘干8min。得到实施例1的不着凉内衣。
实施例2
按实施例1的原料配比和方法制备不着凉内衣，区别仅仅在于：吸湿排汗整理剂原料(质量百分比)：0.5％聚丙烯酰胺、0.15％2-甲基-2-丙烯酸-2,3-二羟基丙酯、0.15％2-羟丙基异丁烯酸酯、0.15％羟基乙叉二膦酸钠、0.15％乙二胺四甲叉膦酸五钠盐、98.9％去离子水。得到实施例2的不着凉内衣。
实施例3
按实施例1的原料配比和方法制备不着凉内衣，区别仅仅在于：吸湿排汗整理剂原料(质量百分比)：0.5％聚丙烯酰胺、0.15％2-甲基-2-丙烯酸-2,3-二羟基丙酯、0.15％2-羟基乙基丙烯酸酯、0.15％羟基乙叉二膦酸钠、0.15％乙二胺四甲叉膦酸五钠盐、98.9％去离子水。得到实施例3的不着凉内衣。
实施例4
按实施例1的原料配比和方法制备不着凉内衣，区别仅仅在于：吸湿排汗整理剂原料(质量百分比)：0.5％聚丙烯酰胺、0.15％2-羟丙基异丁烯酸酯、0.15％2-羟基乙基丙烯酸酯、0.15％羟基乙叉二膦酸钠、0.15％乙二胺四甲叉膦酸五钠盐、98.9％去离子水。得到实施例4的不着凉内衣。
实施例5
按实施例1的原料配比和方法制备不着凉内衣，区别仅仅在于：吸湿排汗整理剂原料(质量百分比)：0.5％聚丙烯酰胺、0.1％2-甲基-2-丙烯酸-2,3-二羟基丙酯、0.1％2-羟丙基异丁烯酸酯、0.1％2-羟基乙基丙烯酸酯、0.3％羟基乙叉二膦酸钠、98.9％去离子水。得到实施例5的不着凉内衣。
实施例6
按实施例1的原料配比和方法制备不着凉内衣，区别仅仅在于：吸湿排汗整理剂原料(质量百分比)：0.5％聚丙烯酰胺、0.1％2-甲基-2-丙烯酸-2,3-二羟基丙酯、0.1％2-羟丙基异丁烯酸酯、0.1％2-羟基乙基丙烯酸酯、0.3％乙二胺四甲叉膦酸五钠盐、98.9％去离子水。得到实施例6的不着凉内衣。
测试例1
吸湿扩散性测试：
(1)每个样品裁取5块试样，每块试样的尺寸为10cm×10cm，试样应平整无皱褶。
(2)将试样放置在标准大气条件下调湿平衡。
(3)将试样平放在试验台上，吸取约0.2ml的水轻轻地滴在试样上，滴管口径距离试样表面应不超过1cm。
(4)仔细观察水滴扩散情况，记录水滴接触试样内层表面至完全渗透扩散(不再呈现镜面反射)至外层的所需时间，精确至0.1s。如果水滴扩散速度较慢，在一定时间(如300s)后仍未完全扩散，则可停止试验，并记录扩散时间为大于设定时间(如300s)。
(5)记录5块试样的平均滴水扩散时间(s)。
这种方法非常简易直观，观察者可以从水滴接触试样内层表面完全渗透扩散到外层所需的时间来评判其吸湿扩散性能。水滴扩散时间越短，说明其吸湿扩散性能越好。测试结果见表1。
表1：面料的平均滴水扩散时间结果表
平均滴水扩散时间(s)
实施例1 4.5
实施例2 8.1
实施例3 8.4
实施例4 7.9
实施例5 7.5
实施例6 7.8
比较实施例1与实施2-4，实施例1(2-甲基-2-丙烯酸-2,3-二羟基丙酯、2-羟丙基异丁烯酸酯、2-羟基乙基丙烯酸酯复配)平均滴水扩散时间明显低于实施例2-4(2-甲基-2-丙烯酸-2,3-二羟基丙酯、2-羟丙基异丁烯酸酯、2-羟基乙基丙烯酸酯中任意二者复配)；比较实施例1与实施例5-6，实施例1(络合剂采用羟基乙叉二膦酸钠、乙二胺四甲叉膦酸五钠盐复配)平均滴水扩散时间明显低于实施例5-6(络合剂采用羟基乙叉二膦酸钠、乙二胺四甲叉膦酸五钠盐中单一原料)。
