CN105754750B - A kind of renovation dry cleaning agent of leather product and preparation method thereof - Google Patents
A kind of renovation dry cleaning agent of leather product and preparation method thereof Download PDFInfo
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- CN105754750B CN105754750B CN201410794792.4A CN201410794792A CN105754750B CN 105754750 B CN105754750 B CN 105754750B CN 201410794792 A CN201410794792 A CN 201410794792A CN 105754750 B CN105754750 B CN 105754750B
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- polyoxyethylene ether
- fatty alcohol
- silicon oil
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Abstract
The present invention provides renovation dry cleaning agents of a kind of leather product and preparation method thereof.The raw material of the renovation dry cleaning agent includes anionic surfactant, fatty alcohol polyoxyethylene ether -9, alkyl glycosides, isomery fatty alcohol polyoxyethylene ether, water-soluble silicon oil, amido silicon oil, dodecanamide propyl dimethyl betaine, ethylene glycol, tasteless ethyl alcohol, citric acid, N- sodium hydroxy methyl glycinate, essence and deionized water.This product is dry-cleaned and is renovated for leather product, is cleaned using the petroleum solvent and surfactant of non-volatility to leather product, using dye migration principle, is carried out renovation arrangement by migration of the organosilicon to dyestuff.
Description
Technical field
The invention belongs to detergent composition field, the renovation dry cleaning agent of specifically a kind of leather product and its
Preparation method.
Background technique
With era development and trend, more and more people are worn, using leather product, such as leather shoes, suede
Leather packet etc., especially in winter, many people wear leather snow boots.But leather is easily dirty, washing will lead to face
Discoloration is shallow, wears, and leather is hardened, and leather product is not easy to do, and influences next use.
Existing leather Refresh Product is mainly dyeing product in the market, though this kind of product can deepen leather
Color, but there are inconvenient for use, easily by other dyeing articles, dye the leather needs of the problems such as uneven and different colours
Different dyestuffs increases use cost, and these products do not have cleaning function, needs first to be cleaned before renovation, increases
Time cost is added.
The present invention can carry out the cleaning and renovation of leather simultaneously, saved time cost, can be used for different colours
Leather renovation, saves use cost and renovation color is uniform.
Summary of the invention
The object of the present invention is to provide a kind of leather product dry cleaning agent and preparation method thereof containing renovation agent.This hair
Bright is a kind of dry-cleaning formula with refurbished function, can be cleaned to leather spot, while turning over to leather
Newly, make the color burn of leather.
The purpose of the present invention is what is be achieved through the following technical solutions:
A kind of leather product dry cleaning agent containing renovation agent, the raw material of the dry cleaning agent includes anion surface active
Agent, fatty alcohol polyoxyethylene ether -9, alkyl glycosides, isomery fatty alcohol polyoxyethylene ether, water-soluble silicon oil, amido silicon oil, laurel
Amido propyl dimethyl betaine, ethylene glycol, tasteless ethyl alcohol, citric acid, N- sodium hydroxy methyl glycinate, essence and deionized water,
The weight part ratio of each raw material are as follows:
Anionic surfactant 0.5 ~ 2
Fatty alcohol polyoxyethylene ether -9 0.1 ~ 1
Alkyl glycosides 0.3 ~ 0.5
Isomery fatty alcohol polyoxyethylene ether 0.5 ~ 2.5
Water-soluble silicon oil 0.1 ~ 0.3
Amido silicon oil 0.01 ~ 4
Dodecanamide propyl dimethyl betaine 0.02 ~ 0.1
Ethylene glycol 3 ~ 5
Tasteless ethyl alcohol 0 ~ 50
Citric acid 0.1 ~ 0.3
N- sodium hydroxy methyl glycinate 0.1 ~ 0.3
Essence 0.2 ~ 0.4
Deionized water 35 ~ 95.
Further, the anionic surfactant is the compound of AES-2, AES-3, AOS or any two raw materials.
It is another object of the present invention to what is be achieved through the following technical solutions:
A kind of preparation method of the leather product dry cleaning agent containing renovation agent, the raw material of the dry cleaner include yin from
Sub- surfactant, fatty alcohol polyoxyethylene ether -9, alkyl glycosides, isomery fatty alcohol polyoxyethylene ether, water-soluble silicon oil, amino
Silicone oil, dodecanamide propyl dimethyl betaine, ethylene glycol, tasteless ethyl alcohol, citric acid, N- sodium hydroxy methyl glycinate, essence and
Deionized water, the weight part ratio of each raw material are as follows:
Anionic surfactant 0.5 ~ 2
Fatty alcohol polyoxyethylene ether -9 0.1 ~ 1
Alkyl glycosides 0.3 ~ 0.5
Isomery fatty alcohol polyoxyethylene ether 0.5 ~ 2.5
Water-soluble silicon oil 0.1 ~ 0.3
Amido silicon oil 0.01 ~ 4
Dodecanamide propyl dimethyl betaine 0.02 ~ 0.1
Ethylene glycol 3 ~ 5
Tasteless ethyl alcohol 0 ~ 50
Citric acid 0.1 ~ 0.3
N- sodium hydroxy methyl glycinate 0.1 ~ 0.3
Essence 0.2 ~ 0.4
Deionized water 35 ~ 95.
The preparation method comprises the following steps:
1) one third room temperature (20 DEG C or so, if temperature is low, can suitably heat) deionized water is added；
2) water-soluble silicon oil, amido silicon oil, ethylene glycol, tasteless ethyl alcohol, isomery rouge are added in Xiang Shangshu deionized water
Fat alcohol polyoxyethylene ether stirs evenly, and obtains mixed liquor A；
3) alkyl glycosides, anionic surfactant and fatty alcohol polyoxyethylene ether -9 are added into mixed liquor A and stirs
Dissolution, obtains mixed liquid B；
4) dissolution of dodecanamide propyl dimethyl betaine is added into mixed liquid B, obtains mixed liquor C；
5) essence, N- sodium hydroxy methyl glycinate are added into mixed liquor C, adds remaining deionized water, obtains mixed liquor D；
6) pH value of the mixed liquor D is adjusted with citric acid, finally with regulation filter filtering, standing and defoaming is to obtain institute
The leather product dry cleaning agent containing renovation agent stated.
The anionic surfactant is the compound of AES-2, AES-3, AOS or any two raw materials.
The characteristics of inventive formulation:
The structure of isomery fatty alcohol polyoxyethylene ether is the alkyl isomery alcohol containing small branch, and steric hindrance is small, is easily dispersed or dissolved in
Water has excellent wetability, permeability and emulsibility, can be used for multifunctional detergent, decontamination solubilizer, household care washing
Agent etc., and good environmental protection.
Water-soluble silicon oil: it is a kind of nonionic surfactant of reactivity, flannelette can be used in form of an aqueous solutions
During leather arranges, improve its feel, antistatic, and can increase resistance to soiling；
Amido silicon oil: in textile industry be used for textile processing, have the function of migrating dyes, can by dye for fabrics from
Bottom is migrated to fabric surface, thus refreshing fabrics；
Dodecanamide propyl dimethyl betaine: have preferable antistatic property, flexibility, can with anion, cation,
Amphoteric ion and nonionic surfactant compatibility；
Tasteless ethyl alcohol: being azeotropic mixture with water, improves the volatility of product, and tasteless ethyl alcohol is handled by deodorization, and irritation subtracts
It is small, it relatively large can use, will not cause harm to the human body；
Ethylene glycol: there is good dissolubility；
The pH value of citric acid regulating solution.
Alkyl glycosides: being synthesized by renewable resource natural fatty alcohol and glucose, is that a kind of performance is more comprehensively novel non-
Ionic surface active agent, surface tension is low, wetting power is strong, strong detergency compatibility is good, biodegrade rapidly it is thorough, can with appoint
What classes of surfactant compounding, synergistic effect are obvious.It is internationally recognized preferred " green " functional surfactant.
N- sodium hydroxy methyl glycinate is preservative, can suppress growth of microorganism in product of the invention, prevent corruption.