测试例2
导湿排汗性测试：
参照标准ISO11092：1993，采用SDL排汗导湿仪测试各实施例和对比例的热阻、湿阻。测试结果见表2。
表2：各实施例及对比例的的热阻、湿阻结果表
热阻(10-3km2W-1) 湿阻(Pam2W-1)
实施例1 9.322 4.231
实施例2 10.795 5.015
实施例3 10.831 5.032
实施例4 10.783 4.958
实施例5 10.754 4.836
实施例6 10.774 4.912
比较实施例1与实施2-4，实施例1(2-甲基-2-丙烯酸-2,3-二羟基丙酯、2-羟丙基异丁烯酸酯、2-羟基乙基丙烯酸酯复配)热阻、湿阻明显低于实施例2-4(2-甲基-2-丙烯酸-2,3-二羟基丙酯、2-羟丙基异丁烯酸酯、2-羟基乙基丙烯酸酯中任意二者复配)；比较实施例1与实施例5-6，实施例1(络合剂采用羟基乙叉二膦酸钠、乙二胺四甲叉膦酸五钠盐复配)热阻、湿阻明显低于实施例5-6(络合剂采用羟基乙叉二膦酸钠、乙二胺四甲叉膦酸五钠盐中单一原料)。
现有技术中并没有具有吸湿排汗性能的内衣，本发明申请人上海喜眠服饰有限公司开创性的发明了一种不着凉内衣，具有很好的吸湿排汗效果，在出现汗时服装不会粘贴皮肤而产生冷湿感，避免着凉，特别具有防感冒的功效。

Claims (5)

1.一种不着凉内衣，其特征在于，由下述重量份的原料织造而成：21-39份Thermocool纤维、61-79份莫代尔纤维、1-4份氨纶；
所述不着凉内衣再经过吸湿排汗处理步骤而得；
所述吸湿排汗处理步骤为将所述不着凉内衣在吸湿排汗整理剂中浸渍；
优选地，所述吸湿排汗整理剂由下述质量百分比的原料组成：0.3-0.7％聚丙烯酰胺、0.1-0.5％交联剂、0.1-0.5％络合剂、余量为水；
优选地，所述的交联剂由2-甲基-2-丙烯酸-2,3-二羟基丙酯、2-羟丙基异丁烯酸酯、2-羟基乙基丙烯酸酯混合而成，所述2-甲基-2-丙烯酸-2,3-二羟基丙酯、2-羟丙基异丁烯酸酯、2-羟基乙基丙烯酸酯的质量比为(1-3)：(1-3)：(1-3)。
2.根据权利要求1所述的不着凉内衣，其特征在于，所述的络合剂由40-60wt％羟基乙叉二膦酸钠和40-60wt％乙二胺四甲叉膦酸五钠盐组成。
3.根据权利要求1或2所述的不着凉内衣的制备方法，其特征在于，包括以下步骤：(1)采用常规方法将Thermocool纤维、莫代尔纤维和氨纶织造成面料，裁剪缝制成内衣；(2)将上述内衣进行亲水处理。
4.根据权利要求3所述的不着凉内衣的制备方法，其特征在于，所述步骤(2)为在75-95℃条件下，将内衣在吸湿排汗整理剂中浸渍20-30min，脱水后，在80-100℃条件下烘干5-10min。
5.根据权利要求4所述的不着凉内衣的制备方法，其特征在于，所述吸湿排汗整理剂由下述质量百分比的原料组成：0.3-0.7％聚丙烯酰胺、0.1-0.5％交联剂、0.1-0.5％络合剂、余量为水。
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