The beneficial effect of leather product dry cleaning agent of the present invention containing renovation agent is:
1, the renovation dry cleaning agent of leather product of the present invention, can be for finding product currently on the market using not
Just, have a single function, renovate the problems such as effect is poor and improve and promoted；
2, the present invention is that a kind of routine use leather renovates dry cleaning agent, cleaning and renovation letter to leather product
Just quick, renovation is uniform；
3, the characteristics of present invention compounding is compound cold with process of a molecule, can be reduced the use of energy, is not required to increase
Special installation；
4, this product is dry-cleaned and is renovated for leather product, living using the petroleum solvent of non-volatility and surface
Leather product is cleaned in property agent, using dye migration principle, is turned over by migration of the organosilicon to dyestuff
It is new to arrange.
Specific embodiment
Embodiment 1
A kind of leather product dry cleaning agent containing renovation agent, the raw material of the dry cleaner includes anion surface active
Agent, fatty alcohol polyoxyethylene ether -9, alkyl glycosides, isomery fatty alcohol polyoxyethylene ether, water-soluble silicon oil, amido silicon oil, laurel
Amido propyl dimethyl betaine, ethylene glycol, tasteless ethyl alcohol, citric acid, N- sodium hydroxy methyl glycinate, essence and deionized water,
The weight part ratio of each raw material are as follows:
Anionic surfactant 0.5 ~ 2
Fatty alcohol polyoxyethylene ether -9 0.1 ~ 1
Alkyl glycosides 0.3 ~ 0.5
Isomery fatty alcohol polyoxyethylene ether 0.5 ~ 2.5
Water-soluble silicon oil 0.1 ~ 0.3
Amido silicon oil 0.01 ~ 4
Dodecanamide propyl dimethyl betaine 0.02 ~ 0.1
Ethylene glycol 3 ~ 5
Tasteless ethyl alcohol 0 ~ 50
Citric acid 0.1 ~ 0.3
N- sodium hydroxy methyl glycinate 0.1 ~ 0.3
Essence 0.2 ~ 0.4
Deionized water 35 ~ 95.
The preparation method of the leather product dry cleaning agent containing renovation agent the following steps are included:
1) one third room temperature (20 DEG C or so, if temperature is low, can suitably heat) deionized water is added；
2) water-soluble silicon oil, amido silicon oil, ethylene glycol, tasteless ethyl alcohol, isomery rouge are added in Xiang Shangshu deionized water
Fat alcohol polyoxyethylene ether stirs evenly, and obtains mixed liquor A；
3) alkyl glycosides, anionic surfactant and fatty alcohol polyoxyethylene ether -9 are added into mixed liquor A and stirs
Dissolution, obtains mixed liquid B；
4) dissolution of dodecanamide propyl dimethyl betaine is added into mixed liquid B, obtains mixed liquor C；
5) essence, N- sodium hydroxy methyl glycinate are added into mixed liquor C, adds remaining deionized water, obtains mixed liquor D；
6) pH value of the mixed liquor D is adjusted with citric acid, finally with regulation filter filtering, standing and defoaming is to obtain institute
The leather product dry cleaning agent containing renovation agent stated.
Unit of weight used is kilogram in the present embodiment, or gram；
Each raw material described in the present embodiment is technical grade；
Each raw material described in the present embodiment is the conventional products sold in the market.
Embodiment 2
The present embodiment is preferred embodiment on that basis of example 1, and raw materials used quality is same as Example 1, described
The weight fraction ratio of each raw material are as follows:
AES-2 2.0
AEO-9 0.25
Alkyl glycosides 0.5
Isomery fatty alcohol polyoxyethylene ether 1.2
Water-soluble silicon oil 0.3
Amido silicon oil 0.05
Dodecanamide propyl dimethyl betaine 0.02
Ethylene glycol 3
Tasteless ethyl alcohol 20
Citric acid 0.2
N- sodium hydroxy methyl glycinate 0.2
Essence 0.3
Deionized water is to 100.
Embodiment 3
The present embodiment is preferred embodiment on that basis of example 1, and raw materials used quality is same as Example 1, described
The weight fraction ratio of each raw material are as follows:
AES-3 0.5
AEO-9 0.5
Alkyl glycosides 0.4
Isomery fatty alcohol polyoxyethylene ether 2.0
Water-soluble silicon oil 0.15
Amido silicon oil 1.0
Dodecanamide propyl dimethyl betaine 0.05
Ethylene glycol 3.0
Tasteless ethyl alcohol 20
Citric acid 0.2
N- sodium hydroxy methyl glycinate 0.15
Essence 0.3
Deionized water is to 100.
Embodiment 4
The present embodiment is preferred embodiment on that basis of example 1, and raw materials used quality is same as Example 1, described
The weight fraction ratio of each raw material are as follows:
AES-2 0.3
AEO-9 0.2
Alkyl glycosides 0.3
Isomery fatty alcohol polyoxyethylene ether 0.8
Water-soluble silicon oil 0.15
Amido silicon oil 0.03
Dodecanamide propyl dimethyl betaine 0.1
Ethylene glycol 4.0
Tasteless ethyl alcohol 35
Citric acid 0.2
N- sodium hydroxy methyl glycinate 0.15
Essence 0.2
Deionized water is to 100.
Embodiment 5
The present embodiment is preferred embodiment on that basis of example 1, and raw materials used quality is same as Example 1, described
The weight fraction ratio of each raw material are as follows:
AES-2 0.15
AES-3 0.15
AEO-9 0.45
Alkyl glycosides 0.3
Isomery fatty alcohol polyoxyethylene ether 2.5
Water-soluble silicon oil 0.1
Amido silicon oil 4.0
Dodecanamide propyl dimethyl betaine 0.02
Ethylene glycol 3.5
Tasteless ethyl alcohol 50
Citric acid 0.2
N- sodium hydroxy methyl glycinate 0.2
Essence 0.4
Deionized water is to 100.
Embodiment 6
The present embodiment is preferred embodiment on that basis of example 1, and raw materials used quality is same as Example 1, described
The weight fraction ratio of each raw material are as follows:
AES-2 0.25
AES-3 0.05
AEO-9 0.5
Alkyl glycosides 0.25
Isomery fatty alcohol polyoxyethylene ether 0.5
Water-soluble silicon oil 0.25
Amido silicon oil 2.5
Dodecanamide propyl dimethyl betaine 0.04
Ethylene glycol 3.0
Tasteless ethyl alcohol 25
Citric acid 0.2
N- sodium hydroxy methyl glycinate 0.2
Essence 0.2
Deionized water is to 100.
The detection method of the present embodiment is according to QB 1873-1993 " Shoe upper leather " and " the leather surface face of QB/T 1327
Color crock fastness test method ", color change (intensification) scores after estimating leather before treatment by more people, confirms
Properties of product.For color change closer to leather true qualities, score is higher, and color is too deep low with without variation score, full marks 5
Point.Test data is as follows:
The detection method of the present embodiment utilizes color according to " textile color showing method " GB/T 21898-2008
Three attributes --- form and aspect, lightness, chroma compares leather color change before and after the processing.
Claims (7)
1. a kind of leather product dry cleaning agent containing renovation agent, which is characterized in that the raw material of the dry cleaning agent is by anion
Surfactant, fatty alcohol polyoxyethylene ether -9, alkyl glycosides, isomery fatty alcohol polyoxyethylene ether, water-soluble silicon oil, amino silicone
It oil, dodecanamide propyl dimethyl betaine, ethylene glycol, tasteless ethyl alcohol, citric acid, N- sodium hydroxy methyl glycinate, essence and goes
Ionized water composition, the weight part ratio of each raw material are as follows:
Anionic surfactant 0.5 ~ 2
Fatty alcohol polyoxyethylene ether -9 0.1 ~ 1
Alkyl glycosides 0.3 ~ 0.5
Isomery fatty alcohol polyoxyethylene ether 0.5 ~ 2.5
Water-soluble silicon oil 0.1 ~ 0.3
Amido silicon oil 0.01 ~ 4
Dodecanamide propyl dimethyl betaine 0.02 ~ 0.1
Ethylene glycol 3 ~ 5
Tasteless ethyl alcohol 1 ~ 50
Citric acid 0.1 ~ 0.3
N- sodium hydroxy methyl glycinate 0.1 ~ 0.3
Essence 0.2 ~ 0.4
Deionized water 35 ~ 95；
The anionic surfactant is the compound of AES-2, AES-3, AOS or any two raw materials.
2. the leather product dry cleaning agent according to claim 1 containing renovation agent, which is characterized in that each raw material
Weight fraction ratio are as follows:
AES-2 2.0
Fatty alcohol polyoxyethylene ether -9 0.25
Alkyl glycosides 0.5
Isomery fatty alcohol polyoxyethylene ether 1.2
Water-soluble silicon oil 0.3
Amido silicon oil 0.05
Dodecanamide propyl dimethyl betaine 0.02
Ethylene glycol 3
Tasteless ethyl alcohol 20
Citric acid 0.2
N- sodium hydroxy methyl glycinate 0.2
Essence 0.3
Deionized water is to 100.
3. the leather product dry cleaning agent according to claim 1 containing renovation agent, which is characterized in that each raw material
Weight fraction ratio are as follows:
AES-3 0.5
Fatty alcohol polyoxyethylene ether -9 0.5
Alkyl glycosides 0.4
Isomery fatty alcohol polyoxyethylene ether 2.0
Water-soluble silicon oil 0.15
Amido silicon oil 1.0
Dodecanamide propyl dimethyl betaine 0.05
Ethylene glycol 3.0
Tasteless ethyl alcohol 20
Citric acid 0.2
N- sodium hydroxy methyl glycinate 0.15
Essence 0.3
Deionized water is to 100.
4. the leather product dry cleaning agent according to claim 1 containing renovation agent, which is characterized in that each raw material
Weight fraction ratio are as follows:
AES-2 0.3
Fatty alcohol polyoxyethylene ether -9 0.2
Alkyl glycosides 0.3
Isomery fatty alcohol polyoxyethylene ether 0.8
Water-soluble silicon oil 0.15
Amido silicon oil 0.03
Dodecanamide propyl dimethyl betaine 0.1
Ethylene glycol 4.0
Tasteless ethyl alcohol 35
Citric acid 0.2
N- sodium hydroxy methyl glycinate 0.15
Essence 0.2
Deionized water is to 100.
5. the leather product dry cleaning agent according to claim 1 containing renovation agent, which is characterized in that each raw material
Weight fraction ratio are as follows:
AES-2 0.15
AES-3 0.15
Fatty alcohol polyoxyethylene ether -9 0.45
Alkyl glycosides 0.3
Isomery fatty alcohol polyoxyethylene ether 2.5
Water-soluble silicon oil 0.1
Amido silicon oil 4.0
Dodecanamide propyl dimethyl betaine 0.02
Ethylene glycol 3.5
Tasteless ethyl alcohol 50
Citric acid 0.2
N- sodium hydroxy methyl glycinate 0.2
Essence 0.4
Deionized water is to 100.
6. the leather product dry cleaning agent according to claim 1 containing renovation agent, which is characterized in that each raw material
Weight fraction ratio are as follows:
AES-2 0.25
AES-3 0.05
Fatty alcohol polyoxyethylene ether -9 0.5
Alkyl glycosides 0.25
Isomery fatty alcohol polyoxyethylene ether 0.5
Water-soluble silicon oil 0.25
Amido silicon oil 2.5
Dodecanamide propyl dimethyl betaine 0.04
Ethylene glycol 3.0
Tasteless ethyl alcohol 25
Citric acid 0.2
N- sodium hydroxy methyl glycinate 0.2
Essence 0.2
Deionized water is to 100.
7. a kind of preparation method of the leather product dry cleaning agent containing renovation agent, which is characterized in that the original of the dry cleaning agent
Material is by anionic surfactant, fatty alcohol polyoxyethylene ether -9, alkyl glycosides, isomery fatty alcohol polyoxyethylene ether, water solubility
Silicone oil, amido silicon oil, dodecanamide propyl dimethyl betaine, ethylene glycol, tasteless ethyl alcohol, citric acid, N- hydroxymethylglycinate
Sodium, essence and deionized water composition, the weight part ratio of each raw material are as follows:
Anionic surfactant 0.5 ~ 2
Fatty alcohol polyoxyethylene ether -9 0.1 ~ 1
Alkyl glycosides 0.3 ~ 0.5
Isomery fatty alcohol polyoxyethylene ether 0.5 ~ 2.5
Water-soluble silicon oil 0.1 ~ 0.3
Amido silicon oil 0.01 ~ 4
Dodecanamide propyl dimethyl betaine 0.02 ~ 0.1
Ethylene glycol 3 ~ 5
Tasteless ethyl alcohol 0 ~ 50
Citric acid 0.1 ~ 0.3
N- sodium hydroxy methyl glycinate 0.1 ~ 0.3
Essence 0.2 ~ 0.4
Deionized water is to 100；
The anionic surfactant is the compound of AES-2, AES-3, AOS or any two raw materials；
The preparation method comprises the following steps:
1) one third deionized water at normal temperature is added；
2) water-soluble silicon oil, amido silicon oil, ethylene glycol, tasteless ethyl alcohol, isomery fatty alcohol are added in Xiang Shangshu deionized water
Polyoxyethylene ether stirs evenly, and obtains mixed liquor A；
3) alkyl glycosides, anionic surfactant and fatty alcohol polyoxyethylene ether -9 are added into mixed liquor A, is mixed molten
Solution, obtains mixed liquid B；
4) dissolution of dodecanamide propyl dimethyl betaine is added into mixed liquid B, obtains mixed liquor C；
5) essence, N- sodium hydroxy methyl glycinate are added into mixed liquor C, adds remaining deionized water, obtains mixed liquor D；
6) pH value of the mixed liquor D is adjusted with citric acid, finally with regulation filter filtering, standing and defoaming obtains described
Leather product dry cleaning agent containing renovation agent.
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| CN201410794792.4A CN105754750B (en) | 2014-12-19 | 2014-12-19 | A kind of renovation dry cleaning agent of leather product and preparation method thereof |
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| CN105754750B true CN105754750B (en) | 2019-03-01 |
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| JP2020007437A (en) * | 2018-07-06 | 2020-01-16 | 木村石鹸工業株式会社 | High draining detergent |
| CN111020069A (en) * | 2019-12-09 | 2020-04-17 | 沈阳翰皇日用品有限公司 | Suede leather care reducing agent |
| CN111117810A (en) * | 2019-12-18 | 2020-05-08 | 魅扬(湖北)科技有限公司 | Multifunctional cleaning agent and preparation method thereof |
| CN111334377B (en) * | 2020-04-08 | 2021-11-23 | 西安优派日化有限公司 | Phase-change down jacket dry cleaning agent and preparation method thereof |
| CN112791683B (en) * | 2020-12-31 | 2022-07-19 | 北京日光旭升精细化工技术研究所 | Cleaning agent preparation device and dry cleaning agent preparation method thereof |
| CN114836270B (en) * | 2022-02-24 | 2024-02-23 | 青岛小鹿先生智能科技有限公司 | Machine-washing shoe-washing liquid and preparation method thereof |
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| CN1040051A (en) * | 1989-07-12 | 1990-02-28 | 金颖逵 | Multifunction detergent and preparation method thereof |
| ES2551227T3 (en) * | 2010-10-29 | 2015-11-17 | The Procter & Gamble Company | Thickened liquid cleaning composition for hard surfaces |
| CN102051278A (en) * | 2011-01-24 | 2011-05-11 | 北京洛娃日化有限公司 | All-purpose cleaning agent |
| CN102553504B (en) * | 2012-01-18 | 2014-12-17 | 朗盛（常州）有限公司 | Preparation method of emulsion, leather care emulsion, and use leather care emulsion |
| CN102618403B (en) * | 2012-03-13 | 2013-07-10 | 宋子奎 | Color-increasing dry cleaning agent composition and preparation method thereof |
| CN103966031A (en) * | 2014-05-30 | 2014-08-06 | 于文 | Environment-friendly leather cleaning care agent and preparation method thereof |
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Address after: 100094 block B, building 1, yard 2, Yongcheng North Road, Yongfeng Industrial base, Haidian District, Beijing Patentee after: Beijing green umbrella Technology Co., Ltd Address before: 100094 block B, building 1, yard 2, Yongcheng North Road, Yongfeng Science Park, Haidian District, Beijing Patentee before: Beijing lvsan Chemical Co., Ltd |